CN106758378A - A kind of textile dyeing increases deep functional agent and preparation method thereof, application - Google Patents
A kind of textile dyeing increases deep functional agent and preparation method thereof, application Download PDFInfo
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- CN106758378A CN106758378A CN201710020124.XA CN201710020124A CN106758378A CN 106758378 A CN106758378 A CN 106758378A CN 201710020124 A CN201710020124 A CN 201710020124A CN 106758378 A CN106758378 A CN 106758378A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65131—Compounds containing ether or acetal groups
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Abstract
Increase deep functional agent and preparation method thereof, application the invention discloses a kind of textile dyeing, the formula that the textile dyeing increases deep functional agent is as follows, in parts by weight for：15 parts of barbaloin, 15 parts of APG, 28 parts of flavones ethylene glycol, 70 parts of water；The preparation method that the textile dyeing increases deep functional agent is that will stand to obtain final product after each composition mixing and stirring in above-mentioned formula；The textile dyeing increases deep functional agent and is applied to during the dyeing process of the direct dyes of fabric or reactive dye.Composition is simple and environmentally friendly in the formula of the deep functional agent of textile dyeing increasing of the invention, it is easy to use, dyeing need not be changed and new equipment is added, can be widely applied to direct dyes, the reactive dyeing of silk, wool, cotton, fiber crops, regenerated celulose fibre fabric and blended union fabric, it is remarkably improved color depth and color fastness, dye dosage can be reduced simultaneously, energy ezpenditure and sewage discharge is reduced, and had a extensive future.
Description
Technical field
The invention belongs to textile dyeing field, and in particular to a kind of textile dyeing increases deep functional agent and preparation method thereof, answers
With.
Background technology
Easily there is poor color fastness in traditional textile dyeing, for example paint not depth, low dye-uptake, crock fastness, washing jail
The problems such as degree difference.If the usual poor fabric of color fastness is encountered rainwater, sweat and rubbed by the external world, color can be produced to come off
Fade, especially the deep and bright-coloured fabric of color and luster, its discolouration phenomena is more prominent；In addition having in the dyestuff of these colour fadings that come off
Machine molecule and heavy metal ion etc. are likely to be absorbed by the body and be detrimental to health by skin, and are wearing or washing
During can also contaminate dirty other fabrics, bring inconvenience to life.In order to improve fabric color fastness, some prints are often added
Dye auxiliary agent, such as when for using direct dyes and reactive dyeing, often add sodium chloride as dyeing accelerant；And
And also need to add sodium carbonate for reactive dyeing（Or sodium acid carbonate）As dye fixing agent, but through these conventional prints
The quality of dye auxiliary agent institute printed fabrics cannot still meet the application demand of high-end customer.
Patent CN201310636510.3 discloses a kind of deep-dyeing agent, its preparation method and improves dyed textiles color fastness
Method, it passes through amido organosilicon, ternary polymerization organosilicon, secondary alcohol APEO, octadecyldimethyl ethoxy season
Ammonium salt, alkyl ketene, paraffin emulsifier and water are prepared to obtain deep-dyeing agent, and dyed fabric then is impregnated into deep-dyeing agent dressing liquid
In, through centrifugal dehydration and drying, then at 190 DEG C of high-temperature process, obtain that there is the fabric for increasing deep function.Although being arranged through its increasing is deep
Fabric color fastness it is high and soft, but the deep-dyeing agent increase it is deep arrange be after dyeing process, and need it is soaking,
Dehydration, drying and high-temperature process, increased dyeing process.
Patent CN201610104901.4 discloses a kind of high-efficiency fiber deep dyeing promoter and preparation method thereof, and it uses first
Base sodium naphthalene sulfonate, sodium lignin sulfonate, organosilicon alkanes monomer, methacryloxypropyl trimethoxy silane, bisphenol-A ring
Oxygen emulsion, salicylate, organic acid, nano titanium oxide, emulsifying agent, initiator and deionized water prepare deep-dyeing agent.Should
The used material composition of invention is complicated and many, and preparation time is long, is unfavorable for that large-scale popularization is used.
The content of the invention
The technical problem of solution：The problems such as easily there is poor color fastness to solve traditional textile dyeing, there is provided a kind of
Environmental protection and the good novel fabric deep dyeing functional agent of application prospect and preparation method thereof, application.
Technical scheme：A kind of textile dyeing increases deep functional agent, and the formula that the textile dyeing increases deep functional agent is as follows, with weight
Part is calculated as：
Barbaloin 1-5 parts
APG 1-5 parts
2-8 parts of flavones ethylene glycol
70 parts of water.
Further, the flavones ethylene glycol is the ginkgo water extract of content 30%, is purchased from the promise chemicals of Ningbo hundred million limited
Company.
A kind of textile dyeing increases the preparation method of deep functional agent, and the preparation method is：Weighed each raw material by above-mentioned formula,
By barbaloin, APG, flavones ethylene glycol and water mixing and stirring, then it is stored at room temperature at least 1 hour, obtains final product fabric dye
Color increases deep functional agent.
A kind of textile dyeing increases the application of deep functional agent, and the textile dyeing increases the direct dye that deep functional agent is applied to fabric
During the dyeing process of material or reactive dye.
In above-mentioned technical proposal, the specific method of the application is：
1）After preparing direct dyes, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into and knit
Thing；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 40 min, take out fabric, 60 DEG C of hot water
Wash 3 times, cold water is washed 3 times, dry.
In above-mentioned technical proposal, the specific method of the application is：
1）After preparing reactive dye, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into and knit
Thing；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium carbonate or bicarbonate
Sodium, then dye and take out after 30 min fabric, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
In above-mentioned technical proposal, the fabric includes that silk, wool, cotton, fiber crops, regenerated celulose fibre fabric or blending are handed over
Woven fabric.
In above-mentioned technical proposal, the textile dyeing increases deep functional agent and is with the consumption of direct dyes or reactive dye：5-
30 mL/L textile dyeings increase deep functional agent：1-5% o.w.f direct dyess or reactive dye.
In above-mentioned technical proposal, the consumption of the sodium chloride is 10 g/L, and the bath raio is 1:40, the direct dyes
Consumption is 1-5% o.w.f, and the consumption that the textile dyeing increases deep functional agent is 5-30 mL/L.
In above-mentioned technical proposal, the consumption of the sodium chloride is 30 g/L, and the bath raio is 1:40, the reactive dye
Consumption is 1-5% o.w.f, and the consumption that the textile dyeing increases deep functional agent is 5-30mL/L；When fabric is cotton, fiber crops, regeneration fibre
When cellulose fiber fabric or blended union fabric, from 10-25 g/L sodium carbonate；When fabric is silk or wool, from 5-
15 g/L sodium acid carbonates.
Beneficial effect：
1）Barbaloin, APG and flavones ethylene glycol, these compositions is used to be applied in textile printing and dyeing in formula of the invention
It is uncommon, furthermore we find that, barbaloin can improve dyeing rate and adsorption effect of the dyestuff to fiber in formula, improve
Color depth；APG can improve set effect of the dyestuff to fiber, promote the hydroxyl on fiber, carboxyl and dyestuff to form chemistry
Key, can improve color fastness and color depth effect；Flavones ethylene glycol can improve osmotic effect of the dyestuff to fiber；This several composition lacks one
Can not, it is used in conjunction with each other, good deep dyeing functional effect has been played jointly.
2）Composition is simple and environmentally friendly in the formula of the deep functional agent of textile dyeing increasing of the invention, easy to use, no
Need change dyeing and add new equipment.
3）Textile dyeing of the invention increases deep functional agent and can be widely applied to silk, wool, cotton, fiber crops, regenerated cellulose fibre
The direct dyes of dimensional fabric and blended union fabric, reactive dyeing.
4）Textile dyeing of the invention increases deep functional agent and is remarkably improved the color depth and color fastness of textile dyeing, while can drop
Low dye consumption, reduces energy ezpenditure and sewage discharge, is a kind of environmental protection, new dyeing function increasing that is effective and having application prospect
Strong agent.
Specific embodiment
For a further understanding of the present invention, the preferred embodiment of the invention is described with reference to embodiment, but
It should be appreciated that these descriptions are simply to further illustrate the features and advantages of the present invention, rather than to the claims in the present invention
Limitation.
Embodiment 1
A kind of textile dyeing increases deep functional agent, and the formula that the textile dyeing increases deep functional agent is as follows, in parts by weight for：
1 part of barbaloin
1 part of APG
2 parts of flavones ethylene glycol
70 parts of water.
Wherein, the flavones ethylene glycol is the ginkgo water extract of content 30%, is purchased from the limited public affairs of promise chemicals of Ningbo hundred million
Department.
The preparation method of above-mentioned fabrics deep dyeing functional agent is：Weighed each raw material by above-mentioned formula, by barbaloin, alkyl
Glucosides, flavones ethylene glycol and water mixing and stirring, are then stored at room temperature 1 hour, obtain final product textile dyeing and increase deep functional agent.
Embodiment 2
A kind of textile dyeing increases deep functional agent, and the formula that the textile dyeing increases deep functional agent is as follows, in parts by weight for：
3 parts of barbaloin
3 parts of APG
5 parts of flavones ethylene glycol
70 parts of water.
Wherein, the flavones ethylene glycol is the ginkgo water extract of content 30%, is purchased from the limited public affairs of promise chemicals of Ningbo hundred million
Department.
The preparation method of above-mentioned fabrics deep dyeing functional agent is：Weighed each raw material by above-mentioned formula, by barbaloin, alkyl
Glucosides, flavones ethylene glycol and water mixing and stirring, are then stored at room temperature 3 hours, obtain final product textile dyeing and increase deep functional agent.
Embodiment 3
A kind of textile dyeing increases deep functional agent, and the formula that the textile dyeing increases deep functional agent is as follows, in parts by weight for：
5 parts of barbaloin
5 parts of APG
8 parts of flavones ethylene glycol
70 parts of water.
Wherein, the flavones ethylene glycol is the ginkgo water extract of content 30%, is purchased from the limited public affairs of promise chemicals of Ningbo hundred million
Department.
The preparation method of above-mentioned fabrics deep dyeing functional agent is：Weighed each raw material by above-mentioned formula, by barbaloin, alkyl
Glucosides, flavones ethylene glycol and water mixing and stirring, are then stored at room temperature 2 hours, obtain final product textile dyeing and increase deep functional agent.
The application of above-mentioned fabrics deep dyeing functional agent, the textile dyeing increases the direct dye that deep functional agent is applied to fabric
During the dyeing process of material or reactive dye.The fabric include silk, wool, cotton, fiber crops, regenerated celulose fibre fabric or
Blended union fabric.
So that the textile dyeing prepared by embodiment 2 increases deep functional agent as an example, its concrete application is described in detail below：
The direct dyes of application examples 1 contaminates cotton
The consumption of each material is in dyeing process：
Direct red 2b： 3 %（o.w.f）
Textile dyeing increases deep functional agent： 15 mL/L
Sodium chloride： 10 g/L
Bath raio： 1:40；
The weight ratio of fabric and water, 1 when the bath raio refers to dyeing:To 1g textile dyeings, it is necessary to add in 40 expression dye baths
40g water；
The concrete technology of dyeing process is：
1）After preparing direct red 2b, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into
Cotton；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 40 min, take out cotton, 60 DEG C of hot water wash 3
Secondary, cold water is washed 3 times, drying.
The direct dyes dyeing silk habotai of application examples 2
The consumption of each material is in dyeing process：
Direct indigo plant GL： 2%（o.w.f）
Textile dyeing increases deep functional agent： 15mL/L
Sodium chloride： 10g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing direct indigo plant GL, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into true
Silk habotai；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 40 min, take out Real Silk Habotai, 60
DEG C hot water wash 3 times, cold water is washed 3 times, drying.
The Dyeing of Cotton Fabric with Reactive Dyes of application examples 3
The consumption of each material is in dyeing process：
Reactive brilliant red GB： 3 %（o.w.f）
Textile dyeing increases deep functional agent： 10 mL/L
Sodium chloride： 30 g/L
Sodium carbonate： 20 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing reactive brilliant red GB, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into
Cotton；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium carbonate, then dye 30
Take out cotton after min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
The reactive dye dyeing silk habotai of application examples 4
The consumption of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Textile dyeing increases deep functional agent： 10 mL/L
Sodium chloride： 20 g/L
Sodium acid carbonate： 6 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into
Real Silk Habotai；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium acid carbonate, then dye
Take out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
Direct dyes used, reactive dye, textile dyeing increase in the application of the deep functional agent of textile dyeing increasing of the invention
The consumption of deep functional agent, sodium chloride, sodium carbonate and sodium acid carbonate is not limited to use above example, and its occurrence can be according to dyestuff
Species, the property of fabric, dyeing etc. carry out appropriate adjustment.
In order to better illustrate the performance that the textile dyeing prepared by the present invention increases deep functional agent, we have done following contrast
Experiment：
The direct dyes of comparative example 1 contaminates cotton
The consumption of each material is in dyeing process：
Direct red 2b： 3 %（o.w.f）
Sodium chloride： 10 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing direct red 2b, 80 DEG C, after stirring are warming up to, place into cotton；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 40 min, take out cotton, 60 DEG C of hot water wash 3
Secondary, cold water is washed 3 times, drying.
The direct dyes dyeing silk habotai of comparative example 2
The consumption of each material is in dyeing process：
Direct indigo plant GL： 2 %（o.w.f）
Sodium chloride： 10 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing direct indigo plant GL, 80 DEG C, after stirring are warming up to, place into silk；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 40 min, take out silk, 60 DEG C of hot water
Wash 3 times, cold water is washed 3 times, dry.
The Dyeing of Cotton Fabric with Reactive Dyes of comparative example 3
The consumption of each material is in dyeing process：
Reactive brilliant red GB： 3 %（o.w.f）
Sodium chloride： 30 g/L
Sodium carbonate： 20 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing reactive brilliant red GB, 80 DEG C, after stirring are warming up to, place into cotton；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium carbonate, then dye 30
Take out cotton after min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
The reactive dye dyeing silk habotai of comparative example 4
The consumption of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Sodium chloride： 20 g/L
Sodium acid carbonate： 6 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C, after stirring are warming up to, place into Real Silk Habotai；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium acid carbonate, then dye
Take out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
The reactive dye dyeing silk habotai of comparative example 5
The consumption of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Functional agent A： 10 mL/L
Sodium chloride： 20 g/L
Sodium acid carbonate： 6 g/L
Bath raio： 1:40；
Wherein, deep functional agent is increased compared to the textile dyeing in application examples 4（Embodiment 2）, the functional agent A formulas in this comparative example
In lack barbaloin, other formula with preparation process with embodiment 2, will not be repeated here.
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, add functional agent A, after stirring, place into Real Silk Habotai；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium acid carbonate, then dye
Take out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
The reactive dye dyeing silk habotai of comparative example 6
The consumption of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Functional agent B： 10 mL/L
Sodium chloride： 20 g/L
Sodium acid carbonate： 6 g/L
Bath raio： 1:40；
Wherein, deep functional agent is increased compared to the textile dyeing in application examples 4（Embodiment 2）, the functional agent B formulas in this comparative example
In lack APG, other formula with preparation process with embodiment 2, will not be repeated here.
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, add functional agent B, after stirring, place into Real Silk Habotai；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium acid carbonate, then dye
Take out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
The reactive dye dyeing silk habotai of comparative example 7
The consumption of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Functional agent C： 10 mL/L
Sodium chloride： 20 g/L
Sodium acid carbonate： 6 g/L
Bath raio： 1:40；
Wherein, deep functional agent is increased compared to the textile dyeing in application examples 4（Embodiment 2）, the functional agent C formulas in this comparative example
In lack flavones ethylene glycol, other formula with preparation process with embodiment 2, will not be repeated here.
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, add functional agent C, after stirring, place into Real Silk Habotai；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium acid carbonate, then dye
Take out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
Performance test
Correlated performance test is carried out to the fabric dyeed by application examples 1-4 and comparative example 1-7 below.
Method of testing
Colorfastness to rubbing：According to GB/T 3920- 2008《Textile color stability tests colour fastness to rubbing》Method, uses unlubricated friction
Wipe and two methods of wet friction, differentiate the staining degree of fabric；
Color fastness to washing：According to standard GB/T/T 3921.2-2008《Textile color stability tests fastness to soaping》Test
K/S values are tested：Yarn dyed fabric is folded 4 layers, using the color measuring and matching systems of Datacolor 600, the K/S of PRINTED FABRIC is determined
Value, determines and is averaged at 4.K/S values are bigger, represent that material is stronger to the absorbability of light, and fabric color is deeper.
Test result
With Real Silk Habotai fabric（56 g/m2）And bafta（105 g/m2）After using the technology of the present invention, above-mentioned each application examples
Contrast as follows with comparative example various performance parameters：
Note：Friction, 3 grades of soaping fastness are qualified, and 5 grades best；K/S values are the bigger the better, and illustrate that color is deeper.
Compared with comparative example 1-4 from application examples 1-4：Application examples 1-4 with the addition of the deep functional agent of increasing, act on cotton, true
After the fabrics such as silk, color depth value K/S numerical value is bigger, and with preferable colorfastness to rubbing and washing fastness.Comparative example 1-4 treatment
Cotton, real silk fabric K/S values are relatively low, and color fastness is poor.
Compared with comparative example 5,6,7 from application examples 4：Function deep-dyeing agent lacks barbaloin composition in comparative example 5, its dye
The K/S values of fabric after color, crock fastness and washing fastness are below application examples 4；Function deep-dyeing agent lacks alkyl sugar in comparative example 6
Glycosides composition, the K/S values of fabric after its dyeing, crock fastness and washing fastness are below application examples 4；Function increases deep in comparative example 7
Agent lacks flavones ethylene glycol composition, the K/S values of fabric after its dyeing, and crock fastness and washing fastness are below application examples 4.
The foregoing description of the disclosed embodiments, enables professional and technical personnel in the field to realize or uses the present invention.
Various modifications to these embodiments will be apparent for those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, the present invention
The embodiments shown herein is not intended to be limited to, and is to fit to and principles disclosed herein and features of novelty phase one
The scope most wide for causing.
Claims (10)
1. a kind of textile dyeing increases deep functional agent, it is characterised in that the formula that the textile dyeing increases deep functional agent is as follows, with weight
Amount part is calculated as：
Barbaloin 1-5 parts
APG 1-5 parts
2-8 parts of flavones ethylene glycol
70 parts of water.
2. textile dyeing according to claim 1 increases deep functional agent, it is characterised in that the flavones ethylene glycol is for content
30% ginkgo water extract.
3. textile dyeing according to claim 1 and 2 increases the preparation method of deep functional agent, it is characterised in that the fabric
The preparation method of deep dyeing functional agent is：Weighed each raw material by above-mentioned formula, by barbaloin, APG, flavones ethylene glycol
With water mixing and stirring, then it is stored at room temperature at least 1 hour, obtains final product textile dyeing and increase deep functional agent.
4. textile dyeing according to claim 1 increases the application of deep functional agent, it is characterised in that the textile dyeing increases deep
Functional agent is applied to during the dyeing process of the direct dyes of fabric or reactive dye.
5. textile dyeing according to claim 4 increases the application of deep functional agent, it is characterised in that the specific side of the application
Method is：
1）After preparing direct dyes, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into and knit
Thing；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 40 min, take out fabric, 60 DEG C of hot water
Wash 3 times, cold water is washed 3 times, dry.
6. textile dyeing according to claim 4 increases the application of deep functional agent, it is characterised in that the specific side of the application
Method is：
1）After preparing reactive dye, 80 DEG C are warming up to, add textile dyeing to increase deep functional agent, after stirring, placed into and knit
Thing；
2）Add sodium chloride to promote dye at 80 DEG C after the min of constant temperature dyeing 5, then after dyeing 20 min, add sodium carbonate or bicarbonate
Sodium, then dye and take out after 30 min fabric, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
7. the textile dyeing according to claim 4 or 5 or 6 increases the application of deep functional agent, it is characterised in that the fabric bag
Include silk, wool, cotton, fiber crops, regenerated celulose fibre fabric or blended union fabric.
8. textile dyeing according to claim 7 increases the application of deep functional agent, it is characterised in that the textile dyeing increases
Deep functional agent is with the consumption of direct dyes or reactive dye：5-30 mL/L textile dyeings increase deep functional agent：1-5% o.w.f are straight
Connect dyestuff or reactive dye.
9. textile dyeing according to claim 5 increases the application of deep functional agent, it is characterised in that the use of the sodium chloride
It is 10 g/L to measure, and the bath raio is 1:40, the consumption of the direct dyes is 1-5% o.w.f, and the textile dyeing increases deep function
The consumption of agent is 5-30 mL/L.
10. textile dyeing according to claim 6 increases the application of deep functional agent, it is characterised in that the use of the sodium chloride
It is 30 g/L to measure, and the bath raio is 1:40, the consumption of the reactive dye is 1-5% o.w.f, and the textile dyeing increases deep function
The consumption of agent is 5-30 mL/L；When fabric is cotton, fiber crops, regenerated celulose fibre fabric or blended union fabric, from 10-
25 g/L sodium carbonate；When fabric is silk or wool, from 5-15 g/L sodium acid carbonates.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109944092A (en) * | 2019-03-05 | 2019-06-28 | 上海兴康化工有限公司 | A kind of reactive dye wool short route dyeing |
| CN112746336A (en) * | 2020-12-24 | 2021-05-04 | 苏州经贸职业技术学院 | Degumming agent for silk fabric, preparation method of degumming agent and degumming method for silk fabric |
| CN114438803A (en) * | 2022-01-26 | 2022-05-06 | 内蒙古工业大学 | Cashmere fiber dyeing and deepening method and deepening agent |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56112583A (en) * | 1980-02-01 | 1981-09-04 | Nikka Chemical Ind Co Ltd | Color darkening agent of polyester fiber dyed article |
| CN102383319A (en) * | 2011-06-16 | 2012-03-21 | 北京泛博化学股份有限公司 | Deepening agent and preparation method thereof |
| CN104846669A (en) * | 2015-05-23 | 2015-08-19 | 青岛东昌瑞纺织品有限公司 | Textile dye |
| CN105671945A (en) * | 2016-04-12 | 2016-06-15 | 湖州吉昌丝绸有限公司 | Environment-friendly deepening agent applicable to polyester fiber |
| CN106192475A (en) * | 2016-09-13 | 2016-12-07 | 广州市番禺区协运来化工用品有限公司 | A kind of fiber deep dyeing promoter and preparation thereof |
-
2017
- 2017-01-12 CN CN201710020124.XA patent/CN106758378B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56112583A (en) * | 1980-02-01 | 1981-09-04 | Nikka Chemical Ind Co Ltd | Color darkening agent of polyester fiber dyed article |
| CN102383319A (en) * | 2011-06-16 | 2012-03-21 | 北京泛博化学股份有限公司 | Deepening agent and preparation method thereof |
| CN104846669A (en) * | 2015-05-23 | 2015-08-19 | 青岛东昌瑞纺织品有限公司 | Textile dye |
| CN105671945A (en) * | 2016-04-12 | 2016-06-15 | 湖州吉昌丝绸有限公司 | Environment-friendly deepening agent applicable to polyester fiber |
| CN106192475A (en) * | 2016-09-13 | 2016-12-07 | 广州市番禺区协运来化工用品有限公司 | A kind of fiber deep dyeing promoter and preparation thereof |
Non-Patent Citations (2)
| Title |
|---|
| 刘旭峰: "染整前处理绿色助剂及新型前处理工艺", 《日用化学品科学》 * |
| 邓永智等: "银杏叶中黄酮的水提取及HPLC测定", 《福建分析测试》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109944092A (en) * | 2019-03-05 | 2019-06-28 | 上海兴康化工有限公司 | A kind of reactive dye wool short route dyeing |
| CN109944092B (en) * | 2019-03-05 | 2021-08-24 | 上海兴康化工有限公司 | Short-process wool dyeing process using reactive dye |
| CN112746336A (en) * | 2020-12-24 | 2021-05-04 | 苏州经贸职业技术学院 | Degumming agent for silk fabric, preparation method of degumming agent and degumming method for silk fabric |
| CN114438803A (en) * | 2022-01-26 | 2022-05-06 | 内蒙古工业大学 | Cashmere fiber dyeing and deepening method and deepening agent |
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