CN106666737A - Method for preparing common sage herb healthcare electuary - Google Patents

Method for preparing common sage herb healthcare electuary Download PDF

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Publication number
CN106666737A
CN106666737A CN201611028059.7A CN201611028059A CN106666737A CN 106666737 A CN106666737 A CN 106666737A CN 201611028059 A CN201611028059 A CN 201611028059A CN 106666737 A CN106666737 A CN 106666737A
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CN
China
Prior art keywords
electuary
bufo siccuss
preparation
sage herb
extract
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611028059.7A
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Chinese (zh)
Inventor
张辉
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Bengbu City Tu Greenhome Vegetable Cooperatives Research
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Bengbu City Tu Greenhome Vegetable Cooperatives Research
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Application filed by Bengbu City Tu Greenhome Vegetable Cooperatives Research filed Critical Bengbu City Tu Greenhome Vegetable Cooperatives Research
Priority to CN201611028059.7A priority Critical patent/CN106666737A/en
Publication of CN106666737A publication Critical patent/CN106666737A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention relates to the field of healthcare tea product making, and discloses a method for preparing a common sage herb healthcare electuary. The common sage herb healthcare electuary is prepared from the following raw materials: common sage herb, pearl powder, citric acid and corn dextrin. The method comprises the following steps: performing superfine crushing on the common sage herb so as to obtain a powder structure of which the particle size is 50-100 nanometers; performing a supercritical carbon dioxide extraction method to extract liposoluble constituents, performing water solution extraction on the obtained solid extract so as to obtain a water soluble extract, mixing a liquid extract with the water soluble extract, adding stevioside and the corn dextrin, and performing a dry-method pelleting process, so as to obtain granules, that is, the common sage herb healthcare electuary. The common sage herb healthcare electuary has the advantages that due to the adoption of techniques of superfine crushing and supercritical carbon dioxide method extraction, small crushed particles can be obtained, lipsoluble and water soluble substances can be extracted, the nutrient components of the common sage herb are greatly utilized, the electuary is sour, sweet and palatable due to other substances, a great number of substances beneficial to human bodies can be replenished, and the electuary is a drink which is convenient to take and has good healthcare effects.

Description

A kind of preparation method of Bufo siccuss grass health instant powder
Technical field
The present invention relates to the making field of health care tea, and in particular to a kind of preparation method of Bufo siccuss grass health instant powder.
Technical background
In recent years, with the continuous improvement of people's living standard, health care consciousness also gradually strengthens, and increasing people are Jing is unsatisfactory for effect that original ordinary tea leaves have, a collection of using the original with special health-care effect so as to emerge in succession Material, processed to make as ordinary tea leaves shape, drinking method identical tea.Bufo siccuss grass has special work(as a kind of to body The plant of effect, is fabricated to Folium Camelliae sinensis by people and drinks, but the mode of this boiled water brewing tea, do not make human body complete Whole nutritional labelings of Bufo siccuss grass Folium Camelliae sinensis are absorbed, some insoluble or refractory components are all resided in tea grounds, significantly in a large number Nutrition and the health care of Bufo siccuss grass is have impact on, the present invention utilizes the side that micronizing and supercritical carbon dioxide extraction method are combined Method makes a kind of health instant powder Bufo siccuss grass, makes powder granule less than 100 nanometers, the complete nutrients matter in Bufo siccuss grass be easy to by Human body the intestines and stomach directly absorbs.
The content of the invention
It is an object of the invention to provide a kind of preparation method of Bufo siccuss grass health instant powder.
The present invention is achieved by the following technical solutions:
A kind of preparation method of Bufo siccuss grass health instant powder, is made up of following raw material:Bufo siccuss grass, Margarita powder, citric acid, stevioside, Corn dextrin.
Including following step:
(1)The Bufo siccuss blade of grass that high-quality is dried is chosen, it is 50-100 nanometers microgranule to be crushed to super micron mill, crush temperature control At 20-30 degree Celsius;
(2)Bufo siccuss grass meal end after crushing is carried out into supercritical carbon dioxide process extraction, isolated solid extraction thing and liquid Solid extraction thing is obtained water-soluble extracting solution using water soluble method, then through centrifugation, filtration, is concentrated under reduced pressure to give solvable by extract Property solid concentrate;
(3)Above-mentioned solid concentrate is mixed with fluid extraction thing, stevioside, corn dextrin is added, is dried, sieves, does Method pelletize, vacuum packaging, gets product
Preferably, supercritical carbon dioxide process extracting pressure is 20-25Mpa, and extraction temperature is 30-35 degree Celsius, separating pressure For 5-10Mpa, separation temperature is 40-45 degree Celsius.
Above-mentioned solid extraction thing using the process that water soluble method obtains water-soluble extracting solution is:It is which to add in solid extraction thing The hot water that 15~20 times of weight, temperature are 65~75 degrees Celsius, then add Margarita powder, citric acid, and insulated and stirred 2~3 is little When, water-soluble extracting solution is separated to obtain with 200 mesh sieves.
Preferably, add Margarita powder amount be mix rear solution weight 0.01-0.03%, add citric acid amount be The 0.5-1.0% of mixing rear solution weight.
Preferably, the centrifugation, the rotating speed for filtering are 8000~40000rpm.
Preferably, the mixed extract of the solid concentrate and fluid extraction thing and stevioside, the addition of corn dextrin Ratio is:Extract 70~80%, sucrose 5~10%, corn dextrin 15~20%.
Preferably, described dry employing is vacuum dried, and is allowed to moisture and reaches 3~6%, vacuum drying process temperature For 60~65 degrees Celsius, vacuum is -0.06Mpa~-0.08Mpa, 3~4 hours drying times.
Preferably, described pelletize is to crush dried mixture, cross 50 mesh sieves using dry granulation, and mixes equal It is even, pelletized with dry granulating machine, 1.0~1.2mm of particle diameter, 1.5~1.8mm of length.
Beneficial effects of the present invention:It is an advantage of the current invention that using micronizing and supercritical carbon dioxide process extraction skill Art, crushing microgranule are little, are extracted fat-soluble and water-soluble substanceses, greatly make use of the nutritional labeling of Bufo siccuss grass, with common side Method is compared, and the protocatechuic acid for utilizing that is absorbed by the body improves 23%, Homoplantaginin and improves 17%, Buddhist nun pool flavonoid glycoside raising 34%, cuneus Euparin improves 25%, and the Margarita powder of addition supplements 18 kinds of aminoacid and a large amount of calcium of needed by human body, and the citric acid of addition not only changes It has been apt to the taste of electuary, and has made insoluble calcium in Margarita powder become solubility calcium be absorbed by the body, the stevioside sugariness of addition 200-300 times of common sucrose, calorific value is but one of three percentages of sucrose, saves cost, be highly suitable for again diabetes, Obesity, arteriosclerotic use, and are the beverages of a great health-care effect conveniently drunk.
Specific embodiment:
Embodiment 1
A kind of preparation method of Bufo siccuss grass health instant powder, is made up of following raw material:Bufo siccuss grass, Margarita powder, citric acid, stevioside, Corn dextrin.
Including following step:
(1)The Bufo siccuss blade of grass that high-quality is dried is chosen, it is 50-100 nanometers microgranule to be crushed to super micron mill, crush temperature control At 20-30 degree Celsius;
(2)Bufo siccuss grass meal end after crushing is carried out into supercritical carbon dioxide process extraction, isolated solid extraction thing and liquid Solid extraction thing is obtained water-soluble extracting solution using water soluble method, then through centrifugation, filtration, is concentrated under reduced pressure to give solvable by extract Property solid concentrate;
(3)Above-mentioned solid concentrate is mixed with fluid extraction thing, stevioside, corn dextrin is added, is dried, sieves, does Method pelletize, vacuum packaging, gets product
Preferably, supercritical carbon dioxide process extracting pressure is 20Mpa, and extraction temperature is 30 degrees Celsius, and separating pressure is 5Mpa, Separation temperature is 40 degrees Celsius.
Above-mentioned solid extraction thing using the process that water soluble method obtains water-soluble extracting solution is:It is which to add in solid extraction thing The hot water that 15 times of weight, temperature are 65 degrees Celsius, then add Margarita powder, citric acid, and insulated and stirred 2 hours uses 200 mesh sieves Separate to obtain water-soluble extracting solution.
Preferably, the amount for adding Margarita powder is mix rear solution weight 0.01%, after adding the amount of citric acid to be mixing The 0.5% of aqueous solution weight.
Preferably, the centrifugation, the rotating speed for filtering are 8000~40000rpm.
Preferably, the mixed extract of the solid concentrate and fluid extraction thing and stevioside, the addition of corn dextrin Ratio is:Extract 70%, sucrose 5%, corn dextrin 15%.
Preferably, described dry employing is vacuum dried, and is allowed to moisture and reaches 3%, and vacuum drying process temperature is 60 Degree Celsius, vacuum be -0.06MpaMpa, 3 hours drying times.
Preferably, described pelletize is to crush dried mixture, cross 50 mesh sieves using dry granulation, and mixes equal It is even, pelletized with dry granulating machine, 1.0~1.2mm of particle diameter, 1.5~1.8mm of length.
Embodiment 2
A kind of preparation method of Bufo siccuss grass health instant powder, is made up of following raw material:Bufo siccuss grass, Margarita powder, citric acid, stevioside, Corn dextrin.
Including following step:
(1)The Bufo siccuss blade of grass that high-quality is dried is chosen, it is 50-100 nanometers microgranule to be crushed to super micron mill, crush temperature control At 20-30 degree Celsius;
(2)Bufo siccuss grass meal end after crushing is carried out into supercritical carbon dioxide process extraction, isolated solid extraction thing and liquid Solid extraction thing is obtained water-soluble extracting solution using water soluble method, then through centrifugation, filtration, is concentrated under reduced pressure to give solvable by extract Property solid concentrate;
(3)Above-mentioned solid concentrate is mixed with fluid extraction thing, stevioside, corn dextrin is added, is dried, sieves, does Method pelletize, vacuum packaging, gets product
Preferably, supercritical carbon dioxide process extracting pressure is 25Mpa, and extraction temperature is 35 degrees Celsius, and separating pressure is 10Mpa, separation temperature are 45 degrees Celsius.
Above-mentioned solid extraction thing using the process that water soluble method obtains water-soluble extracting solution is:It is which to add in solid extraction thing The hot water that 20 times of weight, temperature are 75 degrees Celsius, then add Margarita powder, citric acid, and insulated and stirred 3 hours uses 200 mesh sieves Separate to obtain water-soluble extracting solution.
Preferably, the amount for adding Margarita powder is mix rear solution weight 0.03%, after adding the amount of citric acid to be mixing The 1.0% of aqueous solution weight.
Preferably, the centrifugation, the rotating speed for filtering are 8000~40000rpm.
Preferably, the mixed extract of the solid concentrate and fluid extraction thing and stevioside, the addition of corn dextrin Ratio is:Extract 80%, sucrose 10%, corn dextrin 20%.
Preferably, described dry employing is vacuum dried, and is allowed to moisture and reaches 6%, and vacuum drying process temperature is 65 Degree Celsius, vacuum be -0.08Mpa, 4 hours drying times.
Preferably, described pelletize is to crush dried mixture, cross 50 mesh sieves using dry granulation, and mixes equal It is even, pelletized with dry granulating machine, 1.0~1.2mm of particle diameter, 1.5~1.8mm of length.
Comparative example 1
By the Bufo siccuss of isodose grass through dry in sun, complete, knead, drying is fabricated to Folium Camelliae sinensis.
Comparative example 2
Electuary is fabricated to by prior art using the Bufo siccuss grass of isodose.
The product obtained in embodiment and comparative example, the composition for extracting its beneficial human body are contrasted, as a result such as following table, its In the amount of each composition be raising amount on the basis of comparative example 1:
Project Protocatechuic acid(%) Homoplantaginin(%) Buddhist nun moors flavonoid glycoside(%) Eupacunin(%) Calcium(%)
Embodiment 1 76 68 73 74 46
Embodiment 2 75 69 72 76 47
Comparative example 1 / / / / /
Comparative example 2 32 28 34 35 /
By form it can be seen that the Bufo siccuss grass electuary obtained using the inventive method, the content of each effective ingredient is all higher than existing Technology, greatly make use of the beneficial value of Bufo siccuss grass, and the invention can also supplement the calcium and various aminoacid of human body needs.

Claims (8)

1. the preparation method of a kind of Bufo siccuss grass health instant powder, it is characterised in that be made up of following raw material:Bufo siccuss grass, Margarita powder, lemon Lemon acid, stevioside, corn dextrin;Preparation method includes following step:
(1)The Bufo siccuss blade of grass that high-quality is dried is chosen, it is 50-100 nanometers microgranule to be crushed to super micron mill, crush temperature control At 20-30 degree Celsius;
(2)Bufo siccuss grass meal end after crushing is carried out into supercritical carbon dioxide process extraction, isolated solid extraction thing and liquid Solid extraction thing is obtained water-soluble extracting solution using water soluble method, then through centrifugation, filtration, is concentrated under reduced pressure to give solvable by extract Property solid concentrate;
(3)Above-mentioned solid concentrate is mixed with fluid extraction thing, stevioside, corn dextrin is added, is dried, sieves, does Method pelletize, vacuum packaging, gets product.
2. a kind of preparation method of Bufo siccuss grass health instant powder according to claim 1, it is characterised in that supercritical titanium dioxide Carbon method extracting pressure is 20-25Mpa, and extraction temperature is 30-35 degree Celsius, and separating pressure is 5-10Mpa, and separation temperature is 40- 45 degrees Celsius.
3. a kind of preparation method of Bufo siccuss grass health instant powder according to claim 1, it is characterised in that solid extraction thing profit The process that water-soluble extracting solution is obtained with water soluble method is:In solid extraction thing add be 15~20 times of its weight hot water, temperature For 65~75 degrees Celsius, Margarita powder, citric acid are then added, insulated and stirred 2~3 hours separates water-soluble to carry with 200 mesh sieves Take liquid.
4. the preparation method of the careless health instant powder of a kind of Bufo siccuss according to claim 1,2 or 3, it is characterised in that add precious The amount of pearl powder is the 0.01-0.03% for mixing rear solution weight, and the amount for adding citric acid is the 0.5- for mixing rear solution weight 1.0%。
5. the preparation method of a kind of Bufo siccuss grass health instant powder according to claim 4, it is characterised in that the centrifugation, mistake The rotating speed of filter is 8000~40000rpm.
6. according to a kind of preparation method of the Bufo siccuss grass health instant powder described in claim 4, it is characterised in that the solid concentration Thing with the mixed extract of fluid extraction thing with the adding proportion of stevioside, corn dextrin is:Extract 70~80%, sucrose 5~ 10%, corn dextrin 15~20%.
7. according to a kind of preparation method of the Bufo siccuss grass health instant powder described in claim 6, it is characterised in that described drying is adopted With vacuum drying, be allowed to moisture and reach 3~6%, vacuum drying process temperature is 60~65 degrees Celsius, vacuum for- 0.06Mpa~-0.08Mpa, 3~4 hours drying times.
8. according to a kind of preparation method of the Bufo siccuss grass health instant powder described in claim 7, it is characterised in that described pelletize It is that dried mixture is crushed, 50 mesh sieves, and mix homogeneously is crossed using dry granulation, is pelletized with dry granulating machine, 1.0~1.2mm of particle diameter, 1.5~1.8mm of length.
CN201611028059.7A 2016-11-22 2016-11-22 Method for preparing common sage herb healthcare electuary Pending CN106666737A (en)

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Application Number Priority Date Filing Date Title
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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1895282A (en) * 2005-07-15 2007-01-17 上海高博特微生态研究所有限公司 Calcium supplementary agent and its preparation
CN102240035A (en) * 2011-05-27 2011-11-16 银川泰丰生物科技有限公司 Method for preparing wolfberry extract health-care granules
CN104824257A (en) * 2015-04-09 2015-08-12 安徽省新旭堂茶业有限公司 Diuresis health protection tea capable of eliminating humidity and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1895282A (en) * 2005-07-15 2007-01-17 上海高博特微生态研究所有限公司 Calcium supplementary agent and its preparation
CN102240035A (en) * 2011-05-27 2011-11-16 银川泰丰生物科技有限公司 Method for preparing wolfberry extract health-care granules
CN104824257A (en) * 2015-04-09 2015-08-12 安徽省新旭堂茶业有限公司 Diuresis health protection tea capable of eliminating humidity and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
张彤等: "车前草配方颗粒与其饮片的利尿药效比较研究", 《中国医药指南》 *
张彤等: "车前草配方颗粒正交提取工艺的研究", 《亚太传统医药》 *

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