CN106748239A - A kind of Combination nova medicine fertilizer for preventing and treating potato insect - Google Patents

A kind of Combination nova medicine fertilizer for preventing and treating potato insect Download PDF

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Publication number
CN106748239A
CN106748239A CN201611268274.4A CN201611268274A CN106748239A CN 106748239 A CN106748239 A CN 106748239A CN 201611268274 A CN201611268274 A CN 201611268274A CN 106748239 A CN106748239 A CN 106748239A
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fertilizer
combination
medicine
preventing
insect
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吕昆明
廖华
周伟东
陆明光
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GUANGXI LETU BIOLOGICAL TECHNOLOGY Co Ltd
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GUANGXI LETU BIOLOGICAL TECHNOLOGY Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/40Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N51/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants

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  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of Combination nova medicine fertilizer for preventing and treating potato insect, including Pesticidal combination, fertilizer and medicine fertilizer auxiliary agent, the Pesticidal combination is the two-spot compounding carried out as active ingredient with imidazo-triazine and thiacloprid, and the imidazo-triazine is (1: 20) (10: 1) with the weight ratio of thiacloprid.The invention also discloses the preparation method that the medicine fertilizer is prepared into granule, water solube powder and liquid preparation, raw material is simple, steady quality, and without the resistance to the action of a drug, after application, the double effects for having desinsection to apply fertilizer reach saving of work and time labour-saving effect to gained medicine fertilizer.

Description

A kind of Combination nova medicine fertilizer for preventing and treating potato insect
Technical field
The present invention relates to pesticide new product field, more particularly to a kind of Combination nova medicine fertilizer for preventing and treating potato insect should New product is a kind of agricultural production medicine fertilizer containing insecticide and Fertilizer nutrient simultaneously.
Background technology
Potato, it is high 15-80 centimetres, without hair or by thin pubescence.Stem point aerial stem of plant and subterranean stem two parts.During potato is One of big staple food of state five, it is of high nutritive value, adaptive faculty is strong, yield is big, is the third-largest important cereal crops in the whole world, is only second to Wheat and corn.Potato is stem tuber breeding, can be used as medicine, flat property and sweet taste, can be treated for stomachache, the disease such as Zha ribs, carbuncle swells.As food Thing, its retention cycle is unsuitable oversize, must low temperature, drying, closed preservation.(note:Young shoot has mild toxicity), table on evidence Bright, the Vitamin C content of potato is 4 times or so of apple.
The primary pest of potato is subterranean pest-insect and aphid.Subterranean pest-insect endangers the plant of potato, in ground proximity Place rhizome is bitten broken, whole young plant is died, also can sting food stem tuber in underground, allow white potato shaped into hole, make its susceptible Dye rotten fungus cause to rot.Aphis Homoptera, adult and nymph are at blade, tender stem, young shoot and the tender leaf back side near ground Juice in upper sucking plant body, makes blade turn yellow and crispaturas, and Post flowering is caused harm calyx tube, fruit pin, has a strong impact under peanut blooms Pin and result, moreover it is possible to induce the various virosis of potato.
With China's urbanization, the acceleration of Development of Urbanization, people in the countryside, rural laborer largely shift to city, agriculture Industry production will develop to intensive, scale, efficient direction, the mode of production of resource utilization of raising labour efficiency, improve Increasingly will be paid attention to by people with technical measures.Medicine fertilizer is scientifically one agricultural chemical insecticide and carrier fertilizer organic combination Body, as a kind of multi-functional " medicine fertilizer " product, it has the efficiency of both fertilizer and agricultural chemicals concurrently, and applied once can be completed simultaneously Two or more operations, reach dual or multi-efficiency, realize saving of work and time labour-saving purpose.Scientific progress is sought to multiple Miscellaneous thing is simplified.It is exactly to liberate the productive forces that saving of work and time is laborsaving so that numerous working people liberate from loaded down with trivial details agriculture business Out, go to create more social benefits, meet the reason of " lazyboot's science ", so the generation of medicine fertilizer represents scientific progress, It is the need for modern agriculture with high efficiency develops.
At present, potato medicine fertilizer on the market has various, but remains in many weak points, and medicine fertilizer composition has system Standby complicated, dispensing is complicated, and EDD is short, can reach the purpose of fertilizer, but effect and pays no attention in terms of desinsection, sterilization Think, and desinsection, sterilized and volume increase are difficult to reach effective synergy.
The present invention has filtered out the medicine fertilizer with imidazo-triazine and thiacloprid as insecticide by a large amount of field experiments, right Potato subterranean pest-insect and aphid have good effect, and the desinsection compounded as active ingredient with imidazo-triazine and thiacloprid Agent, at present at home and abroad there is not yet relevant report.
Thiacloprid, it mainly acts on insect nerve engagement caudacoria, is combined by with nAChR, disturbs elder brother Worm nervous system normal conduction, causes the obstruction of neural channel, a large amount of accumulation of acetylcholine is caused, so that insect is extremely emerging Put forth energy, general spasticity, paralysis and it is dead.With stronger interior suction, tag and stomach poison function, with common insecticides such as pyrethroid Class, organic phosphates and carbamates do not have cross resistance, thus can be used for resistance management.
The disclosure of background above technology contents is only used for auxiliary and understands inventive concept of the invention and technical scheme, and it is not Necessarily belong in the prior art of present patent application, the applying date of the above in present patent application is being shown without tangible proof In the case of disclosed, above-mentioned background technology should not be taken to evaluate the novelty and creativeness of the application.
The content of the invention
Actual prevention effect can be significantly improved present invention aim at proposition one kind, the usage amount of agricultural chemicals, extension is reduced The Combination nova medicine fertilizer of a kind of preventing and treating potato insect of desinsection duration of efficacy, to solve the agricultural chemicals that above-mentioned prior art is present The technical problem that prevention effect is poor, usage amount is big, the desinsection duration is short.
Therefore, the present invention proposes a kind of Combination nova medicine fertilizer for preventing and treating potato insect, specific technical scheme is as follows:
A kind of Combination nova medicine fertilizer for preventing and treating potato insect, including Pesticidal combination, fertilizer and medicine fertilizer auxiliary agent, the desinsection group Compound is the weight of the two-spot compounding carried out as active ingredient with imidazo-triazine and thiacloprid, the imidazo-triazine and thiacloprid Amount is than being (1: 20)-(10: 1);
The structural formula of the imidazo-triazine is:
The preparation method of the imidazo-triazine is:By imidacloprid, methyl aminoacetate hydrochloride, tri-n-butylamine and 40% Formalin is dissolved in absolute ethyl alcohol, and 75 DEG C are heated to reflux 6h, and the reaction of TLC Monitoring Carbamate Imidacloprids raw material point finishes (TLC conditions For the volume ratio of ethyl acetate and dichloromethane is 1: 3.5), evaporated under reduced pressure solvent adds 55 DEG C of stirred crystallizations of ethyl acetate, will After feed liquid is cooled to 5 DEG C of insulation 1.5h, decompression suction filtration obtains solid product, and decompression drying obtains imidazo-triazine.Further, The Combination nova medicine fertilizer of described preventing and treating potato insect, the weight ratio of the active ingredient imidazo-triazine and thiacloprid for (1: 5)-(2∶1)。
Further, the Combination nova medicine fertilizer of described preventing and treating potato insect, the Pesticidal combination accounts for the desinsection group The percentage by weight of compound gross weight is 0.05%-5.0%.
Further, the Combination nova medicine fertilizer of described preventing and treating potato insect, the fertilizer can be chemical fertilizer, bio-fertilizer, answer The composite fertilizer in Hefei etc., preferably nitrogenous fertilizer, phosphate fertilizer and/or potash fertilizer mixing.
The nitrogenous fertilizer is preferably urea, ammonium chloride and/or ammonium sulfate, the phosphate fertilizer be preferably MAP, Diammonium phosphate (DAP), Calcium magnesium phosphate and/or calcium superphosphate, the potash fertilizer are preferably potassium chloride and/or potassium sulfate.
Further, the Combination nova medicine fertilizer of the preventing and treating potato insect, can be made any one medicine fertilizer preparation, excellent Choosing is prepared into granule, soluble powder and/or liquid preparation, is most preferably preferably prepared to granule.Can also add in the formulation Enter sustained release component, be made sustained release preparation, reach preferably fertilising and insecticidal effect.
Further, the Combination nova fertilizer granules of described preventing and treating potato insect, the medicine fertilizer auxiliary agent be filler, Dispersant and binding agent;Described filler is one or more the combination in kaolin, montmorillonite, diatomite, clay powder; The dispersant be calcium lignosulfonate, three acyl glycosides oil, tristerin, fatty acid methyl ester in one or more Combination;The binding agent is one or more the combination in starch, cyanoacrylate.
The Combination nova medicine fertilizer of described preventing and treating potato insect, including by the raw material of following parts by weight:Containing imidazo three Pesticidal combination 0.5-50 parts, fertilizer 575-925 parts, filler 50-355 parts, dispersant 6-40 parts, binding agent 11-50 parts of piperazine.
The preparation method of the Combination nova fertilizer granules of the preventing and treating potato insect described in more than one, including following step Suddenly:
S1:Raw material is weighed by weight:Pesticidal combination, fertilizer containing imidazo-triazine, filler, dispersant, binding agent;
S2:Imidazo-triazine active compound, thiacloprid, dispersant, binding agent and filler are well mixed, micronizer is added to In, 325 mesh are crushed to, obtain final product insecticide premix powders;
S3:Insecticide premix powders are well mixed with fertilizer multistage, granulated fertilizer is squeezed into by extruder, drying is extremely Moisture 2.0%-5.0%, obtains final product the Combination nova fertilizer granules of preventing and treating potato insect.
The application of the Combination nova medicine fertilizer of above-described preventing and treating potato insect, can be used for Crops in Applying Fertilizer and insect, The killing or preventing and treating of acarid etc., are preferred for potato fertilization and subterranean pest-insect, the preventing and treating and/or elimination of aphid.
The present invention is compared with prior art, main through the great innovation that further investigation has been made on the basis of traditional medicine fertilizer It is embodied in following several respects:
(1) mechanism of action according to insecticide is different, and selection imidazo-triazine carries out compatibility with thiacloprid;Two kinds of insecticides Active high, insecticidal spectrum and site of action are different, and insecticidal spectrum can be expanded after using with, insecticidal activity is improved, and work as imidazo-triazine When proportioning with thiacloprid is (1: 5)-(2: 1), the co-toxicity to subterranean pest-insect and aphid brings up to more than 150%, manifests Go out significant synergistic effect, when special weight ratio is 1: 1, the co-toxicity to subterranean pest-insect and aphid brings up to 170.59%, Synergistic effect is the most notable.
(2) present invention realizes imidazo-triazine and thiacloprid and the combination of sciences of fertilizer carrier first, successfully develops A kind of brand-new Multifunctional pesticide fertilizer, Fertilizer nutrient composition can guarantee that whole demands of the crops to nutrient, and insecticidal constituent can prevent Or the insects such as subterranean pest-insect, aphid are killed, and mitigate loss of the insect pest to crops, it is particularly suitable with preferable effect of increasing production In potato.
(3) medicine fertilizer of the invention can improve insecticide efficiency, reduce fertilising and number of times of spraying insecticide, and improve fertilizer and agricultural chemicals Utilization rate, while reducing fertilising and pest control cost, it is also possible to reduce the pollution of agricultural chemicals, fertilizer to environment.
(4) present invention for potato fertilization and subterranean pest-insect, the preventing and treating and/or elimination of aphid, application effect is good.
Specific embodiment
The present invention is described in further detail with reference to specific embodiment.It is emphasized that the description below is only Only it is exemplary, rather than in order to limit the scope of the present invention and its application.
First, the preparation method of imidazo-triazine of the present invention
Preparation method:By imidacloprid 100g, methyl aminoacetate hydrochloride 58.9g, tri-n-butylamine 87.8g and 40% formaldehyde Aqueous solution 64.6g is dissolved in 1L absolute ethyl alcohols, and 75 DEG C are heated to reflux 6h, and the reaction of TLC Monitoring Carbamate Imidacloprids raw material point is finished, depressurized Solvent evaporated, adds 800ml 50 DEG C of stirred crystallization 1.5h of ethyl acetate, and after feed liquid is cooled into 5 DEG C of insulation 1.5h, depressurize suction filtration Solid product is obtained, decompression drying obtains imidazo-triazine, yield 92.3%.(TLC conditions are ethyl acetate and dichloromethane Volume ratio is 1: 3.5)
2nd, preparation and application
1. the present invention a kind of preparation and application of the Combination nova fertilizer granules for preventing and treating potato insect
Embodiment 1
A kind of preparation method of the Combination nova fertilizer granules for preventing and treating potato insect, comprises the following steps:
S1:Raw material is weighed by following weight:Pesticidal combination 0.5kg (imidazos three containing imidazo-triazine Yu thiacloprid Piperazine is 1 with the weight ratio of thiacloprid: 20), fertilizer 575kg (nitrogenous fertilizer urea 150kg, ammonium chloride 200kg, phosphate fertilizer MAP 50kg, Diammonium phosphate (DAP) 50kg, potash fertilizer potassium chloride 100kg, potassium sulfate 25kg), filler is kaolin 355kg, dispersant lignin Sulfoacid calcium 40kg, adhesive starch 29.5kg;
S2:Pesticidal combination of the imidazo-triazine with thiacloprid, dispersant, binding agent and filler will be contained to be well mixed, plus To in micronizer, crush, cross 325 mesh sieves, obtain insecticide premix powders;
S3:Insecticide premix powders are well mixed with fertilizer multistage, granulated fertilizer is squeezed into by extruder, drying is extremely Moisture 2.0%, obtains final product.
Field information:
Test group:Every mu of 50kg, when being sowed for potato, ditch spread 1 time are pressed using the fertilizer granules of embodiment 1.
Control group:Applied fertilizer using the fertilizer prepared in embodiment 1, granula dispenser dispersibled using 10% thiacloprid purchased in market, According to the fertilizer and Pesticidal combination ratio of fertilizer granules described in test group, when potato is sowed, while applying fertilizer and applying Medicine is each once.
Result of the test shows:The prevention effect of 45d is at least higher by 27.68% compared with control group after test group medicine.Spread fertilizer over the fields 1 The fertilizer granules of the secondary embodiment of the present invention 1 are that can reach good effect, effectively eliminate or prevent and treat the Ma Ling such as subterranean pest-insect, aphid Potato pest and disease damage.Control group is according to the fertilizer ratio of fertilizer granules described in test group come to potato fertilization, test group Ma Ling Potato yield is higher than control group 20.53%, shows notable sexual clorminance of the invention.
Embodiment 2
A kind of preparation method of the Combination nova fertilizer granules for preventing and treating potato insect, comprises the following steps:
S1:Raw material is weighed by following weight:Composition 1kg containing imidazo-triazine Yu thiacloprid, imidazo-triazine and thiophene The weight ratio of worm quinoline is 1: 10, fertilizer 800kg (nitrogenous fertilizer urea 200kg, ammonium sulfate 300kg, phosphate fertilizer calcium magnesium phosphate 50kg, phosphoric acid One ammonium 100kg, potash fertilizer potassium chloride 150kg), filler is montmorillonite 120kg, dispersant fatty acid methyl ester 40kg, binding agent cyano group Acrylate 39kg;
S2:Composition of the imidazo-triazine with thiacloprid, dispersant, binding agent and filler will be contained to be well mixed, be added to super In atomizer, crush, cross 325 mesh sieves, obtain final product insecticide premix powders;
S3:Insecticide premix powders are well mixed with fertilizer multistage, granulated fertilizer is squeezed into by extruder, drying is extremely Moisture 5.0%, obtains final product.
Field information:
Test group:Every mu of 25kg, when being sowed for potato, ditch spread 1 time are pressed using the fertilizer granules of embodiment 2.
Control group:Applied fertilizer using the fertilizer prepared in embodiment 2, granula dispenser dispersibled using 10% thiacloprid purchased in market, According to the fertilizer and Pesticidal combination ratio of fertilizer granules described in test group, when potato is sowed, while applying fertilizer and applying Medicine is each once.
Result of the test shows:The prevention effect of 45d is at least higher by 30.35% compared with control group after test group medicine.Spread fertilizer over the fields 1 The fertilizer granules of the secondary embodiment of the present invention 2 are that can reach good effect, effectively eliminate or prevent and treat the Ma Ling such as subterranean pest-insect, aphid Potato pest and disease damage.Control group is according to the fertilizer ratio of fertilizer granules described in test group come to potato fertilization, test group Ma Ling Potato yield shows notable sexual clorminance of the invention higher than control 18.24%.
Embodiment 3
A kind of preparation method of the Combination nova fertilizer granules for preventing and treating potato insect, comprises the following steps:
S1:Raw material is weighed by following weight:Composition 8kg containing imidazo-triazine Yu thiacloprid, imidazo-triazine and thiophene The weight ratio of worm quinoline is 1: 5, fertilizer 925kg (nitrogenous fertilizer urea 250kg, ammonium chloride 300kg, phosphate fertilizer MAP 75kg, di(2-ethylhexyl)phosphate Ammonium 100kg, potash fertilizer potassium sulfate 200kg), filler diatomite 50kg, dispersant calcium lignosulfonate and the compatibility of three acyl glycosides oil 1: 2 6kg, adhesive starch and the compatibility 11kg of cyanoacrylate 2: 1;
S2:Composition of the imidazo-triazine with thiacloprid, dispersant, binding agent and filler will be contained to be well mixed, be added to super In atomizer, crush, cross 325 mesh sieves, obtain final product insecticide premix powders;
S3:Insecticide premix powders are well mixed with fertilizer multistage, granulated fertilizer is squeezed into by extruder, drying is extremely Moisture 3.0%, obtains final product.
Field information:
Test group:Every mu of 3.5kg, when being sowed for potato, ditch spread 1 time are pressed using the fertilizer granules of embodiment 3.
Control group:Applied fertilizer using the fertilizer prepared in embodiment 3, granula dispenser dispersibled using 10% thiacloprid purchased in market, According to the fertilizer and Pesticidal combination ratio of fertilizer granules described in test group, when potato is sowed, while applying fertilizer and applying Medicine is each once.
Result of the test shows:The prevention effect of 45d is at least higher by 32.51% compared with control group after test group medicine.Spread fertilizer over the fields 1 The fertilizer granules of the secondary embodiment of the present invention 3 are that can reach good effect, effectively eliminate or prevent and treat the Ma Ling such as subterranean pest-insect, aphid Potato pest and disease damage.Control group is according to the fertilizer ratio of fertilizer granules described in test group come to potato fertilization, test group Ma Ling Potato yield shows notable sexual clorminance of the invention higher than control 16.42%.
Embodiment 4
A kind of preparation method of the Combination nova fertilizer granules for preventing and treating potato insect, comprises the following steps:
S1:Raw material is weighed by following weight:Composition 6kg containing imidazo-triazine Yu thiacloprid, imidazo-triazine and thiophene The weight ratio of worm quinoline is 10: 1, fertilizer 800kg (nitrogenous fertilizer urea 200kg, ammonium chloride 300kg, phosphate fertilizer MAP 75kg, phosphoric acid Two ammonium 50kg, calcium superphosphate 25kg, potash fertilizer potassium sulfate 50kg, potassium chloride 100kg), filler is kaolin and the compatibility of diatomite 1: 1 126kg, dispersant tristerin fat and the compatibility 25kg of fatty acid methyl esters 1: 1, are bonded as agent starch and cyanoacrylate 1: 1 Compatibility 43kg;
S2:Composition of the imidazo-triazine with thiacloprid, stabilizer, binding agent and filler will be contained to be well mixed, be added to super In atomizer, crush, cross 325 mesh sieves, obtain final product insecticide premix powders;
S3:Insecticide premix powders are well mixed with fertilizer multistage, granulated fertilizer is squeezed into by extruder, drying is extremely Moisture 2.8%, obtains final product.
Field information:
Test group:Every mu of 4kg, when being sowed for potato, ditch spread 1 time are pressed using the fertilizer granules of embodiment 4.
Control group:Applied fertilizer using the fertilizer prepared in embodiment 4, granula dispenser dispersibled using 10% thiacloprid purchased in market, According to the fertilizer and Pesticidal combination ratio of fertilizer granules described in test group, when potato is sowed, while applying fertilizer and applying Medicine is each once.
Result of the test shows:The prevention effect of 45d is at least higher by 27.31% compared with control group after test group medicine.Spread fertilizer over the fields 1 The fertilizer granules of the secondary embodiment of the present invention 4 are that can reach good effect, effectively eliminate or prevent and treat the Ma Ling such as subterranean pest-insect, aphid Potato pest and disease damage.Control group is according to the fertilizer ratio of fertilizer granules described in test group come to potato fertilization, test group Ma Ling Potato yield shows notable sexual clorminance of the invention higher than control 12.45%.
2. the preparation and application of the Combination nova medicine fertilizer soluble powder of present invention preventing and treating potato insect
Embodiment 5
A kind of preparation method of the Combination nova medicine fertilizer soluble powder for preventing and treating potato insect, comprises the following steps:
S1:Raw material is weighed by following weight:Composition 50kg containing imidazo-triazine Yu thiacloprid, imidazo-triazine and thiophene The weight ratio of worm quinoline is 2: 1, fertilizer 800kg (nitrogenous fertilizer urea 200kg, ammonium chloride 300kg, phosphate fertilizer MAP 75kg, di(2-ethylhexyl)phosphate Ammonium 50kg, calcium superphosphate 25kg, potash fertilizer potassium sulfate 50kg, potassium chloride 100kg), filler amino acid is matched somebody with somebody with fulvo acid 1: 1 5 125kg, dispersant tristerin 15kg, stabilizer liquid calcium zinc 10kg;
S2:Composition of the imidazo-triazine with thiacloprid, dispersant, stabilizer and filler will be contained to be well mixed, be added to super In atomizer, crush, cross 325 mesh sieves, obtain final product insecticide premix powders;
S3:Insecticide premix powders are well mixed with water soluble fertilizer, filler, are dried to moisture 2.0%, obtained final product.
Field information:
Test group:Every mu of 500g is pressed using the medicine of embodiment 5 fertilizer soluble powder, when being sowed for potato, pesticide-clay mixture method is spread Apply 1 time.
Control group:Applied fertilizer using the fertilizer prepared in embodiment 5, granula dispenser dispersibled using 10% thiacloprid purchased in market, According to the fertilizer and Pesticidal combination ratio of the fertilizer soluble powder of medicine described in test group, when potato is sowed, while fertilising And dispenser is each once.
Result of the test shows:The prevention effect of 45d is at least higher by 44.13% compared with control group after test group medicine.Spread fertilizer over the fields 1 The medicine of the secondary embodiment of the present invention 5 fertilizer soluble powder is that can reach good effect, effectively eliminates or prevent and treat subterranean pest-insect, aphid etc. Potato disease insect pest.Control group is according to the fertilizer ratio of the fertilizer soluble powder of medicine described in test group come to potato fertilization, examination Group potato yield is tested higher than control 13.05%, notable sexual clorminance of the invention is shown.
3. the preparation and application of the Combination nova medical fertilizer liquid body preparation of present invention preventing and treating potato insect
Embodiment 6
A kind of preparation method of the Combination nova medical fertilizer liquid body preparation for preventing and treating potato insect, comprises the following steps:
S1:Raw material is weighed by following weight:Composition 30kg containing imidazo-triazine Yu thiacloprid, imidazo-triazine and thiophene The weight ratio of worm quinoline is 1: 1, fertilizer 850kg (nitrogenous fertilizer urea 200kg, ammonium sulfate 400kg, phosphoric acid diamines 150kg, potassium sulfate 100kg), filler water-soluble amino acids and fulvo acid 1: 2 compatibility 100kg, dispersant tristerin 20kg, stabilization Agent liquid calcium zinc 50kg;
S2:Composition of the imidazo-triazine with thiacloprid, stabilizer, dispersant and filler will be contained to be well mixed, sand is added to In grinding machine, below clipped frosted to 5 microns of material particular diameter, pH is controlled 6.5, obtains final product certain density insecticide premixed liquid;
S3:Insecticide premixed liquid is mixed with fertilizer, clipped machine shearing is uniform, obtains final product.
Field information:
Test group:Every mu of 800g is pressed using the medical fertilizer liquid body preparation of embodiment 6, after seedling is played for potato, sprayed 1 time.
Control group:Applied fertilizer using the fertilizer prepared in embodiment 6, granula dispenser dispersibled using 10% thiacloprid purchased in market, According to the fertilizer and Pesticidal combination ratio of medical fertilizer liquid body preparation described in test group, the after seedling in potato, while fertilising and Dispenser is each once.
Result of the test shows:The prevention effect of 45d is at least higher by 46.28% compared with control group after test group medicine.Spraying 1 The medical fertilizer liquid body preparation of the secondary embodiment of the present invention 6 is that can reach good effect, effectively eliminates or prevent and treat the horses such as subterranean pest-insect, aphid Bell potato pest and disease damage.Control group is according to the fertilizer ratio of medical fertilizer liquid body preparation described in test group come to potato fertilization, test group Potato yield shows notable sexual clorminance of the invention higher than control 10.32%.
Above content is to combine specific/preferred embodiment further description made for the present invention, it is impossible to Assert that specific implementation of the invention is confined to these explanations.Come for general technical staff of the technical field of the invention Say, without departing from the inventive concept of the premise, its embodiment that can also have been described to these makes some replacements or modification, And these are substituted or variant should all be considered as belonging to protection scope of the present invention.

Claims (10)

1. a kind of Combination nova medicine fertilizer for preventing and treating potato insect, including Pesticidal combination, fertilizer and medicine fertilizer auxiliary agent, its feature exists In:The Pesticidal combination is the two-spot compounding carried out as active ingredient with imidazo-triazine and thiacloprid, the imidazo-triazine It is (1: 20)-(10: 1) with the weight ratio of thiacloprid;
The structural formula of the imidazo-triazine is:
2. the Combination nova medicine of preventing and treating potato insect as claimed in claim 1 is fertile, it is characterised in that:The active ingredient imidazoles And triazine and the weight ratio of thiacloprid are (1: 5)-(2: 1).
3. the Combination nova medicine of preventing and treating potato insect as claimed in claim 1 is fertile, it is characterised in that:The Pesticidal combination is accounted for The percentage by weight of the Pesticidal combination gross weight is 0.05%-5.0%.
4. the Combination nova medicine of the preventing and treating potato insect as any one of claim 1-3 is fertile, it is characterised in that:The fertilizer Expect to be nitrogenous fertilizer, phosphate fertilizer and/or potash fertilizer.
5. the Combination nova medicine fertilizer of potato insect is prevented and treated as any one of claim 1-4, it is characterised in that:The nitrogenous fertilizer It is urea, ammonium chloride and/or ammonium sulfate, the phosphate fertilizer is MAP, Diammonium phosphate (DAP), calcium magnesium phosphate and/or calcium superphosphate, institute Potash fertilizer is stated for potassium chloride and/or potassium sulfate.
6. the Combination nova medicine fertilizer of potato insect is prevented and treated as any one of claim 1-5, it is characterised in that:The medicine fertilizer It is prepared into granule, soluble powder and/or liquid preparation.
7. it is a kind of it is as claimed in claim 6 preventing and treating potato insect Combination nova fertilizer granules, it is characterised in that the medicine Fertile auxiliary agent is filler, dispersant and binding agent;
Described filler is one or more the combination in kaolin, montmorillonite, diatomite, clay powder;
The dispersant be calcium lignosulfonate, three acyl glycosides oil, tristerin, fatty acid methyl ester in one or two Combination above;
The binding agent is one or more the combination in starch, cyanoacrylate.
8. the Combination nova medicine of preventing and treating potato insect is fertile as claimed in claim 7, it is characterised in that including by following parts by weight Raw material:Pesticidal combination 0.5-50 parts containing imidazo-triazine, fertilizer 575-925 parts, filler 50-355 parts, dispersant 6-40 Part, binding agent 11-50 parts.
9. a kind of preparation method of the Combination nova fertilizer granules of preventing and treating potato insect as claimed in claim 8, its feature exists In comprising the following steps:
S1:Raw material is weighed by weight:Pesticidal combination, fertilizer containing imidazo-triazine, filler, dispersant, binding agent;
S2:Imidazo-triazine active compound, thiacloprid, dispersant, binding agent and filler are well mixed, are added in micronizer, 325 mesh are crushed to, insecticide premix powders are obtained final product;
S3:Insecticide premix powders are well mixed with fertilizer multistage, granulated fertilizer, drying to moisture are squeezed into by extruder 2.0%-5.0%, obtains final product the Combination nova fertilizer granules of preventing and treating potato insect.
10. a kind of application of the Combination nova medicine fertilizer of preventing and treating potato insect as claimed in any one of claims 1-9 wherein, its feature It is:For potato fertilization and subterranean pest-insect, aphid preventing and treating and/or elimination.
CN201611268274.4A 2016-12-31 2016-12-31 A kind of Combination nova medicine fertilizer for preventing and treating potato insect Pending CN106748239A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108046927A (en) * 2017-12-30 2018-05-18 黑龙江省苗必壮农业科技有限公司 A kind of combination medicine fertilizer for preventing potato blight and preparation method

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1041354A (en) * 1988-09-18 1990-04-18 张约伯 Multi-effect fertilizer for killing insects and resisting withering

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1041354A (en) * 1988-09-18 1990-04-18 张约伯 Multi-effect fertilizer for killing insects and resisting withering

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108046927A (en) * 2017-12-30 2018-05-18 黑龙江省苗必壮农业科技有限公司 A kind of combination medicine fertilizer for preventing potato blight and preparation method

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Application publication date: 20170531