CN106752457A - A kind of finishing coat masking liquid of high glaze inkjet printing canvas and preparation method thereof - Google Patents

A kind of finishing coat masking liquid of high glaze inkjet printing canvas and preparation method thereof Download PDF

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Publication number
CN106752457A
CN106752457A CN201611063948.7A CN201611063948A CN106752457A CN 106752457 A CN106752457 A CN 106752457A CN 201611063948 A CN201611063948 A CN 201611063948A CN 106752457 A CN106752457 A CN 106752457A
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China
Prior art keywords
parts
canvas
inkjet printing
finishing coat
masking liquid
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Pending
Application number
CN201611063948.7A
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Chinese (zh)
Inventor
陆建辉
王玉丰
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JIANGSU GEMEI HIGH-TECH DEVELOPMENT Co Ltd
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JIANGSU GEMEI HIGH-TECH DEVELOPMENT Co Ltd
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Priority to CN201611063948.7A priority Critical patent/CN106752457A/en
Publication of CN106752457A publication Critical patent/CN106752457A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D129/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Coating compositions based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Coating compositions based on derivatives of such polymers
    • C09D129/02—Homopolymers or copolymers of unsaturated alcohols
    • C09D129/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/66—Additives characterised by particle size
    • C09D7/67—Particle size smaller than 100 nm
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Abstract

The invention discloses a kind of finishing coat masking liquid of high glaze inkjet printing canvas, it is made up of each component of following parts by weight：18 25 parts of nano aluminium oxide；15 parts of polyvinyl alcohol；0.5 2 parts of acid；10 20 parts of cosolvent；0.1 0.2 parts of defoamer；20 60 parts of water.Its preparation method is as follows：Polyvinyl alcohol is first dissolved into 7% 10% aqueous solution by metering under the conditions of 80 95 DEG C, it is stand-by；Acid, cosolvent, defoamer and aluminum oxide are successively added in remaining water, dispersion 20 60 minutes, translucent aqueous dispersions are become to it at a high speed, are subsequently adding the stand-by poly-vinyl alcohol solution of dissolving, be slowly stirred 10 30 minutes, filtered, froth breaking, form finished product.The present invention has abandoned the shortcoming of swelling type canvas and matt pool waterproof canvas, has combined the advantage of both the above canvas compared to swelling type and matt pool waterproof canvas, the canvas that the formula and technique productions go out.

Description

A kind of finishing coat masking liquid of high glaze inkjet printing canvas and preparation method thereof
Technical field
The invention belongs to new material technology field, application field is digital ink-jet output medium field, and in particular to a kind of Finishing coat masking liquid of high glaze inkjet printing canvas and preparation method thereof.
Background technology
With ink-jet technology maximization, the maturation of the digital reproduction technology of the rapid and art work is exported, domestic culture is produced Product market is continuously developed, particularly " 80,90 " as consumption main force after, the demand to oil painting ornament is more next It is bigger, digital ink-jet oil painting has been come into huge numbers of families as a kind of new model oil painting, ink-jet canvas also serve as a kind of emerging Industry has gradually developed.
The indoor canvas for using, the predominantly non-watertight oil painting of swelling type and matt pool waterproof are applicable in the market Canvas.The non-watertight canvas development of swelling type is earliest, and its ink-absorbed coated layer is mainly gelatin, polyvinyl alcohol etc. can be dissolved in the thing of water Matter is constituted, and its blotting mechanism is swelling mechanism, first swelling after coating meets water, is finally redissolved, and prints to material surface Quantity of ink is considerably less, therefore only occurs swelling, by ink absorption to coating, bloom can be divided into by the difference of coating gloss The two kinds of canvas in pool and matt pool.Matt pool waterproof canvas is different from the former, and its blotting mechanism is micropore blotting machine Reason, using coated layer as ink-absorbing medium in coating, with polyvinyl alcohol and crosslinkable resin as binding agent, while adding Plus cationic fixing agent, the coating with microcellular structure is formed, coated layer is micron order, with photoextinction, because This coating is matt, is the canvas of indoor oil painting consumption maximum in the market.
Swelling type canvas is water-soluble due to its surface ink-absorbed coated layer, therefore, slow drying speed after its printing made Easily left a trace in journey, it is damage to meet water picture, while be difficult to the protection such as later stage glazing making, be increasingly difficult in adapt to The development in market.
Matt pool waterproof canvas, although current indoor market consumption is maximum, but because it is using micron-sized micro- , used as ink-absorbing medium, coating is matt, i.e., opaque, colour rendering is poor, and color is not bright-coloured for hole silica, is needed after picture printing Glazing treatment, can be only achieved real oil paint effect.
The content of the invention
Goal of the invention：The present invention provides a kind of finishing coat masking liquid of high glaze inkjet printing canvas and preparation method thereof, The production of canvas is applied to, the resistance to water problems of current swelling type canvas is solved, the glossiness of matt pool waterproof canvas is asked Topic, develop the color sex chromosome mosaicism, and reduces the later stage glazing production process of oil painting making.
Technical scheme：A kind of finishing coat masking liquid of high glaze inkjet printing canvas, the top coat is by following heavy Measure each component composition of number：
Nano aluminium oxide 18-25 parts；
Polyvinyl alcohol 1-5 parts；
It is sour 0.5-2 parts；
Cosolvent 10-20 parts；
Defoamer 0.1-0.2 parts；
Water 20-60 parts.
As optimization：The nano aluminium oxide, initial particle is less than 30 nanometers, and crystal formation is divided into α-Al2O3With γ-Al2O3。
As optimization：The polyvinyl alcohol, the polyvinyl alcohol of the degree of polymerization >=2400, the degree of polymerization is bigger, and addition is fewer, can Increase the consumption of aluminum oxide indirectly, and then improve blotting rate of drying, alcoholysis degree can be 88% and 99%.
As optimization：The acid is nitric acid, hydrochloric acid, one or two mixtures of sulfuric acid.
As optimization：The cosolvent is isopropanol, n-butanol, ethanol, dimethylformamide, diethyl monobutyl ether acetate One or more mixtures.
As optimization：The defoamer is tributyl phosphate, the fatty acid ester compounded thing of silicone emulsion, higher alcohols, polyoxy second Alkene polyoxypropylene pentaerythrite ether, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether and polyoxyethylene polyoxypropylene are sweet Oily ether, dimethyl silicone polymer one or more mixtures.
A kind of preparation method of the finishing coat masking liquid of the inkjet printing canvas of high glaze as mentioned, comprises the following steps： Polyvinyl alcohol is first dissolved into the aqueous solution of 7%-10% by metering under the conditions of 80-95 DEG C, it is stand-by；By acid, cosolvent, defoamer Successively it is added in remaining water with aluminum oxide, dispersion 20-60 minutes, becomes translucent aqueous dispersions, then to it at a high speed The poly-vinyl alcohol solution for adding dissolving stand-by, is slowly stirred 10-30 minutes, filters, froth breaking, forms high glaze inkjet printing oil painting The finishing coat masking liquid of cloth.
Beneficial effect：The present invention is compared to swelling type and matt pool waterproof canvas, the oil that the formula and technique productions go out Painting canvas has abandoned the shortcoming of swelling type canvas and matt pool waterproof canvas, combines the advantage of both the above canvas.Tool Body is compared as follows：
。
Specific embodiment
With reference to specific embodiment, the present invention will be described in detail.
Specific embodiment one：
A kind of finishing coat masking liquid of high glaze inkjet printing canvas, the top coat by following parts by weight each component Composition：
18 parts of nano aluminium oxide；
1 part of polyvinyl alcohol；
0.5 part of acid；
10 parts of cosolvent；
0.1 part of defoamer；
20 parts of water.
The nano aluminium oxide, initial particle is less than 30 nanometers, and crystal formation is divided into α-Al2O3。
The polyvinyl alcohol, the polyvinyl alcohol of the degree of polymerization >=2400, the degree of polymerization is bigger, and addition is fewer, can increase indirectly The consumption of aluminum oxide, and then blotting rate of drying is improved, alcoholysis degree can be 88%.
The acid is nitric acid.
The cosolvent is isopropanol, n-butanol.
The defoamer is tributyl phosphate, the fatty acid ester compounded thing of silicone emulsion, higher alcohols.
A kind of preparation method of the finishing coat masking liquid of the inkjet printing canvas of high glaze as mentioned, comprises the following steps： Polyvinyl alcohol is first dissolved into 7% aqueous solution by metering under the conditions of 80 DEG C, it is stand-by；By acid, cosolvent, defoamer and oxidation Aluminium is successively added in remaining water, and dispersion 20 minutes, translucent aqueous dispersions are become to it at a high speed, are subsequently adding dissolving and are treated Poly-vinyl alcohol solution, is slowly stirred 10 minutes, filtering, froth breaking, and the finishing coat for forming high glaze inkjet printing canvas is applied Liquid.
Specific embodiment two：
A kind of finishing coat masking liquid of high glaze inkjet printing canvas, the top coat by following parts by weight each component Composition：
25 parts of nano aluminium oxide；
5 parts of polyvinyl alcohol；
2 parts of acid；
20 parts of cosolvent；
0.2 part of defoamer；
60 parts of water.
The nano aluminium oxide, initial particle is less than 30 nanometers, and crystal formation is divided into γ-Al2O3。
The polyvinyl alcohol, the polyvinyl alcohol of the degree of polymerization >=2400, the degree of polymerization is bigger, and addition is fewer, can increase indirectly The consumption of aluminum oxide, and then blotting rate of drying is improved, alcoholysis degree can be 99%.
The acid is hydrochloric acid.
The cosolvent is ethanol, dimethylformamide.
The defoamer is polyoxyethylene polyoxypropylene pentaerythrite ether, polyoxyethylene polyoxy propyl alcohol amidogen ether, polyoxypropylene Glycerin ether.
A kind of preparation method of the finishing coat masking liquid of the inkjet printing canvas of high glaze as mentioned, comprises the following steps： Polyvinyl alcohol is first dissolved into 10% aqueous solution by metering under the conditions of 95 DEG C, it is stand-by；By acid, cosolvent, defoamer and oxidation Aluminium is successively added in remaining water, and dispersion 60 minutes, translucent aqueous dispersions are become to it at a high speed, are subsequently adding dissolving and are treated Poly-vinyl alcohol solution, is slowly stirred 30 minutes, filtering, froth breaking, and the finishing coat for forming high glaze inkjet printing canvas is applied Liquid.
Specific embodiment three：
A kind of finishing coat masking liquid of high glaze inkjet printing canvas, the top coat by following parts by weight each component Composition：
23 parts of nano aluminium oxide；
3 parts of polyvinyl alcohol；
1 part of acid；
13 parts of cosolvent；
0.17 part of defoamer；
50 parts of water.
The nano aluminium oxide, initial particle is less than 30 nanometers, and crystal formation is divided into γ-Al2O3。
The polyvinyl alcohol, the polyvinyl alcohol of the degree of polymerization >=2400, the degree of polymerization is bigger, and addition is fewer, can increase indirectly The consumption of aluminum oxide, and then blotting rate of drying is improved, alcoholysis degree can be 99%.
The acid is sulfuric acid.
The cosolvent is diethyl monobutyl ether acetate.
The defoamer is polypropylene glycerol aether and polyoxyethylene polyoxypropylene glycerin ether, dimethyl silicone polymer.
A kind of preparation method of the finishing coat masking liquid of the inkjet printing canvas of high glaze as mentioned, comprises the following steps： Polyvinyl alcohol is first dissolved into 8% aqueous solution by metering under the conditions of 87 DEG C, it is stand-by；By acid, cosolvent, defoamer and oxidation Aluminium is successively added in remaining water, and dispersion 40 minutes, translucent aqueous dispersions are become to it at a high speed, are subsequently adding dissolving and are treated Poly-vinyl alcohol solution, is slowly stirred 20 minutes, filtering, froth breaking, and the finishing coat for forming high glaze inkjet printing canvas is applied Liquid.
The present invention is not limited to above-mentioned preferred forms, and anyone can show that other are various under enlightenment of the invention The product of form, however, make any change in its shape or structure, it is every with skill identical or similar to the present application Art scheme, is within the scope of the present invention.

Claims (7)

1. a kind of finishing coat masking liquid of high glaze inkjet printing canvas, it is characterised in that：The top coat is by following heavy Measure each component composition of number：
Nano aluminium oxide 18-25 parts；
Polyvinyl alcohol 1-5 parts；
It is sour 0.5-2 parts；
Cosolvent 10-20 parts；
Defoamer 0.1-0.2 parts；
Water 20-60 parts.
2. the finishing coat masking liquid of high glaze inkjet printing canvas according to claim 1, it is characterised in that：The nanometer Aluminum oxide, initial particle is less than 30 nanometers, and crystal formation is divided into α-Al2O3With γ-Al2O3。
3. the finishing coat masking liquid of high glaze inkjet printing canvas according to claim 1, it is characterised in that：The poly- second Enol, the polyvinyl alcohol of the degree of polymerization >=2400, the degree of polymerization is bigger, and addition is fewer, can indirectly increase the consumption of aluminum oxide, and then Blotting rate of drying is improved, alcoholysis degree can be 88% and 99%.
4. the finishing coat masking liquid of high glaze inkjet printing canvas according to claim 1, it is characterised in that：The acid is Nitric acid, hydrochloric acid, one or two mixtures of sulfuric acid.
5. the finishing coat masking liquid of high glaze inkjet printing canvas according to claim 1, it is characterised in that：The hydrotropy Agent is isopropanol, n-butanol, ethanol, dimethylformamide, one or more mixtures of diethyl monobutyl ether acetate.
6. the finishing coat masking liquid of high glaze inkjet printing canvas according to claim 1, it is characterised in that：The froth breaking Agent is tributyl phosphate, the fatty acid ester compounded thing of silicone emulsion, higher alcohols, polyoxyethylene polyoxypropylene pentaerythrite ether, polyoxy Ethene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether and polyoxyethylene polyoxypropylene glycerin ether, dimethyl silicone polymer it is a kind of or Several mixtures.
7. a kind of preparation method of the finishing coat masking liquid of high glaze inkjet printing canvas as claimed in claim 1, its feature It is：Comprise the following steps：Polyvinyl alcohol is first dissolved into the aqueous solution of 7%-10% by metering under the conditions of 80-95 DEG C, it is stand-by； Acid, cosolvent, defoamer and aluminum oxide are successively added in remaining water, dispersion 20-60 minutes, becomes semi-transparent to it at a high speed Bright aqueous dispersions, are subsequently adding the stand-by poly-vinyl alcohol solution of dissolving, are slowly stirred 10-30 minutes, filter, froth breaking, are formed The finishing coat masking liquid of high glaze inkjet printing canvas.
CN201611063948.7A 2016-11-28 2016-11-28 A kind of finishing coat masking liquid of high glaze inkjet printing canvas and preparation method thereof Pending CN106752457A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106868930A (en) * 2017-02-16 2017-06-20 隋敏 A kind of high light waterproof ink jet painting canvas
CN108705873A (en) * 2018-04-08 2018-10-26 温州创佳影像材料有限公司 One kind tearing not rotten duplex printing RC printing paper and its production technology
CN109594347A (en) * 2018-12-13 2019-04-09 广东高璐美数码科技有限公司 A kind of aluminium system waterproof glossy canvas and preparation method thereof
CN110281692A (en) * 2019-06-27 2019-09-27 沭阳凤凰画材有限公司 A kind of canvas and its mounting frame

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1000767A1 (en) * 1998-11-03 2000-05-17 ILFORD Imaging Switzerland GmbH Recording materials for ink jet printing
CN1544252A (en) * 2003-11-19 2004-11-10 中国乐凯胶片集团公司 Waterproof high light ink jet printing medium
CN103129200A (en) * 2011-11-21 2013-06-05 佳能株式会社 Recording medium

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1000767A1 (en) * 1998-11-03 2000-05-17 ILFORD Imaging Switzerland GmbH Recording materials for ink jet printing
CN1544252A (en) * 2003-11-19 2004-11-10 中国乐凯胶片集团公司 Waterproof high light ink jet printing medium
CN103129200A (en) * 2011-11-21 2013-06-05 佳能株式会社 Recording medium

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106868930A (en) * 2017-02-16 2017-06-20 隋敏 A kind of high light waterproof ink jet painting canvas
CN108705873A (en) * 2018-04-08 2018-10-26 温州创佳影像材料有限公司 One kind tearing not rotten duplex printing RC printing paper and its production technology
CN109594347A (en) * 2018-12-13 2019-04-09 广东高璐美数码科技有限公司 A kind of aluminium system waterproof glossy canvas and preparation method thereof
CN109594347B (en) * 2018-12-13 2021-04-02 广东高璐美数码科技有限公司 Aluminum waterproof high-gloss canvas and preparation method thereof
CN110281692A (en) * 2019-06-27 2019-09-27 沭阳凤凰画材有限公司 A kind of canvas and its mounting frame

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