CN106635502A - Dishwashing liquid, and preparation method thereof - Google Patents

Dishwashing liquid, and preparation method thereof Download PDF

Info

Publication number
CN106635502A
CN106635502A CN201611222909.7A CN201611222909A CN106635502A CN 106635502 A CN106635502 A CN 106635502A CN 201611222909 A CN201611222909 A CN 201611222909A CN 106635502 A CN106635502 A CN 106635502A
Authority
CN
China
Prior art keywords
liquid detergent
weight
wound
antiseptic
surfactant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611222909.7A
Other languages
Chinese (zh)
Inventor
胡波
钟勇财
谢玉国
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIANGXI YIXINTANG MEDICAL TECHNOLOGY Co Ltd
Original Assignee
JIANGXI YIXINTANG MEDICAL TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JIANGXI YIXINTANG MEDICAL TECHNOLOGY Co Ltd filed Critical JIANGXI YIXINTANG MEDICAL TECHNOLOGY Co Ltd
Priority to CN201611222909.7A priority Critical patent/CN106635502A/en
Publication of CN106635502A publication Critical patent/CN106635502A/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2068—Ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2072—Aldehydes-ketones
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2093—Esters; Carbonates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2096—Heterocyclic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/221—Mono, di- or trisaccharides or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/32—Amides; Substituted amides
    • C11D3/323—Amides; Substituted amides urea or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/662—Carbohydrates or derivatives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/90—Betaines

Abstract

The invention belongs to the field of daily chemical product, and more specifically relates to a dishwashing liquid, and a preparation method thereof. The dishwashing liquid comprises, by weight, 30 to 50% of a surfactant, 0.1 to 0.3% of ethylenediaminetetraacetic acid disodium salt, 1 to 5% of seaweed gel, 1 to 5% of an amino acid humectants, 1 to 3% of an antiseptic, 0.5 to 1.5% of a wound healing agent, 0.1 to 3% of citric acid, 0.1 to 0.3% of eugenol, and 31.9 to 66.2% of water. The dishwashing liquid is capable of removing dirt and pesticide residue, and is capable of sterilizing, diminishing inflammation, and promoting healing of wounds; and in addition, the dishwashing liquid possesses no irritation on human body, is green and safe, possesses refreshing flavor, and is capable of moisturizing the skin.

Description

A kind of liquid detergent and preparation method thereof
Technical field
The invention belongs to cosmetics of everyday use field, and in particular to a kind of liquid detergent and preparation method thereof.
Background technology
With the development of society, the continuous improvement of living standard, requirement of the people to liquid detergent also more and more higher, liquid detergent People use daily, but traditional liquid detergent often pays attention to dirt-removing power, but most of product can stimulate skin when using Skin, makes skin damage evil, dry and astringent, coarse or even decortication allergy, not to mention with the function of promoting finger wound to heal.
Chinese patent application CN104293528A discloses a kind of liquid detergent for promoting wound healing, its component weight Measuring proportioning is：11～12.0% sodium sulfate of polyethenoxy ether of fatty alcohol, 0.5～1% little wintergreen essential oil, 2.0～8.0% Protein bio surfactant, 0.2～0.4% amino acid humectant, 0.5～1% KF88,2～4% collagen egg In vain, 0.1～0.5% intercalating agent, 0.5～3% cocounut oil alkylolamides, 0.2～1.0% allantoin, 0.05～0.5% perfume (or spice) Essence, 0.1～1% sodium chloride and, balance of deionized water.The liquid detergent is little to skin irritatin, and user's finger can be promoted to hinder Mouthful healing, but its sterilized and wound healing effect has much room for improvement.
Chinese patent CN102925299B discloses a kind of Green antimicrobial cleanser essence and preparation method and application.The present invention Adopt with Nano Silver and natural plant extracts in mass ratio 1:5～1:1 compound prepared as antiseptic, with 15.0～ 45.0% natural surfactant, 0.1～0.3% chelating agent, 2.0～5.0% thickeners and 0.3～0.9% composite antibacterial Agent prepares Green antimicrobial cleanser essence.The liquid detergent can remove dirt and agriculture is residual, moreover it is possible to effectively sterilized, taste removal, but it is to wound Have no obvious Healing.
The content of the invention
In order to solve problems of the prior art, it is an object of the invention to provide a kind of liquid detergent and its preparation side Method.The liquid detergent that the present invention is provided not only can go dirt and agriculture residual, moreover it is possible to bactericidal antiphlogistic, the healing of promotion wound.Meanwhile, The present invention provide liquid detergent is non-stimulated to human body, green safety, pure and fresh pleasant, and skin care.
The invention provides a kind of liquid detergent, including following components and its percentage by weight：
Surfactant 30-50%, disodium ethylene diamine tetraacetate 0.1-0.3%, algin 1-5%, amino acid humectant 1-5%, antiseptic 1-3%, Wound-healing agent 0.5-1.5%, citric acid 0.1-3%, eugenol 0.1-0.3% and water 31.9- 66.2%.Algin is bought in Xi'an Yu Hua bio tech ltd.
The reasonable science of compatibility of the present invention, each component interacts, and collaboration plays sterilized, promotion wound healing, while Enhance it and go the residual effect of dirt and agriculture.
Further, described liquid detergent is made up of following components and its percentage by weight：
Surfactant 40%, disodium ethylene diamine tetraacetate 0.2%, algin 3%, amino acid humectant 3%, antiseptic 2%th, Wound-healing agent 1%, citric acid 2%, eugenol 0.2% and water 48.6%.
Further, the surfactant by Tea Saponin, APG and dodecyldimethylammonium hydroxide inner salt by weight Than 2:2:1 composition.Tea Saponin is purchased from Hunan Lang Lin biological products Co., Ltd, and APG is purchased from the strong wound biotechnology in Guangzhou to be had Limit company.
Further, the antiseptic is by aloe-emodin, chlorogenic acid and hesperidine by weight 3:1:1 composition.
Further, the Wound-healing agent is by allantoin, vitamin C and Cobastab2By weight 1:3:1 composition.
Meanwhile, present invention provides a kind of preparation method of liquid detergent, comprises the following steps：
S1 heats water to 60-70 DEG C, and stirring adds surfactant and disodium ethylene diamine tetraacetate, stirs, and obtains Solution A；
Step S1 resulting solution A is cooled to 40-50 DEG C by S2, and algin, amino acid humectant, antibacterial are added while stirring Agent and Wound-healing agent, stir, and obtain solution B；
Step S2 resulting solution B is cooled to room temperature by S3, adds lemon acid for adjusting pH value to be 6.5-7.5, is eventually adding fourth Fragrant phenol, stirs, and obtains final product.
Aloe-emodin (C in the liquid detergent that the present invention is provided15H10O5, CAS NO：481-72-1) there is antibacterial, anti-inflammatory to make With；Chlorogenic acid (C16H18O9, CAS NO：327-97-9) there is antibacterial, antiinflammation；Hesperidine (C28H34O15, CAS NO：520- 26-3) the effect with anti-inflammation；Eugenol (C10H12O2, CAS NO：97-53-0) there is strong cloves fragrance and antibacterial Effect；Allantoin (C4H6O3N4, CAS NO：97-59-6) there is the effect for promoting cell growth, accelerating wound healing；Dimension life Plain C (C6H8O6, CAS NO：50-81-7) enhance immunity, promote ossein biosynthesis, be conducive to wound healing；Dimension life Plain B2(C17H20N4O6, CAS NO：83-88-5) participate in the growth metabolism of cell, tissue repair essential nutrient.Compatibility of the present invention Rationally science, each component interaction, cooperate with and play a part of bactericidal antiphlogistic, while the metabolism of cell can be promoted and repaired, Accelerate the healing of wound.
Compared with prior art, the liquid detergent that the present invention is provided not only can go dirt and agriculture residual, moreover it is possible to bactericidal antiphlogistic, Promote the healing of wound.Meanwhile, the present invention provide liquid detergent is non-stimulated to human body, green safety, pure and fresh pleasant, and moisten skin Skin.
Specific embodiment
Below by specific embodiment, the present invention is described in more detail, and these embodiments are only used for the purpose of illustration, It is not intended to limit protection scope of the present invention.
A kind of liquid detergent of embodiment 1
The liquid detergent is made up of following components and its percentage by weight：
Tea Saponin 12%, APG 12%, dodecyldimethylammonium hydroxide inner salt 6%, disodium ethylene diamine tetraacetate 0.1%th, algin 1%, amino acid humectant 1-5%, aloe-emodin 0.6%, chlorogenic acid 0.2%, hesperidine 0.2%, urine Bursin 0.1%, vitamin C 0.3%, Cobastab20.1%th, citric acid 0.1%, eugenol 0.1% and water 66.2%.
Preparation method：
S1 heats water to 65 DEG C, and stirring adds Tea Saponin, APG, dodecyldimethylammonium hydroxide inner salt and ethylenediamine Tetraacethyl disodium, stirs, and obtains solution A；
Step S1 resulting solution A is cooled to 45 DEG C by S2, adds algin, amino acid humectant, aloe big while stirring Flavine, chlorogenic acid, hesperidine, allantoin, vitamin C and Cobastab2, stir, obtain solution B；
Step S2 resulting solution B is cooled to room temperature by S3, adds lemon acid for adjusting pH value to be 7.0, is eventually adding eugenol, Stir, obtain final product
A kind of liquid detergent of embodiment 2
The liquid detergent is made up of following components and its percentage by weight：
Saponin 16%, APG 16%, dodecyldimethylammonium hydroxide inner salt 8%, disodium ethylene diamine tetraacetate 0.2%, Algin 3%, amino acid humectant 3%, aloe-emodin 1.2%, chlorogenic acid 0.4%, hesperidine 0.4%, allantoin 0.2%th, vitamin C 0.6%, Cobastab20.2%th, citric acid 2%, eugenol 0.2% and water 48.6%.
Preparation method is similar to Example 1.
A kind of liquid detergent of embodiment 3
The liquid detergent is made up of following components and its percentage by weight：
Tea Saponin 20%, APG 20%, dodecyldimethylammonium hydroxide inner salt 10%, disodium ethylene diamine tetraacetate 0.3%th, algin 5%, amino acid humectant 5%, aloe-emodin 1.8%, chlorogenic acid 0.6%, hesperidine 0.6%, allantois Element 0.3%, vitamin C 0.9%, Cobastab20.3%th, citric acid 3%, eugenol 0.3% and water 31.9%.
Preparation method is similar to Example 1.
A kind of liquid detergent of comparative example 1
The liquid detergent is made up of following components and its percentage by weight：
Saponin 13.3%, APG 13.3%, dodecyldimethylammonium hydroxide inner salt 13.4%, disodium ethylene diamine tetraacetate 0.2%th, algin 3%, amino acid humectant 3%, aloe-emodin 1.2%, chlorogenic acid 0.4%, hesperidine 0.4%, allantois Element 0.2%, vitamin C 0.6%, Cobastab20.2%th, citric acid 2%, eugenol 0.2% and water 48.6%.
Preparation method is similar to Example 1.
It is with the difference of embodiment 2, by Tea Saponin, APG and dodecyldimethylammonium hydroxide inner salt by weight 2:2:1 replaces with 1:1:1.
A kind of liquid detergent of comparative example 2
The liquid detergent is made up of following components and its percentage by weight：
Saponin 16%, APG 16%, dodecyldimethylammonium hydroxide inner salt 8%, disodium ethylene diamine tetraacetate 0.2%, Algin 3%, amino acid humectant 3%, aloe-emodin 0.66%, chlorogenic acid 0.66%, hesperidine 0.67%, allantoin 0.2%th, vitamin C 0.6%, Cobastab20.2%th, citric acid 2%, eugenol 0.2% and water 48.6%.
Preparation method is similar to Example 1.
It is that the weight of aloe-emodin, chlorogenic acid and hesperidine is compared into 3 with the difference of embodiment 2:1:1 replaces with 1: 1:1。
A kind of liquid detergent of comparative example 3
The liquid detergent is made up of following components and its percentage by weight：
Saponin 16%, APG 16%, dodecyldimethylammonium hydroxide inner salt 8%, disodium ethylene diamine tetraacetate 0.2%, Algin 3%, amino acid humectant 3%, aloe-emodin 1.2%, chlorogenic acid 0.4%, hesperidine 0.4%, allantoin 0.33%th, vitamin C 0.33%, Cobastab20.34%th, citric acid 2%, eugenol 0.2% and water 48.6%.
Preparation method is similar to Example 1.
It is with the difference of embodiment 2, by allantoin, vitamin C and Cobastab2Weight compare 1:3:1 replaces with 1:1: 1。
Test example one, oil cut rate is gone to test
1. test material：Liquid detergent prepared by embodiment 1-3 and comparative example 1-3.
2. test method：
1) slide of the known amount of defiling is inserted and prepare in corresponding wash stand washing；
2) spotter is switched on power, wash temperature is set to 30 DEG C, and speed of gyration is set to 160r/min, wash time It is set to 3min；
3) 5g samples to be tested are weighed in 2500mL hard water, after shaking up, 800mL test solutions is measured respectively in Terg-O-Tometer In 6 washing tubes, when test solution temperature rises to 30 DEG C, rapidly the dirty piece of known weight is accordingly put into washing together with wash stand In bucket, start to count soak time after last wash stand is put into washing tube, while rapidly installing in agitator, soak 1min When, start spotter, start washing, machine autostop during 3min rapidly removes in agitator, wash stand is taken out, after washing Dirty piece presss from both sides hang on original film airing stand one by one, and it is m to hang and dirty piece is put into corresponding weighing frame weighing after the 3h that dries in the air2.Calculate it and go oil cut rate, Formula is as follows：
Remove oil cut rate ω %=(m1-m2)/(m1-m0) × 100%
In formula：m0：Slide quality before defiling, g；m1：Slide quality after defiling, g；m2：The quality of dirty piece, g after washing.
3. result of the test：Oil cut rate test result is gone to be shown in Table 1.
Table 1 goes oil cut rate test result
As shown in Table 1, the liquid detergent that prepared by the present invention goes the oil cut rate higher.And liquid detergent prepared by comparative example 1-3 goes Oil cut rate is poorer than the effect of liquid detergent prepared by comparative example 1-3, the reasonable science of compatibility of the present invention is illustrated, when Tea Saponin, APG It is 2 with the weight ratio of dodecyldimethylammonium hydroxide inner salt:2:When 1, best results of deoiling.
Test example two, BA
1. test material：Liquid detergent prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：Escherichia coli ATCC25922, staphylococcus aureus ATCC6538 and pseudomonas aeruginosa ATCC27853。
3. test method：
According to professional standard QB/T2850-2007 antibacterial bacteriostatic type detergent, fungistatic effect test, embodiment 1-3 are carried out And the activity of the liquid detergent of comparative example 1-3 preparation is 1wt%, action time is 20 minutes, concrete detection data, in detail It is shown in Table 2.
The liquid detergent of table 2 sterilization test result
Known by table 2, the bactericidal effect of liquid detergent prepared by the present invention is preferable.And liquid detergent prepared by comparative example 1-3 is killed Bacterium effect is poorer than the effect of liquid detergent prepared by embodiment of the present invention 1-3, illustrate compatibility of the present invention rationally, science, each component association Same-action plays anti-inflammation, and antiseptic is 3 in the weight ratio of aloe-emodin, chlorogenic acid and hesperidine:1:Bactericidal effect when 1 Most preferably.
Test example three, wound healing assay
1. test material：Liquid detergent prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：Mouse 60, male and female half and half, health.
3. test method：
Mouse is randomly divided into 6 groups, 10 per group, i.e. embodiment 1-3 group and comparative example 1-3 group afterwards will using scalpel The right leg of each group mouse scratches respectively the wound of a length of 2cm.Liquid detergent prepared by embodiment 1-3 and comparative example 1-3 is taken respectively 0.5g is coated in wound, using one week, twice daily, observes its wound healing situation, and it is scored.Wound healing situation mark It is accurate：Wound healing by first intention, refers to that healing is good, the healing of the initial stage without bad reaction；Second class heals, and refers to that healing is not good enough, there is inflammation at healing Disease is reacted；Third class heals, and suppurates to otch.Standards of grading：10 points of total score, 0 point worst, and 10 points best, and fraction more high effect is more It is good.
4. result of the test：Wound healing situation appraisal result is shown in Table 3.
The wound healing situation of table 3 scores
Known by table 3, liquid detergent prepared by the present invention is preferable to the promotion degree of wound healing.Prepared by comparative example 1-3 washes Clean essence is poorer than the promotion degree of liquid detergent prepared by embodiment 1-3 to the promotion degree of wound healing, illustrates that compatibility of the present invention is closed Reason, science, each component interacts, and collaboration plays a part of to promote wound healing, and Wound-healing agent is in allantoin, vitamin C And Cobastab2Weight ratio be 1:3:The speed of wound healing is optimal when 1.

Claims (6)

1. a kind of liquid detergent, it is characterised in that including following components and its percentage by weight：
Surfactant 30-50%, disodium ethylene diamine tetraacetate 0.1-0.3%, algin 1-5%, amino acid humectant 1- 5%th, antiseptic 1-3%, Wound-healing agent 0.5-1.5%, citric acid 0.1-3%, eugenol 0.1-0.3% and water 31.9- 66.2%.
2. liquid detergent as claimed in claim 1, it is characterised in that be made up of following components and its percentage by weight：
Surfactant 40%, disodium ethylene diamine tetraacetate 0.2%, algin 3%, amino acid humectant 3%, antiseptic 2%, Wound-healing agent 1%, citric acid 2%, eugenol 0.2% and water 48.6%.
3. liquid detergent as claimed in claim 1 or 2, it is characterised in that the surfactant by Tea Saponin, APG and Dodecyldimethylammonium hydroxide inner salt is by weight 2:2:1 composition.
4. liquid detergent as claimed in claim 1 or 2, it is characterised in that the antiseptic is by aloe-emodin, chlorogenic acid and orange Skin glucoside is by weight 3:1:1 composition.
5. liquid detergent as claimed in claim 1 or 2, it is characterised in that the Wound-healing agent by allantoin, vitamin C and Cobastab2By weight 1:3:1 composition.
6. the preparation method of the liquid detergent as described in claim 1-5 is arbitrary, it is characterised in that comprise the following steps：
S1 heats water to 60-70 DEG C, and stirring adds surfactant and disodium ethylene diamine tetraacetate, stirs, and obtains solution A；
Step S1 resulting solution A is cooled to 40-50 DEG C by S2, while stirring add algin, amino acid humectant, antiseptic and Wound-healing agent, stirs, and obtains solution B；
Step S2 resulting solution B is cooled to room temperature by S3, adds lemon acid for adjusting pH value to be 6.5-7.5, is eventually adding eugenol, Stir, obtain final product.
CN201611222909.7A 2016-12-27 2016-12-27 Dishwashing liquid, and preparation method thereof Pending CN106635502A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611222909.7A CN106635502A (en) 2016-12-27 2016-12-27 Dishwashing liquid, and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611222909.7A CN106635502A (en) 2016-12-27 2016-12-27 Dishwashing liquid, and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106635502A true CN106635502A (en) 2017-05-10

Family

ID=58832530

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611222909.7A Pending CN106635502A (en) 2016-12-27 2016-12-27 Dishwashing liquid, and preparation method thereof

Country Status (1)

Country Link
CN (1) CN106635502A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107365638A (en) * 2017-08-18 2017-11-21 广西钱隆投资管理有限公司 One kind eliminates the unusual smell liquid detergent and preparation method thereof
CN107418781A (en) * 2017-08-18 2017-12-01 广西钱隆投资管理有限公司 A kind of antibacterial liquid detergent and preparation method thereof
CN107955738A (en) * 2017-12-04 2018-04-24 湖南金昌生物技术有限公司 A kind of Tea Saponin neutrality vegetables and fruits cleaning agent and preparation method thereof
CN111205935A (en) * 2020-01-16 2020-05-29 深圳市恒纬祥科技有限公司 Food-grade detergent and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104479908A (en) * 2014-12-23 2015-04-01 青岛海芬海洋生物科技有限公司 Teacup detergent
CN105255596A (en) * 2015-10-29 2016-01-20 广州赛莱拉生物基因工程有限公司 Antibacterial dish-washing detergent containing argy wormwood leaf extract

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104479908A (en) * 2014-12-23 2015-04-01 青岛海芬海洋生物科技有限公司 Teacup detergent
CN105255596A (en) * 2015-10-29 2016-01-20 广州赛莱拉生物基因工程有限公司 Antibacterial dish-washing detergent containing argy wormwood leaf extract

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107365638A (en) * 2017-08-18 2017-11-21 广西钱隆投资管理有限公司 One kind eliminates the unusual smell liquid detergent and preparation method thereof
CN107418781A (en) * 2017-08-18 2017-12-01 广西钱隆投资管理有限公司 A kind of antibacterial liquid detergent and preparation method thereof
CN107955738A (en) * 2017-12-04 2018-04-24 湖南金昌生物技术有限公司 A kind of Tea Saponin neutrality vegetables and fruits cleaning agent and preparation method thereof
CN111205935A (en) * 2020-01-16 2020-05-29 深圳市恒纬祥科技有限公司 Food-grade detergent and preparation method thereof

Similar Documents

Publication Publication Date Title
CN106635502A (en) Dishwashing liquid, and preparation method thereof
CN101735898B (en) Indigowoad root liquid soap
KR101427099B1 (en) Shampoo soap compositions including effective microorganisms fermentation liquid and native grass powder and Manufacturing method thereof
CN105779165A (en) Washing composition as well as preparation method and application of washing composition
CN103656717B (en) A kind of is main Footgear deodorizer and preparation method thereof based on plant extraction liquid
CN105255596B (en) A kind of Antibiotic liquid detergent containing Folium Artemisiae Argyi extract
CN106362183A (en) Deodorant, preparation method and application thereof
CN111840164A (en) Bacteriostatic moisturizing refreshing wet tissue water and debugging method thereof
CN105534372B (en) It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory
CN106038422A (en) Washing composition and preparation method and application thereof
CN110638725A (en) Wet tissue for infants and preparation method thereof
CN105616292B (en) Tea Saponin shampoo containing Chinese medical extract and preparation method thereof
CN106635563A (en) Weak acid crystal soap for skin health and purification
CN109512741A (en) A kind of essential oil is washed one's hands condensation and preparation method thereof
CN109010178A (en) A kind of shower cream and its production technology
CN104207970A (en) Medical skin-care disinfection hand-cleaning liquid and preparation method thereof
CN106566683A (en) Cleaning liquid as well as preparation method and application thereof
CN114306526B (en) Compound broadleaf holly leaf traditional Chinese medicine extract and application thereof in preparing shower gel or hand sanitizer
CN109674875A (en) Oral ulcer nursing essence
CN111481597B (en) Female herbal bacteriostatic care solution and preparation method thereof
CN104207971A (en) Medical skin-disinfection and -nursing hand-cleaning liquid and preparation method thereof
CN106962400A (en) A kind of high-efficiency plant composition cleanser containing trivalent silver iron and preparation method thereof
KR101578595B1 (en) Hand-disinfectant containing lotus leaf extract and method for manufacturing the same
WO2020057285A1 (en) Atractylodes oil and/or cassia twig oil, production method therefor and use thereof
CN110151582A (en) A kind of deodorization is antibacterial and repairs the function spray and its preparation and application of mucous membrane

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170510