CN106726959A

CN106726959A - A kind of gentle inirritative perfume

Info

Publication number: CN106726959A
Application number: CN201611210620.3A
Authority: CN
Inventors: 晏金; 陈国祥
Original assignee: Hangzhou Sincere Cosmetics Co Ltd
Current assignee: Hangzhou Sincere Cosmetics Co Ltd
Priority date: 2016-12-24
Filing date: 2016-12-24
Publication date: 2017-05-31
Anticipated expiration: 2036-12-24
Also published as: CN106726959B

Abstract

The invention discloses a kind of gentle inirritative perfume, including following parts by weight component：35 parts of deionized water；13 parts of glycerine；8 12 parts of perfume mixture；80 90 parts of ethanol；The perfume mixture includes the first extract and the second extract, first extract includes Flos Rosae Rugosae extract, safranine flower extract, second extract is rhizoma cyperi daughter root extract or rhizome of nutgrass flatsedge berry extract, and rose extract, safranine flower extract, the parts by weight ratio of the second extract are 1:1‑1.5:1.1‑1.3.The present invention has the advantages that gently do not stimulate, do not easily cause human allergy, and fragrance of the invention more gives out persistently and with more having levels sense, so that multiple fragrance interweaves, the women for being particularly suited for workplace is used, and can fully show the graceful, hot, deep of women.

Description

A kind of gentle inirritative perfume

Technical field

The present invention relates to Cosmetic Manufacture technical field, more specifically, it relates to a kind of gentle inirritative perfume.

Background technology

Perfume is a kind of liquid for being mixed with fragrant extract, fixative and ethanol or ethyl acetate, with spices, ethanol and steaming The cosmetics that distilled water etc. is made, can distribute the fragrance of strong, lasting, happy people, can increase the aesthetic feeling and attraction of user. With the improvement of living standards with the transformation of consumption idea, perfume becomes people's daily life, work from a kind of luxury goods An indispensable part in work, study, leisure, amusement；The fragrance of the happy people of perfume adds the color of life, improves people Grade, give gracefulness, fashion, honorable speciality, increasingly pursued and liked by consumers in general.

Contain more stimulating component in existing perfume, easily cause human allergy's phenomenon, the normal of user is used Have undesirable effect, so that these limitations cause the limited of perfume purposes, it is impossible to meet the growing consumption demand of people.

The content of the invention

In view of the shortcomings of the prior art, it is an object of the invention to provide a kind of gentle inirritative perfume, its solution Determine in perfume containing more stimulating component, easily caused human allergy's phenomenon, to the normal using causing bad shadow of user Loud problem, has the advantages that not stimulate gently, does not easily cause human allergy.

To achieve the above object, the invention provides following technical scheme：

A kind of gentle inirritative perfume, including following parts by weight component：

Deionized water 3-5 parts；

Glycerine 1-3 parts；

Perfume mixture 8-12 parts；

Ethanol 80-90 parts；

The perfume mixture include the first extract and the second extract, first extract include Flos Rosae Rugosae extract, Safranine flower extract, second extract is rhizoma cyperi daughter root extract or rhizome of nutgrass flatsedge berry extract, the rose extract, Tibetan Safflower extract, the parts by weight ratio of the second extract are 1:1-1.5:1.1-1.3.

Using above-mentioned technical proposal, perfume mixture includes Flos Rosae Rugosae extract, safranine flower extract, the second extract, And the second extract is rhizoma cyperi daughter root extract or rhizome of nutgrass flatsedge berry extract.Wherein, Flos Rosae Rugosae extract has calm and anti-suppression Yu Zuoyong, can play a part of calm nerves and emotional state, but containing more stimulating component, easily causes human allergy and show As normal use the to user has undesirable effect.Safranine flower extract has pungent smell, and people can be allowed to inhale more quickly Receive, can in time promote the blood oxygen of blood circulation of human body supply, allow user's holding resourceful, mental balance, confident.Its Endocrine pigment can also be adjusted to be precipitated in skin surface, mitigated because endocrinopathy triggers huge work and life stress.Make Effect of its resist oxygen lack of invigorating blood circulation can be to greatest extent played with safranine flower extract, hence it is evident that improve blood microcirculation, made every in vivo One cell is dynamic, makes one to keep optimum mental state constantly.Rhizoma cyperi daughter root extract, rhizome of nutgrass flatsedge berry extract are respectively provided with Antibacterial and antibacterial effect, and with depressed wooden fragrance, and the evaporation rate of rhizoma cyperi seed extract is slower, is held so as to reach Stay for a long time the effect of perfume.

Rose extract, safranine flower extract, the parts by weight ratio of the second extract are 1:1-1.5:1.1-1.3, from And make the perfume of the application after human body skin is applied to, and gradually give out the fragrance for being rich in stereovision successively with body temperature, it is preceding Be adjusted to splendid Rose Essentielle, in be adjusted to the red-hot safranine fragrance of a flower, it be then graceful rhizome of nutgrass flatsedge breath then to adjust so that the fragrance of a flower, The pungent, banksia rose is interweaved together, shows that user's is graceful, hot, deep.

After glycerine is contacted with skin, with the effect for pinning moisture, the moisture being lockable can make fragrance continue to distribute, so that Reach the effect for reducing fragrance volatilizing speed to a certain extent.And it forms diaphragm outside perfume mixture, reduce fragrant , there is the probability of allergic phenomena so as to reduce in the possibility that smart mixture directly acts on skin and causes to stimulate to skin.

Ethanol is a kind of nontoxic and volatile solvent, can fully dissolve and dilute perfume mixture, makes perfume mixture Uniformly it is attached on human body skin；Ethanol is also a kind of carrier volatilizer, and evaporation rate is fast, and range of scatter is small, and dissolving is wherein Perfume mixture reach skin surface after, ethanol quickly volatilizees and departs from perfume mixture, gives full play of the application One's own taste.Additionally, ethanol also has the effect of protection perfume mixture, the oxidation of organic substance is reduced, so as to prolong The shelf-life of the perfume in the application is grown.

Through research（Experiment one）Show, distilled water, ethanol, glycerine are sufficiently mixed each other, and form compound action, have Help reduce stimulation and damage of the perfume mixture to human body skin, the phenomenon of allergy occurs in reduction.Through research（Experiment two）Table Bright, distilled water, ethanol, glycerine form the stability of fragrance volatilizing each other, and improve the quality of fragrance, prevent due to moisture There is the too fast phenomenon of fragrance emissions more in content.

More preferably：The extraction of first extract comprises the following steps：

S1, the petal in the first raw material of the same race and calyx are separated, and by petal through ultrasonic cleansing, are dried, and obtain lustration raw material；

S2, the lustration raw material that will be obtained in step S1 is through supercritical CO₂Extraction, obtains the first extract solution；

S3, the first extract solution that will be obtained in step S2 obtains the first extract through distillation；

First raw material is the firm rose plucked or safflower.

Using above-mentioned technical proposal, the rose or safflower just plucked have the strong fragrance of a flower, and therein effective Fragrance of a flower composition is more；Using petal, the pure degree of Rose Essentielle and the safranine fragrance of a flower is considerably increased.Rose petal or Tibetan Safflower petal is respectively adopted supercritical CO₂The method of extraction is extracted, CO₂It is a kind of inactive gas, typically in extraction process In will not chemically react, extracted component will not go bad because of oxidation.Supercritical CO₂Can will be low in rose or safflower The head Studies of The Aromatic Substances and high boiling body note and bottom note material of boiling point are extracted simultaneously, make the fragrance of the first extract for extracting Closer to rose or the natural flavor of safflower.

More preferably：Drying using air-drying in the step S1, the wind speed of the air drying process is 1-2m/s, institute The temperature for stating air drying process is 25-30 DEG C.

Using above-mentioned technical proposal, soft wind can dry up the moisture of rose or the petal surface of safflower, and 25-30 DEG C of wind is difficult, by the moisture drying inside petal, to be not easy to blow away on the petal of rose or safflower, contributes to Supercritical CO₂Extraction extracts more Flos Rosae Rugosae extract.

More preferably：Supercritical CO in the step S2₂The extraction temperature of extraction is 28-35 DEG C, and extracting pressure is 16-19MPa, extraction time is 1-1.5h, CO₂Flow is 18-20kg/h.

Using above-mentioned technical proposal, contribute to the lower boiling head Studies of The Aromatic Substances and height boiling in rose or safflower petal The body note and bottom note material of point are extracted so that fragrance becomes pure and strong.

More preferably：The absolute pressure distilled in the step S3 is 4-5MPa, and rotating speed is 200-230rpm, flow velocity It is 2.3-2.5mL/min.

Using above-mentioned technical proposal, in supercritical CO₂After extraction, using the method for distillation, make the first extract of acquisition With purity higher, so that the application can give out purer fragrance after use, and make fragrance sustainable more long.

More preferably：The extraction of second extract comprises the following steps：

Step 1, the second qualified raw material is cleaned, is dried, and the raw material of powder second is obtained after size-reduced, 150-200 mesh sieves choosing；

Step 2, the raw material of powder second obtained in step 1 is sufficiently impregnated using the first solvent, obtains leachate；

Step 3, air-distillation is carried out by the leachate obtained in step 2, after being concentrated in vacuo through first time, obtains medicinal extract；

Step 4, the medicinal extract obtained in step 3 is sufficiently impregnated again using the second solvent, vacuum filter, obtains filtrate；

Step 5, the second extract is obtained after filtrate in step 4 is concentrated in vacuo through second；

Second raw material is rhizome of nutgrass flatsedge fruit or rhizome of nutgrass flatsedge root；The first solvent in the step 2 is that concentration is the second of 95-98% Alcohol, the second solvent in the step 4 is that concentration is the ethanol of 92-95%.

Using above-mentioned technical proposal, by the first solvent and the second solvent extraction so that the second extract for obtaining has More sufficient body note and bottom note, ethanol are nontoxic, are difficult to damage human body.Rhizome of nutgrass flatsedge fruit or rhizome of nutgrass flatsedge root can extract out second Extract,, by after the alcohol dipping of 95-98%, the active ingredient of fragrance therein can be lockable, reduce fragrance has for it Scattering and disappearing for effect composition, is favorably improved the content of the active ingredient of fragrance in leachate.And the ethanol of 92-95% is used to medicinal extract Impregnated, the active ingredient of fragrance is more easy to be extracted in medicinal extract, so as to be favorably improved rhizome of nutgrass flatsedge berry extract or rhizoma cyperi The content of daughter root extract, so that the second extract for obtaining is more pure, and reduces the content of wherein impurity.

More preferably：Also include pigment in the perfume, the pigment is CI16035, the weight portion of the pigment Number is 0.1-0.5 parts.

Using above-mentioned technical proposal, pigment can increase the visual effect of perfume in the application, make perfume as represented itself As taste, taste is shown by vision, increase the effect experience of user.

In sum, the invention has the advantages that：

1st, through research（Experiment one）It was found that, perfume mixture is acted on glycerine, ethanol, deionized water mutual cooperation, reduces essence There is the phenomenon of allergy in stimulation and damage of the mixture to human body skin, reduction；

2nd, through research（Experiment two）It was found that, rose extract, safranine flower extract, the parts by weight ratio of the second extract are 1:1-1.5:1.1-1.3, and perfume mixture and glycerine, ethanol, deionized water ratio in prescribed limit, can mix essence The fragrance of compound more gives out persistently and with more having levels sense so that multiple fragrance interweaves, and is particularly suited for the female of workplace Property is used, and can fully show the graceful, hot, deep of women.

Specific embodiment

With reference to embodiment, the present invention will be described in detail.

Embodiment 1：A kind of gentle inirritative perfume, including following parts by weight component：

3 parts of deionized water；

1 part of glycerine；

8 parts of perfume mixture；

90 parts of ethanol；

Wherein, perfume mixture includes that parts by weight ratio is 1:1:1.1 rose extract, safranine flower extract, second carry Take thing.

Rose extract, safranine flower extract extraction process it is identical, as follows extract obtain：

S1, the petal and calyx in the firm rose plucked or safflower are separated, and rose petal or safflower petal are passed through Ultrasonic cleansing, uses wind speed to be air-dried for the wind that 1m/s, temperature are 25 DEG C, obtains lustration raw material；

S2, the lustration raw material that will be obtained in step S1 is through supercritical CO₂Extraction, extraction temperature is 28 DEG C, and extracting pressure is 16MPa, extraction time is 1h, CO₂Flow is 18kg/h, obtains the first extract solution；

S3, through distillation, absolute pressure is 4MPa to the first extract solution that will be obtained in step S2, and rotating speed is 200rpm, and flow velocity is 2.3mL/min, obtains the first extract；

Second extract is rhizoma cyperi daughter root extract, and extraction process comprises the following steps：

Step 1, qualified rhizome of nutgrass flatsedge root is cleaned, is dried, and powder rhizome of nutgrass flatsedge root is obtained after size-reduced, 150-200 mesh sieves choosing；

Step 2, the powder rhizome of nutgrass flatsedge root obtained in step 1 is sufficiently impregnated using the ethanol of 95-98%, obtains leachate；

Step 4, the medicinal extract obtained in step 3 is sufficiently impregnated again using the ethanol of 92-95%, and vacuum filter is filtered Liquid；

Step 5, rhizoma cyperi daughter root extract is obtained after filtrate in step 4 is concentrated in vacuo through second.

Embodiment 2：A kind of gentle inirritative perfume, the difference with embodiment 1 is,

5 parts of deionized water；

3 parts of glycerine；

12 parts of perfume mixture；

80 parts of ethanol；

Perfume mixture includes that parts by weight ratio is 1:1.5:1.1 rose extract, safranine flower extract, the second extraction Thing.In rose extract, the extraction process of safranine flower extract, step S1 uses wind speed to enter for the wind that 2m/s, temperature are 30 DEG C Sector-style is done.Step S2, extraction temperature is 35 DEG C, and extracting pressure is 19MPa, and extraction time is 1.5h, CO₂Flow is 20kg/h. Step S3, absolute pressure is 5MPa, and rotating speed is 230rpm, and flow velocity is 2.5mL/min.

Embodiment 3：A kind of gentle inirritative perfume, the difference with embodiment 1 is,

4 parts of deionized water；

2 parts of glycerine；

10 parts of perfume mixture；

85 parts of ethanol；

Perfume mixture includes that parts by weight ratio is 1:1:1.3 rose extract, safranine flower extract, the second extract. In rose extract, the extraction process of safranine flower extract, step S1 uses wind speed to enter for the wind that 1.5m/s, temperature are 27 DEG C Sector-style is done.Step S2, extraction temperature is 30 DEG C, and extracting pressure is 17MPa, and extraction time is 1.2h, CO₂Flow is 19kg/h. Step S3, absolute pressure is 4.5MPa, and rotating speed is 220rpm, and flow velocity is 2.4mL/min.

Embodiment 4：A kind of gentle inirritative perfume, the difference with embodiment 1 is,

3.5 parts of deionized water；

2.5 parts of glycerine；

11 parts of perfume mixture；

88 parts of ethanol；

Perfume mixture includes that parts by weight ratio is 1:1.5:1.3 rose extract, safranine flower extract, the second extraction Thing.In the extraction process of rhizoma cyperi daughter root extract, step 2 is sufficiently impregnated using 98% ethanol to powder rhizome of nutgrass flatsedge root, Obtain leachate；Step 4, is sufficiently impregnated using 95% ethanol to medicinal extract.

Embodiment 5：A kind of gentle inirritative perfume, the difference with embodiment 1 is, the second extract be the rhizome of nutgrass flatsedge really Extract.

Embodiment 6：A kind of gentle inirritative perfume, the difference with embodiment 1 is, the second extract be the rhizome of nutgrass flatsedge really The mixture of extract and rhizoma cyperi daughter root extract, wherein, the parts by weight of rhizome of nutgrass flatsedge berry extract and rhizoma cyperi daughter root extract Ratio is 1:1,0.1 part of CI16035 pigment is also added wherein.

Embodiment 7：A kind of gentle inirritative perfume, the difference with embodiment 1 is that with the addition of 0.5 part of CI16035 color Element.

Wherein, rhizome of nutgrass flatsedge root or rhizome of nutgrass flatsedge fruit are the India rhizome of nutgrass flatsedge.

Comparative example 1：A kind of perfume, the difference with embodiment 3 is,

1 part of deionized water；

0 part of glycerine；

7 parts of perfume mixture；

85 parts of ethanol；

Perfume mixture includes that parts by weight ratio is 1:0.8:0.5 rose extract, safranine flower extract, the second extraction Thing.

Comparative example 2：A kind of perfume, the difference with comparative example 1 is,

4 parts of deionized water；

0 part of glycerine；

7 parts of perfume mixture；

85 parts of ethanol.

Comparative example 3：A kind of perfume, the difference with comparative example 1 is,

4 parts of deionized water；

2 parts of glycerine；

7 parts of perfume mixture；

85 parts of ethanol；

Perfume mixture includes that parts by weight ratio is 1:1.8:0.5 rose extract, safranine flower extract, the second extraction Thing.

Comparative example 4：A kind of perfume, the difference with comparative example 1 is,

4 parts of deionized water；

2 parts of glycerine；

7 parts of perfume mixture；

55 parts of ethanol；

Perfume mixture includes that parts by weight ratio is 1:0.5:1.8 rose extract, safranine flower extract, the second extraction Thing.

Comparative example 5：A kind of perfume, the difference with embodiment 3 is,

4 parts of deionized water；

2 parts of glycerine；

10 parts of perfume mixture；

55 parts of ethanol.

Test a hypersensitive test

Test specimen：Using the gentle inirritative perfume obtained in embodiment 1-7 as test specimen 1-7, using comparative example The perfume obtained in 1-5 is used as control sample 1-5.

Test method：Choose areal, the age be 25-35 one full year of life, the women white collar subject of sensitiveness skin quality 1200,12 groups are divided into, respectively numbering 1-12.Wherein, 1-7 groups subject uses test specimen 1-7,8-12 respectively Group subject then uses control sample 1-5 respectively.When using, by corresponding sample, equivalent is sprayed at ear to each group subject respectively Afterwards, neck, wrist inner side place, this bears a pretty, delicate skin at three, and is adapted to perfume spraying, and observation each group subject is in perfume (or spice) in 15min Allergic symptom at water smearing.

Result of the test：In first group to the 7th group subject, 100% subject after ear, on the inside of neck, wrist not There is allergic phenomena.

In 8th group of subject, there is allergic phenomena after ear in 80% subject, and 75% subject allergy occurs and shows in neck As allergic phenomena occurs on the inside of wrist in 71% subject.

In 9th group of subject, there is allergic phenomena after ear in 77% subject, and 73% subject allergy occurs and shows in neck As allergic phenomena occurs on the inside of wrist in 70% subject.

In tenth group of subject, there is allergic phenomena after ear in 68% subject, and 61% subject allergy occurs and shows in neck As allergic phenomena occurs on the inside of wrist in 55% subject.

In 11st group of subject, there is allergic phenomena after ear in 65% subject, and 59% subject allergy occurs in neck There is allergic phenomena on the inside of wrist in phenomenon, 58% subject.

In 12nd group of subject, there is allergic phenomena after ear in 61% subject, and 53% subject allergy occurs in neck There is allergic phenomena on the inside of wrist in phenomenon, 52% subject.

The result illustrates that perfume mixture is acted on glycerine, ethanol, deionized water mutual cooperation, gently, and reduces essence There is the phenomenon of allergy in stimulation and damage of the mixture to human body skin, reduction.

Test two subjects experience experiment

Test specimen：Using the gentle inirritative perfume obtained in embodiment 1-3 as test specimen 1-3, using comparative example The perfume obtained in 1-5 is used as control sample 1-5.

Test method：Women white collar subject 800 that choose areal, that the age is 20-45 one full year of life, is divided into 8 groups, respectively numbering 1-8.Wherein, 1-3 groups subject uses test specimen 1-3,4-8 groups subject then to use respectively respectively Control sample 1-5.Corresponding sample after equivalent is applied to ear respectively, is recorded the experience of each group subject by each group subject, then By the olfactory sensations of 12h, the impression of subject is recorded.

Result of the test：In first group to the 3rd group subject, after the corresponding sample smearing of 100% subject perception in 3-5s It is rapid to dry, and the splendid Rose Essentielles of 2-2.5h are persistently distributed, the red-hot safranine fragrance of a flower of 4-5h is persistently distributed afterwards, finally hold It is continuous to distribute the graceful rhizome of nutgrass flatsedge fragrance of 6-7h.

In 4th group of subject, 90% feels that corresponding sample is dried rapidly in 3-5s after smearing, but fragrance occurs more Mixing, wherein, after persistently distributing 0.5h Rose Essentielles, mix Rose Essentielle and the safranine fragrance of a flower together gives out, continue 1- 1.5h, mixes Rose Essentielle, the safranine fragrance of a flower, rhizome of nutgrass flatsedge fragrance and together distributes 1.5-2h afterwards.

In 5th group of subject, 90% feels that corresponding sample is dried rapidly in 3-5s after smearing, but fragrance more mixes, Wherein, after persistently distributing 36min Rose Essentielles, mix Rose Essentielle and the safranine fragrance of a flower together gives out, continue 90- 108min, mixes Rose Essentielle, the safranine fragrance of a flower, rhizome of nutgrass flatsedge fragrance and together distributes 120-150min afterwards.

In 6th group of subject, 90% feels that corresponding sample is dried rapidly in 3-5s after smearing, but fragrance more mixes, Wherein, after persistently distributing 48-66min Rose Essentielles, mix Rose Essentielle and the safranine fragrance of a flower together gives out, continue 95- 115min, mixes Rose Essentielle, the safranine fragrance of a flower, rhizome of nutgrass flatsedge fragrance and together distributes 48-72min afterwards.

In 7th group of subject, 90% feels that corresponding sample is dried in 7-10 after smearing, but fragrance more mixes, wherein, After persistently distributing 48-66min Rose Essentielles, mix Rose Essentielle and the safranine fragrance of a flower together gives out, continue 30-60min, after Mix Rose Essentielle, the safranine fragrance of a flower, rhizome of nutgrass flatsedge fragrance and together distribute 95-115min.

In 8th group of subject, dried in 7-10 after the corresponding sample smearing of 83% subject perception, Rose Essentielle persistently dissipates Hair 1.5-2h, persistently distributes the red-hot safranine fragrance of a flower of 2-2.5h and the graceful rhizome of nutgrass flatsedge fragrance of 3-3.5h successively afterwards.

The result of experiment two shows that rose extract, safranine flower extract, the parts by weight ratio of the second extract are 1: 1-1.5:1.1-1.3, and perfume mixture and glycerine, ethanol, deionized water ratio in prescribed limit, can mix essence The fragrance of thing more gives out persistently and with more having levels sense so that multiple fragrance interweaves, and is particularly suited for the women of workplace Use, can fully show the graceful, hot, deep of women.

The above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-mentioned implementation Example, all technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art Those of ordinary skill for, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications Should be regarded as protection scope of the present invention.

Claims

1. a kind of gentle inirritative perfume, it is characterised in that the component including following parts by weight：

Deionized water 3-5 parts；

Glycerine 1-3 parts；

Perfume mixture 8-12 parts；

Ethanol 80-90 parts；

2. a kind of gentle inirritative perfume according to claim 1, it is characterised in that the extraction of first extract Comprise the following steps：

First raw material is the firm rose plucked or safflower.

3. a kind of gentle inirritative perfume according to claim 2, it is characterised in that the drying in the step S1 is adopted With air-drying, the wind speed of the air drying process is 1-2m/s, and the temperature of the air drying process is 25-30 DEG C.

4. a kind of gentle inirritative perfume according to claim 2, it is characterised in that supercritical CO in the step S2₂ The extraction temperature of extraction is 28-35 DEG C, and extracting pressure is 16-19MPa, and extraction time is 1-1.5h, CO₂Flow is 18-20kg/ h。

5. a kind of gentle inirritative perfume according to claim 2, it is characterised in that is distilled in the step S3 is exhausted It is 4-5MPa to pressure, rotating speed is 200-230rpm, and flow velocity is 2.3-2.5mL/min.

6. a kind of gentle inirritative perfume according to claim 1, it is characterised in that the extraction of second extract Comprise the following steps：

7. a kind of gentle inirritative perfume according to claim 1, it is characterised in that also include color in the perfume Element, the pigment is CI16035, and the parts by weight of the pigment are 0.1-0.5 parts.