CN106726649A - A kind of talcum powder and preparation method thereof - Google Patents
A kind of talcum powder and preparation method thereof Download PDFInfo
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- CN106726649A CN106726649A CN201611210616.7A CN201611210616A CN106726649A CN 106726649 A CN106726649 A CN 106726649A CN 201611210616 A CN201611210616 A CN 201611210616A CN 106726649 A CN106726649 A CN 106726649A
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- Prior art keywords
- talcum powder
- menthol
- anisaldehyde
- eucalyptol
- linalool
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to daily chemical product field, and in particular to a kind of talcum powder and preparation method thereof.The talcum powder that the present invention is provided, including following components and its percentage by weight：Menthol 1 3%, anisaldehyde 0.2 0.6%, eucalyptol 0.1 0.3%, sandalwood oil 0.2 0.6%, linalool 0.1 0.5%, essence 0.1 0.3%, propane diols 1 3%, ethanol 1 2% and corn flour 89.7 96.3%.The talcum powder that the present invention is provided can not only feel well body, miliaria of dispelling, additionally it is possible to mosquito repellent, antibacterial, and gentle non-stimulated.
Description
Technical field
The invention belongs to daily chemical product field, and in particular to a kind of talcum powder and preparation method thereof.
Background technology
The skin of infant is more tender and lovely, and temperature is too high or perspire all easily prickly heat long or eczema, especially in the summer
My god, most of infant all easy prickly heats long, and it is that anti-miliaria is dispelled the effective ways of miliaria to keep the dry and comfortable of skin, therefore, in summer
The use of safely and effectively talcum powder is very necessary to infant.Meanwhile, summer mosquito is various, need of the mothers to talcum powder
Ask except effect is good and does not stimulate, it is safely and effectively outer, it is also desirable to can be with mosquito expelling.
Chinese patent CN1016137B discloses a kind of mosquito-expelling talcum powder, is by the talcum powder with talcum powder as primary raw material
And culicifuge is made；Talcum powder is 92-94.5%, and culicifuge is 8-5.5%.Culicifuge is compound, at least using three
More than kind；Ju Ti Pei Fang is：DETA2.5-5%, DMPP 0-1.5%, menthol 0.5-1.5%, camphor 0.5-2%, dimethyl carbate
No. 67 0-2.5%.The formulation of this mosquito-expelling talcum powder is novel, and significantly, general mosquito repellent time is 6-8 hours to repelling effect, than liquid,
Lotion, cake body class mosquito repellent product it is easy to use, to human body skin without pay effect, it is pollution-free to clothes.Refreshing body in this invention
Powder is talcum powder, unfavorable to infant's body, and the security of culicifuge is relatively low.
Chinese patent application CN104606082A discloses a kind of pure natural baby powder, and the pure natural infant feels well
Body powder be with cornstarch as primary raw material, and be aided with sodium, sodium acid carbonate, montmorillonite, bentonite, bdellium leaf cell extract
The natural constituents such as thing, rough branch elm bark powder, moss rose flower extract, the effect of miliaria of being dispelled with anti-miliaria can be for a long time
Keep baby's Oily skin dry and comfortable, it is not only effectively but also safe, but talcum powder of this invention has no repelling effect.
The content of the invention
In order to solve problems of the prior art, it is an object of the invention to provide a kind of talcum powder and its preparation side
Method.The talcum powder that the present invention is provided can not only feel well body, miliaria of dispelling, additionally it is possible to mosquito repellent, antibacterial, and gentle non-stimulated.
The invention provides a kind of talcum powder, including following components and its percentage by weight：
Menthol 1-3%, anisaldehyde 0.2-0.6%, eucalyptol 0.1-0.3%, sandalwood oil 0.2-0.6%, linalool
0.1-0.5%, essence 0.1-0.3%, propane diols 1-3%, ethanol 1-2% and corn flour 89.7-96.3%.Corn flour is purchased from extensively
Zhou Yingte health foods Co., Ltd.
Compatibility of the present invention is reasonable, science, and each component interacts, and collaboration plays refreshing body, miliaria of dispelling, mosquito repellent, antibacterial.
Further, described talcum powder is made up of following components and its percentage by weight：
Menthol 2%, anisaldehyde 0.4%, eucalyptol 0.2%, sandalwood oil 0.4%, linalool 0.3%, essence 0.2%,
Propane diols 2%, ethanol 1.5% and corn flour 93%.
Meanwhile, present invention also offers a kind of preparation method of talcum powder, comprise the following steps：
S1. propane diols and ethanol are added in container, are stirred, be heated to 60-70 DEG C, peppermint is added while stirring
Alcohol, anisaldehyde, eucalyptol, sandalwood oil, linalool and essence, stir, and obtain solution A；
S2. step S1 resulting solutions A is cooled to 30-40 DEG C, is sprayed onto on corn flour while stirring, stirred, i.e.,
.
Linalool (C in the mosquito-repellent perfume that the present invention is provided10H18O, CAS NO：78-70-6) there is antibacterial, mosquito repellent, mite killing
Effect；Menthol (C10H20O, CAS NO：89-78-1) there is refrigerant, mosquito repellent effect；Eucalyptol (C15H26O, is purchased from Jiangxi
Jishui Daxing perfumery oil factory) there is the effect of mosquito repellent；Anisaldehyde (C8H8O2, CAS NO：123-11-5) the effect with mosquito repellent.
Compatibility of the present invention is reasonable, science, and each component interacts, and collaboration plays refreshing body, miliaria of dispelling, mosquito repellent, antibacterial.
Compared with prior art, the talcum powder that the present invention is provided can not only feel well body, miliaria of dispelling, additionally it is possible to mosquito repellent, antibacterial, and
It is gentle non-stimulated.
Specific embodiment
Below by specific embodiment, the present invention will be further described, and these embodiments are served only for the purpose of illustration, and
It is not limited to protection scope of the present invention.
A kind of talcum powder of embodiment 1
Described talcum powder, is made up of following components and its percentage by weight：
Menthol 1%, anisaldehyde 0.2%, eucalyptol 0.1%, sandalwood oil 0.2%, linalool 0.1%, essence 0.1%,
Propane diols 1%, ethanol 1% and corn flour 96.3%.
Preparation method：
S1. propane diols and ethanol are added in container, stirred, be heated to 65 DEG C, add while stirring menthol,
Anisaldehyde, eucalyptol, sandalwood oil, linalool and essence, stir, and obtain solution A；
S2. step S1 resulting solutions A is cooled to 35 DEG C, is sprayed onto on corn flour while stirring, stirred, obtained final product.
A kind of talcum powder of embodiment 2
Described talcum powder, is made up of following components and its percentage by weight：
Menthol 2%, anisaldehyde 0.4%, eucalyptol 0.2%, sandalwood oil 0.4%, linalool 0.3%, essence 0.2%,
Propane diols 2%, ethanol 1.5% and corn flour 93%.
Preparation method is similar to Example 1.
A kind of talcum powder of embodiment 3
Described talcum powder, is made up of following components and its percentage by weight：
Menthol 3%, anisaldehyde 0.6%, eucalyptol 0.3%, sandalwood oil 0.6%, linalool 0.5%, essence 0.3%,
Propane diols 3%, ethanol 2% and corn flour 89.7%.
Preparation method is similar to Example 1.
A kind of talcum powder of comparative example 1
Described talcum powder, is made up of following components and its percentage by weight：
Menthol 2.4%, eucalyptol 0.2%, sandalwood oil 0.4%, linalool 0.3%, essence 0.2%, propane diols 2%,
Ethanol 1.5% and corn flour 93%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is to be not added with anisaldehyde, increased the consumption of menthol.
A kind of talcum powder of comparative example 2
Described talcum powder, is made up of following components and its percentage by weight：
Menthol 2%, anisaldehyde 0.4%, eucalyptol 0.2%, styrax 0.4%, linalool 0.3%, essence 0.2%,
Propane diols 2%, ethanol 1.5% and corn flour 93%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is that sandalwood oil is replaced into styrax.
Test example one, excitant/corrosion test
1. test material：Talcum powder prepared by embodiment 1-3.
2. subjects：White rabbit 150, body weight 250-300g, male.
3. content of the test：
White rabbit is randomly divided into 3 groups, every group 50, embodiment 1-3 groups is denoted as.24h before experiment, cuts off White Rabbit back ridge
The hair of post both sides, it is respectively 3cm × 3cm not damage epidermis, unhairing scope or so, and is marked.Talcum powder prepared by Example 1-3
Each 0.5g is applied on the skin of mark, and opposite side is blank.Talcum powder is washed away with clear water after 4h, in sight after 1,24,48h
The reaction of recipient site local skin is examined, is pressed《Cosmetics health specification》(version in 2007) skin irritation/corrosion test is carried out
Dermoreaction is scored, and the average value integrated with animal subject carries out overall merit, and it is secondary to observe other poison in addition to excitant
Property effect.
4. result of the test：
Each observing time point top average ＜ 0.5 in experiment, belongs to nonirritant.That is, skin irritation test result
For：It is nonirritant.It is nontoxic non-stimulated therefore the talcum powder of present invention offer is gentleer to skin.
Test example two, repelling effect is tested
1st, test material：Talcum powder prepared by embodiment 1-3 and comparative example 1-2.
2nd, subjects：
Test insect：Culex pipiens pallens (Culex pipiens pallens), 4 days adults of non-blood suction after emergence, male and female are each
Half, experimental condition：26 ± 1 DEG C of temperature, relative humidity 65 ± 10%；
Tester：50, age 15-40 Sui, men and women half and half.
3rd, test method：
Reference literature method is tested, and (National Standard of the People's Republic of China, agriculture chemical registration is with hygienic insecticide room
The 9th part repellant (GB/T13917.9-2009) of the test of pesticide effectiveness and evaluation, 2009).
(1) attack experiment：
It is the lineae ablicantes do not sucked blood for 4 days after 300 emergence are put into the mosquito cage of 40cm × 30cm × 30cm in length × width × height
Yellow-fever mosquito female mosquito.Tester's the back of the hand exposes 4cm × 4cm skins, and remainder tightly covers.Hand is goed deep into mosquito cage to stop
2min, close observation finds that mosquito stops falling, and shakes arm before its mouthpart will be pierced into skin and is driven, and is designated as a test worm and stops
Fall.Tester of the test worm stopping falling of coming more than 30 and test worm are designated as that attack is qualified, and this person and this cage mosquito can be carried out
Repellency test.
(2) repellency test：
Selected from the qualified tester of 35 attacks, men and women half and half.The skin of 5cm × 5cm is respectively drawn in its both hands the back of the hand
Skin area a, wherein hand presses 0.5mg/cm2Dose uniformity smear talcum powder prepared by embodiment 1-3 and comparative example 1-2.Press
4cm × 4cm skins therein are exposed, remainder tightly covers, another hand is blank.Talcum powder 2h is smeared, hand is stretched into
2min in the qualified mosquito cage of attack is placed with, observation whether there is mosquito is come to stop to fall to sucking blood.Tested once every 1h afterwards, as long as
There is a mosquito to come to suck blood sentence and make repellent product failure.Record the effective protecting time (h) of repellent product.
4th, result of the test：The repelling effect (effective protecting time) of each talcum powder is shown in Table 1.
The repelling effect of table 1
| Group | 1 group of embodiment | 2 groups of embodiment | 3 groups of embodiment | 1 group of comparative example | 2 groups of comparative example |
| Mosquito repellent time (h) | 9.2 | 9.4 | 9.0 | 7.5 | 8.1 |
As shown in Table 1, the repelling effect of talcum powder prepared by the present invention is preferable.And talcum powder prepared by comparative example 1-2
Repelling effect is poorer than the repelling effect of talcum powder prepared by embodiment 1-3, illustrate compatibility of the present invention rationally, science, each group split-phase
Interaction, has cooperateed with the effect of mosquito repellent.
Test example three, antibacterial tests
1. test material：Talcum powder prepared by embodiment 1-3 and comparative example 1-2.
2. subjects：Gold-coloured staphylococci bacterium colony and typhoid bacillus bacterium colony.
3. test method：
1) lower floor's aseptic culture medium is prepared：To pouring into 10mL agar mediums in sterilized petri dishes, and condense it.
2) upper strata inoculation medium is prepared：The agar medium 150mL for taking 45 DEG C ± 2 DEG C is put into flask, adds bacterium bacterium
Sum fall for X1Experiment bacterium solution.Vibration flask makes Multiple drug resistance uniform, to pouring into 5mL in each plate in step1, and makes
It condenses.Inoculated agar culture face should use in 1h.
3) plate is respectively placed in 5 big containers of aseptic closed grade, addition etc. is big in this 5 sealing containers
Small beaker is used to deposit the talcum powder 0.5g prepared according to embodiment 1-3 and comparative example 1-2 respectively,
The heater for setting heating small beaker in the bottom of small beaker promotes the volatilization of perfume, the gas in control sealing container
Body composition is identical with aseptic composition of air all the time.By after the culture of 24h, total number of bacterial colonies is X in detection culture medium2,
Bacterial clump reduced rate is calculated according to the following formula.
Bacterial clump reduced rate=(X1-X2)/X1
4. result of the test：The anti-bacterial result is shown in Table 2.
The anti-bacterial result of table 2
As shown in Table 2, the antibacterial effect of talcum powder prepared by the present invention is preferable.And talcum powder prepared by comparative example 1-2
Antibacterial effect is poorer than the effect of talcum powder prepared by embodiment 1-3, illustrate compatibility of the present invention rationally, science, each component phase interaction
With collaboration plays antibacterial, and the antibacterial effect of embodiment 2 is optimal.
Claims (3)
1. a kind of talcum powder, it is characterised in that including following components and its percentage by weight：
Menthol 1-3%, anisaldehyde 0.2-0.6%, eucalyptol 0.1-0.3%, sandalwood oil 0.2-0.6%, linalool 0.1-
0.5%th, essence 0.1-0.3%, propane diols 1-3%, ethanol 1-2% and corn flour 89.7-96.3%.
2. talcum powder as claimed in claim 1, it is characterised in that be made up of following components and its percentage by weight：
Menthol 2%, anisaldehyde 0.4%, eucalyptol 0.2%, sandalwood oil 0.4%, linalool 0.3%, essence 0.2%, the third two
Alcohol 2%, ethanol 1.5% and corn flour 93%.
3. the preparation method of talcum powder as claimed in claim 1 or 2, it is characterised in that comprise the following steps：
S1. propane diols and ethanol are added in container, stirred, be heated to 60-70 DEG C, add while stirring menthol,
Anisaldehyde, eucalyptol, sandalwood oil, linalool and essence, stir, and obtain solution A；
S2. step S1 resulting solutions A is cooled to 30-40 DEG C, is sprayed onto on corn flour while stirring, stirred, obtained final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611210616.7A CN106726649A (en) | 2016-12-24 | 2016-12-24 | A kind of talcum powder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611210616.7A CN106726649A (en) | 2016-12-24 | 2016-12-24 | A kind of talcum powder and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106726649A true CN106726649A (en) | 2017-05-31 |
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ID=58920446
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611210616.7A Pending CN106726649A (en) | 2016-12-24 | 2016-12-24 | A kind of talcum powder and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107582446A (en) * | 2017-08-24 | 2018-01-16 | 广西钱隆投资管理有限公司 | The special talcum powder of one kind adult |
| CN107595729A (en) * | 2017-08-24 | 2018-01-19 | 广西钱隆投资管理有限公司 | A kind of atomizing talcum powder |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102641227A (en) * | 2012-04-24 | 2012-08-22 | 王玉兰 | Corn baby talcum powder |
| CN102697699A (en) * | 2012-06-25 | 2012-10-03 | 南通优尼科化工有限公司 | Baby powder |
-
2016
- 2016-12-24 CN CN201611210616.7A patent/CN106726649A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102641227A (en) * | 2012-04-24 | 2012-08-22 | 王玉兰 | Corn baby talcum powder |
| CN102697699A (en) * | 2012-06-25 | 2012-10-03 | 南通优尼科化工有限公司 | Baby powder |
Non-Patent Citations (1)
| Title |
|---|
| 孙玉秀: "《小化工产品配方与制备》", 31 October 2015, 中国纺织出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107582446A (en) * | 2017-08-24 | 2018-01-16 | 广西钱隆投资管理有限公司 | The special talcum powder of one kind adult |
| CN107595729A (en) * | 2017-08-24 | 2018-01-19 | 广西钱隆投资管理有限公司 | A kind of atomizing talcum powder |
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