CN106770078A - A kind of LIF food detector - Google Patents

A kind of LIF food detector Download PDF

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Publication number
CN106770078A
CN106770078A CN201610998067.8A CN201610998067A CN106770078A CN 106770078 A CN106770078 A CN 106770078A CN 201610998067 A CN201610998067 A CN 201610998067A CN 106770078 A CN106770078 A CN 106770078A
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CN
China
Prior art keywords
laser
data acquisition
lif
workbench
base
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201610998067.8A
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Chinese (zh)
Inventor
刘金杰
吴敏芳
徐静
赵春城
胡勇
蒋韦艳
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Wuxi Xresearch Product Design and Research Co Ltd
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Wuxi Xresearch Product Design and Research Co Ltd
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Priority to CN201610998067.8A priority Critical patent/CN106770078A/en
Publication of CN106770078A publication Critical patent/CN106770078A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/64Fluorescence; Phosphorescence
    • G01N21/6428Measuring fluorescence of fluorescent products of reactions or of fluorochrome labelled reactive substances, e.g. measuring quenching effects, using measuring "optrodes"
    • G01N21/643Measuring fluorescence of fluorescent products of reactions or of fluorochrome labelled reactive substances, e.g. measuring quenching effects, using measuring "optrodes" non-biological material
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00Features of devices classified in G01N21/00
    • G01N2201/06Illumination; Optics
    • G01N2201/061Sources
    • G01N2201/06113Coherent sources; lasers

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  • Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Optics & Photonics (AREA)
  • Molecular Biology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

The invention discloses a kind of LIF food detector, including base and detection workbench, the detection workbench is arranged on base, support frame is connected between workbench and base, support frame bottom surface builds data acquisition device in region, data acquisition device is connected with DSP data processing modules, DSP data processing modules are connected to computer, DSP data processing modules are associated with detection workbench, detection workbench side is provided with laser, convex lens are provided with outside the laser port of laser upper end, laser is fixed on two-dimentional micro actuator top, two-dimentional micro actuator is fixed on lowering or hoisting gear, lowering or hoisting gear is arranged on base top.The present invention can quickly detect the concentration of determinand in food by appropriate Signal acquiring and processing, and practical and convenient, accuracy is high.

Description

A kind of LIF food detector
Technical field
The present invention relates to food detector technical field, specially a kind of LIF food detector.
Background technology
The safe condition of modern society people growing interest food, it is especially exceeded to food additives, residues of pesticides and The related data information growing interest of unauthorized substances is added in food.
Such detector of prior art is primarily present positioning inaccurately, detection mode tradition, the low problem of sensitivity.
The content of the invention
It is an object of the invention to provide a kind of LIF food detector, possesses Signal acquiring and processing fast Speed, detection accuracy advantage high.
To achieve the above object, the present invention provides following technical scheme:A kind of LIF food detector, including Base and detection workbench, the detection workbench are arranged on base, and support frame, support frame are connected between workbench and base Data acquisition device is built in bottom surface region, data acquisition device is connected with DSP data processing modules, DSP data processing moulds Block is connected to computer, and DSP data processing modules are associated with detection workbench, and detection workbench side is provided with laser, Convex lens are provided with outside the laser port of laser upper end, laser is fixed on two-dimentional micro actuator top, and two-dimentional micro actuator is fixed on liter On falling unit, lowering or hoisting gear is arranged on base top.
Preferably, the detection workbench includes NaOH solution tank NaOH to be measured, capillary and sensing element, and sensing element is molten with to be measured Flow container is worked in coordination, and sensing element front end is provided with capillary, and capillary is stretched into NaOH solution tank NaOH to be measured.
Preferably, loophole is offered on the NaOH solution tank NaOH bottom surface to be measured.
Preferably, the data acquisition device includes microcobjective, filter module, optical filter, photomultiplier and data Collector, microcobjective and loophole are arranged on same vertical line, and microcobjective is adjacent with filter module, filter module and Photomultiplier is connected, and photomultiplier top is provided with optical filter, and photomultiplier is connected to data acquisition unit, data acquisition Device transmits signals to DSP data processing modules.
Preferably, the filter module is followed successively by dichroscope, condenser lens, logical filter, band logical filter long from top to bottom.
Compared with prior art, beneficial effects of the present invention are as follows:
The present invention is by setting capillary and laser and registration, two dimension is adjustable, and laser excitation is by biology compatible reaction And the determinand for making to be connected to the mark on sensing element surface and having sends fluorescence and collects, then by appropriate signal Collection and treatment, you can the concentration of determinand in detection food, it is simple and quick, and filter module is adjusted, use Low-angle incident-type light path design, obtains maximum detection sensitivity, can be used for the detection of micro-example.
Brief description of the drawings
Fig. 1 is schematic structural view of the invention;
Fig. 2 is structure detection workbench schematic diagram of the present invention;
Fig. 3 is structured data harvester schematic diagram of the present invention.
In figure:1- bases, 2- lasers, 3- detection workbench, 31- NaOH solution tank NaOHs to be measured, 32- capillaries, 33- sensing elements Part, 34- loopholes, 4- data acquisition devices, 41- microcobjectives, 42- filter modules, 43- optical filters, 44- photomultipliers, 45- data acquisition units, 5-DSP data processing modules, 6- computers, 7- two dimension micro actuators, 8- lowering or hoisting gears, 9- convex lens, 10- Support frame.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made Embodiment, belongs to the scope of protection of the invention.
Fig. 1-3 are referred to, the present invention provides a kind of technical scheme:A kind of LIF food detector, including bottom Seat 1 and detection workbench 3, the detection workbench 3 are arranged on base 1, and support frame 10 is connected between workbench 3 and base 1, Support frame 10 builds data acquisition device 4 in bottom surface region, and data acquisition device 4 is connected with DSP data processing modules 5, DSP Data processing module 5 is connected to computer 6, and DSP data processing modules 5 are associated with detection workbench 3, detect workbench 3 one Side is provided with laser 2, and convex lens 9 are provided with outside the upper end laser port of laser 2, and laser 2 is fixed on two-dimentional micro actuator 7 Portion, two-dimentional micro actuator 7 is fixed on lowering or hoisting gear 8, and lowering or hoisting gear 8 is arranged on the top of base 1.
It is described detection workbench 3 include NaOH solution tank NaOH to be measured 31, capillary 32 and sensing element 33, sensing element 33 with it is to be measured NaOH solution tank NaOH 31 is worked in coordination, and the front end of sensing element 33 is provided with capillary 32, and capillary 32 is stretched into NaOH solution tank NaOH to be measured 31, passed through The effect testing sample of capillary 32 enters and reflects a period of time, and the transmitting golden light of laser 2 simultaneously enters sensing element 33, lures into glimmering Light reflects, simple to operate quick,
Loophole 34 is offered on the bottom surface of NaOH solution tank NaOH to be measured 31, is easy to gather the situation of fluorescent reflection, the data to adopt Acquisition means 4 include microcobjective 41, filter module 42, optical filter 43, photomultiplier 44 and data acquisition unit 45, microcobjective 41 are arranged on same vertical line with loophole 34, and microcobjective 41 is adjacent with filter module 42, filter module 42 and photoelectricity Multiplier tube 44 is connected, and the top of photomultiplier 44 is provided with optical filter 43, and photomultiplier 44 is connected to data acquisition unit 45, number DSP data processing modules 5 are transmitted signals to according to collector 45, strong and weak by signal Analysis can learn the dense of test substance Degree, the filter module 42 is followed successively by dichroscope, condenser lens, logical filter, band logical filter long from top to bottom, obtains great Detection sensitivity can be widely applied to the other fields such as food, medical science, environmental project, agricultural simultaneously.
Operation principle:When using this kind of LIF food detector, sensing element 33 is put into determinand molten In liquid, under the effect of capillary 32, solution enters capillary 32, after reaction certain hour, opens laser 2, and laser is being all-trans Mode into sensing element 33 is penetrated, the evanescent waves produced during multihop propagation excite the fluorescent material for being attached to its surface, glimmering Stimulative substance sends fluorescence, enters after filter module 42, optical filter 43, photomultiplier 44 are acted on after being caught through microcobjective 41 Data acquisition unit 45, and the electric signal for being converted into being directly proportional to fluorescence intensity by DSP data processing modules 5, are sent to computer 6 Be analyzed treatment, computer 6 analyze and process after to data be directly proportional to the concentration of test substance, by the strong of signal Analysis The weak concentration that can learn test substance.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding can carry out various changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention And modification, the scope of the present invention be defined by the appended.

Claims (5)

1. a kind of LIF food detector, including base(1)With detection workbench(3), it is characterised in that:The inspection Survey workbench(3)It is arranged on base(1)On, workbench(3)With base(1)Between be connected with support frame(10), support frame(10)Under Data acquisition device is built in base surface area(4), data acquisition device(4)With DSP data processing modules(5)It is connected, DSP data Processing module(5)It is connected to computer(6), DSP data processing modules(5)With detection workbench(3)It is associated, detect workbench (3)Side is provided with laser(2), laser(2)Convex lens are provided with outside the laser port of upper end(9), laser(2)It is fixed on two Dimension micro actuator(7)Top, two-dimentional micro actuator(7)It is fixed on lowering or hoisting gear(8)On, lowering or hoisting gear(8)It is arranged on base(1)On Side.
2. a kind of LIF food detector according to claim 1, it is characterised in that:The detection workbench (3)Including NaOH solution tank NaOH to be measured(31), capillary(32)And sensing element(33), sensing element(33)With NaOH solution tank NaOH to be measured(31)Mutually It is engaged, sensing element(33)Front end is provided with capillary(32), capillary(32)Stretch into NaOH solution tank NaOH to be measured(31)In.
3. a kind of LIF food detector according to claim 2, it is characterised in that:The NaOH solution tank NaOH to be measured (31)Loophole is offered on bottom surface(34).
4. a kind of LIF food detector according to claim 1, it is characterised in that:The data acquisition dress Put(4)Including microcobjective(41), filter module(42), optical filter(43), photomultiplier(44)And data acquisition unit(45), Microcobjective(41)With loophole(34)It is arranged on same vertical line, microcobjective(41)With filter module(42)It is adjacent, Filter module(42)With photomultiplier(44)It is connected, photomultiplier(44)Top is provided with optical filter(43), photomultiplier transit Pipe(44)It is connected to data acquisition unit(45), data acquisition unit(45)Transmit signals to DSP data processing modules(5).
5. a kind of LIF food detector according to claim 1, it is characterised in that:The filter module (42)Dichroscope, condenser lens, logical filter, band logical filter long are followed successively by from top to bottom.
CN201610998067.8A 2016-11-14 2016-11-14 A kind of LIF food detector Pending CN106770078A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109682754A (en) * 2017-10-19 2019-04-26 中国石油化工股份有限公司 Multichannel analysis of stability analyzer
CN110057808A (en) * 2019-05-27 2019-07-26 中国人民解放军军事科学院军事医学研究院 Sample swivel mount and Raman spectrum detector

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020113136A1 (en) * 2000-09-18 2002-08-22 Talley Douglas G. Optical patternation method
WO2002090955A1 (en) * 2001-05-04 2002-11-14 Niton Corporation X-ray fluorescence combined with laser induced photon spectroscopy
CN1548944A (en) * 2003-05-20 2004-11-24 中国科学院大连化学物理研究所 Micro fluid control chip laser inducing fluorometric analysis instrument
CN1563998A (en) * 2004-04-16 2005-01-12 南京大学 Microcurrent controlled chip detection combiner having general and integral and high efficiency radiation
CN2736759Y (en) * 2004-07-22 2005-10-26 中国科学院大连化学物理研究所 Micro flow controlled chip laser induction fluorescent analyzer
CN103063646A (en) * 2013-01-14 2013-04-24 武汉大学 Dual-purpose laser-induced fluorescence detecting system
CN204575538U (en) * 2015-05-08 2015-08-19 罗强 A kind of laser-induced fluorescence (LIF) food detector

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020113136A1 (en) * 2000-09-18 2002-08-22 Talley Douglas G. Optical patternation method
WO2002090955A1 (en) * 2001-05-04 2002-11-14 Niton Corporation X-ray fluorescence combined with laser induced photon spectroscopy
CN1548944A (en) * 2003-05-20 2004-11-24 中国科学院大连化学物理研究所 Micro fluid control chip laser inducing fluorometric analysis instrument
CN1563998A (en) * 2004-04-16 2005-01-12 南京大学 Microcurrent controlled chip detection combiner having general and integral and high efficiency radiation
CN2736759Y (en) * 2004-07-22 2005-10-26 中国科学院大连化学物理研究所 Micro flow controlled chip laser induction fluorescent analyzer
CN103063646A (en) * 2013-01-14 2013-04-24 武汉大学 Dual-purpose laser-induced fluorescence detecting system
CN204575538U (en) * 2015-05-08 2015-08-19 罗强 A kind of laser-induced fluorescence (LIF) food detector

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109682754A (en) * 2017-10-19 2019-04-26 中国石油化工股份有限公司 Multichannel analysis of stability analyzer
CN109682754B (en) * 2017-10-19 2021-10-01 中国石油化工股份有限公司 Multi-channel stability analyzer
CN110057808A (en) * 2019-05-27 2019-07-26 中国人民解放军军事科学院军事医学研究院 Sample swivel mount and Raman spectrum detector
US11971358B2 (en) 2019-05-27 2024-04-30 Academy Of Military Medical Sciences Sample rotating rack and Raman spectrum detector

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