CN106833850A - A kind of stainless steel processing environment-friendlycutting cutting fluid - Google Patents
A kind of stainless steel processing environment-friendlycutting cutting fluid Download PDFInfo
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- CN106833850A CN106833850A CN201611164598.3A CN201611164598A CN106833850A CN 106833850 A CN106833850 A CN 106833850A CN 201611164598 A CN201611164598 A CN 201611164598A CN 106833850 A CN106833850 A CN 106833850A
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M173/00—Lubricating compositions containing more than 10% water
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/085—Phosphorus oxides, acids or salts
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/087—Boron oxides, acids or salts
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/04—Ethers; Acetals; Ortho-esters; Ortho-carbonates
- C10M2207/046—Hydroxy ethers
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
- C10M2207/124—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms containing hydroxy groups; Ethers thereof
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/284—Esters of aromatic monocarboxylic acids
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/108—Polyethers, i.e. containing di- or higher polyoxyalkylene groups etherified
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
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- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/04—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions having a silicon-to-carbon bond, e.g. organo-silanes
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/06—Organic compounds derived from inorganic acids or metal salts
- C10M2227/061—Esters derived from boron
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/56—Boundary lubrication or thin film lubrication
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/64—Environmental friendly compositions
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
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Abstract
The invention discloses a kind of stainless steel processing environment-friendlycutting cutting fluid, it is related to a kind of cutting fluid, is specifically made up of following material:Cottonseed oil, peanut oil, rice bran oil, borax, oleic diethanola mide borate ester, six phosphate ester of cyclohexanhexanol, isooctyltriethoxysilane, potassium pyrophosphate, sodium citrate, NPE, tripropylene glycol, methyl p-hydroxybenzoate, Phenoxyethanol, water.Obtained cutting liquid energy of the invention forms diaphragm on the metal surface; make lathe, workpiece, cutter from the corrosion of surrounding medium; and with good lubricity, rust-preventing characteristic, permeability and cleaning; the cutting precision and cutting speed of stainless steel process can be effectively improved; and with environmental pollution it is small the characteristics of, use value is higher.
Description
Technical field
The present invention relates to a kind of cutting fluid, and in particular to a kind of stainless steel processing environment-friendlycutting cutting fluid.
Background technology
Cutting fluid be it is a kind of cut used in metal, cut, grind process, for cooling down and lubricating the work of cutter and workpiece
Industry liquid, cutting fluid is formed by various super strong functional auxiliary agents through compound compatibility, is provided simultaneously with good cooling performance, lubricity
Energy, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable feature, be in stainless steel processing essential material it
One.
The base oil mostly refined mineral oil used in water-base cutting fluid conventional at present, refined mineral oil is with a long history,
It is technical maturity, cheap, but its biodegradability is weaker, there is a certain degree of pollution to environment.Plant is used to this people
Thing oil replaces mineral oil, although plant oil degradation capabilities are stronger, but its hydrolysis, oxidation, aging instability limit
Its popularization for using, performance needs further improvement badly.
The content of the invention
The present invention is intended to provide a kind of stainless steel processing environment-friendlycutting cutting fluid.
The present invention is achieved through the following technical solutions:
A kind of stainless steel processing environment-friendlycutting cutting fluid, is made up of the material of following weight portion:
2 ~ 3 parts of cottonseed oils, 1 ~ 2 part of peanut oil, 1.5 ~ 2.5 parts of rice bran oils, 2 ~ 4 parts of boraxs, 4 ~ 6 parts of oleic acid diethyl amide boric acid
Ester, 3 ~ 5 parts of six phosphate ester of cyclohexanhexanol, 1 ~ 2 part of isooctyltriethoxysilane, 0.5 ~ 1.5 part of potassium pyrophosphate, 0.5 ~ 1 part of lemon
Lemon acid sodium, 3 ~ 4 parts of NPEs, 0.5 ~ 1 part of tripropylene glycol, 0.5 ~ 1 part of methyl p-hydroxybenzoate, 0.2 ~ 0.5
Part Phenoxyethanol, 140 ~ 150 parts of water.
Preferably, it is made up of the material of following weight portion:
2.5 parts of cottonseed oils, 1.5 parts of peanut oil, 2 parts of rice bran oils, 3 parts of boraxs, 5 parts of oleic diethanola mide borate esters, 4 parts of hexamethylenes
The phosphate of six alcohol six, 1.5 parts of isooctyltriethoxysilanes, 1 part of potassium pyrophosphate, 0.8 part of sodium citrate, 3.5 parts of nonyl phenols gather
Oxygen vinethene, 0.7 part of tripropylene glycol, 0.8 part of methyl p-hydroxybenzoate, 0.4 part of Phenoxyethanol, 145 parts of water.
Further, the cutting fluid when in use with water by volume 1:Used after 8 ~ 12 dilutions.
A kind of preparation method of stainless steel processing environment-friendlycutting cutting fluid, comprises the following steps:
(1)First cottonseed oil, peanut oil and rice bran oil are mixed jointly, after standing 3 ~ 4 days, it is standby that elimination impurity obtains miscella;
(2)By step(1)The miscella of gained is put into reactor, adds the modification liquid of its gross mass 1 ~ 1.5%, it is heated to 43 ~
47 DEG C, with 800 ~ 900 revs/min of 1.5 ~ 2h of rotating speed stir process after, then move it to temperature for low under conditions of -2 ~ -4 DEG C
Temperature preserves 1 ~ 1.5h, finally carries out filtering the miscella that must be modified standby again;Each material composition and corresponding in the modification liquid
Percentage by weight is as follows:2 ~ 3% magnesium chlorides, 3 ~ 4% zinc sulfate, 1 ~ 2% cerous nitrate, 3 ~ 5% n-hexanes, 2 ~ 4% hexadecyl hydrosulfates
Sodium, 4 ~ 6% ether, balance of water;
(3)By step(2)The same borax of modified miscella of gained, oleic diethanola mide borate ester, six phosphate ester of cyclohexanhexanol,
Isooctyltriethoxysilane, potassium pyrophosphate, sodium citrate, NPE, tripropylene glycol, P-hydroxybenzoic acid first
Ester, Phenoxyethanol, water mixing, heating keeping temperature is 50 ~ 53 DEG C, and cutting fluid is obtained final product after being stirred continuously uniformly.
The present invention has the advantages that:
The present invention reasonably combined cottonseed oil, peanut oil, three kinds of vegetable oil of composition of rice bran oil, improve content of fatty acid very well
Proportioning, improve overall characteristic, it is to avoid the problem of single component function short slab, it is carried out using modification liquid in the preparation
Modification, reduces the content of its colloid, gossypol etc., optimizes the ratio of unrighted acid, its is improved well resistance to
Hydrolysis, anti-aging property, coordinate the collective effect of remaining composition, obtained cutting liquid energy to form diaphragm on the metal surface,
Make lathe, workpiece, cutter from the corrosion of surrounding medium, and with good lubricity, rust-preventing characteristic, permeability and cleaning,
Can effectively improve the cutting precision and cutting speed of stainless steel process, and with environmental pollution it is small the characteristics of, use value
It is higher.
Specific embodiment
Embodiment 1
A kind of stainless steel processing environment-friendlycutting cutting fluid, is made up of the material of following weight portion:
2 parts of cottonseed oils, 1 part of peanut oil, 1.5 parts of rice bran oils, 2 parts of boraxs, 4 parts of oleic diethanola mide borate esters, 3 parts of hexamethylenes six
The phosphate of alcohol six, 1 part of isooctyltriethoxysilane, 0.5 part of potassium pyrophosphate, 0.5 part of sodium citrate, 3 parts of polyoxyethylene nonyl phenyl second
Alkene ether, 0.5 part of tripropylene glycol, 0.5 part of methyl p-hydroxybenzoate, 0.2 part of Phenoxyethanol, 140 parts of water.
Further, the cutting fluid when in use with water by volume 1:Used after 10 dilutions.
A kind of preparation method of stainless steel processing environment-friendlycutting cutting fluid, comprises the following steps:
(1)First cottonseed oil, peanut oil and rice bran oil are mixed jointly, after standing 3 days, it is standby that elimination impurity obtains miscella;
(2)By step(1)The miscella of gained is put into reactor, adds the modification liquid of its gross mass 1%, is heated to 45 DEG C, with
After 850 revs/min of rotating speed stir process 1.8h, then it is Cord blood 1.2h under conditions of -2 DEG C to move it to temperature, finally
Carry out filtering the miscella that must be modified standby again;Each material composition and corresponding percentage by weight are as follows in the modification liquid:
2.5% magnesium chloride, 3.5% zinc sulfate, 1.5% cerous nitrate, 4% n-hexane, 3% sodium hexadecyl sulfate, 5% ether, balance of water;
(3)By step(2)The same borax of modified miscella of gained, oleic diethanola mide borate ester, six phosphate ester of cyclohexanhexanol,
Isooctyltriethoxysilane, potassium pyrophosphate, sodium citrate, NPE, tripropylene glycol, P-hydroxybenzoic acid first
Ester, Phenoxyethanol, water mixing, heating keeping temperature is 52 DEG C, and cutting fluid is obtained final product after being stirred continuously uniformly.
Embodiment 2
A kind of stainless steel processing environment-friendlycutting cutting fluid, is made up of the material of following weight portion:
2.5 parts of cottonseed oils, 1.5 parts of peanut oil, 2 parts of rice bran oils, 3 parts of boraxs, 5 parts of oleic diethanola mide borate esters, 4 parts of hexamethylenes
The phosphate of six alcohol six, 1.5 parts of isooctyltriethoxysilanes, 1 part of potassium pyrophosphate, 0.8 part of sodium citrate, 3.5 parts of nonyl phenols gather
Oxygen vinethene, 0.7 part of tripropylene glycol, 0.8 part of methyl p-hydroxybenzoate, 0.4 part of Phenoxyethanol, 145 parts of water.Remaining method is walked
Suddenly with embodiment 1.
Embodiment 3
A kind of stainless steel processing environment-friendlycutting cutting fluid, is made up of the material of following weight portion:
3 parts of cottonseed oils, 2 parts of peanut oil, 2.5 parts of rice bran oils, 4 parts of boraxs, 6 parts of oleic diethanola mide borate esters, 5 parts of hexamethylenes six
The phosphate of alcohol six, 2 parts of isooctyltriethoxysilanes, 1.5 parts of potassium pyrophosphates, 1 part of sodium citrate, 4 parts of Nonyl phenos
Ether, 1 part of tripropylene glycol, 1 part of methyl p-hydroxybenzoate, 0.5 part of Phenoxyethanol, 150 parts of water.The same embodiment of remaining method and step
1。
Comparative example 1
This comparative example 1 compared with Example 1, with etc. mass parts cottonseed oil replace peanut oil and rice bran oil, in addition
Method and step all same.
Comparative example 2
This comparative example 2 compared with Example 2, does not do modification, i.e., to cottonseed oil, peanut oil, rice bran oil in the preparation
Save preparation process(1)With(2), method and step all same in addition.
Control group
Existing commercially available plant oil base cutting fluid.
In order to contrast effect of the present invention, performance test is carried out to cutting fluid obtained in above-mentioned six kinds of modes, specifically contrast number
According to as shown in table 1 below:
Table 1
One-level grey cast-iron corrosion test(h) | Red copper corrosion test(h) | Corrosion of aluminium alloy is tested(h) | |
Embodiment 1 | 75 | 24 | 9 |
Embodiment 2 | 77 | 25 | 10 |
Embodiment 3 | 76 | 24 | 10 |
Comparative example 1 | 70 | 21 | 7 |
Comparative example 2 | 68 | 21 | 7 |
Control group | 60 | 18 | 6 |
Test method | GB/T6144-85 | GB/T6144-85 | GB/T6144-85 |
The obtained cutting fluid overall characteristic of the present invention can be seen that more preferably by upper table 1, use value is higher.
Claims (4)
1. a kind of stainless steel processing environment-friendlycutting cutting fluid, it is characterised in that be made up of the material of following weight portion:
2 ~ 3 parts of cottonseed oils, 1 ~ 2 part of peanut oil, 1.5 ~ 2.5 parts of rice bran oils, 2 ~ 4 parts of boraxs, 4 ~ 6 parts of oleic acid diethyl amide boric acid
Ester, 3 ~ 5 parts of six phosphate ester of cyclohexanhexanol, 1 ~ 2 part of isooctyltriethoxysilane, 0.5 ~ 1.5 part of potassium pyrophosphate, 0.5 ~ 1 part of lemon
Lemon acid sodium, 3 ~ 4 parts of NPEs, 0.5 ~ 1 part of tripropylene glycol, 0.5 ~ 1 part of methyl p-hydroxybenzoate, 0.2 ~ 0.5
Part Phenoxyethanol, 140 ~ 150 parts of water.
2. a kind of stainless steel processing environment-friendlycutting cutting fluid according to claim 1, it is characterised in that by following weight portion
Material is made:
2.5 parts of cottonseed oils, 1.5 parts of peanut oil, 2 parts of rice bran oils, 3 parts of boraxs, 5 parts of oleic diethanola mide borate esters, 4 parts of hexamethylenes
The phosphate of six alcohol six, 1.5 parts of isooctyltriethoxysilanes, 1 part of potassium pyrophosphate, 0.8 part of sodium citrate, 3.5 parts of nonyl phenols gather
Oxygen vinethene, 0.7 part of tripropylene glycol, 0.8 part of methyl p-hydroxybenzoate, 0.4 part of Phenoxyethanol, 145 parts of water.
3. a kind of stainless steel processing environment-friendlycutting cutting fluid according to claim 1 and 2, it is characterised in that the cutting fluid
When in use with water by volume 1:Used after 8 ~ 12 dilutions.
4. a kind of preparation method of stainless steel processing environment-friendlycutting cutting fluid as claimed in claim 1 or 2, it is characterised in that bag
Include following steps:
(1)First cottonseed oil, peanut oil and rice bran oil are mixed jointly, after standing 3 ~ 4 days, it is standby that elimination impurity obtains miscella;
(2)By step(1)The miscella of gained is put into reactor, adds the modification liquid of its gross mass 1 ~ 1.5%, it is heated to 43 ~
47 DEG C, with 800 ~ 900 revs/min of 1.5 ~ 2h of rotating speed stir process after, then move it to temperature for low under conditions of -2 ~ -4 DEG C
Temperature preserves 1 ~ 1.5h, finally carries out filtering the miscella that must be modified standby again;Each material composition and corresponding in the modification liquid
Percentage by weight is as follows:2 ~ 3% magnesium chlorides, 3 ~ 4% zinc sulfate, 1 ~ 2% cerous nitrate, 3 ~ 5% n-hexanes, 2 ~ 4% hexadecyl hydrosulfates
Sodium, 4 ~ 6% ether, balance of water;
(3)By step(2)The same borax of modified miscella of gained, oleic diethanola mide borate ester, six phosphate ester of cyclohexanhexanol,
Isooctyltriethoxysilane, potassium pyrophosphate, sodium citrate, NPE, tripropylene glycol, P-hydroxybenzoic acid first
Ester, Phenoxyethanol, water mixing, heating keeping temperature is 50 ~ 53 DEG C, and cutting fluid is obtained final product after being stirred continuously uniformly.
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CN102660364A (en) * | 2012-04-17 | 2012-09-12 | 广州市联诺化工科技有限公司 | Non-phosphorus non-silicon aluminum alloy cutting fluid and preparation method thereof |
CN103468382A (en) * | 2013-08-30 | 2013-12-25 | 广州机械科学研究院有限公司 | Boron-free chlorine-free formaldehyde-free microemulsified cutting fluid and application thereof |
CN104403772A (en) * | 2014-10-13 | 2015-03-11 | 巢湖广丰金属制品有限公司 | High-performance metal cutting fluid |
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CN102492533A (en) * | 2011-11-28 | 2012-06-13 | 上海应用技术学院 | Hard water-resistant semi-synthetic metal cutting fluid and preparation method thereof |
CN102618358A (en) * | 2012-03-06 | 2012-08-01 | 上海应用技术学院 | Green micro-emulsification metal machining liquid and preparation method thereof |
CN102660364A (en) * | 2012-04-17 | 2012-09-12 | 广州市联诺化工科技有限公司 | Non-phosphorus non-silicon aluminum alloy cutting fluid and preparation method thereof |
CN103468382A (en) * | 2013-08-30 | 2013-12-25 | 广州机械科学研究院有限公司 | Boron-free chlorine-free formaldehyde-free microemulsified cutting fluid and application thereof |
CN104403772A (en) * | 2014-10-13 | 2015-03-11 | 巢湖广丰金属制品有限公司 | High-performance metal cutting fluid |
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Application publication date: 20170613 |