CN106820146B - Crystal ice powder and preparation method thereof - Google Patents

Crystal ice powder and preparation method thereof Download PDF

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Publication number
CN106820146B
CN106820146B CN201710063250.3A CN201710063250A CN106820146B CN 106820146 B CN106820146 B CN 106820146B CN 201710063250 A CN201710063250 A CN 201710063250A CN 106820146 B CN106820146 B CN 106820146B
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powder
crystal ice
hot water
inner container
ice powder
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CN106820146A (en
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胡荣强
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Chengdu Atohuyo Technology Co ltd
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Chengdu Atohuyo Technology Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65DCONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D31/00Bags or like containers made of paper and having structural provision for thickness of contents
    • B65D31/12Bags or like containers made of paper and having structural provision for thickness of contents with two or more compartments
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65DCONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D31/00Bags or like containers made of paper and having structural provision for thickness of contents
    • B65D31/14Valve bags, i.e. with valves for filling
    • B65D31/145Valve bags, i.e. with valves for filling the filling port being provided in a flat upper sealing-edge
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Confectionery (AREA)

Abstract

The invention relates to crystal ice powder and a preparation method thereof, wherein the crystal ice powder is prepared by uniformly mixing pseudo-acid syrup, auxiliary material liquid and seasoning liquid which are prepared by processing main materials, auxiliary materials and seasonings through a low-temperature ultrahigh-pressure technology, adding a coagulant, and freeze-drying the mixture by a freeze-dryer to obtain the crystal ice powder, and mixing the crystal ice powder and hot water according to the weight ratio of 1: 70-160, wherein the main materials are pseudo-acid syrup, the auxiliary materials are health-care food materials, the seasonings are saccharides and/or substances rich in vitamins, the coagulant is carrageenan or agar, the weight percentage of the main materials is 35-50%, the weight percentage of the auxiliary materials is 9-44.75%, the weight percentage of the seasonings is 20-40%, the weight percentage of the coagulant is 0.25-1.0%, and the sum of the weight percentages of all the components is 100%.

Description

Crystal ice powder and preparation method thereof
Technical Field
The invention relates to ice powder, in particular to crystal ice powder and a manufacturing method thereof.
Background
The ice powder is a cold drink food which is loved by people in summer, and a bowl of ice powder can be eaten in the hot summer of summer inflammation, so that the ice powder is very refreshing. The existing ice powder on the market at present is only supplied by retail stall, and the sanitary condition is poor. Many people want to eat and worry about that the sanitary problem is dare not to eat. Although the raw materials of the ice powder in small packages are also supplied in malls such as supermarkets and the like, the ice powder cannot be directly eaten after being purchased, and can be eaten after being taken home and added with water, heated and cooled, and most of the existing ice powder is only a pure cold drink food and has no more nutrition and health care effects.
In order to solve the problems in the prior art, Chinese patent CN1802980A discloses instant convenient healthy ice powder, which is prepared by processing main materials, auxiliary materials and nutrient condiments into finished products for direct eating or into ice powder sets with different tastes and can be eaten through simple processing. The weight ratio of the main materials is as follows: 10-30 parts of konjak extract, 10-80 parts of seaweed extract and 10-60 parts of bean jelly seed extract. The main material is prepared by mixing the above materials, adding 5-15 times of purified water, heating to 85-100 deg.C, stirring, immediately packaging into food-grade plastic container, sealing with PVC/PPC composite film, sterilizing, and packaging. The ice powder of the invention has the functions of clearing away summer heat, providing vitamins and minerals required by human body, etc. However, the instant convenient and healthy ice powder provided by the patent has at least the following defects:
(1) the instant convenient and healthy ice powder needs to be heated to 85-100 ℃ in the preparation process, and the nutritional ingredients and the taste of each material are easily damaged by high temperature, so that the preparation of the ice powder with smooth and fine outlet and rich nutritional ingredients is not facilitated;
(2) the instant convenient healthy ice powder adopts the konjak extract as the raw material, and because the bonding mode of konjak glucomannan monosaccharide in the konjak extract is similar to that of cellulose, the konjak glucomannan monosaccharide cannot be degraded into monosaccharide to be absorbed in small intestine, the instant convenient healthy ice powder provided by the patent is not suitable for people suffering from diabetes;
(3) the instant convenient and healthy ice powder takes carrageenan, konjac flour and konjac gum as raw materials, contains insoluble starch and suspended small particle impurities, and has low transparency and poor visual effect.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides crystal ice powder which is prepared by uniformly mixing pseudo-acid syrup, auxiliary material liquid and seasoning liquid which are prepared by processing a main material, auxiliary materials and seasonings through a low-temperature ultrahigh-pressure technology, adding a coagulant, and freeze-drying the mixture through a freeze-drying machine, wherein the crystal ice powder is prepared by mixing the hot water with the pseudo-acid syrup according to a weight ratio of 1: 70-160, the main material is pseudo-acid syrup, the auxiliary materials are health-care food materials, the seasonings are saccharides and/or substances rich in vitamins, the coagulant is carrageenan or agar, the main material accounts for 35-50 wt%, the auxiliary materials account for 9-44.75 wt%, the seasonings account for 20-40 wt%, the coagulant accounts for 0.25-1.0 wt%, and the sum of the weight percentages of all the components is 100%.
According to a preferred embodiment, the nicandra physaloides is prepared by the following method: taking and adding the nicandra physaloides seeds into purified water in a weight ratio of 1: 1-10: 1 with the nicandra physaloides seeds, putting the purified water added with the nicandra physaloides seeds into ultrahigh pressure treatment equipment, keeping the ultrahigh pressure for 2-5 min under the conditions of low temperature and ultrahigh pressure of 500-1000 MPa and temperature of below 20 ℃ to obtain nicandra physaloides seed extracting solution, and filtering the nicandra physaloides seed extracting solution to obtain the nicandra physaloides.
According to a preferred embodiment, the auxiliary liquid is prepared by the following method: taking auxiliary materials, adding the auxiliary materials into purified water in a weight ratio of 1: 1-10: 1 to the auxiliary materials, putting the purified water added with the auxiliary materials into ultrahigh pressure treatment equipment, keeping the pressure of the purified water at 500-1000 MPa and the temperature of the purified water below 20 ℃ for 2-10 min to obtain auxiliary material extracting solution, and filtering the auxiliary material extracting solution to obtain the auxiliary material liquid.
According to a preferred embodiment, the seasoning liquid is prepared by the following method: taking seasonings, adding the seasonings into purified water in a weight ratio of 1: 1-10: 1 to the seasonings, putting the purified water added with the seasonings into ultrahigh pressure treatment equipment, keeping the pressure at 500-1000 MPa and the temperature below 20 ℃ for 3-8 min under the conditions of low temperature and ultrahigh pressure to obtain seasoning extracting solution, and filtering the seasoning extracting solution to obtain the seasoning liquid.
According to a preferred embodiment, the auxiliary material liquid and the seasoning liquid are added into the pseudo-acid syrup and uniformly stirred, the coagulant is added into the mixture to obtain a solidified substance containing the pseudo-acid syrup, the auxiliary material liquid and the seasoning liquid, the solidified substance is quickly frozen at the temperature of-10 to-5 ℃ for 30 to 60min, the frozen solidified substance which is quickly frozen into ice is sublimated into water vapor at the pressure of 5.0 to 10.0KPa to be discharged, and the solidified substance is frozen and sublimated to obtain the crystal ice powder.
According to a preferred embodiment, the crystal ice powder is in the form of a liquid-tight ice powder bag with a liquid valve, comprising: the powder filling device comprises a liquid-tight flexible powder bin, an inner container and an outer container, wherein crystal ice powder is stored in the liquid-tight flexible powder bin in advance, the volume of the inner container is larger than that of the flexible powder bin, a connecting pipeline is arranged between the flexible powder bin and the inner container, and a powder diaphragm is arranged in the connecting pipeline.
The outer container of the invention is flexible, the inner container plays the role of a mixing cavity, and the lower end of the inner cavity of the inner container serving as the mixing cavity can be communicated with the flexible powder bin through fluid. The crystal ice powder can also be suitable for aerospace environment or long-distance hiking, and can effectively reduce load when in use. Particularly, the water is required to be boiled to 100 ℃ in the field environment to ensure that bacteria are killed, however, the field condition is difficult to accurately balance whether the water is cooled to a good mixing temperature of 70-75 ℃, hot water is firstly obtained through the inner layer container, heat can be dissipated through the outer layer container, and the crystal ice powder in the flexible powder bin slowly releases into the mixing cavity due to the heat insulation measure of the invention when the water temperature is reduced, so that the crystal ice powder can be optimally prepared.
According to a preferred embodiment, the outer container encloses a flexible powder bin and an inner container which are integrally formed with each other in a liquid-tight manner from the outside, wherein the flexible powder bin and the inner container are respectively injection molded in two different compositions in the same process, so that the flexible powder bin and the inner container can withstand high temperature while the rigidity of the inner container is significantly greater than that of the flexible powder bin, wherein ice powder contained in the flexible powder bin can enter the inner container only after being filled with hot water, so that the mixing of the ice powder and the hot water can be completed by pressing the flexible powder bin. Preferably, the inner container is made of a generally rigid material. The flexible powder bin is made of a common flexible material.
According to a preferred embodiment, the powder diaphragm exists in a screen shape after injection molding, so that crystal ice powder is allowed to be poured into the flexible powder bin; after the crystal ice powder is filled, the powder diaphragm is coated by high-density edible bonding material, so that the powder diaphragm which is not permeable to powder at normal temperature and is melted into hot water at the temperature of more than 50 ℃ is formed, and the crystal ice powder stored in the flexible powder bin can freely enter and exit the inner container in the hot water environment.
When the flexible powder bin and the inner container are manufactured, the powder diaphragm can be simply arranged in the connecting pipeline between the flexible powder bin and the inner container. After powder filling is completed, a step of coating a bonding material is added, and the powder diaphragm is formed into a diaphragm which is not permeable to normal-temperature powder through mutual combination of a viscous or pasty material and a silk screen. However, these viscous or pasty materials can be melted into water under hot water, so that the liquid communication of the connecting pipeline only under the hot water environment can be realized, and the purpose of mixing ice powder and hot water is achieved. In addition, the sticky or pasty materials do not destroy the mouthfeel of the ice powder, but are beneficial to forming the ice powder after cooling.
According to a preferred embodiment, the powder membrane comprises at least two layers, facing the flexible powder silo is a first membrane. Preferably, the first membrane is primarily a first edible material that is gas tight as the adhesive sealing material. Facing the inner container is a second membrane. Preferably, the second diaphragm is already adhered with the first edible material necessarily when the first diaphragm is manufactured, and it is necessary to add a second edible material which melts more slowly under hot water. It is also possible that the first edible material is the same as the second edible material, but the second edible material is used in significantly greater amounts. Preferably, the first and second edible materials are gelatin or sugar coatings or the like.
According to a preferred embodiment the connecting duct is injection moulded from the same composition as the inner receptacle at the end adjacent to the inner receptacle and as the flexible powder bin at the end adjacent to the flexible powder bin. Preferably, the section of the connecting duct for arranging the powder membrane is rigid, not less than, preferably corresponding to the rigidity of the inner container. Preferably, the inner cavity of the section in the connecting duct where the powder membrane is arranged is provided with a radial structure, for example a powder membrane fixing structure in the form of a projection or a recess. The radial structure may also be an internal thread, in particular a quick internal thread, for mounting the powder membrane. Wherein, the first fixing structure aiming at the first layer of diaphragm is preferably a radial boss; the second fixing structure for the second layer of membranes facing the inner container is preferably a fixing mechanism in the form of a notch, so that the wire mesh support for the second layer of membranes can be fixed by means of a snap connection.
According to a preferred embodiment, the outer container is made of a flexible heat conducting material, which is thermally isolated from the inner container by an insulating layer before the hot water is poured, wherein the insulating layer is detachably arranged outside the inner container, so that after the crystal ice powder is mixed with the hot water, the insulating layer is removed to achieve gradual cooling through the outer container made of the flexible heat conducting material. The invention adopts the heat insulation layer, so the temperature can not drop suddenly, further the conglomeration can not be generated, and the taste can not be deteriorated.
According to a preferred embodiment, the insulating layer is preferably made of a material that is very elastic, so that after removal it can be expanded to such an extent that the elastically expanded insulating layer can be placed tightly outside the outer container to form a hand grip, in order to assist the pressing of the flexible powder receptacle by its elastic force, without the user being scalded in the process.
According to a preferred embodiment, the hot water port penetrates the inner container and the outer container so that hot water for preparing the powdered ice is introduced into the cavity of the inner container through the hot water port when the powdered ice is prepared, the hot water port has a one-way valve structure, and the temperature of the hot water introduced into the cavity of the inner container through the one-way valve structure of the hot water port is 50 to 100 ℃.
The invention also provides a preparation method of the crystal ice powder, wherein the crystal ice powder is disposable automatic mixing crystal ice powder, and the disposable automatic mixing crystal ice powder is prepared by the following steps: hot water with the weight ratio of 70-160: 1 to the crystal ice powder is introduced into the cavity of the inner container of the ice powder bag through a hot water port of the ice powder bag storing the crystal ice powder, the outer container of the ice powder bag is extruded to transmit pressure change caused by contraction of the outer container to the flexible powder bin storing the crystal ice powder, and then the crystal ice powder stored in the flexible powder bin enters the cavity of the inner container to be mixed with the hot water to prepare the crystal ice powder.
According to a preferred embodiment, the ice powder bag at least comprises an outer container, an inner container and a flexible powder bin, wherein the outer container is a flexible container, and the inner container is a rigid container and is integrally formed with the flexible powder bin arranged at the lower end of the inner container through a connecting pipeline. Preferably, the outer container is a separate and reusable component.
According to a preferred embodiment, the flexible powder bin is connected in fluid communication to the cavity of the inner receptacle by the connecting duct.
According to a preferred embodiment, the inner container may have different shapes, so that the formed crystal ice powder has different shapes. Preferably, the inner container may be cylindrical, rectangular parallelepiped, square, flower-shaped, butterfly-shaped, etc.
According to a preferred embodiment, the ice powder bag further comprises a hot water port, the hot water port penetrates through the inner container and the outer container, and hot water for preparing the ice powder is introduced into the cavity of the inner container through the hot water port when the ice powder is prepared.
According to a preferred embodiment, the hot water port has a check valve structure, and the temperature of hot water introduced into the cavity of the inner container through the check valve structure of the hot water port is 50 to 100 ℃.
According to a preferred embodiment, the hot water port allows hot water to enter the cavity of the inner container from the outside and does not allow liquid in the cavity of the inner container to escape to the outside. Preferably, the hot water port also allows the gas in the cavity of the inner container to overflow outwards, so that the crystal ice powder in the flexible powder bin and the hot water can be uniformly mixed.
According to a preferred embodiment, the ice powder bag further comprises a heat insulation layer, the heat insulation layer is detachably arranged outside the inner container, and after the crystal ice powder is mixed with hot water, the heat insulation layer is removed to cool the crystal ice powder. Preferably, the insulation layer is a separate and reusable component.
According to a preferred embodiment, a gap between the outer container and the thermal insulation layer is filled with a liquid material in advance, and after the crystal ice powder is mixed with hot water, the outer container is squeezed again to cool the crystal ice powder through the liquid material filled in advance in the gap between the outer container and the thermal insulation layer. Preferably, the liquid material is cold water, ice water or an amine salt solution. The cooling speed of the crystal ice powder can be accelerated by the liquid material. Preferably, the pre-loaded liquid raw material is replaceable.
According to a preferred embodiment, after the crystal ice powder is mixed with hot water, the heat insulation layer is removed, and the outer container is further extruded. On the one hand, the crystal ice powder and hot water can be further uniformly mixed, and on the other hand, the crystal ice powder can be quickly cooled by the aid of the liquid pre-filled between the inner layer and the outer layer, so that the crystal ice powder is prepared.
According to a preferred embodiment, the connecting pipe has a powder membrane which is impermeable to powder at normal temperature and is melted into hot water at a temperature of 50 ℃ or higher so that the crystal ice powder stored in the flexible powder bin enters the cavity of the inner container.
According to a preferred embodiment, the powder membrane is made of edible material with specific taste, and the taste of the crystal ice powder can be changed after the powder membrane is melted into hot water. Preferably, the powder diaphragm is a sugar-coating film made of brown sugar, brown sugar or rock sugar. After the powder diaphragm is mixed with hot water, the sweet taste of the crystal ice powder can be increased.
According to a preferred embodiment, the flexible powder bin is made of an elastic material, when the outer container is squeezed, the pressure change of the pre-filled liquid caused by the contraction of the outer container is transmitted to the flexible powder bin, so that the flexible powder bin is contracted or expanded, and the crystal ice powder stored in the flexible powder bin enters the cavity of the inner container under the condition that the powder diaphragm is melted.
According to a preferred embodiment, when preparing the crystal ice powder, the outer container is squeezed for a plurality of times to uniformly mix the crystal ice powder stored in the flexible powder bin with the hot water introduced into the cavity of the inner container through the hot water port to prepare the crystal ice powder.
The crystal ice powder and the preparation method thereof provided by the invention have the following advantages:
(1) the preparation method of the crystal ice powder provided by the invention is novel, the crystal ice powder can be prepared by adding hot water into the ice powder bag and extruding the outer container of the ice powder bag, the preparation method is simple and practical, the prepared crystal ice powder has moderate toughness, and the crystal ice powder with different shapes can be prepared by the method provided by the invention.
(2) Compared with carrageenan, konjac flour and konjac glucomannan prepared by the prior art, the pseudo-acid syrup, the traditional Chinese medicine liquid and the seasoning liquid prepared by adopting the low-temperature ultrahigh-pressure technology can reduce insoluble starch or other suspended small-particle impurities, and the crystal ice powder prepared by adopting the method provided by the invention has high transparency and good visual effect.
(3) The invention adopts the low-temperature ultrahigh-pressure technology to prepare the nicandra physaloides, the traditional Chinese medicine liquid and the seasoning liquid, can reserve the nutrient components in the nicandra physaloides, the traditional Chinese medicine food material and the seasoning to the maximum extent, simultaneously can completely keep the natural color of each component, and plays the nutrient action of each component to the utmost extent, and the crystal ice powder prepared by the method has the advantages of easier absorption of the nutrient components and better mouthfeel.
(4) The crystal ice powder disclosed by the invention has the health-care functions of cooling, detoxifying, clearing liver, improving eyesight, losing weight, supplementing various vitamins and the like by adding the traditional Chinese medicine food materials and the substances rich in vitamins.
(5) The crystal ice powder is prepared by adopting low-temperature ultrahigh pressure and freeze-drying technology, the preparation method is simple, and compared with the traditional preparation method, the steps of concentration and sterilization are reduced.
Drawings
FIG. 1 is a perspective view of a preferred embodiment of the present invention; and
fig. 2 is a schematic view of a preferred embodiment of the hot water port of the present invention.
List of reference numerals
100: the ice powder bag 110: outer container 120: inner container
130: thermal insulation layer 140: connecting the pipe 150: flexible powder bin
160: hot water port 141: powder membrane 161: upper flange
162: the lower flange 163: fastener 164: o-shaped sealing ring
165: the perforated screw 166: positioning guide sleeve 167: sealing plate
168: elastic member 169: one-way valve core
Detailed Description
The following detailed description is made with reference to the accompanying drawings and examples.
The invention provides crystal ice powder. The crystal ice powder is disposable automatic mixing crystal ice powder. The crystal ice powder is prepared by mixing crystal ice powder and hot water according to the weight ratio of 1: 70-160. Preferably, the crystal ice powder is prepared by mixing the crystal ice powder and hot boiled water according to the weight ratio of 1: 100-120. Preferably, the temperature of the hot boiled water is 50-100 ℃. The crystal ice powder comprises main materials, auxiliary materials, seasonings and a coagulant. The main material, the auxiliary material and the seasoning are processed by a low-temperature ultrahigh-pressure technology to prepare the nicandra physaloides, the auxiliary material liquid and the seasoning liquid. Mixing the pseudo-acid syrup, the auxiliary material liquid and the seasoning liquid uniformly, adding a coagulant, and freeze-drying by a freeze dryer to obtain the crystal ice powder. The preparation method of the invention can reserve the nutrient components in the nicandra physaloides, the auxiliary materials and the seasonings to the maximum extent, simultaneously can completely keep the natural color of each component, and the nutrient components in the crystal ice powder prepared by the method are easier to absorb and have better mouthfeel.
According to a preferred embodiment, the crystal ice powder of the invention is prepared by the following steps: the main material, the auxiliary material and the seasoning are processed by a low-temperature ultrahigh-pressure technology to prepare the nicandra physaloides, the auxiliary material liquid and the seasoning liquid. Mixing the pseudo-acid syrup, the auxiliary material liquid and the seasoning liquid uniformly, adding a coagulant, and freeze-drying by a freeze dryer to obtain the crystal ice powder.
According to a preferred embodiment, the nicandra physaloides is prepared by the following method: taking and adding the nicandra physaloides seeds into purified water in a weight ratio of 1: 1-10: 1 of the nicandra physaloides seeds, putting the purified water added with the nicandra physaloides seeds into ultrahigh pressure treatment equipment, and keeping the ultrahigh pressure treatment equipment for 2-5 min under the conditions of low temperature and ultrahigh pressure of 500-1000 MPa and temperature of below 20 ℃ to obtain the nicandra physaloides seed extracting solution. Filtering the nicandra physaloides seed extract to obtain the nicandra physaloides.
According to a preferred embodiment, the auxiliary liquid is prepared by the following method: taking auxiliary materials, adding the auxiliary materials into purified water in a weight ratio of 1: 1-10: 1 to the auxiliary materials, putting the purified water added with the auxiliary materials into ultrahigh pressure treatment equipment, and keeping the pressure at 500-1000 MPa and the temperature below 20 ℃ for 2-10 min under the conditions of low temperature and ultrahigh pressure to obtain an auxiliary material extracting solution. And filtering the auxiliary material extracting solution to obtain the auxiliary material liquid.
According to a preferred embodiment, the seasoning liquid is prepared by the following method: taking seasonings, adding the seasonings into purified water in a weight ratio of 1: 1-10: 1 to the seasonings, putting the purified water with the seasonings into ultrahigh pressure treatment equipment, and keeping the purified water at a low temperature of below 20 ℃ for 3-8 min under the conditions of a pressure of 500-1000 MPa to obtain a seasoning extracting solution. Filtering the flavoring extract to obtain flavoring liquid.
The invention adopts the low-temperature ultrahigh-pressure extraction technology, completely adopts a physical processing method, does not need concentration or chemical solvent addition, and simultaneously, covalent bonds in raw materials are basically not damaged. In the process of preparing the extracting solution, the fresh food materials change color, taste and quality of the raw materials due to the existence of the enzymes of the fresh food materials, the influence on the quality of the raw materials is large, and the enzymes can be inactivated by adopting a low-temperature ultrahigh-pressure technology, so that the quality of the raw materials is improved. The invention realizes the sterilization treatment of the raw materials while preparing the extracting solution, and does not need to separately adopt the sterilization step, thereby shortening the technical process for preparing the crystal ice powder. The low-temperature ultrahigh-pressure technology can also prevent the raw materials and the extracting solution from being polluted by microorganisms and prolong the preservation time.
According to a preferred embodiment, the auxiliary material liquid and the seasoning liquid are added into the pseudo-acid syrup and uniformly stirred, and a coagulant containing the pseudo-acid syrup, the auxiliary material liquid and the seasoning liquid is obtained after the coagulant is added into the mixture.
According to a preferred embodiment, the congelation is quickly frozen at the temperature of-10 to-5 ℃ for 30 to 60min, and the congelation quickly frozen into ice is sublimated into water vapor at 5.0 to 10.0KPa and is discharged. Freezing and sublimating the solidified substance to obtain the crystal ice powder.
The invention adopts the freeze-drying technology to prepare the congelation into the finished product, can ensure that various nutrient components such as protein, vitamin and the like in the food, particularly volatile heat-sensitive components are not lost, can keep the original nutrient components to the maximum extent, and effectively prevents oxidation, nutrient component conversion and state change in the drying process.
According to a preferred embodiment, the main material is nicandra physaloides. The adjuvant is health food material. The flavoring agent is saccharide and/or vitamin-rich material. The coagulant is carrageenan or agar. The weight percentage of the main material is 35-50%. The auxiliary materials account for 9-44.75% by weight. The weight percentage of the seasoning is 20-40%. The weight percentage of the coagulant is 0.25-1.0%. The sum of the weight percentages of the components is 100 percent. The crystal ice powder prepared by the method can be used for preparing crystal ice powder with smooth and exquisite outlet light sensation. The consumption of the coagulant is low, so that the crystal ice powder with proper toughness can be prepared.
According to a preferred embodiment, the health-care food material is a traditional Chinese medicine food material or a fruit. The Chinese medicinal food material comprises one or more of herba Menthae, Glycyrrhrizae radix, radix Pseudostellariae, fructus Lycii, Carthami flos, lignum Santali albi, pericarpium Citri Tangerinae, rhizoma Zingiberis recens, radix et rhizoma Rhei, Ganoderma, flos Rosae Rugosae, semen Cassiae and fructus Jujubae. The traditional Chinese medicine food materials are not limited to the above materials, and may also comprise one or more of health preserving and health promoting traditional Chinese medicine food materials such as chrysanthemum, honeysuckle, lotus leaf, donkey-hide gelatin and the like. The crystal ice powder disclosed by the invention has multiple health-care functions of cooling, detoxifying, clearing liver, improving eyesight, losing weight and the like by adding the traditional Chinese medicine food materials.
According to a preferred embodiment, the fruit is a neutral fruit or a cool or warm fruit. The neutral fruit is selected from one or more of fructus Vitis Viniferae, fructus Citri Limoniae, fructus Chaenomelis and mume fructus. The fruit is suitable for consumers with various constitutions. The cool fruit is selected from one or more of watermelon, melon, pear, banana, mulberry, persimmon, dragon fruit, strawberry, loquat and tomato. The fruit is suitable for consumers with heat constitution. The warm fruit is selected from one or more of durian, dateplum persimmon, mango, litchi, peach, longan, kumquat and cherry. The fruit is suitable for consumers with deficiency-cold constitution. According to the requirements of consumers, the proper fruit types are selected, so that the crystal ice powder can be suitable for consumers with various constitutions and has the functions of health preservation and health care.
According to a preferred embodiment, the saccharide comprises one or more of fructose, honey, brown sugar and brown sugar. Preferably, the saccharide is fructose. Because the fructose has the characteristics of difficult causing decayed teeth, lower calorie than other sugars, small influence on blood sugar and the like, the fructose is adopted to replace the traditional white granulated sugar, rock sugar or cane sugar, and the worry of people about the problems of decayed teeth, obesity, blood sugar increase and the like caused by eating sugar is eliminated. The vitamin-rich material comprises one or more of fructus kaki, fructus Pruni, semen glycines, semen Arachidis Hypogaeae, fructus Actinidiae chinensis, fructus crataegi, fructus Zizaniae Caduciflorae and cheese. The vitamin-rich material is not limited thereto, and may further include one or more of other vitamin-rich materials such as orange, grapefruit, almond, oat, and milk. The crystal ice powder has the health-care function of supplementing various vitamins.
The invention also provides a preparation method of the crystal ice powder. The preparation method comprises the following steps: hot water with the weight ratio of 70-160: 1 to the crystal ice powder is introduced into the cavity of the inner container 120 of the ice powder bag 100 through the hot water port 160 of the ice powder bag 100 storing the crystal ice powder. The outer container 110 of the ice powder bag 100 is pressed to transmit the pressure change caused by the contraction of the outer container 110 to the flexible powder bin 150 storing the crystal ice powder. So that the crystal ice powder stored in the flexible powder bin 150 enters the cavity of the inner container 120 and is mixed with hot water to prepare the crystal ice powder. Preferably, the method for preparing the crystal ice powder at least comprises the following steps:
s1: the crystal ice powder is stored in the flexible powder bin 150 of the ice powder bag 100.
S2: hot water is introduced into the inner container 120 through the hot water port 160, wherein the weight ratio of the hot water to the crystal ice powder in the flexible powder bin 150 is 70-160: 1.
S3: the outer container 110 is repeatedly pressed to make the powdered crystal ice in the flexible powder bin 150 enter the cavity of the inner container 120.
S4: the heat insulation layer 130 is removed, and the outer container 110 is repeatedly pressed again to cool the crystal ice powder through the liquid material pre-loaded in the gap between the outer container 110 and the heat insulation layer 130.
FIG. 1 shows a perspective view of a preferred embodiment of the present invention. As shown in fig. 1, the ice powder bag 100 includes an outer container 110, an inner container 120, an insulation layer 130, a connection pipe 140, a flexible powder bin 150, and a hot water port 160. Wherein, the inner container 120, the connecting pipe 140 and the flexible powder bin 150 are of an integrally formed structure. The upper port of the inner container 120 is detachably provided with a hot water port 160 penetrating the inner container 120 and the outer container 110. An insulation layer 130 is detachably disposed between the inner container 120 and the outer container 110. The liquid material is pre-filled between the insulating layer 130 and the outer container 110. The preparation method of the crystal ice powder provided by the invention is novel, the crystal ice powder can be prepared by adding hot water into the ice powder bag and extruding the outer container of the ice powder bag, the preparation method is simple and practical, the prepared crystal ice powder has moderate toughness, and the crystal ice powder with different shapes can be prepared by the method provided by the invention.
According to a preferred embodiment, the outer container 110 is a flexible container. When preparing the powdered ice, the pressure inside the powdered ice bag 100 can be caused to vary by pressing the flexible outer container 110. Preferably, the outer container 110 is a separate and reusable component. Preferably, the flexible material is a polymer material, such as PE, PET, PA, and composites thereof. The outer container 110 is made of flexible polymer material, so that the cost is low and the practicability is high. Preferably, the outer container 110 has an opening that can be opened and closed. The opening which can be opened and closed is a concave-convex airtight seal.
According to a preferred embodiment, the inner container 120 is a rigid container. Preferably, inner container 120 is made of one of the existing rigid materials. Preferably, the inner container 120 is also made of a heat insulating material so that it is not burned when preparing the powdered crystal ice. The inner container 120 is used for molding the ice powder. The inner receptacle 120 is integrally formed with a flexible powder hopper 150 provided at a lower end of the inner receptacle 120 through a connecting pipe 140. The inner container 120 may have different shapes so that the prepared crystal ice powder has different shapes after being molded. Preferably, the inner container 120 may be cylindrical, rectangular parallelepiped, square, flower-shaped, butterfly-shaped, or the like. Preferably, the outer container 110 has an opening that can be opened and closed. The opening which can be opened and closed is a concave-convex airtight seal.
According to a preferred embodiment, an insulation layer 130 is detachably provided between the inner container 120 and the outer container 110. After the hot water is introduced into the inner container 120, the insulation layer 130 serves to insulate to prevent the temperature of the outer container 110 from rising. After the crystal ice powder is mixed with hot water, the heat insulation layer 130 is removed to cool the crystal ice powder. Preferably, the insulation layer 130 is a separate and reusable component. Preferably, the insulation layer 130 is made of one of the existing insulation materials.
According to a preferred embodiment, the gap between the outer container and the insulating layer 130 of 110 is pre-filled with a liquid material. After the powder is mixed with the hot water, the outer container 110 is squeezed again to cool the powder through the liquid material pre-loaded in the gap between the outer container 110 and the thermal insulation layer 130. Preferably, the liquid material is cold water, ice water or an amine salt solution. The cooling speed of the crystal ice powder can be accelerated by the liquid material. Preferably, the liquid raw material contained in advance can be replaced. The liquid material loaded in advance has a heat absorption function, so that the cooling of the crystal ice powder can be accelerated, and the storage time of the crystal ice powder can be prolonged.
According to a preferred embodiment, after mixing the powdered crystal ice with hot water, the thermal insulation layer 130 is removed and the outer container 110 is further pressed. On one hand, the ice powder and hot water can be further mixed uniformly, and on the other hand, the quick cooling can be realized through the pre-filled liquid, so that the crystal ice powder is prepared.
According to a preferred embodiment, the connecting pipe 140 is a passage for the powdered crystal ice to enter the cavity of the inner container 120. The connecting tube 140 has a powder membrane 141 that is impermeable to powder at normal temperature. The powder diaphragm 141 is melted into hot water at a temperature of 50 ℃ or higher so that the powder of the crystal ice stored in the flexible powder bin 150 enters the cavity of the inner container 120. Preferably, the powder membrane 141 is made of edible material with specific taste, and the taste of the crystal ice powder can be changed after the powder membrane 141 is melted into hot water. Preferably, the powder membrane is a sugar-coated film made of brown sugar, brown sugar or crystal sugar. The taste of the powder membrane 141 is not limited thereto, and may have a fruity taste, a sour taste, or the like.
According to a preferred embodiment, the flexible powder bin 150 is used for storing crystal ice powder. The flexible powder bin 150 is made of an elastic material. When the outer container 110 is squeezed, the pressure change of the pre-filled liquid caused by the contraction of the outer container 110 is transmitted to the flexible powder bin 150, so that the flexible powder bin 150 contracts or expands, and further, the crystal ice powder stored in the flexible powder bin 150 enters the cavity of the inner container 120 under the condition that the powder membrane 141 is melted. Preferably, when preparing the ice powder, the outer container 110 is pressed several times to uniformly mix the ice powder stored in the flexible powder bin 150 with the hot water introduced into the cavity of the inner container 120 through the hot water port 160 to prepare the ice powder.
According to a preferred embodiment, the hot water port 160 is used to introduce hot water into the cavity of the inner receptacle 120. The hot water port 160 penetrates the inner container 120 and the outer container 110. When preparing the ice powder, hot water for preparing the ice powder is introduced into the cavity of the inner container 120 through the hot water port 160. Preferably, the hot water port 160 has a check valve structure, and the temperature of the hot water introduced into the cavity of the inner container 120 through the check valve structure of the hot water port 160 is 50 to 100 ℃. Preferably, the hot water port 160 is detachably connected to the outer receptacle 110 and the inner receptacle 120.
Fig. 2 shows a schematic view of the check valve of a preferred embodiment of the hot water port 160 of the present invention. As shown in fig. 2, the check valve of the present invention includes at least an upper flange 161, a lower flange 162, a fastening member 163, an O-ring 164, a piercing screw 165, a positioning guide sleeve 166, a sealing plate 167, an elastic member 168, and a check valve core 169. The upper flange 161 and the lower flange 162 are connected together by fasteners 163. An O-ring 164 is disposed between the upper flange 161 and the lower flange 162. The positioning guide sleeve 166 is fixed to the upper flange 161 by a through-hole screw 165. A sealing plate 167 is provided between the upper flange 161 and the positioning guide sleeve 166. One end of the check valve spool 169 is provided on the lower flange 162 via an elastic member 168, and the other end is provided on the seal plate 167. The check valve spool 169 is slidable up and down in the axial direction of the positioning guide sleeve 166. Preferably, the fastener 163 is a bolt. Preferably, the elastic member 168 is a spring. Preferably, the sealing plate 167 is a rubber sealing plate. The hot water port 160 of the present invention adopts a check valve structure, which can prevent the liquid in the inner container 120 from overflowing outwardly.
When the hot water heating valve is used, the upper end of the one-way valve is a hot water inlet, hot water pushes the one-way valve core 169 to move downwards through the perforated screw 165, the one-way valve core 169 is separated from the sealing plate 167, and therefore hot water can flow to the lower end outlet. When the hot water at the upper end stops injecting, the one-way valve core 169 moves upwards under the resultant force of the elastic component 168 at the lower end and the hot water, and the one-way valve core 169 is contacted with the sealing plate 167 and is pressed firmly, so that the purpose of stopping the flow is achieved.
The raw material weights and the component ratios of the powdered crystal ice of examples 1 to 8 are shown in table 1 below.
TABLE 1 weight of raw materials and component ratio of crystal ice powder of each example
Figure BDA0001220062290000131
As shown in Table 2 below, the process conditions for preparing the pseudo-acid syrup, the auxiliary material liquid and the seasoning liquid and the process conditions for freeze-drying in examples 1 to 8 are described.
TABLE 2 Process conditions for the preparation of crystalline Ice powder of the examples
Figure BDA0001220062290000132
Figure BDA0001220062290000141
TABLE 3 Process conditions for preparing Crystal Ice powder of each example
Examples Ratio of hot water to crystal ice powder Temperature of hot water
1 70∶1 50
2 80∶1 55
3 100∶1 60
4 120∶1 70
5 130∶1 75
6 140∶1 85
7 150∶1 90
8 160∶1 95
Example 1
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. This example prepares the powder of crystal ice by:
s101: adding the main material of the nicandra physaloides seeds into purified water in a weight ratio of 1: 1-10: 1, putting the purified water added with the nicandra physaloides seeds into ultrahigh pressure treatment equipment, and keeping the pressure at 700MPa and the temperature below 10 ℃ for 3.5min under the low-temperature ultrahigh pressure condition to obtain the nicandra physaloides seed extracting solution. Filtering the nicandra physaloides seed extract to obtain the nicandra physaloides.
S102: adding the auxiliary materials into purified water in a weight ratio of 1: 1-10: 1, putting the purified water added with the auxiliary materials into ultrahigh pressure treatment equipment, and keeping the pressure at 800MPa and the temperature below 5 ℃ for 6.0min under the conditions of low temperature and ultrahigh pressure to obtain an auxiliary material extracting solution. And filtering the auxiliary material extracting solution to obtain the auxiliary material liquid.
S103: adding the seasoning into purified water with the weight ratio of the seasoning to the purified water being 1: 1-10: 1, putting the purified water with the seasoning into ultrahigh pressure treatment equipment, and keeping the purified water at the low temperature below 12 ℃ for 5.0min under the conditions of the pressure of 700MPa and the temperature of below 12 ℃ to obtain seasoning extracting solution. Filtering the flavoring extract to obtain flavoring liquid.
S104: and adding the auxiliary material liquid and the seasoning liquid into the pseudo-acid syrup, uniformly stirring, and adding a coagulant into the mixture to obtain a solidified substance containing the pseudo-acid syrup, the auxiliary material liquid and the seasoning liquid.
S105: quickly freezing the solidified substance at-7 deg.C for 40min, sublimating ice into water vapor at 7.0KPa, and lyophilizing to obtain crystal ice powder.
This example prepares crystal ice powder by:
s201: the crystal ice powder is stored in the flexible powder bin 150 of the ice powder bag 100.
S202: hot water is introduced into the inner container 120 through the hot water port 160 at a weight ratio of 70: 1 to the crystal ice powder in the flexible powder bin 150, and the temperature of the hot water is 50 ℃.
S203: the outer container 110 is repeatedly pressed to make the powdered crystal ice in the flexible powder bin 150 enter the cavity of the inner container 120.
S204: the heat insulation layer 130 is removed, and the outer container 110 is repeatedly pressed again to cool the crystal ice powder through the liquid material pre-loaded in the gap between the outer container 110 and the heat insulation layer 130.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder has the effects of supplementing vitamin C, nourishing blood, promoting blood circulation, lowering blood pressure, reducing blood fat, inhibiting thrombosis, protecting heart and the like.
Example 2
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. Powder of crystal ice and powder of crystal ice were prepared by the same method as in example 1, and the process conditions for the preparation are shown in tables 2 and 3.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder of the embodiment has the effects of supplementing vitamin B6, clearing away summer-heat, promoting urination, quenching thirst and the like.
Example 3
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. Powder of crystal ice and powder of crystal ice were prepared by the same method as in example 1, and the process conditions for the preparation are shown in tables 2 and 3.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder of the embodiment has the effects of supplementing vitamin B12, quenching thirst, relieving summer heat, relieving cough, reducing phlegm, invigorating stomach, promoting digestion and the like.
Example 4
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. Powder of crystal ice and powder of crystal ice were prepared by the same method as in example 1, and the process conditions for the preparation are shown in tables 2 and 3.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder of the embodiment has various health-care effects of supplementing vitamin E, soothing liver, activating blood circulation, clearing brain, reducing pathogenic fire, resisting depression, calming the heart and the like.
Example 5
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. Powder of crystal ice and powder of crystal ice were prepared by the same method as in example 1, and the process conditions for the preparation are shown in tables 2 and 3.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder of the embodiment has various health-care effects of supplementing vitamin C, cooling blood, beautifying, improving dry skin and the like. The rose has strong flower fragrance, so the rose also has certain curative effect on treating the ozostomia; in addition, the crystal ice powder prepared by the formula can help digestion, so that the crystal ice powder also has the effect of losing weight.
Example 6
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. Powder of crystal ice and powder of crystal ice were prepared by the same method as in example 1, and the process conditions for the preparation are shown in tables 2 and 3.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder of the embodiment has multiple health-care effects of supplementing vitamin A, clearing liver, improving eyesight, relaxing bowel, purging liver fire, reducing blood fat, losing weight and the like.
Example 7
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. Powder of crystal ice and powder of crystal ice were prepared by the same method as in example 1, and the process conditions for the preparation are shown in tables 2 and 3.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder of the embodiment has the effects of supplementing vitamin B1, vitamin B6 and vitamin E, clearing summer heat, promoting diuresis, eliminating edema, reducing blood fat, relaxing bowels, soothing liver and keeping health and the like.
Example 8
The main material, the auxiliary material, the seasoning and the coagulant in table 1 were weighed. Powder of crystal ice and powder of crystal ice were prepared by the same method as in example 1, and the process conditions for the preparation are shown in tables 2 and 3.
The crystal ice powder of the embodiment is crystal clear, cool, fragrant and sweet, tender, smooth and tasty, and can meet the requirements of consumers with various constitutions; the crystal ice powder of the embodiment has rich nutrition, easy absorption of nutrient components and good taste; the crystal ice powder has the effects of supplementing vitamin B6, tonifying kidney, replenishing vital essence, nourishing liver, improving eyesight, moistening lung, reducing blood pressure, reducing blood fat, preventing arteriosclerosis and the like, and has good curative effects on dizziness and tinnitus, blurred vision, hypomnesis caused by liver and kidney deficiency, eye fatigue caused by long-term use of a computer and the like.
The crystal ice powders prepared in examples 1 to 8 were examined for transparency. The detection method comprises the following steps: the transmittance of the crystal ice powder prepared in examples 1 to 8 was measured by an ultraviolet spectrophotometer. The detection conditions are as follows: a quartz cuvette: 1 cm; wavelength: 460 nm; reference solution: and (3) water. Meanwhile, 3 common transparent crystal ice powders in the market are taken as comparative examples 1 to 3, and the light transmittance is detected for comparison. Table 4 shows the transparency test results of the reference solution, the samples of comparative examples 1 to 3, and the samples of example 1 to example 8.
TABLE 4 results of transparency test of reference solution, comparative example and samples of each example
Sample (I) Light transmittance% Sample (I) Light transmittance% Sample (I) Light transmittance%
Distilled water
100 Example 1 92.7 Example 5 94.3
Comparative example 1 82.0 Example 2 90.8 Example 6 91.5
Comparative example 2 81.7 Example 3 90.0 Example 7 90.2
Comparative example 3 80.6 Example 4 93.2 Example 8 93.9
From the transmittance results, the greater the transmittance, the higher the transparency at the same wavelength. As can be seen from the detection results in Table 4, the crystal ice powder prepared by the method has higher transparency than common crystal ice powder on the market, and the light transmittance is within the range of 90.0-95.0%. From the data in table 4, it can be found that the light transmittance of the crystal ice powder is not significantly affected when the ratio of the raw materials for preparing the crystal ice powder is changed.
Due to the difference of ingredients and manufacturing processes among various foods, the crystal ice powder and the manufacturing method thereof provided by the invention are not suitable for manufacturing other foods except the ice powder, and are particularly not suitable for manufacturing the cake powder. The ice powder bag provided by the invention is specially used for making ice powder, and the structure of the ice powder bag is designed according to the characteristics of the ice powder in the making process, so that the ice powder bag provided by the invention is not suitable for other foods except the ice powder, and is particularly not suitable for making ice cake powder.
It should be noted that the above-mentioned embodiments are exemplary, and that those skilled in the art, having benefit of the present disclosure, may devise various arrangements that are within the scope of the present disclosure and that fall within the scope of the invention. It should be understood by those skilled in the art that the present specification and figures are illustrative only and are not limiting upon the claims. The scope of the invention is defined by the claims and their equivalents.

Claims (8)

1. The crystal ice powder is characterized in that the crystal ice powder is prepared by uniformly mixing pseudo-acid syrup prepared by processing a main material, an auxiliary material and a seasoning through a low-temperature ultrahigh-pressure technology, an auxiliary material liquid and a seasoning liquid, adding a coagulant, and freeze-drying the mixture by a freeze-dryer to prepare the crystal ice powder and hot water according to the weight ratio of 1: 70-160, wherein,
the main material is nicandra physaloides, the auxiliary material is a health-care food material, the seasoning is sugar and/or a substance rich in vitamins, the coagulant is carrageenan or agar, the weight percentage of the main material is 35-50%, the weight percentage of the auxiliary material is 9-44.75%, the weight percentage of the seasoning is 20-40%, the weight percentage of the coagulant is 0.25-1.0%, and the sum of the weight percentages of the components is 100%,
the crystal ice powder is filled in a liquid-tight ice powder bag (100) with a liquid valve, and the ice powder bag (100) comprises: a liquid-tight flexible powder bin (150) pre-storing crystal ice powder, an inner container (120) with the volume larger than that of the flexible powder bin and an outer container (110), and
a connecting pipeline (140) is arranged between the flexible powder bin (150) and the inner container (120), a powder diaphragm (141) is arranged in the connecting pipeline (140), the powder diaphragm (141) is a sugar coating film made of brown sugar, yellow sugar or rock sugar,
the outer container (110) encloses a flexible powder bin (150) and an inner container (120) which are integrally formed with each other in a liquid-tight manner from the outside,
when the outer container (110) is squeezed, the pressure change of the pre-filled liquid caused by the contraction of the outer container (110) is transmitted to the flexible powder bin (150) so as to contract or expand the flexible powder bin (150), and then the crystal ice powder stored in the flexible powder bin (150) enters the cavity of the inner container (120) under the condition that the powder diaphragm (141) is melted,
wherein the flexible powder bin (150) and the inner container (120) are respectively injection molded by two different components in the same process, so that the flexible powder bin (150) and the inner container (120) can bear high temperature, meanwhile, the rigidity of the inner container (120) is obviously greater than that of the flexible powder bin (150), and in addition, the flexible powder bin (150) and the inner container (120) can bear high temperature, and in addition, the rigidity of the inner container (120) is also obviously greater than that of the flexible powder bin (150), and
the crystal ice powder contained in the flexible powder bin (150) can enter the inner layer container (120) only after hot water is filled in so as to complete the mixing of the crystal ice powder and the hot water by extruding the flexible powder bin (150),
a hot water port (160) for introducing hot water into the cavity of the inner container (120), the hot water port (160) penetrating the inner container (120) and the outer container (110),
the hot water port (160) is provided with a one-way valve structure, the one-way valve structure at least comprises an upper flange (161), a lower flange (162), a fastener (163), an O-shaped sealing ring (164), a perforation screw (165), a positioning guide sleeve (166), a sealing plate (167), an elastic component (168) and a one-way valve core (169),
the upper flange (161) and the lower flange (162) are connected together through the fastener (163), an O-shaped sealing ring (164) is arranged between the upper flange (161) and the lower flange (162), the positioning guide sleeve (166) is fixed on the upper flange (161) through a perforated screw (165), the sealing plate (167) is arranged between the upper flange (161) and the positioning guide sleeve (166), one end of the one-way valve core (169) is arranged on the lower flange (162) through an elastic component (168), the other end of the one-way valve core is arranged on the sealing plate (167), and the one-way valve core (169) can slide up and down along the axial direction of the positioning guide sleeve (166).
2. The crystal ice powder according to claim 1, wherein the pseudoacid syrup is prepared by the following method: taking pseudo-wintercherry seeds, adding the pseudo-wintercherry seeds into purified water with the weight ratio of the pseudo-wintercherry seeds to the pseudo-wintercherry seeds being 1: 1-10: 1, putting the purified water with the pseudo-wintercherry seeds into ultrahigh pressure treatment equipment, keeping the ultrahigh pressure for 2-5 min at the low temperature of 500-1000 MPa and the temperature of below 20 ℃ to obtain a pseudo-wintercherry seed extracting solution, and filtering the pseudo-wintercherry seed extracting solution to obtain the pseudo-wintercherry;
the auxiliary material liquid is prepared by the following method: taking auxiliary materials, adding the auxiliary materials into purified water in a weight ratio of 1: 1-10: 1 to the auxiliary materials, putting the purified water added with the auxiliary materials into ultrahigh pressure treatment equipment, keeping the pressure of the purified water at 500-1000 MPa and the temperature of the purified water below 20 ℃ for 2-10 min under the low-temperature ultrahigh pressure condition to obtain auxiliary material extracting solution, and filtering the auxiliary material extracting solution to obtain the auxiliary material liquid;
the seasoning liquid is prepared by the following method: taking seasonings, adding the seasonings into purified water in a weight ratio of 1: 1-10: 1 to the seasonings, putting the purified water added with the seasonings into ultrahigh pressure treatment equipment, keeping the pressure at 500-1000 MPa and the temperature below 20 ℃ for 3-8 min under the conditions of low temperature and ultrahigh pressure to obtain seasoning extracting solution, and filtering the seasoning extracting solution to obtain the seasoning liquid.
3. The crystal ice powder as claimed in claim 2, wherein the auxiliary material liquid and the seasoning liquid are added to the pseudo-acid syrup and uniformly stirred, the coagulant is added to the mixture to obtain a solidified substance containing the pseudo-acid syrup, the auxiliary material liquid and the seasoning liquid, the solidified substance is quickly frozen at a temperature of-10 to-5 ℃ for 30 to 60min, the ice is sublimated into water vapor to be discharged from the solidified substance which is quickly frozen into ice at 5.0 to 10.0KPa, and the frozen and sublimated solidified substance is used for obtaining the crystal ice powder.
4. Crystal ice powder according to any of the previous claims, characterised in that said powder membrane (141) is in a mesh-like form after injection moulding, so as to allow said powder to be poured into said flexible powder silo (150); after the crystal ice powder is filled, coating the powder membrane (141) with edible bonding material to form the powder membrane (141) which is not permeable to powder at normal temperature but is melted into hot water at the temperature of more than 50 ℃ so that the crystal ice powder stored in the flexible powder bin (150) can freely enter and exit the inner container (120) in a hot water environment.
5. Crystal ice powder according to claim 4, characterised in that the powder membrane (141) comprises at least a first membrane facing the flexible powder silo (150) and a second membrane facing the inner container (120),
the first layer of membrane is made of a first edible material with good air tightness as an adhesive sealing material, and the second layer of membrane is made of a first edible material and a second edible material which can be slowly melted under hot water as an adhesive sealing material.
6. Crystal ice powder according to claim 5, characterised in that the connecting duct (140) is injection moulded with the same composition as the inner container (120) at the end close to the inner container (120), and the connecting duct (140) is injection moulded with the same composition as the flexible powder silo (150) at the end close to the flexible powder silo (150); and is
The section of the connecting pipe (140) for arranging the powder diaphragm (141) has rigidity not lower than that of the inner container (120), and a radial powder diaphragm fixing structure is arranged in the inner cavity of the section of the connecting pipe (140) for arranging the powder diaphragm (141).
7. Crystal ice powder according to claim 6, characterised in that the outer container (110) is made of a flexible and heat-conducting material, the outer container (110) being thermally insulated from the inner container (120) by an insulating layer (130) before being filled with hot water, wherein the insulating layer (130) is removably arranged outside the inner container (120) so that after the crystal ice powder is mixed with hot water, the insulating layer (130) is removed to achieve a gradual cooling through the outer container (110) made of a flexible and heat-conducting material.
8. The powdered crystal ice according to claim 7, wherein a hot water port (160) is formed through the inner container (120) and the outer container (110) so that hot water for preparing the powdered crystal ice is introduced into the cavity of the inner container (120) through the hot water port (160), the hot water port (160) has a check valve structure, and the temperature of the hot water introduced into the cavity of the inner container (120) through the check valve structure of the hot water port (160) is 50 to 100 ℃.
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CN111109426A (en) * 2020-02-24 2020-05-08 四川御皇科技有限公司 Formula of glutinous rice cake ice powder and preparation method thereof
CN112262973B (en) * 2020-08-28 2022-08-26 昆明理工大学 Preparation method of nicandra physaloides gel food
CN112027353A (en) * 2020-09-27 2020-12-04 萧县徐老三食品有限公司 Sandwich biscuit and eating method

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CN104687061A (en) * 2015-02-13 2015-06-10 成都市亚丁胡杨生态农业有限公司 Health preservation nicandra physalodes jelly and preparation method thereof as well as preparation method of nicandra physalodes jelly powder

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CN1863713A (en) * 2003-10-07 2006-11-15 Sika技术股份公司 Method for processing a material and packing container for carrying out this method
CN103080268A (en) * 2010-09-24 2013-05-01 朱塞佩·撒塞拉 Flexible container having a built-in auto-heating or auto-refrigerating element
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