CN106752213A - A kind of preparation method of transparent heat insulating dope - Google Patents
A kind of preparation method of transparent heat insulating dope Download PDFInfo
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- CN106752213A CN106752213A CN201611241740.XA CN201611241740A CN106752213A CN 106752213 A CN106752213 A CN 106752213A CN 201611241740 A CN201611241740 A CN 201611241740A CN 106752213 A CN106752213 A CN 106752213A
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- tetrafluoroethene
- waterglass
- preparation
- butanol
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
- C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
Abstract
The invention discloses a kind of preparation method of transparent heat insulating dope, preparation process：1）Weigh monocomponent polyurethane, waterglass, Ludox, polyvinyl alcohol, carboxymethylcellulose calcium, calcium chloride, diatomite, mica powder, lithopone, titanium dioxide, manganese dioxide, n-butanol, tetrafluoroethene and asbestos fibre；2）Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reactor of agitator and thermometer, 70 90 DEG C are warming up to, 40 80min are stirred, mixing speed is 800 1200 revs/min；3）90 110 DEG C are warming up to, surplus stock is added, mix 80 120min, 20 40min are ground in grinder, filtered and packaged.Coating appearance of film obtained by the present invention is transparent smooth, the 15min of surface drying 5, does solid work 16 20h；The 70J of impact strength 50,12 grades of adhesive force；Water resistance immerses 10 15d in 30 DEG C of water, non-foaming not fall off；Anti-scratch load is high, shore hardness 0.25 0.45, can extensively produce and constantly replace current material.
Description
Technical field
The present invention relates to paint field, more particularly to a kind of preparation method of transparent heat insulating dope.
Background technology
Insulating moulding coating is one kind, reflection thermal-optical type, short time limit, the functional coating of instant effect for growing up in recent years.
Thermal insulating coating has three kinds, isolation conduction type insulating moulding coating, reflection type thermal insulation coating and radiation type heat-insulation from the classification of characteristic principle is main
Coating.Except above-mentioned three types insulating moulding coating, has there are a kind of heat insulating coatings in external heat insulating function coating, except tool
Beyond the advantage of standby above-mentioned insulating moulding coating, more for peculiar heat insulation effect.
Earlier 1970s, U.S. coating expert utilizes material under vacuum conditions, its molecular vibration heat transfer
The characteristic being wholly absent with convection current conduction two ways, using NASA spacecraft heat-barrier material technologies, by particle diameter 6-10um's
Spherical hollow ceramics microvesicle is filled out and is suspended from inertia latex binder（It is aqueous）In, obtain a kind of high-performance, the heat insulating material of high-quality
Material --- ceramic microvesicle heat insulating coatings.Since then, use hollow particle as filler with the excellent thermal insulation coatings of processability
Focus as the research of particular function coating.
Analyzed by solar spectrum energy, the solar energy overwhelming majority is in visible ray and near infrared region, i.e. 400~1800nm models
Enclose.In the wave-length coverage, reflectivity is higher, and the effect of heat insulation of coating is better.Therefore the coating of high reflectance can be obtained, instead
Solar heat is penetrated to reach heat-insulated purpose.Transparent heat insulating dope be it is a kind of can be by the heat in sunshine（Mainly infrared ray portion
Divide and produce）Reflected back by coating surface, keep visible ray here, so as to the nano transparent heat-insulating for producing heat-insulation transparent effect is applied
Material.
Existing transparent heat insulating dope main component is tin indium oxide, due to the special performance that tin indium oxide has, to too
Solar spectrum has preferably selectivity, is to be currently known in semi-conducting material to solve the optimal material of heat-insulating problem combination property.
Therefore selection nano-indium stannum oxide prepares transparent heat insulating dope, it is ensured that its high-performance.As a kind of environmentally friendly water
Property coating, it not only translucency it is good, and can effectively completely cut off sun heat radiation, need to only brush several microns of thickness, so that it may make
Indoor/outdoor temperature-difference reaches 6 degrees centigrades, and infrared shielding rate reaches 70%, it is seen that light transmission rate reaches 80%, and ultraviolet stop reaches
To 99%, even if do not turn on the aircondition can also reach the effect of " cool in summer and warm in winter ", can be widely applied on automobile and all kinds of buildings, should
Product selects nano inorganic material, with functions such as excellent ageing-resistant, stain resistant is self-cleaning, antistatic, anti-dazzle, radiation proofs.
With social city, technicalization, hommization development, how to design and develop that a kind of fast drying, adhesive force is strong, punching
Hit intensity is high, hardness is high and anti-scratch load good transparent heat insulating dope is to meet the market demand, is very important.
The content of the invention
The technical problem of solution：
The application is for existing coating effect of heat insulation is poor, adhesive force is low, drying is slow and the low technical problem of hardness, there is provided Yi Zhongtou
The preparation method of bright insulating moulding coating.
Technical scheme：
A kind of preparation method of transparent heat insulating dope of the present invention, its preparation process is as follows：
The first step：Weigh monocomponent polyurethane, waterglass, Ludox, polyvinyl alcohol, carboxymethylcellulose calcium, calcium chloride, diatom
Soil, mica powder, lithopone, titanium dioxide, manganese dioxide, n-butanol, tetrafluoroethene and asbestos fibre；
Second step：Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reaction of agitator and thermometer
In kettle, 70-90 DEG C is warming up to, stirs 40-80min, mixing speed is 800-1200 revs/min；
3rd step：90-110 DEG C is warming up to, surplus stock is added, mixes 80-120min, 20-40min is ground in grinder,
Filter and package.
Used as one embodiment of the present invention, each raw materials by weight portion proportioning of the present invention is as follows：The poly- ammonia of one-component
100 parts of ester, waterglass 1-5 parts, Ludox 2-6 parts, polyvinyl alcohol 6-10 parts, carboxymethylcellulose calcium 5-25 parts, calcium chloride 5-25
Part, diatomite 8-12 parts, mica powder 10-30 parts, lithopone 15-35 parts, titanium dioxide 3-7 parts, manganese dioxide 12-18 parts, positive fourth
Alcohol 40-60 parts, tetrafluoroethene 15-55 parts, asbestos fibre 25-45 parts.
Used as one embodiment of the present invention, each raw materials by weight portion proportioning of the present invention is as follows：The poly- ammonia of one-component
100 parts of ester, waterglass 2-4 parts, Ludox 3-5 parts, polyvinyl alcohol 7-9 parts, carboxymethylcellulose calcium 10-20 parts, calcium chloride 10-20
Part, diatomite 9-11 parts, mica powder 15-25 parts, lithopone 20-30 parts, titanium dioxide 4-6 parts, manganese dioxide 14-16 parts, positive fourth
Alcohol 45-55 parts, tetrafluoroethene 25-45 parts, asbestos fibre 30-40 parts.
Used as one embodiment of the present invention, each raw materials by weight portion proportioning of the present invention is as follows：The poly- ammonia of one-component
100 parts of ester, 2 parts of waterglass, 3 parts of Ludox, 7 parts of polyvinyl alcohol, 10 parts of carboxymethylcellulose calcium, 10 parts of calcium chloride, diatomite 9
Part, 15 parts of mica powder, 20 parts of lithopone, 4 parts of titanium dioxide, 14 parts of manganese dioxide, 45 parts of n-butanol, 25 parts of tetrafluoroethene, asbestos
30 parts of fiber.
Used as one embodiment of the present invention, each raw materials by weight portion proportioning of the present invention is as follows：The poly- ammonia of one-component
100 parts of ester, 4 parts of waterglass, 5 parts of Ludox, 9 parts of polyvinyl alcohol, 20 parts of carboxymethylcellulose calcium, 20 parts of calcium chloride, diatomite 11
Part, 25 parts of mica powder, 30 parts of lithopone, 6 parts of titanium dioxide, 16 parts of manganese dioxide, 55 parts of n-butanol, 45 parts of tetrafluoroethene, asbestos
40 parts of fiber.
Used as one embodiment of the present invention, each raw materials by weight portion proportioning of the present invention is as follows：The poly- ammonia of one-component
100 parts of ester, 3 parts of waterglass, 4 parts of Ludox, 8 parts of polyvinyl alcohol, 15 parts of carboxymethylcellulose calcium, 15 parts of calcium chloride, diatomite 10
Part, 20 parts of mica powder, 25 parts of lithopone, 5 parts of titanium dioxide, 15 parts of manganese dioxide, 50 parts of n-butanol, 35 parts of tetrafluoroethene, asbestos
35 parts of fiber.
Beneficial effect：
Compared to the prior art, obtained coating products have following technique effect to the present invention：1st, appearance of film is transparent smooth,
Surface drying 5-15min, does solid work 16-20h；2nd, impact strength 50-70J, adhesive force 1-2 grades；3rd, water resistance immerses 10- in 30 DEG C of water
15d, it is non-foaming not fall off；4th, anti-scratch load is high, shore hardness 0.25-0.45, can extensively produce and constantly replace existing
Material.
Specific embodiment
Embodiment 1:
Proportioning weighs 100 parts of monocomponent polyurethane, 1 part of waterglass, 2 parts of Ludox, 6 parts of polyvinyl alcohol, carboxylic first by weight
5 parts of base cellulose, 5 parts of calcium chloride, 8 parts of diatomite, 10 parts of mica powder, 15 parts of lithopone, 3 parts of titanium dioxide, 12 parts of manganese dioxide,
40 parts of n-butanol, 15 parts of tetrafluoroethene, 25 parts of asbestos fibre.
Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reactor of agitator and thermometer
In, 70 DEG C are warming up to, 40min is stirred, mixing speed is 800 revs/min.
90 DEG C are warming up to, surplus stock is added, mix 80min, 20min is ground in grinder, filtered and packaged.
Appearance of film is transparent smooth, surface drying 15min, does solid work 20h；Impact strength 50J, 2 grades of adhesive force；Water resistance immersion 30
10d in DEG C water, it is non-foaming not fall off；Anti-scratch load is high, shore hardness 0.25, can extensively produce and constantly replace existing material
Material.
Embodiment 2:
Proportioning weighs 100 parts of monocomponent polyurethane, 5 parts of waterglass, 6 parts of Ludox, 10 parts of polyvinyl alcohol, carboxylic first by weight
25 parts of base cellulose, 25 parts of calcium chloride, 12 parts of diatomite, 30 parts of mica powder, 35 parts of lithopone, 7 parts of titanium dioxide, manganese dioxide 18
Part, 60 parts of n-butanol, 55 parts of tetrafluoroethene, 45 parts of asbestos fibre.
Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reactor of agitator and thermometer
In, 90 DEG C are warming up to, 80min is stirred, mixing speed is 1200 revs/min.
110 DEG C are warming up to, surplus stock is added, mix 120min, 40min is ground in grinder, filtered and packaged.
Appearance of film is transparent smooth, surface drying 13min, does solid work 19h；Impact strength 55J, 2 grades of adhesive force；Water resistance immersion 30
12d in DEG C water, it is non-foaming not fall off；Anti-scratch load is high, shore hardness 0.3, can extensively produce and constantly replace existing material
Material.
Embodiment 3:
Proportioning weighs 100 parts of monocomponent polyurethane, 2 parts of waterglass, 3 parts of Ludox, 7 parts of polyvinyl alcohol, carboxylic first by weight
10 parts of base cellulose, 10 parts of calcium chloride, 9 parts of diatomite, 15 parts of mica powder, 20 parts of lithopone, 4 parts of titanium dioxide, manganese dioxide 14
Part, 45 parts of n-butanol, 25 parts of tetrafluoroethene, 30 parts of asbestos fibre.
Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reactor of agitator and thermometer
In, 70 DEG C are warming up to, 40min is stirred, mixing speed is 800 revs/min.
90 DEG C are warming up to, surplus stock is added, mix 80min, 20min is ground in grinder, filtered and packaged.
Appearance of film is transparent smooth, surface drying 10min, does solid work 18h；Impact strength 60J, 2 grades of adhesive force；Water resistance immersion 30
13d in DEG C water, it is non-foaming not fall off；Anti-scratch load is high, shore hardness 0.35, can extensively produce and constantly replace existing material
Material.
Embodiment 4:
Proportioning weighs 100 parts of monocomponent polyurethane, 4 parts of waterglass, 5 parts of Ludox, 9 parts of polyvinyl alcohol, carboxylic first by weight
20 parts of base cellulose, 20 parts of calcium chloride, 11 parts of diatomite, 25 parts of mica powder, 30 parts of lithopone, 6 parts of titanium dioxide, manganese dioxide 16
Part, 55 parts of n-butanol, 45 parts of tetrafluoroethene, 40 parts of asbestos fibre.
Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reactor of agitator and thermometer
In, 90 DEG C are warming up to, 80min is stirred, mixing speed is 1200 revs/min.
110 DEG C are warming up to, surplus stock is added, mix 120min, 40min is ground in grinder, filtered and packaged.
Appearance of film is transparent smooth, surface drying 8min, does solid work 17h；Impact strength 65J, adhesion 1 grade；Water resistance immersion 30
14d in DEG C water, it is non-foaming not fall off；Anti-scratch load is high, shore hardness 0.4, can extensively produce and constantly replace existing material
Material.
Embodiment 5:
Proportioning weighs 100 parts of monocomponent polyurethane, 3 parts of waterglass, 4 parts of Ludox, 8 parts of polyvinyl alcohol, carboxylic first by weight
15 parts of base cellulose, 15 parts of calcium chloride, 10 parts of diatomite, 20 parts of mica powder, 25 parts of lithopone, 5 parts of titanium dioxide, manganese dioxide 15
Part, 50 parts of n-butanol, 35 parts of tetrafluoroethene, 35 parts of asbestos fibre.
Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reactor of agitator and thermometer
In, 80 DEG C are warming up to, 60min is stirred, mixing speed is 1000 revs/min.
100 DEG C are warming up to, surplus stock is added, mix 100min, 30min is ground in grinder, filtered and packaged.
Appearance of film is transparent smooth, surface drying 5min, does solid work 16h；Impact strength 70J, adhesion 1 grade；Water resistance immersion 30
15d in DEG C water, it is non-foaming not fall off；Anti-scratch load is high, shore hardness 0.45, can extensively produce and constantly replace existing material
Material.
All components in above example can be with commercially available.
The above embodiments are intended to illustrate the present invention, rather than limitation, therefore with it is of the invention
Any change in claims suitable implication and scope, is all considered as being included within the scope of the claims.
Claims (6)
1. a kind of preparation method of transparent heat insulating dope, it is characterised in that：Preparation process is as follows：
The first step：Weigh monocomponent polyurethane, waterglass, Ludox, polyvinyl alcohol, carboxymethylcellulose calcium, calcium chloride, diatom
Soil, mica powder, lithopone, titanium dioxide, manganese dioxide, n-butanol, tetrafluoroethene and asbestos fibre；
Second step：Monocomponent polyurethane, waterglass, n-butanol and tetrafluoroethene input are provided with the reaction of agitator and thermometer
In kettle, 70-90 DEG C is warming up to, stirs 40-80min, mixing speed is 800-1200 revs/min；
3rd step：90-110 DEG C is warming up to, surplus stock is added, mixes 80-120min, 20-40min is ground in grinder,
Filter and package.
2. the preparation method of a kind of transparent heat insulating dope according to claim 1, it is characterised in that：Each raw material is by weight
Amount number proportioning is as follows：100 parts of monocomponent polyurethane, waterglass 1-5 parts, Ludox 2-6 parts, polyvinyl alcohol 6-10 parts, carboxylic first
5-25 parts of base cellulose, calcium chloride 5-25 parts, diatomite 8-12 parts, mica powder 10-30 parts, lithopone 15-35 parts, titanium dioxide 3-
7 parts, manganese dioxide 12-18 parts, n-butanol 40-60 parts, tetrafluoroethene 15-55 parts, asbestos fibre 25-45 parts.
3. the preparation method of a kind of transparent heat insulating dope according to claim 1, it is characterised in that：Each raw material is by weight
Amount number proportioning is as follows：100 parts of monocomponent polyurethane, waterglass 2-4 parts, Ludox 3-5 parts, polyvinyl alcohol 7-9 parts, carboxymethyl
Cellulose 10-20 parts, calcium chloride 10-20 parts, diatomite 9-11 parts, mica powder 15-25 parts, lithopone 20-30 parts, titanium dioxide 4-
6 parts, manganese dioxide 14-16 parts, n-butanol 45-55 parts, tetrafluoroethene 25-45 parts, asbestos fibre 30-40 parts.
4. the preparation method of a kind of transparent heat insulating dope according to claim 1, it is characterised in that：Each raw material is by weight
Amount number proportioning is as follows：100 parts of monocomponent polyurethane, 2 parts of waterglass, 3 parts of Ludox, 7 parts of polyvinyl alcohol, carboxymethylcellulose calcium
10 parts, 10 parts of calcium chloride, 9 parts of diatomite, 15 parts of mica powder, 20 parts of lithopone, 4 parts of titanium dioxide, 14 parts of manganese dioxide, n-butanol
45 parts, 25 parts of tetrafluoroethene, 30 parts of asbestos fibre.
5. the preparation method of a kind of transparent heat insulating dope according to claim 1, it is characterised in that：Each raw material is by weight
Amount number proportioning is as follows：100 parts of monocomponent polyurethane, 4 parts of waterglass, 5 parts of Ludox, 9 parts of polyvinyl alcohol, carboxymethylcellulose calcium
20 parts, 20 parts of calcium chloride, 11 parts of diatomite, 25 parts of mica powder, 30 parts of lithopone, 6 parts of titanium dioxide, 16 parts of manganese dioxide, positive fourth
55 parts of alcohol, 45 parts of tetrafluoroethene, 40 parts of asbestos fibre.
6. the preparation method of a kind of transparent heat insulating dope according to claim 1, it is characterised in that：Each raw material is by weight
Amount number proportioning is as follows：100 parts of monocomponent polyurethane, 3 parts of waterglass, 4 parts of Ludox, 8 parts of polyvinyl alcohol, carboxymethylcellulose calcium
15 parts, 15 parts of calcium chloride, 10 parts of diatomite, 20 parts of mica powder, 25 parts of lithopone, 5 parts of titanium dioxide, 15 parts of manganese dioxide, positive fourth
50 parts of alcohol, 35 parts of tetrafluoroethene, 35 parts of asbestos fibre.
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| CN201611241740.XA CN106752213A (en) | 2016-12-29 | 2016-12-29 | A kind of preparation method of transparent heat insulating dope |
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| CN201611241740.XA CN106752213A (en) | 2016-12-29 | 2016-12-29 | A kind of preparation method of transparent heat insulating dope |
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| CN104789101A (en) * | 2015-04-07 | 2015-07-22 | 苏州绿科环保新材料有限公司 | Energy-saving type transparent coating with functions of heat reflection and heat insulation |
-
2016
- 2016-12-29 CN CN201611241740.XA patent/CN106752213A/en active Pending
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| CN101550313A (en) * | 2008-09-27 | 2009-10-07 | 深圳市德厚科技有限公司 | Polyurethane BTO nano transparent heat insulation coating |
| CN101899249A (en) * | 2009-05-25 | 2010-12-01 | 上海复甲新型材料科技有限公司 | Transparent thermal insulation anti-ultraviolet coating and preparation method thereof |
| CN101648794A (en) * | 2009-09-21 | 2010-02-17 | 吕海涛 | Dry-type heat-insulating waterproof coating |
| CN102477253A (en) * | 2010-11-26 | 2012-05-30 | 深圳市嘉达高科产业发展有限公司 | Glass heat insulation paint with variable heat insulation and light transmittance performances and preparation process thereof |
| CN104789101A (en) * | 2015-04-07 | 2015-07-22 | 苏州绿科环保新材料有限公司 | Energy-saving type transparent coating with functions of heat reflection and heat insulation |
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Application publication date: 20170531 |