CN106701482A - Rapid preparation method of healthcare mulberry wine - Google Patents
Rapid preparation method of healthcare mulberry wine Download PDFInfo
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- CN106701482A CN106701482A CN201611252114.0A CN201611252114A CN106701482A CN 106701482 A CN106701482 A CN 106701482A CN 201611252114 A CN201611252114 A CN 201611252114A CN 106701482 A CN106701482 A CN 106701482A
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- extraction
- health care
- wine
- mulberries
- mulberry health
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
Abstract
The invention discloses a rapid preparation method of healthcare mulberry wine. The rapid preparation method comprises the following steps: adding mulberries to a wine-based solvent for soaking, wherein the solid-liquid mass ratio of the mulberries to the wine-based solvent is 1:10-1:50; using a flash extraction technology for rapid extraction after soaking, and centrifugally separating the extract to obtain supernatant that is mother liquor of the healthcare mulberry wine; concentrating the mother liquor to obtain a concentrated solution with the content of total anthocyanin of not less than 50 mg/100 ml; blending the concentrated solution with Baijiu to prepare a product of the healthcare mulberry wine. The rapid preparation method provided by the invention utilizes the flash extraction technology for completing the rapid and efficient extraction of functional components while performing continuous tissue fragmentation, thereby synchronously and efficiently complete the tissue fragmentation and the extraction of efficient components; the pertinence for the extraction of functional components is strong; the mother liquor of the healthcare wine is separated centrifugally; the rapid preparation method is simple in operation and low in cost, greatly shortens the production cycle from several hours in the traditional extraction process to several minutes while ensuring the extraction rate of the functional components, has high extraction efficiency, and is suitable for industrial large-scale production.
Description
Technical field
The invention belongs to food processing field, a kind of fast preparation method of mulberry health care wine is specifically related to.
Technical background
The history of the existing thousands of years of health liquor, is the important component of chinese medicine science.The successive dynasties medicine of China writes
Almost there is medicinal liquor to control the record of disease body-building in work bar none, the health care consciousness of people strengthens increasingly, and some health liquors are
As the first-selection that people drink.With the progress of science and technology, health liquor technology of preparing is also from traditional Chinese medicine infusing drugs in wine technological development
Effective ingredient is made the functional health of high content in using the modernization meanses extraction Chinese medicine such as extraction, extraction and biofermentation
Wine.
Mulberries（Cornus officinale Sieb. et Zucc）It is the ripening fruits of Moraceae deciduous tree mulberry tree, it is main
Originate in the province such as Guangdong, Guangxi, Zhejiang, Henan.China's successive dynasties the traditional Chinese medical science book on Chinese herbal medicine, generally acknowledge mulberries have liver-kidney tonifying, nourishing yin and nourishing blood,
Dark hair improving eyesight, effect of removing spot and prolonging life.Modern medicine carries out pharmacology, the result of drug effect toxicity test to mulberries and also indicates that, mulberries
The activity of enzyme in animal body can be improved, suppresses the generation of harmful substance, enhancing cold-resistant, ability of enduring hardships, delaying cell aging are prevented
Vascular sclerosis, and improve the functions such as human body is immune.By it is believed that being the Natural Food that a class has alimentary health-care function
Product.
Main active component is anthocyanin in mulberries, with anti-inflammatory, anti-oxidant, prevention of cardiovascular disease and improvement glycolipid
Various health promotions and the prevention from suffering from the diseases effects such as metabolism；Anthocyanin is safe and nontoxic as a kind of natural pigment, aboundresources, also
Interior free yl, prevention diabetes, protection eyesight etc. can be effectively removed, healthcare function is widely recognized as.
Morat have nourish, take care of health, enriching blood, beneficial liver, kidney tonifying, improving eyesight the effects such as, its traditional preparation method mainly with
Based on liquor-making raw material and health-care medicinal co-fermentation are brewed, although technique is more ripe, quality control hardly possible, mouthfeel effect are still suffered from
Not good shortcoming；And currently conventional modern extraction technique mainly has extraction, circumfluence method, ultrasonic extraction, there is extraction
Time is long, extracts incomplete, and Extracting temperature is high, and active ingredient is easily destroyed, and the shortcomings of production cost is high, is not suitable for extensive work
Industry metaplasia is produced.
Homogenate extraction technology is a kind of new and effective extractive technique broken for plant soft, sclerous tissues, its extraction process
Combined by broken wall and extraction, principle is by high speed machine shearing force and super dynamic molecule diafiltration techniques, by knife chamber
Powerful negative pressure, forms DC pulse, is carried out continuously historrhexis, fine particle is crushed material within the several seconds, and make effectively
Composition is rapidly reached tissue internal and external equilibrium, and extraction purpose is reached through separation of solid and liquid.The technology can be avoided effectively under normal temperature condition
The destruction of composition, short with extraction time, solvent load is few, the advantages of extraction efficiency is high, meets very much current functional health wine
Fast and efficiently industrial production demand.
The content of the invention
The technical problem to be solved in the present invention is that to overcome existing health care method for preparing medicated wine to there is extraction time long, effective
Composition is easily destroyed, extract not exclusively, the shortcoming of high energy consumption, there is provided it is a kind of it is simple and easy to apply, rapidly and efficiently, be adapted to industrial scale
The preparation method of the mulberry health care wine of production.
In order to solve the above technical problems, the present invention is comprised the following steps：
1）Soaked during mulberries are added into wine base solvent, mulberries are 1 with the solid-liquid mass ratio of wine base solvent:10~1:50；
2）Application homogenate extraction technology carries out rapid extraction after immersion, and extract solution is centrifuged, and gained supernatant is mulberries
Health liquor mother liquor；
3）Concentrate of the Anthocyanin content no less than 50 mg/100mL will be obtained after above-mentioned mother liquor concentrations；
4）By above-mentioned concentrate and white spirit mixing, mulberry health care wine product is modulated into.
The alcoholic strength of the wine base is 10~60%vol.
The immersion, its soak time is 0.5-1 hours.
The mulberries are mulberries fresh fruit or dry mulberries or medicinal mulberries medicine materical crude slice.
The rapid extraction refers to that 2~3 extractions were completed in 10 minutes, is extracted 1~3 minute every time.
The Extracting temperature during rapid extraction is 20~50 DEG C.
The application homogenate extraction technology is to use flash extracter；The rotating speed of the flash extracter is 3000~5000
r/min；The extract solution was with 2000~6000 r/min rotating speeds centrifugation 5~20 minutes.
The concentration is concentrated under reduced pressure using rotary evaporator.
Described blending is by concentrate and white wine by volume 1~3:100 ratio is mixed, and is modulated into alcoholic strength and is
The mulberry health care wine product of 10~50%vol.
Mulberry health care wine is obtained using above method step.
The beneficial effects of the invention are as follows：
It is of the invention main using homogenate extraction technology and centrifugal separation technology, carry out connective tissue using homogenate extraction technology and crush
While, the rapidly and efficiently extraction of functional component is completed, tissue is completed synchronous high-efficiency to be crushed and extracts active ingredients, function
Constituents extraction is with strong points, is centrifuged out health liquor mother liquor, and method is simple to operate, low cost；Carried in assurance function composition
On the premise of taking rate, the production cycle is greatly shortened, a few minutes, extraction efficiency are shorten to by several hours of traditional extraction technique
It is high；In whole extraction process, temperature conditionss are room temperature, and stability is high；It is adapted to carry out industrial scale production.
Specific embodiment
Embodiment 1
The g of mulberries medicine materical crude slice 26.7 is taken, plus 30 times are measured wine base of the alcohol concentrations for 45%vol as solvent, and 45 points are soaked at room temperature
Clock, the rapid extraction of tissue crushing and active ingredient is completed using homogenate extraction technology synchronous high-efficiency, and extract solution is centrifuged,
Gained supernatant is mulberry health care distiller's yeast liquid.The present embodiment carries out rapid extraction using flash extracter, using homogenate extraction
Device carry out connective tissue it is broken while, complete the rapidly and efficiently extraction of functional component, obtain carrying rich in anthocyanin type components
Liquid is taken, is 4000r/min by flash extracter rotational speed regulation, Extracting temperature is 25 DEG C of room temperature conditions, point 2 extractions, interval 2~
3 minutes, extract 1~3 minute every time.Extract solution is with 2000~6000 r/min rotating speeds centrifugation 5~20 minutes, extract solution warp
After centrifugation removal slag, gained supernatant is mulberry health care distiller's yeast liquid.
Detection：Anthocyanin content in ultraviolet-ray visible absorbing spectrophotometry extract solution.
Reagent and material：High purity water, Cyanidin -3-O- glucose glucosides standard items.
Using the content of the total anthocyanin of ultraviolet-ray visible absorbing spectrophotometry at the nm of maximum absorption wavelength 535.Flower
Color glycosides recovery rate is：
In formula：V is extract solution cumulative volume, mL；N is extension rate；M is the molecular weight of Cy-3-glu（449.2）；ε is Cy-3-
The extinction coefficient of glu, its value is 26900；M is the weight of raw material, unit g.
Sample detection：Above-mentioned health liquor mother liquor 1mL is taken, after the wine base with alcohol concentration as 45%vol dilutes 10 times, through purple
Outward-visible absorbance spectrophotometer detects the content of total anthocyanin.Functional component anthocyanin content is 76 in final measure mother liquor
µg/mL。
The above-mentioned rotated evaporator of health liquor mother liquor prepared functional component anthocyanin content concentrated under reduced pressure is no less than 50
The mulberry health care distiller's yeast concentrated liquor of mg/100mL.
By concentrate according to volume ratio be 1:100 ratio adds white wine original plasm wine, mixes, and is preserved under normal temperature.On demand
Blent, be modulated into the mulberry health care wine product that alcoholic strength is 10%vol.
Embodiment 2
The g of mulberries medicine materical crude slice 32 is taken, plus 25 times are measured wine base of the alcohol concentrations for 25%vol as solvent, are soaked 30 minutes at room temperature,
The rapid extraction of tissue crushing and active ingredient is completed using homogenate extraction technology synchronous high-efficiency, extract solution is centrifuged, institute
Obtain supernatant and be mulberry health care distiller's yeast liquid.The present embodiment carries out rapid extraction using flash extracter, using flash extracter
Carry out connective tissue it is broken while, complete the rapidly and efficiently extraction of functional component, obtain the extraction rich in anthocyanin type components
Liquid, is 4500r/min by flash extracter rotational speed regulation, and Extracting temperature is 30 DEG C of room temperature conditions, point 2 extractions, interval 2~3
Minute, extract 1~3 minute every time.Extract solution is with 2000~6000 r/min rotating speeds centrifugation 5~20 minutes, extract solution warp
After centrifugation removal slag, gained supernatant is mulberry health care distiller's yeast liquid.
Anthocyanin content detection method is with embodiment 1.
Sample detection：Above-mentioned health liquor mother liquor 1mL is taken, after the wine base with alcohol concentration as 55%vol dilutes 10 times, through purple
Outward-visible absorbance spectrophotometer detects the content of total anthocyanin.Functional component anthocyanin content is 71 in final measure mother liquor
µg/mL。
The above-mentioned rotated evaporator of health liquor mother liquor prepared functional component anthocyanin content concentrated under reduced pressure is no less than 50
The mulberry health care distiller's yeast concentrated liquor of mg/100ml.
By concentrate according to volume ratio be 2:100 ratio adds white wine original plasm wine, mixes, and is preserved under normal temperature.On demand
Blent, be modulated into the mulberry health care wine product that alcoholic strength is 32%vol.
Embodiment 3
The g of dry mulberries 22.8 is taken, plus 35 times are measured wine base of the alcohol concentrations for 35%vol as solvent, are soaked 40 minutes at room temperature,
The rapid extraction of tissue crushing and active ingredient is completed using homogenate extraction technology synchronous high-efficiency, extract solution is centrifuged, institute
Obtain supernatant and be mulberry health care distiller's yeast liquid.The present embodiment carries out rapid extraction using flash extracter, using flash extracter
Carry out connective tissue it is broken while, complete the rapidly and efficiently extraction of functional component, obtain the extraction rich in anthocyanin type components
Liquid, is 3500r/min by flash extracter rotational speed regulation, and Extracting temperature is 35 DEG C of room temperature conditions, point 3 extractions, interval 1~2
Minute, extract 1~3 minute every time.Extract solution is with 2000~6000 r/min rotating speeds centrifugation 5~20 minutes, extract solution warp
After centrifugation removal slag, gained supernatant is mulberry health care distiller's yeast liquid.
Anthocyanin content detection method is with embodiment 1.
Sample detection：Above-mentioned health liquor mother liquor 1mL is taken, after the wine base with alcohol concentration as 35%vol dilutes 10 times, through purple
Outward-visible absorbance spectrophotometer detects the content of total anthocyanin.Functional component anthocyanin content is 75 in final measure mother liquor
µg/mL。
The above-mentioned rotated evaporator of health liquor mother liquor prepared functional component anthocyanin content concentrated under reduced pressure is no less than 50
The mulberry health care distiller's yeast concentrated liquor of mg/100mL.
By concentrate according to volume ratio be 3:100 ratio adds white wine original plasm wine, mixes, and is preserved under normal temperature.On demand
Blent, be modulated into the mulberry health care wine product that alcoholic strength is 48 %vol.
Embodiment 4
The g of mulberries fresh fruit 40 is taken, plus 20 times are measured wine base of the alcohol concentrations for 40%vol as solvent, are soaked 30 minutes at room temperature,
The rapid extraction of tissue crushing and active ingredient is completed using homogenate extraction technology synchronous high-efficiency, extract solution is centrifuged, institute
Obtain supernatant and be mulberry health care distiller's yeast liquid.The present embodiment carries out rapid extraction using flash extracter, using flash extracter
Carry out connective tissue it is broken while, complete the rapidly and efficiently extraction of functional component, obtain the extraction rich in anthocyanin type components
Liquid, is 4000r/min by flash extracter rotational speed regulation, and Extracting temperature is 30 DEG C of room temperature conditions, point 2 extractions, interval 1~2
Minute, extract 1~3 minute every time.Extract solution is with 2000~6000 r/min rotating speeds centrifugation 5~20 minutes, extract solution warp
After centrifugation removal slag, gained supernatant is mulberry health care distiller's yeast liquid.
Anthocyanin content detection method is with embodiment 1.
Sample detection：Above-mentioned health liquor mother liquor 1mL is taken, after the wine base with alcohol concentration as 40%vol dilutes 10 times, through purple
Outward-visible absorbance spectrophotometer detects the content of total anthocyanin.Functional component anthocyanin content is 78 in final measure mother liquor
µg/mL。
The above-mentioned rotated evaporator of health liquor mother liquor prepared functional component anthocyanin content concentrated under reduced pressure is no less than 50
The mulberry health care distiller's yeast concentrated liquor of mg/100mL.
By concentrate according to volume ratio be 3:100 ratio adds white wine original plasm wine, mixes, and is preserved under normal temperature.On demand
Blent, be modulated into the mulberry health care wine product that alcoholic strength is 42 %vol.
Claims (10)
1. a kind of fast preparation method of mulberry health care wine, it is characterized in that comprising the following steps：
1）Soaked during mulberries are added into wine base solvent, mulberries are 1 with the solid-liquid mass ratio of wine base solvent:10~1:50；
2）Application homogenate extraction technology carries out rapid extraction after immersion, obtains the extract solution rich in anthocyanin type components, extract solution
It is centrifuged removing slag, gained supernatant is mulberry health care distiller's yeast liquid；
3）Concentrate of the Anthocyanin content no less than 50 mg/100mL will be obtained after above-mentioned mother liquor concentrations；
4）By above-mentioned concentrate and white spirit mixing, mulberry health care wine product is modulated into.
2. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that the alcoholic strength of the wine base is
10~60%vol.
3. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that the immersion, its soak time
It is 0.5-1 hours.
4. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that the mulberries are mulberries fresh fruit
Or dry mulberries or medicinal mulberries medicine materical crude slice.
5. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that the rapid extraction refer to
2~3 extractions are completed in 10 minutes, is extracted 1~3 minute every time.
6. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that the carrying during rapid extraction
Temperature is taken for 20~50 DEG C.
7. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that the application homogenate extraction skill
Art is to use flash extracter；The rotating speed of the flash extracter is 3000~5000 r/min；The extract solution with 2000~
6000 r/min rotating speeds centrifugations 5~20 minutes.
8. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that the concentration is steamed using rotation
Hair device is concentrated under reduced pressure.
9. the fast preparation method of mulberry health care wine according to claim 1, it is characterized in that described blending is by concentrate
With white wine by volume 1~3:100 ratio is mixed, and is modulated into the mulberry health care wine that alcoholic strength is 10~50%vol and is produced
Product.
10. a kind of mulberry health care wine, it is characterized in that the health liquor obtained according to any methods described of claim 1~9.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611252114.0A CN106701482A (en) | 2016-12-30 | 2016-12-30 | Rapid preparation method of healthcare mulberry wine |
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| CN201611252114.0A CN106701482A (en) | 2016-12-30 | 2016-12-30 | Rapid preparation method of healthcare mulberry wine |
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ID=58906129
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101314753A (en) * | 2008-07-03 | 2008-12-03 | 王跃进 | Method for preparing brandy fruit wine with mulberry |
| CN101319185A (en) * | 2007-06-05 | 2008-12-10 | 王晓明 | Colorful white spirit and preparation method thereof |
| CN101366523A (en) * | 2008-10-15 | 2009-02-18 | 张志超 | Health-care medicinal liquor and its preparing process |
| CN101735927A (en) * | 2009-12-30 | 2010-06-16 | 四川南充市丝绸(进出口)有限公司 | Method for producing mulberry fruit wine |
| CN104189088A (en) * | 2014-08-13 | 2014-12-10 | 河南中医学院 | Application of mulberry fruit extract in preparation of hypoglycaemic agent |
| CN105254609A (en) * | 2015-11-27 | 2016-01-20 | 江苏万村爱农农业科技有限公司 | Blueberry anthocyanin extracting method |
| CN105524036A (en) * | 2016-01-12 | 2016-04-27 | 北京宝得瑞健康产业有限公司 | High-efficiency low-consumption grape seed procyanidine extraction method |
| CN105533760A (en) * | 2015-12-09 | 2016-05-04 | 重庆三零三科技有限公司 | Preparation of mulberry pomace water-soluble dietary fiber |
-
2016
- 2016-12-30 CN CN201611252114.0A patent/CN106701482A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101319185A (en) * | 2007-06-05 | 2008-12-10 | 王晓明 | Colorful white spirit and preparation method thereof |
| CN101314753A (en) * | 2008-07-03 | 2008-12-03 | 王跃进 | Method for preparing brandy fruit wine with mulberry |
| CN101366523A (en) * | 2008-10-15 | 2009-02-18 | 张志超 | Health-care medicinal liquor and its preparing process |
| CN101735927A (en) * | 2009-12-30 | 2010-06-16 | 四川南充市丝绸(进出口)有限公司 | Method for producing mulberry fruit wine |
| CN104189088A (en) * | 2014-08-13 | 2014-12-10 | 河南中医学院 | Application of mulberry fruit extract in preparation of hypoglycaemic agent |
| CN105254609A (en) * | 2015-11-27 | 2016-01-20 | 江苏万村爱农农业科技有限公司 | Blueberry anthocyanin extracting method |
| CN105533760A (en) * | 2015-12-09 | 2016-05-04 | 重庆三零三科技有限公司 | Preparation of mulberry pomace water-soluble dietary fiber |
| CN105524036A (en) * | 2016-01-12 | 2016-04-27 | 北京宝得瑞健康产业有限公司 | High-efficiency low-consumption grape seed procyanidine extraction method |
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Application publication date: 20170524 |