CN106723046A - A kind of functional food composite and application - Google Patents
A kind of functional food composite and application Download PDFInfo
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- CN106723046A CN106723046A CN201710036877.XA CN201710036877A CN106723046A CN 106723046 A CN106723046 A CN 106723046A CN 201710036877 A CN201710036877 A CN 201710036877A CN 106723046 A CN106723046 A CN 106723046A
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- 235000013376 functional food Nutrition 0.000 title claims abstract description 18
- 239000002131 composite material Substances 0.000 title claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 18
- 241000026010 Dendrobium candidum Species 0.000 claims abstract description 15
- 241000192656 Nostoc Species 0.000 claims abstract description 15
- 244000025254 Cannabis sativa Species 0.000 claims abstract description 12
- 241000320380 Silybum Species 0.000 claims abstract description 12
- 235000010841 Silybum marianum Nutrition 0.000 claims abstract description 12
- 235000020237 cranberry extract Nutrition 0.000 claims abstract description 12
- 238000004880 explosion Methods 0.000 claims description 46
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 39
- 239000007788 liquid Substances 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- 239000003480 eluent Substances 0.000 claims description 12
- 239000011347 resin Substances 0.000 claims description 9
- 229920005989 resin Polymers 0.000 claims description 9
- 239000006228 supernatant Substances 0.000 claims description 9
- 108090000790 Enzymes Proteins 0.000 claims description 7
- 102000004190 Enzymes Human genes 0.000 claims description 7
- 229940088598 enzyme Drugs 0.000 claims description 7
- 239000004952 Polyamide Substances 0.000 claims description 6
- 229960000583 acetic acid Drugs 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
- 238000004108 freeze drying Methods 0.000 claims description 6
- 239000012362 glacial acetic acid Substances 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 229920002647 polyamide Polymers 0.000 claims description 6
- 238000001179 sorption measurement Methods 0.000 claims description 6
- 238000000859 sublimation Methods 0.000 claims description 6
- 230000008022 sublimation Effects 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 108010059892 Cellulase Proteins 0.000 claims description 3
- 108091005804 Peptidases Proteins 0.000 claims description 3
- 239000004365 Protease Substances 0.000 claims description 3
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 3
- 101000693530 Staphylococcus aureus Staphylokinase Proteins 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- 235000012545 Vaccinium macrocarpon Nutrition 0.000 claims description 3
- 235000002118 Vaccinium oxycoccus Nutrition 0.000 claims description 3
- 244000291414 Vaccinium oxycoccus Species 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- 238000005422 blasting Methods 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims description 3
- 235000004634 cranberry Nutrition 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 239000012530 fluid Substances 0.000 claims description 3
- 235000013305 food Nutrition 0.000 claims description 3
- 238000007710 freezing Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 claims description 3
- 230000036039 immunity Effects 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 230000007935 neutral effect Effects 0.000 claims description 3
- 238000001556 precipitation Methods 0.000 claims description 3
- 235000019419 proteases Nutrition 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- 239000008107 starch Substances 0.000 claims description 3
- 230000002708 enhancing effect Effects 0.000 abstract description 6
- 230000036541 health Effects 0.000 abstract description 6
- 230000001363 autoimmune Effects 0.000 abstract description 4
- 239000008280 blood Substances 0.000 abstract description 3
- 210000004369 blood Anatomy 0.000 abstract description 3
- 210000001124 body fluid Anatomy 0.000 abstract description 3
- 239000010839 body fluid Substances 0.000 abstract description 3
- 230000007969 cellular immunity Effects 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 230000014509 gene expression Effects 0.000 abstract description 3
- 230000004727 humoral immunity Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000000638 stimulation Effects 0.000 abstract description 3
- 238000005119 centrifugation Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003862 health status Effects 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 208000033065 inborn errors of immunity Diseases 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 208000028529 primary immunodeficiency disease Diseases 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8984—Dendrobium
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/66—Microorganisms or materials therefrom
- A61K35/74—Bacteria
- A61K35/748—Cyanobacteria, i.e. blue-green bacteria or blue-green algae, e.g. spirulina
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/45—Ericaceae or Vacciniaceae (Heath or Blueberry family), e.g. blueberry, cranberry or bilberry
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
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Abstract
The invention discloses a kind of functional food composite and application, the functional food is prepared from by the component of following weight portion：10 15 parts of extract of Milk Thistle grass, 13 19 parts of nostoc freeze-dried powder, 10 15 parts of Cranberry extract, 12 17 parts of dendrobium candidum extract.The present invention not only has the function of enhancing cellular immunity and humoral immunity, by Stimulation effect cell factor and the number of ways such as its gene expression can also be improved play its immune enhancing function, invigorating qi for tranquilization of the present invention, strengthen the body resistance to consolidate the constitution, it is clearing heat and detoxicating, allay excitement be healthy and strong, nourishes blood and promotes the production of body fluid, QI invigorating salubrity, function of human body is adjusted from root, human autoimmune's function is improved, away from inferior health.
Description
Technical field
The present invention relates to field of food, and in particular to a kind of functional food composite and application.
Background technology
In daily life, psychological pressure is excessive, long-term nutrition is bad, live no rule, overworked, hormone abuse etc.
The immunity degradation of human body can be caused, long-time hypoimmunity, human body would be at sub-health state.Sub-health state is not
Disconnected Change and Development, can not such as be improved in time, it is more likely that be converted into disease.There is data to suggest that, there is 75% people in the whole world
In sub-health state.Inferior health has turned into universal, global problem, and the health status of modern allows of no optimist.Therefore, carry
Human autoimmune's function high is just remote from inferior health, moves towards the basic method of health.
The content of the invention
Object of the present invention is to provide a kind of functional food composite and application.
To achieve the above object, the technical scheme taken of the present invention is：
A kind of functional food composite, is prepared from by the component of following weight portion：
10-15 parts of extract of Milk Thistle grass, 13-19 parts of nostoc freeze-dried powder, Cranberry extract 10-15 parts, dendrobium candidum
Extract 12-17 parts.
Wherein, the Milk Thistle grass extract is as obtained by prepared by following steps：
Milk Thistle grass is taken, measure water with 10-15 times decocts extraction 2-4 times respectively, and each 0.5-2h merges extract solution, is concentrated into
Relative density is 1.10~1.20g/ml at 65 DEG C, adds ethanol to make the percent by volume of alcohol content up to 50-80%, and it is heavy to stand
Form sediment, filtration obtains precipitation solution, dry, pulverize into dry extract.
Wherein, nostoc freeze-dried powder is as obtained by prepared by following steps：
Take and be placed in after nostoc is cleaned steam explosion treatment three times in steam-explosion jar, freeze-drying obtains nostoc freeze-dried powder；Q wherein,
It is 0.6-0.9Mpa, 60-90 degrees Celsius of temperature, time 7-23min, second explosion treatment that first time explosion treatment keeps pressure
Holding pressure is 0.9-1.1Mpa, 90-110 degrees Celsius of temperature, time 0.9-1.3min, and third time explosion treatment holding pressure is
3-5Mpa, 60-80 degrees Celsius of temperature, time 0.9-2.9min.
Wherein, the freeze-drying includes the treatment of pre-freeze treatment separate explosion, distillation treatment separate explosion treatment, pre-freeze treatment time
Explosion treatment selects quick-frozen mode, and pre-freezing temperature is 11 DEG C, pre-freeze time 8h；In distillation treatment separate explosion treatment, sublimation temperature
It it is -13 DEG C, vacuum is 270pa, sublimation time 230min.
Wherein, the Cranberry extract is as obtained by prepared by following steps：
It is placed in steam-explosion jar after Cranberry is cleaned, it is 1.7-2.3MPa to be passed through nitrogen to steam explosion pressure inside the tank, and steam is quick-fried
After tear reason 0.9-2.9min, after being cooled to room temperature, add by cellulase: the mixing gained of alkali protease in mass ratio 2: 3
Complex enzyme, be combined enzyme dosage for raw material weight 0.7-2.3%, 0.5-2h is digested at being maintained at 30-45 DEG C, filter, obtain enzyme
Solution liquid；Directly by neutral alumina column, resin column blade diameter length ratio is 1: 5-1: 10 to enzymolysis liquid, respectively with 1-4 times of cylinder ponding, 1-
3 times of ethanol solutions of column volume 95% elute removal of impurities, and the ethanol of the 0.3-0.6% glacial acetic acid -55% (1: 1) with 5-7 times of column volume is molten
Liquid is eluted, and collects eluent；After flinging to the glacial acetic acid and ethanol in eluent, micro-wave vacuum obtains Cranberry extract.
Wherein, the dendrobium candidum extract is prepared by the following method：
S1, the dendrobium candidum that clean will be drained are placed in steam-explosion jar, and it is 0.7- to be first passed through nitrogen to steam explosion pressure inside the tank
1.5MPa, explosion treatment 8-29min；Then it is 1.5-1.9MPa to be passed through steam to steam explosion pressure inside the tank rapidly, at steam blasting
After reason 0.6-2.6min, room temperature is concentrated into relative density 1.10-1.20, is spray-dried concentrate, obtains powder；
S2, in powder add 3-8 times of water, by mass percentage be 0.5-2% ratio add neutral proteinase, 30-
0.5-2h is digested at 50 DEG C, is filtered, obtain enzymolysis liquid；
S3, by naturally to thaw again after the zymotic fluid quick freeze of gained, age of starch is precipitated in making extract；Collect supernatant
Liquid, remainder centrifugation is collected centrifugal liquid and is incorporated in supernatant；
S4, by supernatant with the flow velocity of 3-7BV/h by macroporous resin column, after Dynamic Adsorption saturation, with deionized water with
The above-mentioned macroporous resin column of flow velocity drip washing of 5-8BV/h is colourless to efflux, then with the ethanol that volume fraction is 50%-70% with 8-
The flow velocity of 12BV/h is eluted, and collects eluent, is concentrated under reduced pressure, and obtains medicinal extract；
S5, will after medicinal extract water dissolves with the flow velocity of 3-5BV/h by polyamide column, after Dynamic Adsorption saturation, use 3-7BV
Deionized water with the above-mentioned polyamide column of flow velocity drip washing of 2-10BV/h, then with the ethanol that volume fraction is 30%-50% with 5-
The flow velocity of 10BV/h is eluted, and collection has eluent, is spray-dried, and obtains dendrobium candidum extract.
A kind of application of above-mentioned functional food composite, can be used for the making of the food of enhance immunity.
The invention has the advantages that：
Not only there is the function of enhancing cellular immunity and humoral immunity, moreover it is possible to by Stimulation effect cell factor and improve it
The number of ways such as gene expression play its immune enhancing function, invigorating qi for tranquilization of the present invention, strengthen the body resistance to consolidate the constitution, it is clearing heat and detoxicating, allay excitement it is strong
Body, nourishes blood and promotes the production of body fluid, QI invigorating salubrity, function of human body is adjusted from root, human autoimmune's function is improved, away from inferior health.
Specific embodiment
In order that objects and advantages of the present invention become more apparent, the present invention is carried out further with reference to embodiments
Describe in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair
It is bright.
In following examples, the Milk Thistle grass extract for being used is as obtained by prepared by following steps：
Milk Thistle grass is taken, measure water with 10-15 times decocts extraction 2-4 times respectively, and each 0.5-2h merges extract solution, is concentrated into
Relative density is 1.10~1.20g/ml at 65 DEG C, adds ethanol to make the percent by volume of alcohol content up to 50-80%, and it is heavy to stand
Form sediment, filtration obtains precipitation solution, dry, pulverize into dry extract.
The nostoc freeze-dried powder for being used is as obtained by prepared by following steps：
Take and be placed in after nostoc is cleaned steam explosion treatment three times in steam-explosion jar, freeze-drying obtains nostoc freeze-dried powder；Q wherein,
It is 0.6-0.9Mpa, 60-90 degrees Celsius of temperature, time 7-23min, second explosion treatment that first time explosion treatment keeps pressure
Holding pressure is 0.9-1.1Mpa, 90-110 degrees Celsius of temperature, time 0.9-1.3min, and third time explosion treatment holding pressure is
3-5Mpa, 60-80 degrees Celsius of temperature, time 0.9-2.9min.
The freeze-drying for being used includes the treatment of pre-freeze treatment separate explosion, distillation treatment separate explosion treatment, pre-freeze treatment time
Explosion treatment selects quick-frozen mode, and pre-freezing temperature is 11 DEG C, pre-freeze time 8h；In distillation treatment separate explosion treatment, sublimation temperature
It it is -13 DEG C, vacuum is 270pa, sublimation time 230min.
The Cranberry extract for being used is as obtained by prepared by following steps：
It is placed in steam-explosion jar after Cranberry is cleaned, it is 1.7-2.3MPa to be passed through nitrogen to steam explosion pressure inside the tank, and steam is quick-fried
After tear reason 0.9-2.9min, after being cooled to room temperature, add by cellulase: the mixing gained of alkali protease in mass ratio 2: 3
Complex enzyme, be combined enzyme dosage for raw material weight 0.7-2.3%, 0.5-2h is digested at being maintained at 30-45 DEG C, filter, obtain enzyme
Solution liquid；Directly by neutral alumina column, resin column blade diameter length ratio is 1: 5-1: 10 to enzymolysis liquid, respectively with 1-4 times of cylinder ponding, 1-
3 times of ethanol solutions of column volume 95% elute removal of impurities, and the ethanol of the 0.3-0.6% glacial acetic acid -55% (1: 1) with 5-7 times of column volume is molten
Liquid is eluted, and collects eluent；After flinging to the glacial acetic acid and ethanol in eluent, micro-wave vacuum obtains Cranberry extract.
The dendrobium candidum extract for being used is prepared by the following method：
S1, the dendrobium candidum that clean will be drained are placed in steam-explosion jar, and it is 0.7- to be first passed through nitrogen to steam explosion pressure inside the tank
1.5MPa, explosion treatment 8-29min；Then it is 1.5-1.9MPa to be passed through steam to steam explosion pressure inside the tank rapidly, at steam blasting
After reason 0.6-2.6min, room temperature is concentrated into relative density 1.10-1.20, is spray-dried concentrate, obtains powder；
S2, in powder add 3-8 times of water, by mass percentage be 0.5-2% ratio add neutral proteinase, 30-
0.5-2h is digested at 50 DEG C, is filtered, obtain enzymolysis liquid；
S3, by naturally to thaw again after the zymotic fluid quick freeze of gained, age of starch is precipitated in making extract；Collect supernatant
Liquid, remainder centrifugation is collected centrifugal liquid and is incorporated in supernatant；
S4, by supernatant with the flow velocity of 3-7BV/h by macroporous resin column, after Dynamic Adsorption saturation, with deionized water with
The above-mentioned macroporous resin column of flow velocity drip washing of 5-8BV/h is colourless to efflux, then with the ethanol that volume fraction is 50%-70% with 8-
The flow velocity of 12BV/h is eluted, and collects eluent, is concentrated under reduced pressure, and obtains medicinal extract；
S5, will after medicinal extract water dissolves with the flow velocity of 3-5BV/h by polyamide column, after Dynamic Adsorption saturation, use 3-7BV
Deionized water with the above-mentioned polyamide column of flow velocity drip washing of 2-10BV/h, then with the ethanol that volume fraction is 30%-50% with 5-
The flow velocity of 10BV/h is eluted, and collection has eluent, is spray-dried, and obtains dendrobium candidum extract.
Embodiment 1
A kind of functional food composite, is prepared from by the component of following weight portion：
10-15 parts of extract of Milk Thistle grass, 13-19 parts of nostoc freeze-dried powder, Cranberry extract 10-15 parts, dendrobium candidum
Extract 12-17 parts.
Embodiment 2
A kind of functional food composite, is prepared from by the component of following weight portion：
10-15 parts of extract of Milk Thistle grass, 13-19 parts of nostoc freeze-dried powder, Cranberry extract 10-15 parts, dendrobium candidum
Extract 12-17 parts.
Embodiment 3
A kind of functional food composite, is prepared from by the component of following weight portion：
10-15 parts of extract of Milk Thistle grass, 13-19 parts of nostoc freeze-dried powder, Cranberry extract 10-15 parts, dendrobium candidum
Extract 12-17 parts.
Put into practice through substantial amounts for the treatment of case, the preparation obtained by the present embodiment not only has enhancing cellular immunity and humoral immunity
Function, moreover it is possible to by Stimulation effect cell factor and improve the number of ways such as its gene expression and play its immune enhancing function,
Invigorating qi for tranquilization of the present invention, strengthen the body resistance to consolidate the constitution, it is clearing heat and detoxicating, allay excitement be healthy and strong, nourishes blood and promotes the production of body fluid, QI invigorating salubrity, from root adjust human body machine
Can, human autoimmune's function is improved, away from inferior health.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (7)
1. a kind of functional food composite, it is characterised in that be prepared from by the component of following weight portion：
10-15 parts of extract of Milk Thistle grass, 13-19 parts of nostoc freeze-dried powder, Cranberry extract 10-15 parts, dendrobium candidum extraction
Thing 12-17 parts.
2. a kind of functional food composite according to claim 1, it is characterised in that the Milk Thistle grass extract by with
Lower step prepares gained：
Milk Thistle grass is taken, measure water with 10-15 times decocts extraction 2-4 times respectively, and each 0.5-2h merges extract solution, is concentrated into 65 DEG C
When relative density be 1.10~1.20g/ml, add ethanol to make the percent by volume of alcohol content up to 50-80%, staticly settle, filter
Cross, obtain precipitation solution, dry, pulverize into dry extract.
3. a kind of functional food composite according to claim 1, it is characterised in that nostoc freeze-dried powder is by following step
It is rapid to prepare gained：
Take and be placed in after nostoc is cleaned steam explosion treatment three times in steam-explosion jar, freeze-drying obtains nostoc freeze-dried powder；Q wherein, first
It is 0.6-0.9Mpa, 60-90 degrees Celsius of temperature, time 7-23min that separate explosion treatment keeps pressure, and second explosion treatment keeps
Pressure is 0.9-1.1Mpa, 90-110 degrees Celsius of temperature, time 0.9-1.3min, and it is 3- that third time explosion treatment keeps pressure
5Mpa, 60-80 degrees Celsius of temperature, time 0.9-2.9min.
4. a kind of functional food composite according to claim 3, it is characterised in that the freeze-drying including pre-freeze at
The treatment of reason separate explosion, distillation treatment separate explosion treatment, the pre-freeze treatment separate explosion treatment quick-frozen mode of selection, pre-freezing temperature is 11
DEG C, pre-freeze time 8h；In distillation treatment separate explosion treatment, sublimation temperature is -13 DEG C, and vacuum is 270pa, sublimation time
230min。
5. a kind of functional food composite according to claim 1, it is characterised in that the Cranberry extract by with
Lower step prepares gained：
It is placed in steam-explosion jar after Cranberry is cleaned, it is 1.7-2.3MPa to be passed through nitrogen to steam explosion pressure inside the tank, at steam blasting
After reason 0.9-2.9min, after being cooled to room temperature, add as cellulase: answering obtained by the mixing of alkali protease in mass ratio 2: 3
Synthase, it is the 0.7-2.3% of raw material weight to be combined enzyme dosage, and 0.5-2h is digested at being maintained at 30-45 DEG C, is filtered, and obtains enzymolysis liquid；
Directly by neutral alumina column, resin column blade diameter length ratio is 1: 5-1: 10 to enzymolysis liquid, respectively with 1-4 times of cylinder ponding, 1-3 times of post
The ethanol solution of volume 95% elutes removal of impurities, is washed with 0.3-0.6% glacial acetic acid -55% ethanol (1: 1) solution of 5-7 times of column volume
It is de-, collect eluent；After flinging to the glacial acetic acid and ethanol in eluent, micro-wave vacuum obtains Cranberry extract.
6. a kind of functional food composite according to claim 1, it is characterised in that the dendrobium candidum extract passes through
It is prepared by following methods：
S1, the dendrobium candidum that clean will be drained are placed in steam-explosion jar, and it is 0.7-1.5MPa to be first passed through nitrogen to steam explosion pressure inside the tank,
Explosion treatment 8-29min；Then it is 1.5-1.9MPa, Steam explosion treatment 0.6- to be passed through steam to steam explosion pressure inside the tank rapidly
After 2.6min, room temperature is concentrated into relative density 1.10-1.20, is spray-dried concentrate, obtains powder；
S2, in powder add 3-8 times of water, by mass percentage be 0.5-2% ratio add neutral proteinase, 30-50 DEG C
Lower enzymolysis 0.5-2h, filtering, obtains enzymolysis liquid；
S3, by naturally to thaw again after the zymotic fluid quick freeze of gained, age of starch is precipitated in making extract；Collect supernatant,
Remainder is centrifuged, and collects centrifugal liquid and is incorporated in supernatant；
S4, by supernatant with the flow velocity of 3-7BV/h by macroporous resin column, after Dynamic Adsorption saturation, with deionized water with 5-
The above-mentioned macroporous resin column of flow velocity drip washing of 8BV/h is colourless to efflux, then with the ethanol that volume fraction is 50%-70% with 8-
The flow velocity of 12BV/h is eluted, and collects eluent, is concentrated under reduced pressure, and obtains medicinal extract；
S5, will after medicinal extract water dissolves with the flow velocity of 3-5BV/h by polyamide column, after Dynamic Adsorption saturation, with 3-7BV go from
Sub- water with the above-mentioned polyamide column of flow velocity drip washing of 2-10BV/h, then with the ethanol that volume fraction is 30%-50% with 5-10BV/h
Flow velocity eluted, collection have eluent, be spray-dried, obtain dendrobium candidum extract.
7. a kind of application of functional food composite according to claim 1, it is characterised in that can be used for enhance immunity
Food making.
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| CN201710036877.XA CN106723046A (en) | 2017-01-14 | 2017-01-14 | A kind of functional food composite and application |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710036877.XA CN106723046A (en) | 2017-01-14 | 2017-01-14 | A kind of functional food composite and application |
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| CN110693007A (en) * | 2019-10-25 | 2020-01-17 | 李玉保 | Probiotics compound nutrient for inhibiting gynecological inflammation and promoting cell metabolism and preparation method thereof |
| CN110772629A (en) * | 2019-10-25 | 2020-02-11 | 国众兴合生物医药科技有限公司 | Probiotics compound botanical drug for treating gynecological inflammation and improving immunity and preparation method thereof |
| CN110916078A (en) * | 2019-12-17 | 2020-03-27 | 内蒙古阴山优麦食品有限公司 | Method for preparing oat fiber brewing powder by using oats |
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