CN106833187A - A kind of high abrasion-resistant environmental protection type water paint - Google Patents
A kind of high abrasion-resistant environmental protection type water paint Download PDFInfo
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- CN106833187A CN106833187A CN201611245972.2A CN201611245972A CN106833187A CN 106833187 A CN106833187 A CN 106833187A CN 201611245972 A CN201611245972 A CN 201611245972A CN 106833187 A CN106833187 A CN 106833187A
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- parts
- water paint
- environmental protection
- protection type
- high abrasion
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/45—Anti-settling agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention relates to technical field of coatings, and in particular to a kind of high abrasion-resistant environmental protection type water paint.Technical scheme is as follows：The water paint mainly includes 40 parts of water, 20 parts of acrylic emulsion, 0.3 part of defoamer, 12 parts of coffee function additive, 0.8 part of antiseptic, 1 part of dispersant, 2 parts of anti-settling agent, 0.9 part of levelling agent, and described anti-settling agent is by as follows into being grouped into：3 parts of rilanit special, 0.5 1 parts of sodium chloride；Described antiseptic includes the raw material of following mass fraction：0.5 part of polyurethane, 0.2 part of shitosan, 2 parts of Honegsukle flower P.E.Water paint composition disclosed by the invention is reasonable, and low cost, the compatibility between each component is good, good environmental protection；Waste resource coffee grounds is made full use of, after being processed to according to certain carbonization, the auxiliary agent of water paint is made, resource utilization is improve.
Description
Technical field
The present invention relates to a kind of high abrasion-resistant environmental protection type water paint, belong to technical field of coatings.
Background technology
In house decoration, by the harmful substances such as formaldehyde, benzene homologues, TVOC that various finishing materials are brought are caused
House ornamentation pollution and room air in harmful substance it is exceeded.The mouth for seriously having disturbed people is often lived.Human body is for a long time
Absorbing this gas containing formaldehyde can give rise to diseases, and serious goes back entail dangers to the life security of people.Therefore to finishing
Room and the furniture of new purchase afterwards will carry out the improvement of room air pollution, and eliminate the pernicious gas that new furniture is brought
Pollution.To ensure the content of indoor harmful gas within the scope of national regulation, people are made to live in an environment for health
In.Room after finishing and the room air pollution produced by the furniture of new purchase substantially have two sources：One is finishing
Or the surface coating of furniture, such as common paint generally all with organic solvent as paint solvent, these solvents contain benzene homologues,
VOC etc. harmful polluter.Another is the adhesive for being bonded various materials.
On the one hand water paint currently used in the market contains organic solvent in itself, formaldehyde etc. is volatilized after use and is harmful to
Material, another aspect coating can not have certain suction-operated such as activated carbon in itself.In addition, generally also there is film forming in water paint
When drying time it is long, film elasticity easily it is aging, flintiness is bad, it is impossible to effectively protection wall plaster bottom intensity so that
Produce metope cracking, come off, not only influence building attractive in appearance, and metope ftractures, the problems such as be easily caused metope leak, while water
Soluble paint is subject to biological damage, produces mouldy discoloration etc. to bring inconvenience to user.
The content of the invention
For deficiency of the prior art, it is an object of the invention to provide a kind of high abrasion-resistant environmental protection type water paint, can inhale
Attached indoor formaldehyde, organic pollutant etc., also with high into film hardness, the characteristics of wearability strong waterproof again.
Technical scheme is as follows：A kind of high abrasion-resistant environmental protection type water paint, by the raw material group of following mass fraction
Into：
40 parts of water
20 parts of acrylic emulsion
1-2 parts of coffee function additive
0.8 part of antiseptic
1 part of dispersant
2 parts of anti-settling agent
0.9 part of levelling agent
0.3 part of defoamer；
The preparation method of described coffee function additive is as follows：(1) it is 10- by 5 parts of drying of coffee grounds to moisture
15%, powder is made using pulverizer, 5 parts of shitosan is added, the two is well mixed, it is made 2-3mm using granulator granulation
Particle；(2) 30 parts of 0.6 part of dissolved in purified water amyloses, 0.6 part of polyethylene glycol are used；(3) particle of step (1) is added
Enter in the mixed liquor of step (2) preparation to impregnate 8 hours, afterwards in 80 DEG C of drying to moisture 8%；(4) it is step (3) is dry
In microwave high-temperature sintering furnace, 800-1000 DEG C carbonizes 10 hours particle after dry under nitrogen atmosphere；(5) by the particle after charing
It is made the powder that particle size is 50-100 μm；
Described anti-settling agent is by as follows into being grouped into：3 parts, sodium chloride 0.5-1 parts of rilanit special；
Described antiseptic includes the raw material of following mass fraction：0.5 part of polyurethane, 0.2 part of shitosan, honeysuckle are extracted
2 parts of thing.
Further, the mass fraction of described coffee function additive is 1 part.
Further, the mass fraction of sodium chloride is 1 part in described anti-settling agent.
Further, described high abrasion-resistant environmental protection type water paint preparation method is as follows：
(1) acrylic emulsion is mixed with water；
(2) to antiseptic, levelling agent, coffee function additive, dispersant is sequentially added in step (1), stir 20 minutes；
(3) after the mixture for obtaining step (2) is stirred 10 minutes with the rotating speed of 1500rpm, defoamer, anti-settling is added
Agent, stirs, and filters and packages.
Beneficial effects of the present invention are as follows：
(1) water paint composition disclosed by the invention is reasonable, and low cost, the compatibility between each component is good, environmental-protecting performance
It is good；
(2) the coffee function additive of the submicron size particle used in water paint of the present invention, by interior after charing process
Portion's adsorbable gas componant containing hole, such as formaldehyde, VOC etc.；Due to complicated component in coffee grounds, it is impossible to according to prior art
The preparation method of middle activated carbon is simply processed, and needs first to coordinate the shitosan with coffee grounds equal quality number in preparation process, this
Pellet hardness after sample charing can just meet use requirement, with good wearability；In addition, amylose is compared with amylopectin
Using effect is good；
(3) present invention makes full use of waste resource coffee grounds, after being processed to according to certain carbonization, is made aqueous
The auxiliary agent of coating, improves resource utilization；
(4) addition of micron-sized coffee function additive, dissolubility and antibacterial ability to water paint bring certain
Influence, need to coordinate the special applicable anti-settling agent being made up of rilanit special and sodium chloride to be used together, and the present invention is simultaneously
It is prepared for being specially adapted for the antiseptic of water paint of the present invention.
Specific embodiment
Technical scheme is further described with reference to specific embodiment, but the present invention is not with any shape
Formula is limited to embodiment content.Test method described in embodiment unless otherwise specified, is conventional method；Such as without special theory
Bright, the reagent and biomaterial are commercially obtained.Levelling agent, dispersant, defoamer are in following examples
This area any one.
Embodiment 1
The preparation method of coffee function additive is as follows in the present embodiment：(1) it is by 5 grams of drying to moistures of coffee grounds
10%, powder is made using pulverizer, 5 grams of shitosan is added, the two is well mixed, it is made 3mm's using granulator granulation
Particle；(2) 30 grams of 0.6 gram of dissolved in purified water amyloses, 0.6 gram of polyethylene glycol are used；(3) particle of step (1) is added
Impregnated in the mixed liquor prepared to step (2) 8 hours, afterwards in 80 DEG C of drying to moisture 8%；(4) step (3) is dried
In microwave high-temperature sintering furnace, lower 800 DEG C of nitrogen atmosphere is carbonized 10 hours particle afterwards；(5) particle after charing is made grain
Footpath size is 80 μm of powder；
A kind of high abrasion-resistant environmental protection type water paint, is made up of the raw material of following mass fraction：
40 grams of water
20 grams of acrylic emulsion
1 gram of coffee function additive
0.8 gram of antiseptic
1 gram of dispersant
2 grams of anti-settling agent
0.9 gram of levelling agent
0.3 gram of defoamer；
Described anti-settling agent is by as follows into being grouped into：3 grams of rilanit special, 0.5 gram of sodium chloride；
Described antiseptic includes the raw material of following mass fraction：0.5 gram of polyurethane, 0.2 gram of shitosan, honeysuckle are extracted
2 grams of thing.
The preparation method of described high abrasion-resistant environmental protection type water paint is as follows：
(1) acrylic emulsion is mixed with water；
(2) to antiseptic, levelling agent, multifunctional coating auxiliary agent, dispersant is sequentially added in step (1), stir 20 minutes；
(3) after the mixture for obtaining step (2) is stirred 10 minutes with the rotating speed of 1500rpm, defoamer, anti-settling agent are added
And coalescents, stir, filter and package.
Embodiment 2
The preparation method of coffee function additive is as follows in the present embodiment：(1) it is by 5 grams of drying to moistures of coffee grounds
15%, powder is made using pulverizer, 5 grams of shitosan is added, the two is well mixed, it is made 3mm's using granulator granulation
Particle；(2) 30 grams of 0.6 gram of dissolved in purified water amyloses, 0.6 gram of polyethylene glycol are used；(3) particle of step (1) is added
Impregnated in the mixed liquor prepared to step (2) 8 hours, afterwards in 80 DEG C of drying to moisture 8%；(4) step (3) is dried
In microwave high-temperature sintering furnace, lower 800 DEG C of nitrogen atmosphere is carbonized 10 hours particle afterwards；(5) particle after charing is made grain
Footpath size is 50 μm of powder；
A kind of high abrasion-resistant environmental protection type water paint, is made up of the raw material of following mass fraction：
40 grams of water
20 grams of acrylic emulsion
2 grams of coffee function additive
0.8 gram of antiseptic
1 gram of dispersant
2 grams of anti-settling agent
0.9 gram of levelling agent
0.3 gram of defoamer；
Described anti-settling agent is by as follows into being grouped into：3 grams of rilanit special, 1 gram of sodium chloride；
Described antiseptic includes the raw material of following mass fraction：0.5 gram of polyurethane, 0.2 gram of shitosan, honeysuckle are extracted
2 grams of thing.
The preparation method of described high abrasion-resistant environmental protection type water paint is as follows：
(1) acrylic emulsion is mixed with water；
(2) to antiseptic, levelling agent, multifunctional coating auxiliary agent, dispersant is sequentially added in step (1), stir 20 minutes；
(3) after the mixture for obtaining step (2) is stirred 10 minutes with the rotating speed of 1500rpm, defoamer, anti-settling agent are added
And coalescents, stir, filter and package.
Embodiment 3
Shitosan is not used in method and step (1) prepared by the present embodiment coffee function additive, other are with embodiment 2.
Embodiment 4
Method prepared by the present embodiment coffee function additive replaces amylose with the amylopectin of equal quality number, its
He is with embodiment 2.
Embodiment 5
In addition to anti-settling agent is commercially available organobentonite in raw material, other are with embodiment 2 for the present embodiment.
Embodiment 6
In addition to antiseptic is the different thiophene mistake quinoline ketone of commercially available 5- chloro-2-methyls -3- in raw material, other are with implementation for the present embodiment
Example 2.
Performance test
The VOC content of above-mentioned coating is tested according to GB18582-2008, is tested according to GB1720, GB1728, GB1732
The adhesive force of above-mentioned coating, drying time and impact resistance, the results are shown in Table 1.
Table 1
Bactericide is tested
Escherichia coli, black-koji mould even spread are had the slide of above-mentioned coating, through 0,5,15,30,60,120 hours
It is placed in physiological saline after being gently stained with bacterium solution with swab stick afterwards, is vibrated, take 0.5mL in culture dish, culture medium is added, in culture medium 48
Hour, number clump count is taken out, sterilizing rate is calculated according to formula：Sterilizing rate=(clump count after initial clump count-sterilization)/initial bacterium
Fall number × 100%, the results are shown in Table 2.
Table 2
By Tables 1 and 2 as can be seen that coating antibiosis fungicidal properties of the invention is good, harmful substance volatilization is few, film forming is fast,
Without additionally adding coalescents, cost is reduced, the present invention proposes a kind of water paint difference of hardness, harmful substance of solving and waves
Send out new departure of serious problems.
Formaldehyde removing effect detection method
Foundation《JC/T 1074-2008 function of purifying indoor air coating material purifying properties》
According to the theoretical brushing amount of product, four pieces of 500mm × 500mm glass plate (thickness are brushed to even application method
4mm~6mm) a surface, tested after drying 24h in experimental cabin.
The test piece and blank glass plate that will be prepared are respectively put into sample chamber and contrast cabin, and four pieces are placed in each cabin
In on specimen holder, the one of model brushing sample places plate facing to cabin center.
One glass dish is put into the bottom of experimental cabin, then closed test takes 3 μ L and analyze pure first with micro syringe
Aldehyde solution, is dropped in glass dish by injection orifice, closed injection orifice.
Its concentration of gas test in cabin is gathered after closed 1h, this concentration is initial concentration (n0), gas in cabin is gathered after 24h
And its concentration is tested, this concentration is termination concentration (n1).Fan 30min is opened before collection gas, is closed during sampling.By GB/T
16129 concentration for using AHMT spectrophotometric analysis formaldehyde.
Sample purification efficiency calculation formula is：R (%)=(n1-n2)/n1× 100%；
Wherein：R- purification efficiencies (%)；
n1- contrast cabin surveys gas and terminates concentration, and unit is every cubic metre of milligram (mg/m3)；
n2- sample chamber surveys gas and terminates concentration, and unit is every cubic metre of milligram (mg/m3)。
By test, water paint purifying formaldehyde efficiency prepared by embodiment 2 is 90.6%, more than required by national standard
75%, and the water paint PARA FORMALDEHYDE PRILLS(91,95) purification efficiency of the preparation of embodiment 3 is 20%, illustrate the present invention with excellent purification
The effect of formaldehyde.
The present invention illustrates detailed process equipment of the invention and technological process by above-described embodiment, but the present invention is not
Above-mentioned detailed process equipment and technological process are confined to, that is, do not mean that the present invention has to rely on above-mentioned detailed process equipment and work
Skill flow could be implemented.Person of ordinary skill in the field it will be clearly understood that any improvement in the present invention, to product of the present invention
Addition, selection of concrete mode of the equivalence replacement and auxiliary element of each raw material etc., all fall within protection scope of the present invention and public affairs
Within the scope of opening.
Claims (4)
1. a kind of high abrasion-resistant environmental protection type water paint, it is characterised in that be made up of the raw material of following mass fraction：
40 parts of water
20 parts of acrylic emulsion
1-2 parts of coffee function additive
0.8 part of antiseptic
1 part of dispersant
2 parts of anti-settling agent
0.9 part of levelling agent
0.3 part of defoamer；
The preparation method of described coffee function additive is as follows：(1) it is 10-15% to moisture by 5 parts of drying of coffee grounds, makes
Powder is made of pulverizer, 5 parts of shitosan is added, the two is well mixed, the particle of 2-3mm is made using granulator granulation；
(2) 30 parts of 0.6 part of dissolved in purified water amyloses, 0.6 part of polyethylene glycol are used；(3) particle of step (1) is added to step
(2) impregnated in the mixed liquor for preparing 8 hours, afterwards in 80 DEG C of drying to moisture 8%；(4) by dried of step (3)
In microwave high-temperature sintering furnace, 800-1000 DEG C carbonizes 10 hours grain under nitrogen atmosphere；(5) particle after charing is made particle diameter
Size is 50-100 μm of powder；
Described anti-settling agent is by as follows into being grouped into：3 parts, sodium chloride 0.5-1 parts of rilanit special；
Described antiseptic includes the raw material of following mass fraction：0.5 part of polyurethane, 0.2 part of shitosan, Honegsukle flower P.E 2
Part.
2. a kind of high abrasion-resistant environmental protection type water paint as claimed in claim 1, it is characterised in that described coffee function additive
Mass fraction be 1 part.
3. a kind of high abrasion-resistant environmental protection type water paint as claimed in claim 1, it is characterised in that chlorination in described anti-settling agent
The mass fraction of sodium is 1 part.
4. a kind of high abrasion-resistant environmental protection type water paint as claimed in claim 1, it is characterised in that preparation method is as follows：
(1) acrylic emulsion is mixed with water；
(2) to antiseptic, levelling agent, coffee function additive, dispersant is sequentially added in step (1), stir 20 minutes；
(3) after the mixture for obtaining step (2) is stirred 10 minutes with the rotating speed of 1500rpm, defoamer, anti-settling agent are added, is stirred
Mix uniform, filter and package.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611245972.2A CN106833187A (en) | 2016-12-29 | 2016-12-29 | A kind of high abrasion-resistant environmental protection type water paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611245972.2A CN106833187A (en) | 2016-12-29 | 2016-12-29 | A kind of high abrasion-resistant environmental protection type water paint |
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| CN106833187A true CN106833187A (en) | 2017-06-13 |
Family
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| CN201611245972.2A Pending CN106833187A (en) | 2016-12-29 | 2016-12-29 | A kind of high abrasion-resistant environmental protection type water paint |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110396863A (en) * | 2018-04-24 | 2019-11-01 | 施泓亦 | Synthetic paper and its manufacturing method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110396863A (en) * | 2018-04-24 | 2019-11-01 | 施泓亦 | Synthetic paper and its manufacturing method |
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