CN106722773A - A kind of bioactivity selenium-rich salt and preparation method thereof - Google Patents
A kind of bioactivity selenium-rich salt and preparation method thereof Download PDFInfo
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- CN106722773A CN106722773A CN201710032217.4A CN201710032217A CN106722773A CN 106722773 A CN106722773 A CN 106722773A CN 201710032217 A CN201710032217 A CN 201710032217A CN 106722773 A CN106722773 A CN 106722773A
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- Prior art keywords
- selenium
- rich
- enriched
- salt
- added
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- 239000011669 selenium Substances 0.000 title claims abstract description 62
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 title claims abstract description 56
- 229910052711 selenium Inorganic materials 0.000 title claims abstract description 56
- 150000003839 salts Chemical class 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 20
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims abstract description 14
- 239000000284 extract Substances 0.000 claims abstract description 11
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 11
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 11
- 239000011780 sodium chloride Substances 0.000 claims abstract description 10
- 244000068988 Glycine max Species 0.000 claims abstract description 9
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 9
- 235000013312 flour Nutrition 0.000 claims abstract description 9
- 239000004475 Arginine Substances 0.000 claims abstract description 7
- 241000167854 Bourreria succulenta Species 0.000 claims abstract description 7
- 241000238557 Decapoda Species 0.000 claims abstract description 7
- 244000022372 Diospyros lotus Species 0.000 claims abstract description 7
- 235000003333 Diospyros lotus Nutrition 0.000 claims abstract description 7
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 7
- 240000007019 Oxalis corniculata Species 0.000 claims abstract description 7
- 235000016499 Oxalis corniculata Nutrition 0.000 claims abstract description 7
- 235000004976 Solanum vernei Nutrition 0.000 claims abstract description 7
- 241000352057 Solanum vernei Species 0.000 claims abstract description 7
- 244000269722 Thea sinensis Species 0.000 claims abstract description 7
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000019693 cherries Nutrition 0.000 claims abstract description 7
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 7
- 239000008103 glucose Substances 0.000 claims abstract description 7
- 235000011164 potassium chloride Nutrition 0.000 claims abstract description 7
- 239000001103 potassium chloride Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 235000019832 sodium triphosphate Nutrition 0.000 claims abstract description 7
- ODKSFYDXXFIFQN-BYPYZUCNSA-P L-argininium(2+) Chemical compound NC(=[NH2+])NCCC[C@H]([NH3+])C(O)=O ODKSFYDXXFIFQN-BYPYZUCNSA-P 0.000 claims abstract description 4
- 150000001875 compounds Chemical class 0.000 claims description 9
- 238000000855 fermentation Methods 0.000 claims description 9
- 230000004151 fermentation Effects 0.000 claims description 9
- 238000001556 precipitation Methods 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- 239000000654 additive Substances 0.000 claims description 6
- 230000000996 additive effect Effects 0.000 claims description 6
- 239000003814 drug Substances 0.000 claims description 6
- 238000000703 high-speed centrifugation Methods 0.000 claims description 6
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 6
- 235000015097 nutrients Nutrition 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 239000006228 supernatant Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000000265 homogenisation Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 4
- 241000894006 Bacteria Species 0.000 claims description 3
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 3
- 239000007853 buffer solution Substances 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 235000014655 lactic acid Nutrition 0.000 claims description 3
- 239000004310 lactic acid Substances 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 238000000967 suction filtration Methods 0.000 claims description 3
- 235000021419 vinegar Nutrition 0.000 claims description 3
- 239000000052 vinegar Substances 0.000 claims description 3
- 241000220317 Rosa Species 0.000 claims 1
- 235000013305 food Nutrition 0.000 abstract description 7
- 229910019142 PO4 Inorganic materials 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 3
- 230000000050 nutritive effect Effects 0.000 abstract description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract description 2
- 239000010452 phosphate Substances 0.000 abstract description 2
- BWGVNKXGVNDBDI-UHFFFAOYSA-N Fibrin monomer Chemical group CNC(=O)CNC(=O)CN BWGVNKXGVNDBDI-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000000751 protein extraction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
A kind of bioactivity selenium-rich salt of the present invention, is made from the following raw materials in parts by weight：Potassium chloride 10 14, selenium-rich purple potato 45, glucose 0.1 0.2, creeping oxalis 2 2.6, Folium Apocyni Veneti 1.5 2.1, edible salt 271 300,0.08 0.09mol/L NaCl solutions 10 12, selenium-enriched tea leaf 68, selenium-enriched soybean flour 34, the fruit of date plum 12, roseleaf 12, appropriate protein extract, appropriate sodium tripolyphosphate, arginine 0.01 0.02, snow cherry 23, shrimp 24.The present invention processes fribrillin using selenium-enriched soybean flour, when the edible salt is used for food, good water-retaining property, organoleptic attribute and emulsibility can be provided for food, the present invention cooperates with phosphate treated using super-pressure, fribrillin can be promoted to form good gel, the mouthfeel of food can be effectively enriched, and enhance the nutritive value of its selenium-rich, application prospect is extensive.
Description
Technical field
The present invention relates to edible salt technical field, more particularly to a kind of bioactivity selenium-rich salt and preparation method thereof.
Background technology
With the improvement of people's living condition, requirement to edible salt also more and more higher, but traditional edible salt is directed to
Property it is poor, will not also select to use different edible salts because of cuisine, the mouthfeel that this has resulted in dish is general, and nutrition is also
It is single, thus how for different cuisines come the different salt of selective use, be exactly a kind of brand-new, more healthy
Research direction.
The object of the invention is exactly to make up the defect of prior art, there is provided a kind of bioactivity selenium-rich salt and its preparation side
Method.
The present invention is achieved by the following technical solutions：
A kind of bioactivity selenium-rich salt, is made from the following raw materials in parts by weight：
Potassium chloride 10-14, selenium-rich purple potato 4-5, glucose 0.1-0.2, creeping oxalis 2-2.6, Folium Apocyni Veneti 1.5-2.1, food
With salt 271-300,0.08-0.09mol/L NaCl solution 10-12, selenium-enriched tea leaf 6-8, selenium-enriched soybean flour 3-4, fruit of date plum 1-2,
Roseleaf 1-2, appropriate protein extract, appropriate sodium tripolyphosphate, arginine 0.01-0.02, snow cherry 2-3, shrimp 2-4.
A kind of preparation method of bioactivity selenium-rich salt, comprises the following steps：
(1) Folium Apocyni Veneti, snow cherry, selenium-enriched tea leaf, the fruit of date plum, creeping oxalis are mixed, the flooding measured with 10-13 times
Afterwards, concoction is filtered to obtain, then it is spray-dried, obtain selenium-rich traditional Chinese medicine powder；
(2) above-mentioned selenium-rich purple potato, roseleaf are mixed, are added in the water of 50-61 times of compound weight, break into slurry,
Above-mentioned selenium-rich traditional Chinese medicine powder is added, is well mixed, add the lactic acid bacteria of compound weight 1-2%, the sealing thermal insulation 4- at 30-35 DEG C
10 hours, above-mentioned arginine is added, stirred to normal temperature, suction filtration obtains Selenium-enriched fermentation filtrate；
(3) above-mentioned potassium chloride is taken, is mixed with Selenium-enriched fermentation filtrate, stirred, be spray-dried, obtain selenium-rich salt fines；
(4) shrimp is added in the protein extract of 10-14 times of its weight, high-speed homogenization 1-2 minutes, then is placed in 3-4
DEG C, high speed centrifugation 10-15min under 4800-5000r/min rotating speeds, abandon supernatant, add the 2-3 times of protein extraction of volume of precipitation
Liquid and 0.08-0.09mol/L NaCl solutions, high-speed homogenization 25-30s add vinegar, and pH is to 6.25-6.5 for regulation, then is placed in
2-3 DEG C, high speed centrifugation 10-15min under 4500-5000r/min rotating speeds, abandon supernatant, obtain precipitation fribrillin；
(5) above-mentioned precipitation fribrillin, selenium-enriched soybean flour are mixed, is added to 200-250 times of compound weight and steams
In distilled water, the sodium tripolyphosphate of the 6-7% of fribrillin content is added, stirred, add above-mentioned glucose, fermentation
Filtrate, stirs, and is sent in 30-35 DEG C of water-bath, heats 1.5-2h, is re-fed into autoclave, in temperature 20-25
DEG C, under pressure 350-400MPa environment, pressurize 14-15min, discharging obtains Se-enriched nutrient additive；
(6) above-mentioned edible salt, Se-enriched nutrient additive and selenium-rich salt fines are mixed, is stirred, by drying, very
Empty package, obtains final product.
Described protein extract is made up of the raw material of following each concentration：0.1-0.2mol/L NaCl、0.002-
0.003mol/L MgCl2、0.001-0.0015mol/L EDTA、0.1-0.12mol/LNaH2PO4Buffer solution.
It is an advantage of the invention that：
The present invention processes fribrillin using selenium-enriched soybean flour, can be food when the edible salt is used for food
Good water-retaining property, organoleptic attribute and emulsibility are provided, the present invention cooperates with phosphate treated, can promote myogen using super-pressure
Fibrin forms good gel, can effectively enrich the mouthfeel of food, and enhances the nutritive value of its selenium-rich, application
Prospect is extensive.
Specific embodiment
A kind of bioactivity selenium-rich salt, is made from the following raw materials in parts by weight：
Potassium chloride 10, selenium-rich purple potato 4, glucose 0.1, creeping oxalis 2.6, Folium Apocyni Veneti 2.1, edible salt 271-300,
0.09mol/L NaCl solutions 10-12, selenium-enriched tea leaf 6, selenium-enriched soybean flour 3, the fruit of date plum 1, roseleaf 1, protein extract are fitted
Amount, appropriate sodium tripolyphosphate, arginine 0.01, snow cherry 2, shrimp 4.
A kind of preparation method of bioactivity selenium-rich salt, it is comprised the following steps：
(1) Folium Apocyni Veneti, snow cherry, selenium-enriched tea leaf, the fruit of date plum, creeping oxalis are mixed, after 13 times of floodings of amount, filter
Concoction is obtained, then it is spray-dried, obtain selenium-rich traditional Chinese medicine powder；
(2) above-mentioned selenium-rich purple potato, roseleaf are mixed, is added in the water of 61 times of compound weight, break into slurry, added
Above-mentioned selenium-rich traditional Chinese medicine powder, is well mixed, the lactic acid bacteria of addition compound weight 2%, sealing thermal insulation 8 hours at 30-35 DEG C, plus
Enter above-mentioned arginine, stir to normal temperature, suction filtration obtains Selenium-enriched fermentation filtrate；
(3) above-mentioned potassium chloride is taken, is mixed with Selenium-enriched fermentation filtrate, stirred, be spray-dried, obtain selenium-rich salt fines；
(4) shrimp is added in the protein extract of 14 times of its weight, even -2 minutes of high speed, then is placed in 4 DEG C, 5000r/
High speed centrifugation 15min under min rotating speeds, abandons supernatant, adds precipitation 3 times of protein extracts and 0.09mol/L NaCl of volume
Solution, high-speed homogenization 30s adds vinegar, and pH is to 6.25 for regulation, then be placed in 2 DEG C, high speed centrifugation under 5000r/min rotating speeds
10min, abandons supernatant, obtains precipitation fribrillin；
(5) above-mentioned precipitation fribrillin, selenium-enriched soybean flour are mixed, is added to 200-250 times of compound weight and steams
In distilled water, the 7% of fribrillin content sodium tripolyphosphate is added, stirred, add above-mentioned glucose, fermentation filter
Liquid, stirs, and is sent in 35 DEG C of water-baths, heats 1.5h, is re-fed into autoclave, in 25 DEG C of temperature, pressure
Under 400MPa environment, pressurize 15min, discharging obtains Se-enriched nutrient additive；
(6) above-mentioned edible salt, Se-enriched nutrient additive and selenium-rich salt fines are mixed, is stirred, by drying, very
Empty package, obtains final product.
A kind of preparation method of bioactivity selenium-rich salt, described protein extract is made up of the raw material of following each concentration：
0.2mol/L NaCl、0.003mol/L MgCl2、0.0015mol/L EDTA、0.12mol/LNaH2PO4Buffer solution.
Claims (3)
1. a kind of bioactivity selenium-rich salt, it is characterised in that be made from the following raw materials in parts by weight：
Potassium chloride 10-14, selenium-rich purple potato 4-5, glucose 0.1-0.2, creeping oxalis 2-2.6, Folium Apocyni Veneti 1.5-2.1, edible salt
271-300,0.08-0.09mol/L NaCl solution 10-12, selenium-enriched tea leaf 6-8, selenium-enriched soybean flour 3-4, fruit of date plum 1-2, rose
Petal 1-2, appropriate protein extract, appropriate sodium tripolyphosphate, arginine 0.01-0.02, snow cherry 2-3, shrimp 2-4.
2. a kind of preparation method of bioactivity selenium-rich salt as claimed in claim 1, it is characterised in that comprise the following steps：
(1) Folium Apocyni Veneti, snow cherry, selenium-enriched tea leaf, the fruit of date plum, creeping oxalis are mixed, after the 10-13 times of flooding measured, filter
Concoction is obtained, then it is spray-dried, obtain selenium-rich traditional Chinese medicine powder；
(2) above-mentioned selenium-rich purple potato, roseleaf are mixed, is added in the water of 50-61 times of compound weight, break into slurry, added
Above-mentioned selenium-rich traditional Chinese medicine powder, is well mixed, and adds the lactic acid bacteria of compound weight 1-2%, and sealing thermal insulation 4-10 is small at 30-35 DEG C
When, above-mentioned arginine is added, stir to normal temperature, suction filtration obtains Selenium-enriched fermentation filtrate；
(3) above-mentioned potassium chloride is taken, is mixed with Selenium-enriched fermentation filtrate, stirred, be spray-dried, obtain selenium-rich salt fines；
(4) shrimp is added in the protein extract of 10-14 times of its weight, high-speed homogenization 1-2 minutes, then be placed in 3-4 DEG C,
High speed centrifugation 10-15min under 4800-5000r/min rotating speeds, abandons supernatant, add the 2-3 times of protein extract of volume of precipitation with
And 0.08-0.09mol/L NaCl solutions, high-speed homogenization 25-30s, vinegar is added, pH is to 6.25-6.5 for regulation, then is placed in 2-3
DEG C, high speed centrifugation 10-15min under 4500-5000r/min rotating speeds, abandon supernatant, obtain precipitation fribrillin；
(5) above-mentioned precipitation fribrillin, selenium-enriched soybean flour are mixed, is added to 200-250 times of distilled water of compound weight
In, the sodium tripolyphosphate of the 6-7% of fribrillin content is added, stir, add above-mentioned glucose, fermentation filter
Liquid, stirs, and is sent in 30-35 DEG C of water-bath, heats 1.5-2h, is re-fed into autoclave, in temperature 20-25
DEG C, under pressure 350-400MPa environment, pressurize 14-15min, discharging obtains Se-enriched nutrient additive；
(6) above-mentioned edible salt, Se-enriched nutrient additive and selenium-rich salt fines are mixed, is stirred, by drying, vacuum packet
Dress, obtains final product.
3. the preparation method of a kind of bioactivity selenium-rich salt as described in claim 1,2, it is characterised in that：Described albumen is carried
Liquid is taken to be made up of the raw material of following each concentration：0.1-0.2mol/L NaCl、0.002-0.003mol/L MgCl2、0.001-
0.0015mol/L EDTA、0.1-0.12mol/LNaH2PO4Buffer solution.
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| CN201710032217.4A CN106722773A (en) | 2017-01-16 | 2017-01-16 | A kind of bioactivity selenium-rich salt and preparation method thereof |
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|---|---|---|---|
| CN201710032217.4A CN106722773A (en) | 2017-01-16 | 2017-01-16 | A kind of bioactivity selenium-rich salt and preparation method thereof |
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| CN106722773A true CN106722773A (en) | 2017-05-31 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108041556A (en) * | 2017-12-29 | 2018-05-18 | 安徽华欣蔬菜种植专业合作社 | A kind of taurine cladding purslane selenium-rich edible salt and preparation method thereof |
| CN108157913A (en) * | 2017-12-27 | 2018-06-15 | 天津佰亿达企业管理股份有限公司 | A kind of Jin Weita salt and preparation method thereof |
| CN108208742A (en) * | 2017-12-29 | 2018-06-29 | 安徽华欣蔬菜种植专业合作社 | A kind of purslane invigorating the spleen selenium-rich edible salt and preparation method thereof |
| CN108294283A (en) * | 2017-12-29 | 2018-07-20 | 安徽华欣蔬菜种植专业合作社 | A kind of antifatigue mushroom selenium edible salt of purslane and preparation method thereof |
| CN110651989A (en) * | 2019-10-29 | 2020-01-07 | 郑兴福 | A selenium-containing edible salt prepared from selenium-rich plants and its preparation method |
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- 2017-01-16 CN CN201710032217.4A patent/CN106722773A/en active Pending
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Non-Patent Citations (1)
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108157913A (en) * | 2017-12-27 | 2018-06-15 | 天津佰亿达企业管理股份有限公司 | A kind of Jin Weita salt and preparation method thereof |
| CN108041556A (en) * | 2017-12-29 | 2018-05-18 | 安徽华欣蔬菜种植专业合作社 | A kind of taurine cladding purslane selenium-rich edible salt and preparation method thereof |
| CN108208742A (en) * | 2017-12-29 | 2018-06-29 | 安徽华欣蔬菜种植专业合作社 | A kind of purslane invigorating the spleen selenium-rich edible salt and preparation method thereof |
| CN108294283A (en) * | 2017-12-29 | 2018-07-20 | 安徽华欣蔬菜种植专业合作社 | A kind of antifatigue mushroom selenium edible salt of purslane and preparation method thereof |
| CN110651989A (en) * | 2019-10-29 | 2020-01-07 | 郑兴福 | A selenium-containing edible salt prepared from selenium-rich plants and its preparation method |
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Application publication date: 20170531 |