CN106665637A - Mixture containing trifloxystrobin and blastidin - Google Patents
Mixture containing trifloxystrobin and blastidin Download PDFInfo
- Publication number
- CN106665637A CN106665637A CN201611219856.3A CN201611219856A CN106665637A CN 106665637 A CN106665637 A CN 106665637A CN 201611219856 A CN201611219856 A CN 201611219856A CN 106665637 A CN106665637 A CN 106665637A
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- Prior art keywords
- trifloxystrobin
- blasticidin
- weight ratio
- mixture
- effect
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
- A01N47/44—Guanidine; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
- A01N37/50—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids the nitrogen atom being doubly bound to the carbon skeleton
Abstract
The invention relates to a mixture containing trifloxystrobin and blastidin. The effective ingredients are composed of trifloxystrobin, binapacryl and blastidin at a weight ratio of (10-15):(5-8):(5-8). The mixture is obvious in field control effect, can quickly become effective, has a stable system and has a long-lasting pesticide effect; the dosing times can be reduced; the cost can be lowered; the fast-acting property of the mixture is excellent; on the seventh day after application, the control effect is optimal as high as 93.6% and is obviously higher than that of a contrast example.
Description
Technical field
The present invention relates to a kind of fungicide mixture, specifically a kind of mixture containing trifloxystrobin and blasticidin-Ss.
Background technology
Trifloxystrobin, chemical name：2- sec-butyl -4,6- dinitrophenyl -3- methyl butene acid esters is a kind of brown, have light
The solid of micro- aromatic odor, it is water insoluble, it is dissolved in most organic solvents.Trifloxystrobin is non-internal-absorting acaricide, has speed to mite class
Effect act on, it is effective to each stage of ovum, larva, old worm, Apiss etc. are picked flowers insecticide and natural enemy it is harmless, have lasting effect, it is right
Resistance mite class is also effective.It is effective to powdery mildew as antibacterial, it is mainly used in preventing and treating the mite class on Fructus Mali pumilae, pears, impression and Cotton Gossypii
And powdery mildew, concentration 0.025%~0.05% (effective ingredient).There are some poisoning to immature Fructus Lycopersici esculenti, Fructus Vitis viniferae and Flos Rosae Rugosae.
The disabling phase is 60 days before harvesting.
Blasticidin-Ss are called " powder for curing rice blast " " Bradley leaf this ", are the antibiotic extracted in a kind of bacteria culture fluid from unwrapping wire,
It is generally used for preventing and treating rice blast, Helminthosporium of brown spot of rice, Oryza sativa L. sclerotiniose etc..The growth of yeast and mycete can be suppressed.Agriculturally
Using be blasticidin-Ss sulfate and lauric acid sulfate.To Fish avirulence, it is mainly used to prevent and treat rice blast and pole
Hair bar belongs to microbial disease.Blasticidin-Ss also have certain prevention effect to water rice brown spot and sclerotium oryzicola, to water
The infection rate of cercosporiosis of rice viral disease also has reduction to act on, and when concentration is more than 40mg/L, poisoning easily occurs.It is mainly used in preventing and treating
Rice blast, including Seedling rice blast, leaf pestilence, panicle blast etc., also there is certain preventive effect to water rice brown spot and sclerotium oryzicola, also
The infection rate of rice stripe disease can be reduced.It is harmless to crop with 1% wettable powder, 250~500 times of liquid sprayings.Send out in rice shoot
When before disease to first meeting scab, sprayed 1~2 time with 2% cream, 500~1 000 times of liquid stem and leaf, per minor tick 7 days or so.
Binapacryl class wide-spectrum bactericide be from natural product Strobilurins as antibacterial lead compound successfully
The new fungicides of one class of exploitation.With efficient, wide spectrum, protection, treat, root out, permeating, systemic activity, resistance to rainwater punching
The characteristics such as brush, lasting period length.To nearly all Mycophytes (Ascomycetes, Basidiomycetess, Oomycete and Fungi Imperfecti), disease is such as
Powdery mildew, rust, Ying's rot, net blotch, downy mildew, rice blast etc. have good activity.Except having spy to powdery mildew, leaf spot
Effect is outer, has good activity to rust, downy mildew, damping-off, Fructus Mali pumilae apple scab, sclerotinia rot of colza.To crop safety, because its
Soil, it is capable of being fast degraded in water, thus it is environmentally safe.Because binapacryl has the performances such as wide spectrum, infiltration, quick distribution, crop
Absorb it is fast, in addition its there is absorbability upwards, therefore resistance of rainwater washing against performance is good, the lasting period is long, therefore is considered as the second filial generation
Methoxy acrylic bactericide.Binapacryl protection activity is excellent, and with certain therapeutic activity, and activity does not receive environment
Affect, be spore germination and their early stage stage using optimal period, but to scab, each period is active.
The content of the invention
The present invention is directed to the deficiencies in the prior art, there is provided a kind of mixture containing trifloxystrobin and blasticidin-Ss.
To achieve these goals, present invention employs technical scheme below：
A kind of mixture containing trifloxystrobin and blasticidin-Ss, effective ingredient is by trifloxystrobin, binapacryl and blasticidin-Ss according to weight
Amount ratio 10~15:5~8:5~8 compounding compositions.
Used as the preferred embodiment of the present invention, the trifloxystrobin, binapacryl, the weight ratio of blasticidin-Ss are the ︰ 6 of 12 ︰ 7,
Under this proportioning, its disinfection and deinsectization best results.
When finished product is prepared, following adjuvant can be selected：
The mixture containing trifloxystrobin and blasticidin-Ss：Percentage by weight is 5~15%；
Dispersant：Percentage by weight be 5~15%, the dispersant be triethyl group hexyl phosphoric acid, sodium lauryl sulphate,
Cellulose derivative and one or more of fatty acid polyethylene glycol ester.
Auxiliary agent：Percentage by weight is 10~25%, and the auxiliary agent is ethylenediaminetetraacetic acid, lignosulfonates, polycarboxylic acids
One or more of salt and alkylnaphthalene sulfonate formaldehyde condensation products.
Water：Surplus.
Compared with prior art, the beneficial effect that the present invention possesses：
Significantly, rapid-action, stable system, lasting medicine can reduce times for spraying to the field control effect of the present invention, reduce
Cost, illustrates the quick-acting of built agent very well, and in dispenser the 7th day, its prevention effect reached most preferably, reaches as high as 93.6%, than
Comparative example is significantly improved.
Specific embodiment
Embodiment 1
It is made up of the component of following percentage by weight meter：8%, 13% point of the mixture of trifloxystrobin of the present invention and blasticidin-Ss
Powder, 18% auxiliary agent, surplus are supplemented by water.
Mixture according to weight ratio meter, trifloxystrobin of the present invention and blasticidin-Ss includes following component：Wo Jun Zhi ︰ pleasures are killed
The ︰ 6 of Man ︰ blasticidin-Ss=12 ︰ 7；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and cellulose derivative for 5 ︰ 5；
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and lignosulfonates for 4 ︰ 5；
Preparation method：By trifloxystrobin, binapacryl, blasticidin-Ss, triethyl group hexyl phosphoric acid, cellulose derivative, ethylenediamine tetraacetic
Acetic acid and lignosulfonates add water in container, stir, and obtain the mixture of trifloxystrobin and blasticidin-Ss.
Embodiment 2
It is made up of the component of following percentage by weight meter：5%, 15% point of the mixture of trifloxystrobin of the present invention and blasticidin-Ss
Powder, 25% auxiliary agent, surplus are supplemented by water.
Mixture according to weight ratio meter, trifloxystrobin of the present invention and blasticidin-Ss includes following component：Wo Jun Zhi ︰ pleasures are killed
The ︰ 7 of Man ︰ blasticidin-Ss=15 ︰ 8；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and sodium lauryl sulphate for 5 ︰ 5
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and polycarboxylate for 4 ︰ 5
Preparation method is with embodiment 1.
Embodiment 3
It is made up of the component of following percentage by weight meter：The mixture 15%, 15% of trifloxystrobin of the present invention and blasticidin-Ss
Dispersant, 10 auxiliary agents, surplus are supplemented by water.
Mixture according to weight ratio meter, trifloxystrobin of the present invention and blasticidin-Ss includes following component：Wo Jun Zhi ︰ pleasures are killed
The ︰ 8 of Man ︰ blasticidin-Ss=13 ︰ 5；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and fatty acid polyethylene glycol ester for 5 ︰ 5；
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and alkylnaphthalene sulfonate formaldehyde condensation products for 4 ︰ 5；
Preparation method is with embodiment 1.
Embodiment 4
It is made up of the component of following percentage by weight meter：5%, 12% point of the mixture of trifloxystrobin of the present invention and blasticidin-Ss
Powder, 10% auxiliary agent, surplus are supplemented by water.
Mixture according to weight ratio meter, trifloxystrobin of the present invention and blasticidin-Ss includes following component：Wo Jun Zhi ︰ pleasures are killed
The ︰ 5 of Man ︰ blasticidin-Ss=14 ︰ 7；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and sodium lauryl sulphate for 5 ︰ 4；
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and alkylnaphthalene sulfonate formaldehyde condensation products for 5 ︰ 5；
Preparation method is with embodiment 1.
Embodiment 5
It is made up of the component of following percentage by weight meter：8%, 8% point of the mixture of trifloxystrobin of the present invention and blasticidin-Ss
Powder, 15% auxiliary agent, surplus are supplemented by water.
Mixture according to weight ratio meter, trifloxystrobin of the present invention and blasticidin-Ss includes following component：Wo Jun Zhi ︰ pleasures are killed
The ︰ 7 of Man ︰ blasticidin-Ss=11 ︰ 8；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and sodium lauryl sulphate for 4 ︰ 5；
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and lignosulfonates for 3 ︰ 5；
Preparation method is with embodiment 1.
Embodiment 6
It is made up of the component of following percentage by weight meter：8%, 12% point of the mixture of trifloxystrobin of the present invention and blasticidin-Ss
Powder, 20% auxiliary agent, surplus are supplemented by water.
Mixture according to weight ratio meter, trifloxystrobin of the present invention and blasticidin-Ss includes following component：Wo Jun Zhi ︰ pleasures are killed
The ︰ 6 of Man ︰ blasticidin-Ss=10 ︰ 8；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and cellulose derivative for 5 ︰ 5；
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and lignosulfonates for 4 ︰ 5；
Preparation method is with embodiment 1.
Comparative example 1
It is made up of the component of following percentage by weight meter：Effective ingredient 8%, 8% dispersant, 15% auxiliary agent, surplus are by water
Supplement.
According to weight ratio meter, this comparative example effective ingredient includes following component：The happy ︰ of Sha Man ︰ blasticidin-Ss=12 ︰ 3 of Wo Jun Zhi ︰
20；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and cellulose derivative for 5 ︰ 5；
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and lignosulfonates for 4 ︰ 5；
Preparation method is with reference to embodiment 1.
The mixture of the trifloxystrobin of comparative example 2 and blasticidin-Ss
It is made up of the component of following percentage by weight meter：The mixture 15%, 15% of trifloxystrobin of the present invention and blasticidin-Ss
Dispersant, 25% auxiliary agent, surplus are supplemented by water.
According to weight ratio meter, this comparative example effective ingredient includes following component：The happy ︰ of Sha Man ︰ blasticidin-Ss=12 ︰ 0 of Wo Jun Zhi ︰
7；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and sodium lauryl sulphate for 5 ︰ 5；
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and lignosulfonates for 5 ︰ 4；
Preparation method is with reference to embodiment 1.
Comparative example 3
It is made up of the component of following percentage by weight meter：Effective ingredient 5%, 5% dispersant, 10% auxiliary agent, surplus are by water
Supplement.
According to weight ratio meter, this comparative example effective ingredient includes following component：The happy ︰ of Sha Man ︰ blasticidin-Ss=12 ︰ 6 of Wo Jun Zhi ︰
0；
Dispersant is made up of according to weight ratio triethyl group hexyl phosphoric acid and sodium lauryl sulphate for 5 ︰ 5
Auxiliary agent is made up of according to weight ratio ethylenediaminetetraacetic acid and lignosulfonates for 5 ︰ 5；
Preparation method is with reference to embodiment 1.
By embodiment 1~6, mixture obtained in comparative example 1~3, the sterilization applied to the field of apple tree white lead fungus diseases
Effect is tested.
(1) test method：
Select one piece of apple cultivation ground as experimental plot, wherein apple tree growing way is identical, and apple leaf is endangered by powdery mildew
Uniformly, it is 10 little sections by field division, wherein 9 small pieces areas apply respectively the mixed of embodiment 1~6 and comparative example 1~3
Agent, mixture is diluted 5000 times and afterwards apple tree is administered by the way of spraying, and remaining little section is used as blank.
Dispenser three times during test, carry out the investigation of state of an illness radix before first time dispenser, applied for the second time within 7 days after first time dispenser
Medicine, carries out third time dispenser in 10 days after second dispenser, institutes an inquiry pesticide supplying effect within 7 days after third time dispenser.
Investigation method is that every cell takes at random 5 points of investigation, and per is looked into four section apple trees, randomly select during investigation 20 it is long
Gesture is identical, and leaf area size identical blade is marked, the incidence observed before and after mark blade dispenser.Scab is pressed per blade
The percentage rate classification of leaf area, record total number of sheets, the sick number of sheets and sick level are accounted for, the grade scale of disease index is：
It is 0 grade, disease-free；
1 grade, lesion area accounts for less than the 5% of full wafer leaf area；
3 grades, lesion area accounts for the 6%~15% of full wafer leaf area；
5 grades, lesion area accounts for the 16%~35% of full wafer leaf area；
7 grades, lesion area accounts for the 36%~50% of full wafer leaf area；
9 grades, lesion area accounts for more than the 50% of full wafer leaf area.
Disease index investigation before three times, i.e. medicine is investigated altogether in test, the 7th day and the 15th day investigation state of an illness refers to after third time medicine
Number, according to following calculating preventive effect：
(2) bactericidal effect result and analysis, as shown in table 1 to the field control result of Fructus Mali pumilae powdery mildew.
Each embodiment of table 1 and comparative example prevent and treat result to Fructus Mali pumilae powdery mildew
The embodiment of the present invention 1~6 prevent and treat Fructus Mali pumilae powdery mildew effect is significant, 7 days after medication, 15 days highest preventive effects be
89.56%, illustrate the field control effect of the present invention significantly, rapid-action, stable system, lasting medicine can reduce times for spraying,
Reduces cost, illustrates the quick-acting of built agent very well, and in dispenser the 7th day, its prevention effect reached most preferably, reaches as high as
89.56%, it is significantly improved than comparative example, in dispenser the 15th day, built agent remained to keep higher bactericidal effect, shows this
Built agent has very high lasting effect.With the preventive effect highest of embodiment 1 in embodiments of the invention, each component of embodiment 1 is illustrated
Preferably, the drug effect of effective ingredient is able to fully persistently play synergistic action effect.Composition pesticide described in comparative example 1~3 with
Embodiment is compared, and it lacks some components or Ingredient Wt ratio differs more with more excellent proportioning, and its preventive effect is greatly reduced, further
The each component synergism of the embodiment of the present invention 1 is illustrated, each component is indispensable, if lack some components can cause under effect
Drop.
Claims (1)
1. a kind of mixture containing trifloxystrobin and blasticidin-Ss, it is characterised in that effective ingredient is by trifloxystrobin, binapacryl and pestilence of going out
Element is according to weight than 10~15:5~8:5~8 compounding compositions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611219856.3A CN106665637A (en) | 2016-12-26 | 2016-12-26 | Mixture containing trifloxystrobin and blastidin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611219856.3A CN106665637A (en) | 2016-12-26 | 2016-12-26 | Mixture containing trifloxystrobin and blastidin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106665637A true CN106665637A (en) | 2017-05-17 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611219856.3A Withdrawn CN106665637A (en) | 2016-12-26 | 2016-12-26 | Mixture containing trifloxystrobin and blastidin |
Country Status (1)
| Country | Link |
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| CN (1) | CN106665637A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101836635A (en) * | 2010-01-08 | 2010-09-22 | 深圳诺普信农化股份有限公司 | Antiseptic composition waterborne preparation and method for preparing same |
| CN102578130A (en) * | 2007-10-09 | 2012-07-18 | 中国中化股份有限公司 | Fungicidal composition |
-
2016
- 2016-12-26 CN CN201611219856.3A patent/CN106665637A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102578130A (en) * | 2007-10-09 | 2012-07-18 | 中国中化股份有限公司 | Fungicidal composition |
| CN101836635A (en) * | 2010-01-08 | 2010-09-22 | 深圳诺普信农化股份有限公司 | Antiseptic composition waterborne preparation and method for preparing same |
Non-Patent Citations (1)
| Title |
|---|
| 赵日瑾: "新型杀螨剂——乐杀螨", 《新农业》 * |
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Application publication date: 20170517 |