CN106879584A - Insect aerosol and preparation method thereof - Google Patents
Insect aerosol and preparation method thereof Download PDFInfo
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- CN106879584A CN106879584A CN201710305142.2A CN201710305142A CN106879584A CN 106879584 A CN106879584 A CN 106879584A CN 201710305142 A CN201710305142 A CN 201710305142A CN 106879584 A CN106879584 A CN 106879584A
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- Prior art keywords
- insect aerosol
- insect
- aerosol
- phenothrin
- permethrin
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/24—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms
- A01N43/26—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings
- A01N43/28—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3
- A01N43/30—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3 with two oxygen atoms in positions 1,3, condensed with a carbocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
- A01N61/02—Mineral oils; Tar oils; Tar; Distillates, extracts or conversion products thereof
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Zoology (AREA)
- Dentistry (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of insect aerosol and preparation method thereof.The insect aerosol is mainly prepared from by each component of following mass percent:Rich_d_transallethrin 0.1% 0.5%, d-phenothrin 0.1% 0.5%, Permethrin 0.1% 0.5%, oxidation of piperonyl butoxide 0.2% 0.7%, kerosene 10% 20%, propellant 20% 45% and water 35% 60%.The insect aerosol desinsection efficiently and Environmental Safety.
Description
Technical field
The present invention relates to daily-use chemical industry technical field, more particularly to a kind of insect aerosol and preparation method thereof.
Background technology
The insects such as fly, mosquito all carry infection class germ, influence the normal life of the mankind, and can endanger the body of the mankind
Health.Because insect aerosol is easy to use, people generally can murder insect using it.But, the desinsection gas in conventional art
The insecticidal effect of mist agent is poor, and user increases the dosage of insect aerosol in order to strengthen insecticidal effect.Thus can
Cause the toxic residue amount of insect aerosol big, influence user healthy and also more serious to the pollution of environment.This
Outward, by the insecticide that long-term use is heavy dose of, insect can also produce anti-drug resistance, and then can more reduce insect aerosol
Using effect.
The content of the invention
Based on this, it is necessary to provide a kind of desinsection efficiently and the insect aerosol of Environmental Safety and preparation method thereof.
A kind of insect aerosol, is mainly prepared from by each component of following mass percent:Rich d-trans allyl chrysanthemum
Ester 0.1%-0.5%, d-phenothrin 0.1%-0.5%, Permethrin 0.1%-0.5%, oxidation of piperonyl butoxide 0.2%-
0.7%, kerosene 10%-20%, propellant 20%-45% and water 35%-60%.
Wherein in one embodiment, the mass percent of the oxidation of piperonyl butoxide is 0.2%-0.3%.
Wherein in one embodiment, the also essence including 0.01%-0.1%.
Wherein in one embodiment, 2, the 6- di-tert-butyl-4-methy phenols also including 0.01%-0.1%, 0.2%-
0.7% sapn 120 and the Tween 80 of 0.01%-0.1%.
Wherein in one embodiment, rich_d_transallethrin 0.21%, d-phenothrin 0.199%, chlorine chrysanthemum
Ester 0.274%, oxidation of piperonyl butoxide 0.3%, kerosene 10.344%, liquefied petroleum gas 44%, essence 0.05%, 2, the uncles of 6- bis-
Butyl -4- methylphenols 0.05%, sapn 120 0.4%, Tween 80 0.04% and water 44.133%.
In any of the above embodiment, the propellant is liquefied petroleum gas.It is used as projectile by using liquefied petroleum gas
Agent, its Environmental Safety.
Insect aerosol uses the esbiothrin of 0.1%-0.5%, the dextrorotation of 0.1%-0.5% in the present invention
Phenothrin, the Permethrin of 0.1%-0.5%, the oxidation of piperonyl butoxide of 0.2%-0.7%, the kerosene of 10%-20%,
The propellant of 20%-45% and the water of 35%-60%.Inventor in the present invention is tested and is studied by substantial amounts of creativeness
The mass percent scope of the insect aerosol said components and said components is arrived.By controlling said components and above-mentioned
The mass percent scope of component, it is ensured that there is preferably collaboration facilitation, its insect aerosol for preparing between each component
Desinsection efficiently and Environmental Safety.
The oxidation of piperonyl butoxide of the 0.2%-0.7% in the present invention and the esbiothrin of 0.1%-0.5%,
The insecticidal active ingredient of the d-phenothrin of 0.1%-0.5% and the Permethrin of 0.1%-0.5% is worked in coordination when using, oxygen
Change piperonyl butoxide can break esbiothrin, d-phenothrin and Permethrin molecular binding affinities, make to kill
The molecule of worm active ingredient further divides, and improves the activity of esbiothrin, d-phenothrin and Permethrin, enters
And significantly improve the insecticidal effect of insecticide.And the dextrorotation of the oxidation of piperonyl butoxide of 0.2%-0.7% and 0.1%-0.5%
The insecticidal active ingredient of the Permethrin of trans allethrin, the d-phenothrin of 0.1%-0.5% and 0.1%-0.5% can be with
Complex compound is formed, the mixed-functional oxidase of mosquito can be suppressed to prevent mosquito from developing immunity to drugs.
The kerosene of 10%-20% has stronger adherence and permeability, and 0.2%- to the wax coat on polypide surface
0.7% oxidation of piperonyl butoxide also has efficiently oozing property of rush, and it improves d-trans allyl jointly with the kerosene of 10%-20%
The penetration capacity of chrysanthemum ester, d-phenothrin and Permethrin, can rapidly destroy the wax coat of insect, make the insecticidal active ingredient can be with
Go deep into polypide body, significantly improve the insecticidal effect and insecticide efficiency of insecticide.
The desinsection of esbiothrin, d-phenothrin and dextrorotation phenylate chrysanthemum containing less dosage in the present invention
Aerosol can just meet the effect of efficient insecticide, and oxidation of piperonyl butoxide and kerosene are environment-friendly type raw material.Therefore, should
Insect aerosol is small to the body-stimulating of user, and toxic residue is few, more environment-friendly and safer.
A kind of preparation method of insect aerosol is provided in addition with necessity.
A kind of preparation method of insect aerosol as described in above-mentioned any one embodiment is comprised the following steps:
Amounts of components according to the insect aerosol described in any of the above-described embodiment weighs each component;
By the rich_d_transallethrin, the d-phenothrin, the Permethrin, the oxidation piperonyl fourth
The stirring mixing of ether, the kerosene and the water, is made feed liquid;
Sealed after the feed liquid is injected into container filling;
To propellant is injected in the container filling, aerosol lid in pressure obtains the insect aerosol.
Wherein in an implementation, the step of stirring also is included during the mixing, the time of the stirring is 10-
30min。
The preparation method process is simple of the insect aerosol, it is easy to operate, be suitable for industrialization production, can extensive use.
Specific embodiment
For the ease of understanding the present invention, the present invention will be described more fully below.The present invention can be with many not
With form realize, however it is not limited to embodiment described herein.On the contrary, the purpose for providing these embodiments is made to this
The understanding of disclosure of the invention content is more thorough comprehensive.
Unless otherwise defined, all of technologies and scientific terms used here by the article with belong to technical field of the invention
The implication that technical staff is generally understood that is identical.The term for being used in the description of the invention herein is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.
Component used is commercially available mill run in the embodiment of the present invention.
Essence odor type of the invention used comprising jasmine fragrance, osmanthus flower fragrant, green tea odor type, rose scent, lavender flavor type,
The odor types such as lily odor type, orchid odor type and lemon flavor.
Preferred embodiment in detail below is that insect aerosol of the invention is further described, rather than to the present invention
Limitation.
Embodiment 1-6:
Each component content according to being specified in table 1 prepares the insect aerosol of embodiment 1-6 respectively, and its preparation method includes
Following steps:
(1) with liquid:
Amounts of components according to each component content insect aerosol specified in table 1 weighs each component.
2,6- di-tert-butyl-4-methy phenols and Permethrin kerosene are dissolved into obtain component A.If it is existing that crystallization occurs in Permethrin
As that can be used after 50-60 DEG C of heating water bath melts.
Rich_d_transallethrin, d-phenothrin, sapn 120, Tween 80, essence, component A are separately added into coal
Poured into Agitation Tank in oil, start agitator, 15min-30min is stirred with rated speed, obtain solution B.
After solution B sampling detection active ingredient is qualified, oxidation of piperonyl butoxide is added in solution B and starts agitator,
15min-30min is stirred with rated speed, solution C is obtained.
Sampling detection physical and chemical index, checks qualified past solution C to add deionized water and stir, and obtains milky sticky
Shape feed liquid.
(2) embedding:Sealed after the feed liquid is injected into canned container using filling and sealing machine.
(3) inflate:Quantitative oil liquefied gas and gland are filled with embedding product.
(4) 55 DEG C of water-baths are leaked hunting:Water-bath is soaked, and covers the edge curling seal of aerosol container, must not have bubble to emerge, water-bath inspection
5 minutes leakage time.
(5) button, examination spray, product is added to penetrate code, add aerosol cap:Plus button is in examination and sprays examination spray, after examination spray is qualified
Product penetrates code and adds aerosol cap, obtains environmentally friendly without alveolitoid air freshener.
(6) check:According to the inventory of above-mentioned prescription, continuous production 3 batches, inspection structure shows, in keeping life
Comply with relevant regulations.
The raw material composition of the insect aerosol of the embodiment 1-6 of table 1
Comparative example 1:
A kind of insect aerosol, is prepared from by each component of following mass percent:Rich_d_transallethrin
0.212%, d-phenothrin 0.229%, Permethrin 0.196%, kerosene 41.027%, liquefied petroleum gas 58.336%.
Comparative example 2:
A kind of insect aerosol, is prepared from by each component of following mass percent:Rich_d_transallethrin
0.212%, d-phenothrin 0.229%, Permethrin 0.197%, essence 0.079%, kerosene 40.347%, liquefied petroleum gas
58.936%.
Comparative example 3:
A kind of insect aerosol, is prepared from by each component of following mass percent:Rich_d_transallethrin
0.6%, d-phenothrin 0.6%, Permethrin 0.6%, oxidation of piperonyl butoxide 0.1%, kerosene 10%, liquefied petroleum gas
44%, essence 0.05%, 2,6- di-tert-butyl-4-methy phenols 0.05%, sapn 120 0.4%, Tween 80 0.04% and water
43.56%.
Comparative example 4:
A kind of insect aerosol, is prepared from by each component of following mass percent:Rich_d_transallethrin
0.2%, d-phenothrin 0.2%, Permethrin 0.2%, oxidation of piperonyl butoxide 0.8%, kerosene 10%, liquefied petroleum gas
44%, essence 0.05%, 2,6- di-tert-butyl-4-methy phenols 0.05%, sapn 120 0.4%, Tween 80 0.04% and water
44.06%.
Comparative example 5:
A kind of insect aerosol, is prepared from by each component of following mass percent:Decis 0.22%, tetramethrin
0.22%, cypermethrin 0.22%, piperonyl butoxide 0.4%, kerosene 12%, liquefied petroleum gas 44% and water 42.94%.
Test example 1:
The effect that embodiment 1 to 3 and comparative example 1 to 5 are used for desinsection is counted, 2 are as a result see the table below.
The insect aerosol comparative efficacy test's result of table 2
Note:1. experiment insect is mosquito and housefly, and each period carries out four experiments, and experiment insect is 200 every time.
Comparing result:As shown in Table 2, relative to comparative example 1 to 5, the mosquitos and flies 24h death rates are significantly improved embodiment 1 to 3,
5min is knocked down, 10min is knocked down and 15min to knock down mosquito number also relatively more, it was demonstrated that the desinsection of the insect aerosol in the present invention
Efficiency high, insecticide efficiency is fast.Embodiment 1 is preferable relative to the insecticidal effect of embodiment 2 and 3, therefore embodiment 1 is insecticidal aerosol
The better formula of agent.
Test example 2:
Stability survey is carried out under 50 DEG C of hot environment to embodiment 1, comparative example 1, comparative example 3 and comparative example 5 respectively
Examination, test result such as table 3 below.
The insect aerosol stability test result of table 3
It can be seen from the stability test result shown in table 3, the insect aerosol of embodiment 1 is placed in the environment of 50 DEG C
After three months, atomizing effect is good, good stability;Tank valve is unchanged, and sealing is good, safe.Therefore, embodiment 1
Insect aerosol good stability of the insect aerosol relative to comparative example 1, comparative example 3 and comparative example 5, it is safe.
Each technical characteristic of the embodiment can be combined arbitrarily above, to make description succinct, not to above-mentioned implementation
The all possible combination of each technical characteristic in example is all described, as long as however, the combination of these technical characteristics does not exist
Contradiction, is all considered to be the scope of this specification record.
The embodiment only expresses several embodiments of the invention above, and its description is more specific and detailed, but not
Can therefore be construed as limiting the scope of the patent.It should be pointed out that for the person of ordinary skill of the art,
Without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection model of the invention
Enclose.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (8)
1. a kind of insect aerosol, it is characterised in that be mainly prepared from by each component of following mass percent:Rich dextrorotation is anti-
Formula allethrin 0.1%-0.5%, d-phenothrin 0.1%-0.5%, Permethrin 0.1%-0.5%, aoxidize piperonyl fourth
Ether 0.2%-0.7%, kerosene 10%-20%, propellant 20%-45% and water 35%-60%.
2. insect aerosol according to claim 1, it is characterised in that the mass percent of the oxidation of piperonyl butoxide
It is 0.2%-0.3%.
3. insect aerosol according to claim 1, it is characterised in that the also essence including 0.01%-0.1%.
4. insect aerosol according to claim 3, it is characterised in that the tertiary fourths of 2,6- bis- also including 0.01%-0.1%
Base -4- methylphenols, the sapn 120 and the Tween 80 of 0.01%-0.1% of 0.2%-0.7%.
5. insect aerosol according to claim 4, it is characterised in that rich_d_transallethrin 0.21%, dextrorotation
Phenothrin 0.199%, Permethrin 0.274%, oxidation of piperonyl butoxide 0.3%, kerosene 10.344%, propellant 44% is fragrant
0.05,2,6- of essence di-tert-butyl-4-methy phenols 0.05%, sapn 1200.4%, Tween 80 0.04% and water 44.133%.
6. the insect aerosol according to claim any one of 1-5, it is characterised in that the propellant is liquefied petroleum
Gas.
7. the preparation method of a kind of insect aerosol as described in claim any one of 1-6, it is characterised in that including following step
Suddenly:
Amounts of components according to the insect aerosol any one of claim 1 to 6 weighs each component;
By the rich_d_transallethrin, the d-phenothrin, the Permethrin, the oxidation of piperonyl butoxide,
The kerosene and water stirring mixing, are made feed liquid;
Sealed after the feed liquid is injected into container filling;
To propellant is injected in the container filling, aerosol lid in pressure obtains the insect aerosol.
8. the preparation method of insect aerosol according to claim 7, it is characterised in that the time of the stirring mixing is
10-30min。
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108967438A (en) * | 2018-09-17 | 2018-12-11 | 珠海市佳弘科技有限公司 | A kind of water base hygienic biocide aerosol and preparation method thereof that Aircraft bin uses |
CN113767928A (en) * | 2021-08-12 | 2021-12-10 | 广东莱雅新化工科技有限公司 | Synergistic insecticide and preparation method thereof |
CN115444006A (en) * | 2022-10-10 | 2022-12-09 | 浙江绿岛科技有限公司 | Slow-release insecticidal aerosol and preparation method thereof |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108967438A (en) * | 2018-09-17 | 2018-12-11 | 珠海市佳弘科技有限公司 | A kind of water base hygienic biocide aerosol and preparation method thereof that Aircraft bin uses |
CN113767928A (en) * | 2021-08-12 | 2021-12-10 | 广东莱雅新化工科技有限公司 | Synergistic insecticide and preparation method thereof |
CN115444006A (en) * | 2022-10-10 | 2022-12-09 | 浙江绿岛科技有限公司 | Slow-release insecticidal aerosol and preparation method thereof |
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