CN102477253A - Glass heat insulation paint with variable heat insulation and light transmittance performances and preparation process thereof - Google Patents
Glass heat insulation paint with variable heat insulation and light transmittance performances and preparation process thereof Download PDFInfo
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- CN102477253A CN102477253A CN2010105618619A CN201010561861A CN102477253A CN 102477253 A CN102477253 A CN 102477253A CN 2010105618619 A CN2010105618619 A CN 2010105618619A CN 201010561861 A CN201010561861 A CN 201010561861A CN 102477253 A CN102477253 A CN 102477253A
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Abstract
The invention relates to a glass heat insulation paint with variable heat insulation and light transmittance performances and a preparation process thereof. The paint comprises the following components (by weight): 50 to 80 parts of transparent resin, 0 to 15 parts of a cosolvent, 10 to 50 parts of nanometer heat insulation slurry, 0 to 0.5 part of an antifoaming agent, 0 to 0.5 part of a substrate wetting agent, 0 to 0.5 part of a leveling agent, 0 to 3.0 parts of a toughening agent and 0 to 10.0 parts of temperature-sensitive color paste. According to the invention, the glass heat insulation paint can automatically adjust a shading coefficient and visible light transmittance according to the intensity of solar radiation; a paint film has good performance; the preparation process is simple; construction of the paint is convenient; the paint can satisfy different demands for heat insulation and lighting performances in sunny days, overcast days and cloudy days and in summer and winter, can be used in an region which is hot in summer and warm in winter or even in a cold region, and is applicable to both heat insulation of architectural glass and heat insulation of glass and transparent substrates used in automobiles and the like needing heat insulation treatment.
Description
Technical field
The present invention relates to building material technical field, particularly a kind of heat insulation and variable glass heat-insulating coating and ME of light transmission.
Background technology
China is vast in territory, and the each department climate difference is very big, and the energy-saving design in construction of different areas requires different.GB 50176-1993 " code for thermal design of civil buildings " to the design requirements of hot summer and warm winter region is: must fully satisfy anti-heat request in summer, generally can not consider Winter protection.In general, it is that summer, refrigeration was very expensive with raise 4 times of required energy consumption once of temperature that temperature is reduced once required energy consumption, and for hot summer and warm winter region, the heat-insulating problem in summer that solves building is significant to building energy conservation.At southern area, the ratio that the indoor/outdoor temperature-difference heat transfer accounts in whole heat transfer is less, and the heat effect that solar radiation produces is to cause the major cause of indoor overheating in summer.And the consumption more than 40% of building energy consumption is on glass door and window, so the power saving that solves glass is the most important thing of hot summer and warm winter region building energy conservation.
The conventional glass provision for thermal insulation mainly contains heat reflection (sunlight control) glass and low radiation (Low-E) glass.But the former visible light transmissivity is lower, has a strong impact on indoor lighting, causes the interior lighting energy consumption to increase, and has the problem of light pollution; The latter costs an arm and a leg, and production and processing technology is complicated, and in life-time service, the plated film of low emissivity glass is prone to oxidation and causes heat insulating function to lose efficacy.
The Clear paint of glass heat-proof had appearred on the market can be used in recent years; This coating can form Clear coating behind drying and forming-film on glass; Visible light had higher transmittance; And infrared light is had good barrier property, reach good effect of heat insulation thereby be implemented on the basis of sufficient printing opacity.Compare with pad pasting glass, the visible transmission of this coating does not influence indoor lighting than high; With Low-E glassy phase ratio, do not have the problem of plated film oxidation forfeiture heat insulating function, and cost is low, production and processing technology is simple.
But based on the kind and the characteristic of employed heat insulating function pigment, the sheltering coefficient of the existing Clear paint that is used for glass heat-proof is about 1 with the ratio of visible transmission ratio.As use the little product of sheltering coefficient, though can guarantee good effect of heat insulation, when the cloudy day, because visible transmission has influenced indoor lighting than also little, the illumination energy consumption of extra increase also is unfavorable for whole building energy conservation.But like the bigger Clear paint that is used for glass heat-proof of use visible transmission, but can't realize good effect of heat insulation, can't reach the requirement of building energy conservation.In the city, South Area of hot summer and warm winter region,, need not to consider the heating in winter like Guangzhou; But in the North Area of hot summer and warm winter region, like Foochow, the winter heating energy consumption accounts for 45% of annual total energy consumption, hope that solar heat can inlet chamber this moment in, bigger visible transmission ratio is promptly arranged, but needs good heat insulation, promptly less sheltering coefficient summer equally.Even at cold district, like Beijing, also hoping has good effect of heat insulation in summer, gets hot but do not influence the sun in winter again simultaneously.To above-mentioned situation, as use the existing coating products that is used for glass heat-proof, sheltering coefficient and visible transmission ratio can't meet the demands simultaneously, and this problem has also influenced the promotion and application of glass heat-insulating coating on market.
Summary of the invention
The present invention provides a kind of glass heat-insulating coating, can regulate the glass heat-insulating coating and the ME of sheltering coefficient and visible transmission ratio along with intensity of solar radiation automatically.
To achieve these goals, technical scheme provided by the invention is:
A kind of heat insulation and variable glass heat-insulating coating of light transmission, it comprises following component (according to ratio of weight and number):
Transparent resin: 50～80 parts
Solubility promoter: 0～15 part
Nano heat-insulating slurry: 10～50 parts
Skimmer: 0～0.5 part
Base material wetting agent: 0～0.5 part
Flow agent: 0～0.5 part
Toughner: 0～3.0 part
Temperature-sensitive mill base: 0～10.0 part.
Preferably, described transparent resin can be various transparent resins such as transparent silicon resinoid, transparent polyurethane resin, transparent fluorocarbon resin, transparent Synolac.
Preferably, said nano heat-insulating slurry is: a kind of in nano antimony tin oxide slurry, nano-indium stannum oxide slurry, nano indium oxide slurry, nano-stannic oxide slurry, the nano-aluminium oxide slurry or or several kinds mixture.
Preferably, said solubility promoter is ethylene glycol monobutyl ether, diethylene glycol monobutyl ether, Ucar 35 butyl ether, dipropylene glycol butyl ether, propylene glycol monomethyl ether or dipropylene glycol methyl ether.
Preferably, said toughner is organo silane coupling agent, Witcizer 300 or DOP.
Preferably, said temperature-sensitive mill base is: organic type of material or inorganic matter a kind of, or the mixture of several kinds of organic type of materials or several kinds of inorganic matters; Or several kinds of mixtures that several types of materials and inorganic matter are arranged.
The present invention also provides the ME of the variable glass heat-insulating coating of a kind of heat insulation and light transmission, each component of getting the said ratio of weight and number of technique scheme, according to following steps:
A, in paint mixing tank, add and add transparent resin and nano heat-insulating slurry successively, under 500～800rpm, stir 5～10min;
B, rotating speed transfer to 1000～1200rpm, add solubility promoter, stir 5～10min;
C, add skimmer and base material wetting agent successively, rotating speed transfers to 1200～1500rpm, stirs 10～20min;
D, rotating speed transfer to 800～1000rpm, add flow agent, stir 10～20min;
E, rotating speed transfer to 500～800rpm, add toughner, stir 10～15min;
F, adding temperature-sensitive mill base stir 5～10min;
G, rotating speed transfer to 400～600rpm, and stirring 10～20min carries out froth breaking and obtains the said heat insulation and variable glass heat-insulating coating of light transmission.
Technical scheme through embodiment of the present invention; Has following beneficial effect: glass heat-insulating coating provided by the invention and ME; This glass heat-insulating coating can be regulated the glass heat-insulating coating of sheltering coefficient and visible transmission ratio automatically along with intensity of solar radiation, and paint film property is good, production technique simple, easy construction.Solved present glass heat-insulating coating can't take into account fine and cloudy, cloudy and summer and winter to heat insulation and demands of different lighting performance, Application Areas can be extended to hot summer and warm winter region even cold district.It is heat insulation to can be applicable to building glass, also can be applicable to glass and transparent substrate heat insulation that automobile etc. need carry out heat insulation processing.
Embodiment
In order to make the object of the invention, technical scheme and advantage clearer, below, the present invention is further elaborated through embodiment.Should be appreciated that specific embodiment described herein only in order to explanation the present invention, and be not used in qualification the present invention.
The embodiment of the invention provides a kind of heat insulation and variable glass heat-insulating coating of light transmission, and it comprises following component (according to ratio of weight and number):
Transparent resin: 50～80 parts
Solubility promoter: 0～15 part
Nano heat-insulating slurry: 10～50 parts
Skimmer: 0～0.5 part
Base material wetting agent: 0～0.5 part
Flow agent: 0～0.5 part
Toughner: 0～3.0 part
Temperature-sensitive mill base: 0～10.0 part.
In the present embodiment, concrete, described transparent resin can be various transparent resins such as transparent silicon resinoid, transparent polyurethane resin, transparent fluorocarbon resin, transparent Synolac.
In the present embodiment; Concrete, said nano heat-insulating slurry is: a kind of in nano antimony tin oxide (ATO) slurry, nano-indium stannum oxide (ITO) slurry, nano indium oxide (In2O3) slurry, nano-stannic oxide (SnO2) slurry, nano-aluminium oxide (Al2O3) slurry or or several kinds mixture.Wherein preferably this nano heat-insulating slurry is the ATO slurry.
In the present embodiment, concrete, said solubility promoter is ethylene glycol monobutyl ether, diethylene glycol monobutyl ether, Ucar 35 butyl ether, dipropylene glycol butyl ether, propylene glycol monomethyl ether or dipropylene glycol methyl ether etc.For preventing paint film when construction whiting.
In the present embodiment, concrete, said toughner is organo silane coupling agent, Witcizer 300 or DOP.Said toughner increases the snappiness of paint film, avoids paint film generation of cracks in use, and the sticking power on smooth basal planes such as glass of can promoting to film.
In the present embodiment, concrete, said temperature-sensitive mill base is: organic type of material or inorganic matter a kind of, or the mixture of several kinds of organic type of materials or several kinds of inorganic matters; Or several kinds of mixtures that several types of materials and inorganic matter are arranged.Said temperature-sensitive mill base is: can be that Thermoreversibly off-color material or optical radiation cause the reversible color material.
The embodiment of the invention also provides the ME of the variable glass heat-insulating coating of a kind of heat insulation and light transmission, gets each component of the said ratio of weight and number that the foregoing description provides, according to following steps:
A, in paint mixing tank, add and add transparent resin and nano heat-insulating slurry successively, 500～800rpm (rev/min) stir down 5～10min (minute);
B, rotating speed transfer to 1000～1200rpm, add solubility promoter, stir 5～10min;
C, add skimmer and base material wetting agent successively, rotating speed transfers to 1200～1500rpm, stirs 10～20min;
D, rotating speed transfer to 800～1000rpm, add flow agent, stir 10～20min;
E, rotating speed transfer to 500～800rpm, add toughner, stir 10～15min;
F, adding temperature-sensitive mill base stir 5～10min;
G, rotating speed transfer to 400～600rpm, and stirring 10～20min carries out froth breaking and obtains the said heat insulation and variable glass heat-insulating coating of light transmission.
The sheltering coefficient of the glass heat-insulating coating that the heat insulation and light transmission of above-mentioned ME is variable can be regulated according to solar radiation intensity with the visible transmission ratio automatically; Solved present glass heat-insulating coating can't take into account fine and cloudy, cloudy and summer and winter to heat insulation and demands of different lighting performance, Application Areas can be extended to hot summer and warm winter region even cold district.It is heat insulation to can be applicable to building glass, also can be applicable to glass and transparent substrate heat insulation that automobile etc. need carry out heat insulation processing.
The concrete manufacturing embodiment of the variable glass heat-insulating coating of several heat insulation and light transmissions is provided below:
Embodiment 1:
In paint mixing tank, add the transparent organic silicon resin (FJN-9804, Changzhou City Jianuo Organic Silicon Co., Ltd) and the 15 parts of ATO slurries (ATO-8220-PMA, Shanghai Huzheng Nano-Tech Co., Ltd.) that add 80 parts successively, under 500rpm, stir 10min; Slowly improve rotating speed to 1000rpm, add 10 parts ethylene glycol monobutyl ether gradually, stir 5min; Skimmer (
Gol 0011 that adds 0.3 part successively; OMG Borchers GmbH) and 0.2 part base material wetting agent (
LA-50; EthoxChemicals); Improve rotating speed to 1500rpm, stir 15min; Reduce rotating speed to 800rpm, adds 0.2 part flow agent (Keper 191, triumphant general auxiliary agent ltd), stirring 15min; The Witcizer 300 toughner that adds 2 parts stirs 10min; Add 3 parts of temperature-sensitive mill bases (outstanding color printing floral material ltd), stir 10min; Reduce rotating speed to 500rpm, froth breaking 20min.
Embodiment 2:
In paint mixing tank, add the transparent organic silicon resin (FJN-9804, Changzhou City Jianuo Organic Silicon Co., Ltd) and the 40 parts of ATO slurries (Luoyang boat Material Insitute) that add 50 parts successively, under 800rpm, stir 10min; Slowly improve rotating speed to 1000rpm, add 10 parts diethylene glycol monobutyl ether gradually, stir 8min; Skimmer (
Gol 0011 that adds 0.4 part successively; OMG Borchers GmbH) and 0.2 part base material wetting agent (
LA-50; Ethox Chemicals); Improve rotating speed to 1200rpm, stir 20min; Reduce rotating speed to 800rpm, adds 0.4 part flow agent (Keper 191, triumphant general auxiliary agent ltd), stirring 10min; The DOP toughner that adds 1 part stirs 10min; Add 5 parts of temperature-sensitive mill bases (Dongguan rise printing coating company), stir 20min; Reduce rotating speed to 500rpm, froth breaking 20min.
Embodiment 3:
In paint mixing tank, add transparent polyurethane resin (
XP 2593/1 that adds 50 parts successively; Bayer AG) and 45 parts of ATO slurries (Luoyang boat Material Insitute), under 800rpm, stir 10min; Slowly improve rotating speed to 1200rpm, add 6 parts ethylene glycol monobutyl ether gradually, stir 8min; Skimmer (
0670 that adds 0.4 part successively; OMG Borchers GmbH) and 0.2 part base material wetting agent (
Wet-270; Evonik Tego Chemie GmbH); Improve rotating speed to 1200rpm, stir 20min; Reduce rotating speed to 800rpm, add 0.4 part flow agent (AcrysolTMRM-2020, Rohm and Haas Company), stir 20min; The silane coupling agent (KH-560, Jiangsu Chenguang Coincident Dose Co., Ltd.) that adds 2 parts stirs 10min; Add 8 parts of temperature-sensitive mill bases (
Marker 80; Matsui Shikiso Chemical Co., Ltd.), stir 15min; Reduce rotating speed to 500rpm, froth breaking 20min.
Embodiment 4:
In paint mixing tank, add transparent polyurethane resin (
XP 2593/1 that adds 70 parts successively; Bayer AG) and 25 parts of ATO slurries (Luoyang boat Material Insitute), under 600rpm, stir 5min; Slowly improve rotating speed to 1200rpm, add 6 parts ethylene glycol monobutyl ether gradually, stir 8min; Skimmer (
0670 that adds 0.4 part successively; OMG Borchers GmbH) and 0.3 part base material wetting agent (
Wet-270; Evonik Tego Chemie GmbH); Improve rotating speed to 1200rpm, stir 20min; Reduce rotating speed to 800rpm, add 0.4 part flow agent (AcrysolTMRM-2020, Rohm and Haas Company), stir 20min; The silane coupling agent (KH-560, Jiangsu Chenguang Coincident Dose Co., Ltd.) that adds 2 parts stirs 10min; Add 10 parts of temperature-sensitive mill bases (
Marker 80; Matsui Shikiso Chemical Co., Ltd.), stir 15min; Reduce rotating speed to 500rpm, froth breaking 20min.
With the coating of preparation in the foregoing description 1～4, on the common white glass of 6mm, to film, thickness is 15 μ m, performance is seen table 1 and table 2.
Table 1: optical property (sheltering coefficient/visible transmission ratio)
Annotate: the 6mm white glass of 0 in the table 1 for filming.
Table 2: physicals
The above is merely preferred embodiment of the present invention, not in order to restriction the present invention, all any modifications of within spirit of the present invention and principle, being done, is equal to and replaces and improvement etc., all should be included within protection scope of the present invention.
Claims (7)
1. the heat insulation and variable glass heat-insulating coating of light transmission is characterized in that, comprises following component (according to ratio of weight and number):
Transparent resin: 50～80 parts
Solubility promoter: 0～15 part
Nano heat-insulating slurry: 10～50 parts
Skimmer: 0～0.5 part
Base material wetting agent: 0～0.5 part
Flow agent: 0～0.5 part
Toughner: 0～3.0 part
Temperature-sensitive mill base: 0～10.0 part.
2. heat insulation according to claim 1 and the variable glass heat-insulating coating of light transmission is characterized in that described transparent resin can be various transparent resins such as transparent silicon resinoid, transparent polyurethane resin, transparent fluorocarbon resin, transparent Synolac.
3. heat insulation according to claim 1 and the variable glass heat-insulating coating of light transmission; It is characterized in that said nano heat-insulating slurry is: a kind of in nano antimony tin oxide slurry, nano-indium stannum oxide slurry, nano indium oxide slurry, nano-stannic oxide slurry, the nano-aluminium oxide slurry or or several kinds mixture.
4. heat insulation according to claim 1 and the variable glass heat-insulating coating of light transmission is characterized in that said solubility promoter is ethylene glycol monobutyl ether, diethylene glycol monobutyl ether, Ucar 35 butyl ether, dipropylene glycol butyl ether, propylene glycol monomethyl ether or dipropylene glycol methyl ether.
5. heat insulation according to claim 1 and the variable glass heat-insulating coating of light transmission is characterized in that said toughner is organo silane coupling agent, Witcizer 300 or DOP.
6. heat insulation according to claim 1 and the variable glass heat-insulating coating of light transmission is characterized in that said temperature-sensitive mill base is: organic type of material or inorganic matter a kind of, or the mixture of several kinds of organic type of materials or several kinds of inorganic matters; Or several kinds of mixtures that several types of materials and inorganic matter are arranged.
7. the ME of the variable glass heat-insulating coating of heat insulation and light transmission is characterized in that,
The weighting profit requires each component of 1 said ratio of weight and number, according to following steps:
A, in paint mixing tank, add and add transparent resin and nano heat-insulating slurry successively, under 500～800rpm, stir 5～10min;
B, rotating speed transfer to 1000～1200rpm, add solubility promoter, stir 5～10min;
C, add skimmer and base material wetting agent successively, rotating speed transfers to 1200～1500rpm, stirs 10～20min;
D, rotating speed transfer to 800～1000rpm, add flow agent, stir 10～20min;
E, rotating speed transfer to 500～800rpm, add toughner, stir 10～15min;
F, adding temperature-sensitive mill base stir 5～10min;
G, rotating speed transfer to 400～600rpm, and stirring 10～20min carries out froth breaking and obtains the said heat insulation and variable glass heat-insulating coating of light transmission.
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| CN2010105618619A CN102477253A (en) | 2010-11-26 | 2010-11-26 | Glass heat insulation paint with variable heat insulation and light transmittance performances and preparation process thereof |
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| CN102732108A (en) * | 2012-07-16 | 2012-10-17 | 惠州市彩田化工实业有限公司 | Aqueous self-cleaning transparent heat-insulated nano-dope capable of fully shielding infrared ray and ultraviolet ray |
| CN102775073A (en) * | 2012-07-09 | 2012-11-14 | 华尔润玻璃产业股份有限公司 | Process for producing heat-insulated glass by roller coating method |
| CN103387762A (en) * | 2013-08-13 | 2013-11-13 | 武汉羿阳科技有限公司 | Solvent type transparent nanometer thermal insulation sizing agent and application method thereof |
| CN103642322A (en) * | 2013-12-26 | 2014-03-19 | 深圳市嘉达高科产业发展有限公司 | High infrared reflectance ratio aqueous building coating color paste and preparation method thereof |
| CN104098981A (en) * | 2013-04-12 | 2014-10-15 | 南京工业大学 | Preparation method of photochromic heat-insulation functional coating |
| CN105860690A (en) * | 2016-05-06 | 2016-08-17 | 安徽和润特种玻璃有限公司 | Wear-resistant heat-resistant high-transparency anti-dazzle glass coating |
| CN106590076A (en) * | 2016-12-15 | 2017-04-26 | 深圳大学 | Graphene modified inorganic paint and preparation method thereof |
| CN106752213A (en) * | 2016-12-29 | 2017-05-31 | 苏州远略知识产权运营有限公司 | A kind of preparation method of transparent heat insulating dope |
| CN106800876A (en) * | 2016-12-29 | 2017-06-06 | 苏州远略知识产权运营有限公司 | A kind of transparent heat insulating dope |
| CN106883692A (en) * | 2017-03-23 | 2017-06-23 | 东莞市蓝琼实业投资有限公司 | Vehicle glass thermal insulation protection spray and its production technology |
| CN109111846A (en) * | 2018-07-04 | 2019-01-01 | 山东汇龙色釉新材料科技有限公司 | A kind of nano transparent glass thermal insulation paint and its preparation process |
| CN109825141A (en) * | 2019-02-26 | 2019-05-31 | 成都其其小数科技有限公司 | A kind of transparent heat insulation diaphragm and preparation method for glass of building |
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| CN102775073A (en) * | 2012-07-09 | 2012-11-14 | 华尔润玻璃产业股份有限公司 | Process for producing heat-insulated glass by roller coating method |
| CN102732108B (en) * | 2012-07-16 | 2015-04-08 | 惠州市彩田化工实业有限公司 | Aqueous self-cleaning transparent heat-insulated nano-dope capable of fully shielding infrared ray and ultraviolet ray |
| CN102732108A (en) * | 2012-07-16 | 2012-10-17 | 惠州市彩田化工实业有限公司 | Aqueous self-cleaning transparent heat-insulated nano-dope capable of fully shielding infrared ray and ultraviolet ray |
| CN104098981A (en) * | 2013-04-12 | 2014-10-15 | 南京工业大学 | Preparation method of photochromic heat-insulation functional coating |
| CN103387762A (en) * | 2013-08-13 | 2013-11-13 | 武汉羿阳科技有限公司 | Solvent type transparent nanometer thermal insulation sizing agent and application method thereof |
| CN103642322B (en) * | 2013-12-26 | 2015-06-24 | 深圳市嘉达高科产业发展有限公司 | High infrared reflectance ratio aqueous building coating color paste and preparation method thereof |
| CN103642322A (en) * | 2013-12-26 | 2014-03-19 | 深圳市嘉达高科产业发展有限公司 | High infrared reflectance ratio aqueous building coating color paste and preparation method thereof |
| CN105860690A (en) * | 2016-05-06 | 2016-08-17 | 安徽和润特种玻璃有限公司 | Wear-resistant heat-resistant high-transparency anti-dazzle glass coating |
| CN106590076A (en) * | 2016-12-15 | 2017-04-26 | 深圳大学 | Graphene modified inorganic paint and preparation method thereof |
| WO2018108015A1 (en) * | 2016-12-15 | 2018-06-21 | 深圳大学 | Graphene modified inorganic coating and preparation method therefor |
| CN106752213A (en) * | 2016-12-29 | 2017-05-31 | 苏州远略知识产权运营有限公司 | A kind of preparation method of transparent heat insulating dope |
| CN106800876A (en) * | 2016-12-29 | 2017-06-06 | 苏州远略知识产权运营有限公司 | A kind of transparent heat insulating dope |
| CN106883692A (en) * | 2017-03-23 | 2017-06-23 | 东莞市蓝琼实业投资有限公司 | Vehicle glass thermal insulation protection spray and its production technology |
| CN109111846A (en) * | 2018-07-04 | 2019-01-01 | 山东汇龙色釉新材料科技有限公司 | A kind of nano transparent glass thermal insulation paint and its preparation process |
| CN109825141A (en) * | 2019-02-26 | 2019-05-31 | 成都其其小数科技有限公司 | A kind of transparent heat insulation diaphragm and preparation method for glass of building |
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Application publication date: 20120530 |