CN106819544A - One kind extracts shepherd's purse Thick many candies and prepares compound chicken chelating iron powder - Google Patents

Abstract

Shepherd's purse Thick many candies are extracted the invention discloses one kind and prepare compound chicken chelating iron powder, be made from the following raw materials in parts by weight：Gorgon fruit 30 40, moyashi 10 15, grifola frondosus 20 25, shepherd's purse 40 50, radix polygonati officinalis 67, Flos Semen Lablab Album 34, jujube 8 12, ferric trichloride, ferrous chloride, trisodium citrate, casein, trypsase, lactic acid bacteria, appropriate amount of water.Trisodium citrate can promote the chelating of grifola frondosus and iron ion.Dissolubility of the iron in alimentary canal intestines can be effectively improved after iron and Hydrolysates of Casein chelating, strengthens immunity of organisms, improve anti-stress ability.Gorgon fruit can improve absorption of the body to mineral matters such as iron, calcium after lactobacillus-fermented, play a part of to cooperate with chelating iron powder, and bean sprouts slurries microwave treatment can be improved into enzymolysis efficiency.Shepherd's purse Thick many candies have certain inhibitory action to Escherichia coli, bacillus subtilis, staphylococcus aureus, salmonella.

Description

One kind extracts shepherd's purse Thick many candies and prepares compound chicken chelating iron powder

Technical field

Compound chicken chelated iron is prepared the present invention relates to field of feed, more particularly to a kind of shepherd's purse Thick many candies that extract Powder.

Background technology

Iron is the biological element that animal body grows, and in feedstuff industry, its addition form mainly has inorganic iron, has Machine iron etc..The long-term use of inorganic iron can bring a series of problem, therefore limes reacting dose to use.And Organic Iron has life higher Thing potency and good chemical stability, and structure is closer to the ferro element of natural form in animal body, thus be easier Absorbed by animal body, and then reach the effect for improving feed addictive utilization rate, gradually instead of inorganic iron.Animal alimentary canal The ability for absorbing iron is poor, and absorptivity only has 5-30%.Duodenum is the major absorption site of iron, after iron enters enteric cavity, must A kind of chelate must be combined into related endogenous or exogenous ligand, by that could be digested by body after easyization diffusion, Absorb and utilize.《The research and development of Hydrolysates of Casein chelated iron》Refer to that iron ion will be entered by intestinal mucosa layer in one text Blood, it is desirable to have specific carrier.After its corresponding ligand is combined, it is possible to by amino acid and the movement system of peptide It is transported through with Amino Acid Absorption passage, it is to avoid competition occurs with other mineral elements and flys up and down, most chelated iron is complete at last Transport out intestinal mucosa and enter blood, improve utilization rate of the body to iron.Vandergrift it is proposed that, metal and amino acid, After peptide chelating, metal Absorption And Metabolism situation in vivo depends entirely on the amino acid and peptide for chelating therewith.Chelating amino acids The chemical constitution of iron stabilization makes it be more conducive to absorb close to the natural form of enzyme in animal body, can make to be located at after being absorbed The ferro element at chelating center is not disturbed by other factors, can be just directly delivered in target organ and enzyme system, and then play a role. 《The Study on Preparation of grifolan chelated iron》Refer to that grifola frondosus are nutritious in one text, especially grifolan has Multiple biological activities, with various functions such as antitumor, anti-aging, enhance immunity, research shows that polysaccharide has and metal knot The ability of conjunction coordination, and polysaccharide and Fe³⁺Being combined the complex to be formed has stronger stability and stimulates small to stomach, and pair is made With also small, it acts not only as chalybeate for body provides required iron, can also play polysaccharide medical value in itself simultaneously And strengthen its bioactivity.

The content of the invention

The object of the invention is exactly to make up the defect of prior art, there is provided one kind extracts shepherd's purse Thick many candies and prepares compound chicken With chelating iron powder.

The present invention is achieved by the following technical solutions：

One kind extracts shepherd's purse Thick many candies and prepares compound chicken chelating iron powder, is made from the following raw materials in parts by weight：Gorgon fruit 30-40, Moyashi 10-15, grifola frondosus 20-25, shepherd's purse 40-50, radix polygonati officinalis 6-7, Flos Semen Lablab Album 3-4, jujube 8-12, ferric trichloride, dichloro Change iron, trisodium citrate, casein, trypsase, lactic acid bacteria, appropriate amount of water.

Shepherd's purse Thick many candies are extracted according to claims 1 and prepare compound chicken chelating iron powder, preparation method it is specific Step is as follows：

(1) add suitable quantity of water to grind to form slurry grifola frondosus, regulation pH is 7-8, be then that 570-580W microwave treatments are crushed with power Cell 5-6 minutes, under 60-70 DEG C of water temperature condition water bath with thermostatic control heating extraction 2-3 hour, after centrifugation grifolan liquid and Grifola frondosus slag charge；

(2) grifolan liquid Rotary Evaporators are concentrated into original 1/3rd, add ferric trichloride, trisodium citrate Stir, at 50-55 DEG C, chelated 30-40 minutes under the conditions of pH5.5-5.6, spray drying obtains grifolan chelated iron Powder；

(3) casein addition trypsase is stirred, adjusts pH8.0-8.5, digested 3-4 minutes under the conditions of 37-42 DEG C, After adding ferrous chloride to stir, at 50-55 DEG C, chelated 30-40 minutes under the conditions of pH5.5-5.6, spray drying obtains amino Acid chelating iron powder；

(4) Gorgon fruit is put into clear water and is soaked 8-9 hour, grind to form centrifugation after slurry, take supernatant, then by 95-100 DEG C of moyashi Scalding 2-3 minutes, with the water mill slurry of 10-12 times of moyashi quality, slurries process 20-30 through microwave power 180-200W Appropriate papain is added after second, hydrolyzate pH value 7.0-7.2 is controlled, hydrolyzed 50-60 minutes under the conditions of 50-55 DEG C, from Remove sediment after the heart, then add lactic acid bacteria after mixing with above-mentioned supernatant, fermented 40-48 hours at being 42-45 DEG C in temperature, Obtain Gorgon fruit zymotic fluid；

(5) Flos Semen Lablab Album, jujube addition suitable quantity of water is ground into juice, heating is boiled, and separates mixed juice and mixing slag, shepherd's purse, jade Powder is made after bamboo drying to be well mixed with above-mentioned mixed juice, surpass under the conditions of ultrasonic power 400-420W, 70-75 DEG C of temperature Sonication times 35-40 minutes, then be well mixed with the grifola frondosus slag charge of above-mentioned mixing slag, step 1, obtain mixed material；

(6) the Gorgon fruit zymotic fluid of step 4 is well mixed with the mixed material of step 5, is spray-dried, then the ash tree with step 2 Flower polysaccharide chelating iron powder, the chelating amino acids iron powder of step 3 and other residual components are well mixed, you can.

It is an advantage of the invention that：Microwave treatment grifola frondosus not only have quick and uniform heating function, can also be because promoting The membranolysis of material and accelerate polysaccharide molecule to the infiltration of matrix and dissolving, polysaccharide is rapidly discharged, thus Rate rises with the extension of microwave time.Trisodium citrate can promote the chelating of grifola frondosus and iron ion as catalyst.Junket Albumen can generate various natural physiological active peptides through enzyme hydrolysis, wherein containing bioactive peptide of the class rich in seryl phosphoric acid cluster：Junket Protein phosphatase polypeptide.Fe under certain condition²⁺Can be chelated with CPP, form a kind of soluble complexes-casein phosphorus Sour peptide chelated iron.After iron is chelated with Hydrolysates of Casein, dissolubility of the iron in alimentary canal especially small intestine can be effectively improved, and It is proportional that the height of dissolution rate absorbs iron with body.Meanwhile, Hydrolysates of Casein chelated iron can resist the low pH environment of stomach and The decomposition that enzyme causes, protection iron reaches intestinal epithelial cell with stable state.Amino acid chelated iron can strengthen immunity of organisms, Immune response is improved, promotes Cellular Immunity and humoral immunity ability, improve anti-stress ability.Through trypsin hydrolysis Hydrolysates of Casein and Fe²⁺Fe can be protected after chelating²⁺, it is to avoid interactive influenceed by other nutrients are negative.Gorgon fruit Absorption of the body to mineral matters such as iron, calcium can be improved after lactobacillus-fermented, plays a part of to cooperate with chelating iron powder, while newborn The metabolins such as substantial amounts of organic acid, alcohols, vitamin and various amino acid can be also produced during acid bacteria fermentation, it is rotten with suppression Lose bacterium, improve the physiological functions such as digestibility.Bean sprouts slurries microwave treatment can be improved into enzymolysis efficiency.Shepherd's purse Thick many candies are to big Enterobacteria, bacillus subtilis, staphylococcus aureus, salmonella have certain inhibitory action.

Specific embodiment

One kind extracts shepherd's purse Thick many candies and prepares compound chicken chelating iron powder, is made from the following raw materials in parts by weight：Gorgon fruit 30, Moyashi 10, grifola frondosus 20, shepherd's purse 40, radix polygonati officinalis 6, Flos Semen Lablab Album 3, jujube 8, ferric trichloride, ferrous chloride, trisodium citrate, Casein, trypsase, lactic acid bacteria, appropriate amount of water.

Shepherd's purse Thick many candies are extracted according to claims 1 and prepare compound chicken chelating iron powder, preparation method it is specific Step is as follows：

(1) suitable quantity of water is added to grind to form slurry grifola frondosus, regulation pH is 7, is then 5 points of 570W microwave treatments smudge cells with power Clock, water bath with thermostatic control heating extraction 2 hours, obtain grifolan liquid and grifola frondosus slag charge under 60 DEG C of water temperature conditions after centrifugation；

(2) grifolan liquid Rotary Evaporators are concentrated into original 1/3rd, add ferric trichloride, trisodium citrate Stir, at 50 DEG C, chelated 30 minutes under the conditions of pH5.5, spray drying, obtain grifolan chelating iron powder；

(3) casein addition trypsase is stirred, adjusts pH8.0, digested 3 minutes under the conditions of 37 DEG C, add dichloro After change iron stirs, at 50 DEG C, chelated 30 minutes under the conditions of pH5.5, spray drying obtains chelating amino acids iron powder；

(4) Gorgon fruit is put into clear water and is soaked 8 hours, be centrifuged after grinding to form slurry, take supernatant, then by the hot water of 95 DEG C of moyashi Blanching 2 minutes, with 10 times of water mill slurry of moyashi quality, slurries add appropriate pawpaw egg after being processed 20 seconds through microwave power 180W White enzyme, control hydrolyzate pH value 7.0, hydrolyzes 50 minutes under the conditions of 50 DEG C, removes sediment after centrifugation, then with above-mentioned supernatant Lactic acid bacteria is added after mixing, is fermented 40 hours at being 42 DEG C in temperature, obtain Gorgon fruit zymotic fluid；

(5) Flos Semen Lablab Album, jujube addition suitable quantity of water is ground into juice, heating is boiled, and separates mixed juice and mixing slag, shepherd's purse, jade Powder is made after bamboo drying to be well mixed with above-mentioned mixed juice, at ultrasonic wave under the conditions of ultrasonic power 400W, temperature 70 C 35 minutes reason time, then be well mixed with the grifola frondosus slag charge of above-mentioned mixing slag, step 1, obtain mixed material；

(6) the Gorgon fruit zymotic fluid of step 4 is well mixed with the mixed material of step 5, is spray-dried, then the ash tree with step 2 Flower polysaccharide chelating iron powder, the chelating amino acids iron powder of step 3 and other residual components are well mixed, you can.

In order to further illustrate application value of the invention, implement people by 200 chickens according to age in days, body weight, health status, Chicken is equally divided into two groups of experimental group and control group by sex ratio identical principle, and experimental group is fed and adds chicken feed of the invention The feed of additive, control group feeds the feed for not increasing additive of the present invention, and experimental period is 3 months, and result of the test is：Feeding Amount improves 12%, and sick rate reduction by 7%, death rate reduction by 9%, rate of body weight gain improves 10%, and aquaculture cost reduction by 15% improves feed Utilization ratio, improves the culture benefit of chicken.

Claims (2)

1. a kind of shepherd's purse Thick many candies that extract prepare compound chicken chelating iron powder, it is characterised in that by the raw material system of following weight portion Into：Gorgon fruit 30-40, moyashi 10-15, grifola frondosus 20-25, shepherd's purse 40-50, radix polygonati officinalis 6-7, Flos Semen Lablab Album 3-4, jujube 8-12, Ferric trichloride, ferrous chloride, trisodium citrate, casein, trypsase, lactic acid bacteria, appropriate amount of water.

2. shepherd's purse Thick many candies are extracted according to claims 1 and prepares compound chicken chelating iron powder, it is characterised in that preparation side Method is comprised the following steps that：

(1) add suitable quantity of water to grind to form slurry grifola frondosus, regulation pH is 7-8, be then that 570-580W microwave treatments are crushed with power Cell 5-6 minutes, under 60-70 DEG C of water temperature condition water bath with thermostatic control heating extraction 2-3 hour, after centrifugation grifolan liquid and Grifola frondosus slag charge；

(2) grifolan liquid Rotary Evaporators are concentrated into original 1/3rd, add ferric trichloride, trisodium citrate Stir, at 50-55 DEG C, chelated 30-40 minutes under the conditions of pH5.5-5.6, spray drying obtains grifolan chelated iron Powder；

(3) casein addition trypsase is stirred, adjusts pH8.0-8.5, digested 3-4 minutes under the conditions of 37-42 DEG C, After adding ferrous chloride to stir, at 50-55 DEG C, chelated 30-40 minutes under the conditions of pH5.5-5.6, spray drying obtains amino Acid chelating iron powder；

(4) Gorgon fruit is put into clear water and is soaked 8-9 hour, grind to form centrifugation after slurry, take supernatant, then by 95-100 DEG C of moyashi Scalding 2-3 minutes, with the water mill slurry of 10-12 times of moyashi quality, slurries process 20-30 through microwave power 180-200W Appropriate papain is added after second, hydrolyzate pH value 7.0-7.2 is controlled, hydrolyzed 50-60 minutes under the conditions of 50-55 DEG C, from Remove sediment after the heart, then add lactic acid bacteria after mixing with above-mentioned supernatant, fermented 40-48 hours at being 42-45 DEG C in temperature, Obtain Gorgon fruit zymotic fluid；

(5) Flos Semen Lablab Album, jujube addition suitable quantity of water is ground into juice, heating is boiled, and separates mixed juice and mixing slag, shepherd's purse, jade Powder is made after bamboo drying to be well mixed with above-mentioned mixed juice, surpass under the conditions of ultrasonic power 400-420W, 70-75 DEG C of temperature Sonication times 35-40 minutes, then be well mixed with the grifola frondosus slag charge of above-mentioned mixing slag, step 1, obtain mixed material；

(6) the Gorgon fruit zymotic fluid of step 4 is well mixed with the mixed material of step 5, is spray-dried, then the ash tree with step 2 Flower polysaccharide chelating iron powder, the chelating amino acids iron powder of step 3 and other residual components are well mixed, you can.