CN106876611B - 一种用于oled显示的复合蓝光材料的制备方法及应用 - Google Patents
一种用于oled显示的复合蓝光材料的制备方法及应用 Download PDFInfo
- Publication number
- CN106876611B CN106876611B CN201611195588.6A CN201611195588A CN106876611B CN 106876611 B CN106876611 B CN 106876611B CN 201611195588 A CN201611195588 A CN 201611195588A CN 106876611 B CN106876611 B CN 106876611B
- Authority
- CN
- China
- Prior art keywords
- blue light
- light material
- preparation
- composite blue
- composite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000463 material Substances 0.000 title claims abstract description 91
- 239000002131 composite material Substances 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 13
- 229920002098 polyfluorene Polymers 0.000 claims abstract description 12
- 229920000128 polypyrrole Polymers 0.000 claims abstract description 11
- 238000007639 printing Methods 0.000 claims abstract description 9
- 238000000227 grinding Methods 0.000 claims abstract description 8
- 239000000758 substrate Substances 0.000 claims abstract description 6
- 239000011248 coating agent Substances 0.000 claims abstract description 3
- 238000000576 coating method Methods 0.000 claims abstract description 3
- 238000007761 roller coating Methods 0.000 claims abstract description 3
- 230000001052 transient effect Effects 0.000 claims abstract description 3
- 238000006116 polymerization reaction Methods 0.000 claims abstract 2
- MHOFGBJTSNWTDT-UHFFFAOYSA-M 2-[n-ethyl-4-[(6-methoxy-3-methyl-1,3-benzothiazol-3-ium-2-yl)diazenyl]anilino]ethanol;methyl sulfate Chemical compound COS([O-])(=O)=O.C1=CC(N(CCO)CC)=CC=C1N=NC1=[N+](C)C2=CC=C(OC)C=C2S1 MHOFGBJTSNWTDT-UHFFFAOYSA-M 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 11
- 239000002270 dispersing agent Substances 0.000 claims description 8
- 239000003999 initiator Substances 0.000 claims description 8
- HYZJCKYKOHLVJF-UHFFFAOYSA-N 1H-benzimidazole Chemical compound C1=CC=C2NC=NC2=C1 HYZJCKYKOHLVJF-UHFFFAOYSA-N 0.000 claims description 7
- 150000003254 radicals Chemical class 0.000 claims description 7
- NSPMIYGKQJPBQR-UHFFFAOYSA-N 4H-1,2,4-triazole Chemical class C=1N=CNN=1 NSPMIYGKQJPBQR-UHFFFAOYSA-N 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- JRKICGRDRMAZLK-UHFFFAOYSA-L peroxydisulfate Chemical compound [O-]S(=O)(=O)OOS([O-])(=O)=O JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 claims description 4
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 4
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 claims description 3
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 3
- PJANXHGTPQOBST-VAWYXSNFSA-N Stilbene Natural products C=1C=CC=CC=1/C=C/C1=CC=CC=C1 PJANXHGTPQOBST-VAWYXSNFSA-N 0.000 claims description 3
- 125000002252 acyl group Chemical group 0.000 claims description 3
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 3
- PJANXHGTPQOBST-UHFFFAOYSA-N stilbene Chemical compound C=1C=CC=CC=1C=CC1=CC=CC=C1 PJANXHGTPQOBST-UHFFFAOYSA-N 0.000 claims description 3
- 235000021286 stilbenes Nutrition 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 3
- 238000010422 painting Methods 0.000 abstract description 2
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 6
- 230000005525 hole transport Effects 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 5
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- MCJGNVYPOGVAJF-UHFFFAOYSA-N quinolin-8-ol Chemical class C1=CN=C2C(O)=CC=CC2=C1 MCJGNVYPOGVAJF-UHFFFAOYSA-N 0.000 description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000011368 organic material Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000005725 8-Hydroxyquinoline Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- NIHNNTQXNPWCJQ-UHFFFAOYSA-N fluorene Chemical compound C1=CC=C2CC3=CC=CC=C3C2=C1 NIHNNTQXNPWCJQ-UHFFFAOYSA-N 0.000 description 2
- 239000003446 ligand Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 229960003540 oxyquinoline Drugs 0.000 description 2
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 2
- 238000011020 pilot scale process Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- 230000004044 response Effects 0.000 description 2
- 238000002444 silanisation Methods 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- -1 spiro fluorenes Chemical class 0.000 description 2
- 239000001226 triphosphate Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 125000004105 2-pyridyl group Chemical group N1=C([*])C([H])=C([H])C([H])=C1[H] 0.000 description 1
- 229920000265 Polyparaphenylene Polymers 0.000 description 1
- WTKZEGDFNFYCGP-UHFFFAOYSA-N Pyrazole Chemical class C=1C=NNC=1 WTKZEGDFNFYCGP-UHFFFAOYSA-N 0.000 description 1
- 239000006087 Silane Coupling Agent Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- REDXJYDRNCIFBQ-UHFFFAOYSA-N aluminium(3+) Chemical compound [Al+3] REDXJYDRNCIFBQ-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000005684 electric field Effects 0.000 description 1
- 238000005401 electroluminescence Methods 0.000 description 1
- 238000000295 emission spectrum Methods 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000003760 hair shine Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 229910003471 inorganic composite material Inorganic materials 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 125000003226 pyrazolyl group Chemical group 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
- 125000003003 spiro group Chemical group 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- 238000012719 thermal polymerization Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
- H10K85/10—Organic polymers or oligomers
- H10K85/111—Organic polymers or oligomers comprising aromatic, heteroaromatic, or aryl chains, e.g. polyaniline, polyphenylene or polyphenylene vinylene
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K50/00—Organic light-emitting devices
- H10K50/10—OLEDs or polymer light-emitting diodes [PLED]
- H10K50/11—OLEDs or polymer light-emitting diodes [PLED] characterised by the electroluminescent [EL] layers
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K71/00—Manufacture or treatment specially adapted for the organic devices covered by this subclass
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Manufacturing & Machinery (AREA)
- Electroluminescent Light Sources (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611195588.6A CN106876611B (zh) | 2016-12-22 | 2016-12-22 | 一种用于oled显示的复合蓝光材料的制备方法及应用 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611195588.6A CN106876611B (zh) | 2016-12-22 | 2016-12-22 | 一种用于oled显示的复合蓝光材料的制备方法及应用 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106876611A CN106876611A (zh) | 2017-06-20 |
CN106876611B true CN106876611B (zh) | 2018-06-15 |
Family
ID=59163861
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201611195588.6A Expired - Fee Related CN106876611B (zh) | 2016-12-22 | 2016-12-22 | 一种用于oled显示的复合蓝光材料的制备方法及应用 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106876611B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112378890B (zh) * | 2020-10-28 | 2024-04-05 | 国合通用测试评价认证股份公司 | 一种基于磷光寿命判定琥珀产地的方法 |
CN115558487A (zh) * | 2022-07-01 | 2023-01-03 | 苏州新启材料科技有限公司 | 一种oled器件掺杂材料制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101113331A (zh) * | 2007-07-16 | 2008-01-30 | 华东师范大学 | 一种硅酸盐发光材料及其制备方法 |
CN103194234A (zh) * | 2013-04-12 | 2013-07-10 | 天津理工大学 | 一种蓝光激发的固溶体荧光材料 |
CN103833790A (zh) * | 2013-12-25 | 2014-06-04 | 石家庄诚志永华显示材料有限公司 | 一系列有机磷光oled材料 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100490206C (zh) * | 2003-12-25 | 2009-05-20 | 华南理工大学 | 有机/高分子发光二极管 |
-
2016
- 2016-12-22 CN CN201611195588.6A patent/CN106876611B/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101113331A (zh) * | 2007-07-16 | 2008-01-30 | 华东师范大学 | 一种硅酸盐发光材料及其制备方法 |
CN103194234A (zh) * | 2013-04-12 | 2013-07-10 | 天津理工大学 | 一种蓝光激发的固溶体荧光材料 |
CN103833790A (zh) * | 2013-12-25 | 2014-06-04 | 石家庄诚志永华显示材料有限公司 | 一系列有机磷光oled材料 |
Also Published As
Publication number | Publication date |
---|---|
CN106876611A (zh) | 2017-06-20 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN100509827C (zh) | 电致发光材料 | |
CN103601614B (zh) | 四苯乙烯衍生物及含该衍生物的白光有机电致发光器件 | |
CN102731406B (zh) | 菲并咪唑衍生物及在制备电致发光器件方面的应用 | |
CN100586243C (zh) | 一种红色有机电致发光器件及其制备方法 | |
CN102775398B (zh) | 一种新型双极性材料及其应用 | |
CN104099084A (zh) | 一种蓝色有机电致荧光材料其制备方法及应用 | |
CN101220034B (zh) | 一种∧-型超格斯碱衍生物类有机电致发光材料 | |
CN102136550A (zh) | 一种白光有机电致发光器件及其制备方法 | |
CN104004026A (zh) | 一种电负性磷光材料 | |
CN106876611B (zh) | 一种用于oled显示的复合蓝光材料的制备方法及应用 | |
CN103666455A (zh) | 一种新颖螺芴氧杂蒽类有机发光材料及其制备 | |
CN203085547U (zh) | 一种可变色发光元件、像素结构及显示装置 | |
CN101654430B (zh) | 一种宽带电子传输材料及其制备和应用 | |
CN100546067C (zh) | 一种有机电致发光器件及其制备方法 | |
CN102130301B (zh) | 基于色转换的白光有机电致发光器件及其制备方法 | |
CN102924520A (zh) | 具有双极载流子传输性能的蓝色磷光主体材料及制备方法 | |
CN107915737A (zh) | 一种含有咪唑结构的衍生物及其制备方法和有机电致发光器件 | |
CN101051673B (zh) | 一种能发出青光、紫光和白光的有机电致发光器件 | |
CN109761847A (zh) | 一种苯甲酰亚胺衍生物及其制备方法与应用 | |
CN109943321A (zh) | 具有延迟荧光性质的esipt发光材料及其制备方法与应用 | |
CN110396050B (zh) | 一种白光有机发光二极管及其制备方法 | |
CN108623515A (zh) | 含有不饱和含氮杂环的二氢蒽类化合物、有机电致发光器件及显示装置 | |
CN109768151B (zh) | 一种照明和显示用多色led及其制备方法 | |
CN101440088B (zh) | 金属有机配合物及其制备方法及发光材料和发光器件 | |
CN107903273A (zh) | 一种二苯并咪唑衍生物及其制备方法和有机发光器件 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20180517 Address after: 529000 39 East Sea Road, Jianghai District, Jiangmen, Guangdong Applicant after: Jiangmen Hailing Furnishings & Accssaries Co.,Ltd. Address before: 610091 Donghai Road, Jiao long industrial port, Qingyang District, Chengdu, Sichuan 4 Applicant before: CHENDU NEW KELI CHEMICAL SCIENCE Co.,Ltd. CHINA |
|
TA01 | Transfer of patent application right | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
CP03 | Change of name, title or address |
Address after: 528421 floor 1, No. 6, Tongyu West Road, caosan entrepreneurship Park, Guzhen Town, Zhongshan City, Guangdong Province (residence declaration) Patentee after: Zhongshan haijialing Home Accessories Co.,Ltd. Address before: 529000, No. 39 East harmony Road, Jianghai District, Guangdong, Jiangmen Patentee before: Jiangmen Hailing Furnishings & Accssaries Co.,Ltd. |
|
CP03 | Change of name, title or address | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180615 |
|
CF01 | Termination of patent right due to non-payment of annual fee |