CN106622073A - Waste gas purifying and weighing integrated reaction kettle device - Google Patents
Waste gas purifying and weighing integrated reaction kettle device Download PDFInfo
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- CN106622073A CN106622073A CN201611101539.1A CN201611101539A CN106622073A CN 106622073 A CN106622073 A CN 106622073A CN 201611101539 A CN201611101539 A CN 201611101539A CN 106622073 A CN106622073 A CN 106622073A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/10—Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00081—Tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/18—Details relating to the spatial orientation of the reactor
- B01J2219/185—Details relating to the spatial orientation of the reactor vertical
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention relates to a waste gas purifying and weighing integrated reaction kettle device which comprises a kettle body, a waste gas treating and purifying device and a weighing device arranged at the top of the kettle body. A kettle cover is arranged at the top of the kettle body, a material inlet, a gas discharging hole and a thermometer sleeve are arranged on the kettle cover, and the waste gas treating and purifying device is positioned at the upper end of the kettle body and fixed through a mounting frame. By arranging a waste gas filtering layer, a waste gas adsorbing layer and a waste gas ventilating layer, a lot of high-concentration organic waste gas generated in the process of reaction for preparing adhesive resin can be treated and absorbed to reach discharging standards; a ventilating wall plate having a certain inclination angle is arranged, so that noise in the process when a fan runs can be lowered. The waste gas purifying and weighing integrated reaction kettle device is compact in structure, high in automation level and convenient and simple to operate.
Description
Technical field
The invention belongs to resin processing equipment technical field, and in particular to a kind of to weigh integral type reaction for waste gas purification
Kettle device.
Background technology
Reactor is widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying,
The pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.;Material
Matter typically has carbon manganese steel, stainless steel, zirconium, Ni-based(Kazakhstan, Monel, inconel)Alloy and other composites.Reactor
Broad understanding has the rustless steel container for physically or chemically reacting, and is set according to the structure that different process conditions demands carries out container
Meter and parameter configuration, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, to realize technological requirement
The mixture response function of heating, evaporation, cooling and low high speed.
Adhesive agent is also referred to as adhesive, binder, in 1742 by American Henry Al Kut doctors(Dr. Harry
Coover)Invention.Refer to by the glutinous material together of two objects, according to the characteristic of wanted bonding material(Mainly surface characteristic,
Such as roughness), using different adhesive agents;Binder is in fact the resin of dilution, and resin inherently has stickiness.
Reactor is conventional chemical industry equipment;During reaction prepares adhesive, it will usually produce substantial amounts of high concentration
Organic exhaust gas, this aspect derives from the gas-phase product of synthetic reaction, on the other hand from the volatilization for reacting solvent after heating.
Because synthetic reaction generally will be heated, or exothermic reaction produces heat, raises the temperature of charge in reactor, so as to
Significantly increase the organic concentration in reactor top gas phase.
Generally, reactor top is provided with blast pipe, and waste gas is discharged into reactor.Cause to prevent reactor from discharging waste gas
Atmosphere pollution, by blast pipe discharge waste gas lead to exhaust treatment system process it is qualified after could discharge.Existing one kind
Technical scheme, in the top of exhaust outlet gas skirt is installed, and gas skirt is connected with collecting pipe, and waste gas is sent to into exhaust-gas treatment
System.The deficiency of this technical scheme is, when the negative pressure of gas skirt it is not enough, or blast pipe discharge the flow or pressure of waste gas compared with
When big, waste gas can not all collected by gas skirt, and a part of waste gas can be directly diffused in air and form pollution.It is existing another
A kind of technical scheme, is that blast pipe is directly connected to into collecting pipe, it is possible to guarantee that the waste gas that blast pipe is discharged is fully entered
Exhaust treatment system process.The deficiency of this scheme is, in order to realize discharging in a organized way, collecting pipe needs to be born with certain
Pressure, directly connect with blast pipe carries out negative-pressure ward equivalent to reactor, significantly increases the discharge capacity of reactor waste gas.This
The load of emission-control equipment is not only increased, and causes the waste of organic solvent;Meanwhile, reactor fan and gas collection
Noise problem produced by pipeline can directly affect in such an environment for a long time the healthy of worker than larger.
In addition, the material thrown in into reactor is typically first placed on electronic scale and weighs, then entering by reactor
Material mouth is put into kettle, the mode of such manual control charging, the weight of the difficult accurate control feed liquid of comparison, application condition
Greatly;Also to ensure that the feeding port for throwing in material is accurately docked with the charging aperture of reactor simultaneously, once docking is inaccurate, can spill into
Product material, causes the loss of material, if material is poisonous or inflammable and explosive material, the generation for easily causing the accident, and
And existing reactor single function, inefficiency, mixing effect are poor, it is impossible to meet the demand of modernization Chemical Manufacture.
For above-mentioned technical problem, therefore need to be improved.
The content of the invention
The present invention is to overcome above-mentioned defect of the prior art, there is provided a kind of anti-for waste gas purification integral type of weighing
Kettle device is answered, the device can carry out purified treatment during reactor prepares adhesive agent to waste gas, it is also possible to reduce noise dirty
Dye, meanwhile, precise control weight can be carried out to the material for adding, it is ensured that the qualification rate of adhesive agent product, the apparatus structure is simple,
It is easy to use.
In order to reach object above, the technical solution adopted in the present invention is:It is a kind of to weigh integral type for waste gas purification
Reaction kettle device, including kettle, exhaust gas purification device and the weighing device at the top of kettle;Set at the top of the kettle
There is kettle cover, kettle cover is provided with charging aperture, steam vent and thermometer boss;Exhaust gas purification device is located at the upper end of kettle and leads to
Cross installing rack to fix;The bottom of exhaust gas purification device is provided with the first connecting tube in trumpet type, the first connection bottom of the tube
It is connected with steam vent;The thermometer boss is stretched in kettle and upper end is fixed on the kettle cover, the thermometer boss
Thermometer is inside set, autoclave body bottom is provided with discharging opening;Agitating device is provided with kettle;The bottom of kettle is arranged installs bracing frame;Institute
Weighing device is stated including storage bin;The lower end of storage bin is provided with two discharging openings of tapered cavity;Storage bin lower end is provided with
The LOAD CELLS corresponding with discharging opening, is provided with connected terminal box by LOAD CELLS;Terminal box is installed on title
Retransmit on the side wall of sensor, the centre position of two discharging openings extends vertically be provided with deflector upwards, deflector is located at storage bin
Interior, the height of deflector is the 1/2 of storage bin height, and the upper port of storage bin is provided with material inlet valve, corresponding, goes out
The lower port of material mouth is provided with discharge gate, and discharge gate bottom is connected with buffering filtering chamber, buffers the bottom of filtering chamber
The flexible discharger slip awaing tube of connection one, the lower end connection reducing mechanism of flexible discharger slip awaing tube;The reducing mechanism includes screw feeding
Machine, screw feeding motor spindle is provided with connecting tube, and the bottom of self-conveyor feed is also equipped with Weighing mechanism and self-conveyor feed
On be provided with motor, self-conveyor feed is connected by connecting tube with Weighing mechanism;The Weighing mechanism includes being installed on connecting tube
On weight sensor and material tremie pipe;Material tremie pipe is connected with the charging aperture on kettle;The upper end peace of material tremie pipe
Equipped with material blanking control valve door;Weight sensor is connected with material blanking control valve door;The agitating device includes driving
Motor, bracing frame, shaft and stirring paddle mechanism;Bracing frame is fixedly arranged on kettle cover, and motor is located on bracing frame, shaft
One end and motor rotate and be connected, the other end is passed through in kettle and stirs paddle mechanism and be connected;The exhaust-gas treatment purification dress
Put including housing, the waste gas filter layer laid successively from the bottom to top in housing, waste gas adsorption layer and waste air ventilation layer;Waste gas
Filter layer, between waste gas adsorption layer and waste air ventilation layer gap is respectively kept with;The waste gas filter layer is labyrinth type filter layer, should
Labyrinth type filter layer is waveform bilayer paper structure, and before and after the duplex paper perforate is intersected;Waste gas adsorption layer is activated carbon filter layer,
Activated carbon is filled with activated carbon filter layer.
Used as a preferred embodiment of the present invention, the waste air ventilation layer includes being located in housing leading to certain knuckle
Wind passage;The vent passages are formed by connecting by least two pieces identicals ventilation wallboards;Vent passages lower end is connected with for fixing
The reinforcement of ventilation wallboard.
Used as a preferred embodiment of the present invention, the ventilation wallboard is connected by the first linkage section, the second linkage section and the 3rd
Connect section to be formed by fixedly connecting, be integrally formed;First linkage section is vertical with the top of housing to be connected, and the 3rd linkage section hangs down with reinforcement
Direct-connected to connect, the second linkage section is oblique, for connecting the first linkage section and the 3rd linkage section.
As the equal length of a preferred embodiment of the present invention, second linkage section and the 3rd linkage section;First connects
The length for connecing section is the 1/2 of the 3rd connection segment length;Second linkage section and the first linkage section and the 3rd linkage section in 25 °~
65 ° of angle is inclined.
Used as a preferred embodiment of the present invention, the case top is provided with discharge duct, and discharge duct lower end is installed
There is trumpet type suction opeing, trumpet type suction opeing upper end is provided with air exhauster.
As a preferred embodiment of the present invention, on the kettle body sidewall steam inlet and steam (vapor) outlet are separately installed with;
Steam pipe is connected between steam inlet and steam (vapor) outlet, steam pipe annular is laid in the inwall of kettle, the steam pipe with stirring
Paddle mechanism keeps certain spacing.
Used as a preferred embodiment of the present invention, the stirring paddle mechanism includes from top to bottom being laid in successively on shaft
Hinging type stirrer paddle, pusher blade and four leaf swept-back blades;After hinging type stirrer paddle, pusher blade and four leaves
The formula blade of plunderring is socketed on shaft, is removable connection with shaft;The hinging type stirrer paddle, pusher blade and four
Leaf swept-back blade is equidistantly laid on shaft;The blade tip of the four leaves swept-back blade is in sharp portion.
Used as a preferred embodiment of the present invention, the kettle cover has the pressure sensor under extending to the cavity of kettle,
Pressure sensor connects temperature and pressure device for digit-displaying, and by temperature and pressure device for digit-displaying the pressure in kettle is shown.
As a preferred embodiment of the present invention, PLC control system is also included, the PLC control system and weighing and sensing
The electrical connection of device, terminal box and weight sensor.
Used as a preferred embodiment of the present invention, the material inlet valve, discharge gate adopt air cylinder driven, material inlet valve
Also carry hand door.
The invention has the beneficial effects as follows:
1. one kind that the present invention is provided is weighed integral type reaction kettle device for waste gas purification, and there is the device precise control to feed
The function of speed, reduces the artificial danger that material is directly put into reactor, reduces the labour intensity of operator, improves
Execute-in-place environment, improves the security of reaction unit;Connected using steam inlet, steam (vapor) outlet and steam pipe so that
The heat exchange efficiency of reactor is greatly improved, and heat exchange response speed greatly speeds up;It is sealing in the operating process of liquid material,
Material reaches environmental pollution and the wasting of resources for avoiding that Chang Kou Installed material strips come in reactor container from storage tank Jing delivery pumps;
2. it is comprehensive by using hinging type stirrer paddle, pusher blade and four three kinds of different stirrer paddles of leaf swept-back blade
Conjunction make use of the advantage of three kinds of blades, had both changed and has mixed that uneven, polymerization efficiency is low to ask present in traditional agitating mode
Topic, causes reaction stability to significantly improve again;
3. PLC control system realize the typing of the Weighing process data of the material of whole reaction kettle device, collection, contrast,
The functions such as quantitative control, and can be communicated with computer control system by data-interface, realize intelligentized control method;
4. by arranging waste gas filter layer, waste gas adsorption layer and waste air ventilation layer, can be to preparing adhesive resin mistake in reaction
Substantial amounts of high-concentration organic waste gas are produced in journey to be processed, is absorbed, reach discharge standard, while arrange that there is certain inclination angle
The ventilation wallboard of degree, can reduce noise during fan operation, and the apparatus structure is compact, high degree of automation, operation side
Just it is simple;
5. the present invention has integrated level high, and high degree of automation is user-friendly for operation, easy to maintenance simple, quantitatively accurately, environmental protection etc.
Feature, with good application value.
Description of the drawings
Fig. 1 is embodiment of the present invention structural representation;
Reference in figure:Installing rack 1, housing 2, waste gas filter layer 3, waste gas adsorption layer 4, waste air ventilation layer 5, vent passages 6,
Ventilation wallboard 7, the first linkage section 7-1, the second linkage section 7-2, the 3rd linkage section 7-3, storage bin 8, discharging opening 9, deflector 10,
Kettle 11, charging aperture 12, discharging opening 13 installs bracing frame 14, kettle cover 15, steam vent 16, reinforcement 17, discharge duct 18, loudspeaker
Type suction opeing 19, LOAD CELLS 20, terminal box 21, discharge gate 22, flexible discharger slip awaing tube 23, material inlet valve 24, buffering
Filtering chamber 25, self-conveyor feed 26, motor 27, connecting tube 28, Weighing mechanism 29, weight sensor 29-1, material tremie pipe
29-2, blanking control valve door 29-3, motor 30, bracing frame 31, shaft 32, steam inlet 33, steam (vapor) outlet 34, steam
Pipe 35, hinging type stirrer paddle 36, pusher blade 37, four leaf swept-back blades 38, pressure sensor 39, pressure device for digit-displaying
40, thermometer boss 41, air exhauster 42, the first connecting tube 43.
Specific embodiment
The embodiment of the present invention is elaborated below in conjunction with the accompanying drawings.
Embodiment 1:It is as shown in figure 1, one kind is weighed integral type reaction kettle device for waste gas purification including kettle 11, useless
Gas disposal purifier and the weighing device located at the top of kettle 11;The top of the kettle 11 is provided with kettle cover 15, on kettle cover 15
It is provided with charging aperture 12, steam vent 16 and thermometer boss 41;Exhaust gas purification device is located at the upper end of kettle 11 and by peace
Shelve 1 fixation;The bottom of exhaust gas purification device is provided with the first connecting tube 43 in trumpet type, the bottom of the first connecting tube 43
It is connected with steam vent 16;By arranging exhaust gas purification device, using the first connecting tube, 43 pairs prepare adhesive in reaction
Substantial amounts of high-concentration organic waste gas are produced in resin process to be processed, is absorbed, reach discharge standard, can greatly mitigate environment
Pollution, protects well that employee's is healthy.
Thermometer boss 41 is stretched in kettle 11 and upper end is fixed on the kettle cover 15, sets in the thermometer boss 41
Thermometer, thermometer can at any time show the temperature in kettle 11, and to using bringing convenience, the bottom of kettle 11 is provided with discharging opening 13;
Agitating device is provided with kettle 11;The bottom of kettle 11 is arranged installs bracing frame 14, installs bracing frame 14 and causes the reactor dress
The stability put is more preferable, using safer.
Weighing device includes storage bin 8;The lower end of storage bin 8 is provided with two discharging openings 9 of tapered cavity;Storage bin
8 lower ends are provided with the LOAD CELLS 20 corresponding with discharging opening 9, and connected terminal box is provided with by LOAD CELLS 20
21;Terminal box 21 is installed on the side wall of LOAD CELLS 20, and the centre position of two discharging openings 9 extends vertically to be provided with upwards leads
Stream plate 10, deflector 10 is located in storage bin 8, and the height of deflector 10 is the 1/2 of the height of storage bin 8, what deflector 10 was arranged
Purpose is to make 24 mouthfuls of materials for falling of each material inlet valve, uniformly by two discharging openings 9 of the corresponding tapered cavity in its lower end
Flow out, it is ensured that inventory is balanced on each discharging opening 9, realizes uniform blanking, reduces the stability of the solid weighing device.
The upper port of storage bin 8 is provided with material inlet valve 24, corresponding, and the lower port of discharging opening 9 is provided with unloads
Material valve 22, the bottom of discharge gate 22 is connected with buffering filtering chamber 25, and the bottom for buffering filtering chamber 25 connects a flexibility
Discharger slip awaing tube 23, the lower end connection reducing mechanism of flexible discharger slip awaing tube 23;The position of flexible discharger slip awaing tube 23 is arranged, and makes buffered
Filter chamber room 25 be capable of the lifting of flexible discharger slip awaing tube 23 and lift, the solid that moves left and right and move to meet differing heights claims
Refitting is put, and can make have as little as possible between the port of material tremie pipe 29-2 and the upper surface of charging aperture 12 of kettle 11 as far as possible
Distance is reducing flour dust overflow;The LOAD CELLS 20 corresponding with discharging opening 9, weighing and sensing are set at the position of discharging opening 9
Device 20 is electrically connected with terminal box 21, for detecting storage bin 8 in material weights.
Reducing mechanism includes self-conveyor feed 26, and the bottom of self-conveyor feed 26 is provided with connecting tube 28, self-conveyor feed 26
Bottom be also equipped with being provided with motor 27 on Weighing mechanism 29 and self-conveyor feed 26, self-conveyor feed 26 pass through connecting tube
28 are connected with Weighing mechanism 29;Weighing mechanism 29 includes the weight sensor 29-1 and material tremie pipe being installed in connecting tube 28
29-2;Material tremie pipe 29-2 is connected with the charging aperture 12 on kettle 11;The upper end of material tremie pipe 29-2 is provided with material
Material control valve 29-3;Weight sensor 29-1's is connected with material blanking control valve door 29-3;By self-conveyor feed 26 pairs
The stirring and processing of material, according to actual needs, the charging frequency of adjustable screw charger 26 drives screw feeding by motor 27
Machine 26 rotates, and the material for processing enters to Weighing mechanism 29 by connecting tube 28, and by Weighing mechanism 29 quantifying feed is realized
Purpose, the apparatus structure is simple, and reasonable in design, detachability is good, is easily installed and changes, and fault rate is low, stability in use
Good, the device has the function of precise control charging rate, reduces the artificial danger that solid material is directly put into kettle 11
Property, the labour intensity of operator is reduced, execute-in-place environment is improved, improve the security of reaction unit.
Material inlet valve 24, discharge gate 22 adopt air cylinder driven, material inlet valve 24 also to carry hand door, facilitate user
Debugging, maintenance.Dust explosion protection type proximity switch is filled on material inlet valve 24, the detection and control of the bin gate position of material inlet valve 24 is carried out
System, it is ensured that the security that material is added.
The agitating device includes motor 30, bracing frame 31, shaft 32 and stirring paddle mechanism;Bracing frame 31 is fixed
On kettle cover 15, motor 30 is located on bracing frame 31, and one end of shaft 32 rotates with motor 30 and is connected, the other end
It is passed through in kettle 11 and is connected with stirring paddle mechanism.
Exhaust gas purification device includes housing 2, the waste gas filter layer 3 laid successively from the bottom to top in housing 2, gives up
Gas adsorption layer 4 and waste air ventilation layer 5;Waste gas filter layer 3, between waste gas adsorption layer 4 and waste air ventilation layer 5 gap is respectively kept with;
Waste gas filter layer 3 is labyrinth type filter layer, and the labyrinth type filter layer is waveform bilayer paper structure, intersects before and after the duplex paper and opens
Hole;Waste gas adsorption layer 4 is that activated carbon is filled with activated carbon filter layer, activated carbon filter layer.
The labyrinth type filter layer is waveform bilayer paper structure, and before and after the duplex paper perforate is intersected;Labyrinth type filter layer is adopted
Made with ground paper, particular/special requirement is had no to the ground paper that labyrinth type filter layer is adopted, corrugated paper can be adopted, in agitating device to kettle
The adhesive resin raw material for preparing in 11 is stirred, and waste gas passes through the connecting tube 43 of steam vent 16 and first when housing 2,
Under the operation of air exhauster 42, when labyrinth type filter layer, the particulate matter contained by the inside can be because used for the pernicious gas in waste gas
Property and cyclogenesis adhere on labyrinth type filter layer, meanwhile, for the ease of clear up labyrinth type filter layer on filtration particle, give up
Gas filter layer 3 is to be detachably connected with housing 2;Waste gas adsorption layer 4 is filled with work in activated carbon filter layer, activated carbon filter layer
Property charcoal;Waste gas impurity after waste gas filter layer 3 is filtered, by the air draught of air exhauster 42 so that waste gas impurity is by property charcoal
The activated carbon of filter layer is adsorbed, effectively to remove removing exhaust gas impurity in waste organic solvent gas, finally, tail gas up to standard by row
Feed channel 18 is entered in air.
Waste air ventilation layer 5 includes being located at the vent passages 6 with certain knuckle in housing 2;The vent passages 6 are by least two
Block identical ventilation wallboard 7 is formed by connecting;The lower end of vent passages 6 is connected with for the reinforcement 22 of fixed ventilation wallboard 7;Using
Vent passages 6 cause air exhauster 25 in running, effectively reduce the interference of noise.
Ventilation wallboard 7 is formed by fixedly connecting by the first linkage section 7-1, the second linkage section 7-2 and the 3rd linkage section 7-3, and one
It is body formed;First linkage section 7-1 is vertical with the top of housing 2 to be connected, and the 3rd linkage section 7-3 is vertical with reinforcement 22 to be connected, the
Two linkage section 7-2 are oblique, for connecting the first linkage section 7-1 and the 3rd linkage section 7-3.
Using such scheme so that in operation, the wind direction for being absorbed runs from the bottom to top air exhauster 25, the adjacent the 3rd
The vent passages 6 that linkage section 7-3 is formed are vertical direction, in motion process on wind direction, because the second linkage section 7-2 is in incline
Ramp-like setting, the wind of upward vertical movement can touch the second linkage section 7-2, produce wind direction skew, give wind direction certain stagnant
Use is given over to, while so that wind speed is reduced, and then reduction blower fan moves brought noise.
Optimize for the ease of the height of the waste air ventilation layer 5 so that the structure of emission-control equipment is more convenient and utilizes
Rate is high, the equal length of the second linkage section 7-2 and the 3rd linkage section 7-3;The length of the first linkage section 7-1 is the 3rd linkage section 7-
The 1/2 of 3 length;While ensureing to reduce noise, and ventilation efficiency can be caused higher.
Second linkage section 7-2 and the first linkage section 7-1 and the 3rd linkage section 7-3 is inclined in 25 °~35 ° of angle;This dress
The the second linkage section 7-2 for putting is 50 ° of inclinations, and the effect for reducing noise is more preferable.
Steam inlet 33 and steam (vapor) outlet 34 are separately installed with the side wall of kettle 11;Steam inlet 33 and steam (vapor) outlet 34 it
Between be connected with steam pipe 35, the annular of steam pipe 35 is laid in the inwall of kettle 11, the steam pipe 35 with stirring paddle mechanism keep one
Fixed spacing;In can realizing stirring paddle mechanism to adhesive resin material whipping process using such scheme, add while stirring
Heat so that the adhesive resin material of stirring is heated evenly, the reaction time of material accelerates, and makes reaction more abundant, improves
Mixing effect and stirring efficiency of the adhesive resin material in kettle 11, this apparatus structure is simple, easy to use.
Stirring paddle mechanism includes the hinging type stirrer paddle 36, push-paddle being from top to bottom laid in successively on shaft 32
The leaf swept-back blade 38 of leaf 37 and four;By arranging three kinds of different stirrer paddles, stirring efficiency and mixing quality are made all significantly
Improve, bring great convenience to agitating procedure so that stirring efficiency is effectively improved, improve mixing quality;Meanwhile,
Hinging type stirrer paddle 36, the pusher leaf swept-back blade 38 of blade 37 and four are set, are so arranged in whipping process and are subject to
Resistance it is less, while good action of turbulent flow can be carried out to material web so that stirring is more uniform.
Hinging type stirrer paddle 36, the pusher leaf swept-back blade 38 of blade 37 and four are socketed on shaft 32, and are stirred
Mix the removable connection of axle 32;It is easy to hinging type stirrer paddle 36, the maintenance of the pusher leaf swept-back blade 38 of blade 37 and four, energy
Enough conveniently fast disassemblings are changed, and cleaning is easy, and can change different stirring paddle mechanisms according to process condition, are realized optimal
Mixing effect, use range is wide, and service efficiency is high.
Hinging type stirrer paddle 36, the pusher leaf swept-back blade 38 of blade 37 and four are equidistantly laid on shaft 32,
So that stirring is more uniform so that stirring efficiency is effectively improved, and improves mixing quality.
Because four leaf swept-back blades 38 are located at the bottommost of reactor, material is thrown in from charging aperture 12 to reactor
During, pass sequentially through hinging type stirrer paddle 36, the stirring of the pusher leaf swept-back blade 38 of blade 37 and four so that material
Stirring it is more uniform, meanwhile, the blade tip of four leaf swept-back blades 38 is in sharp portion, further increases cutting for material
Cut efficiency and cutting utilization rate.
Also just because of the blade tip of four leaf swept-back blade 38 is in sharp portion so that front shear force is larger, it is sufficient to make monomer
Material be separated into fine droplets and can uniformly be suspended in liquid phase, be easy to polymerization and will not agglomeration pile up it is blocking;The stream circulation of stirring liquid is special
Property it is good, liquid can be made to produce simultaneously and axially and radially to be moved;So that liquid carries out sufficiently circulation to eliminate the uneven of temperature
Property, heat-transfer effect is good, and discharge rate is big;Liquid phase circulation is per minute good up to 5~10 mass transfer effects in kettle, and reaction in kettle can be made equal
It is even consistent;Adapt to the change of proportion during vinylite preparation manipulation;Can with one layer of stirrer paddle replace several layers other
The paddle of pattern, makes to simplify the structure easy to maintenance.
By using hinging type stirrer paddle 36, pusher blade 37 and four 38 3 kinds of different stirrings of leaf swept-back blade
Blade, fully utilizes the advantage of three kinds of blades, has both changed and has mixed uneven, polymerization efficiency present in traditional agitating mode
Low problem, causes reaction stability to significantly improve again;In order to increase service life and using effect, hinging type paddle
Leaf 36, the pusher leaf swept-back blade 38 of blade 37 and four are propeller agitator, hinging type stirrer paddle 36, push-paddle
The leaf swept-back blade 38 of leaf 37 and four is solid forging and forms, and stress is more concentrated, not easy fracture.
Kettle cover 15 has the pressure sensor 39 under extending to, the connection temperature of pressure sensor 39 and pressure to the cavity of kettle 11
Power device for digit-displaying 40, shows the pressure in kettle 11, it is ensured that the safety in utilization of reactor by temperature and pressure device for digit-displaying 40.
A kind of waste gas purification apparatus of multifunctional reaction still, also includes PLC control system, the PLC control system with claim
Retransmit sensor 20, terminal box 21 and weight sensor 29-1 electrical connection;By LOAD CELLS 20 and weight sensor 29-1 point
The weight of material is weighed respectively after other material and smashing to adding, the PLC control system control for then passing the result to
System, PLC control system is adjusted according to pre-setting, meanwhile, warning function is additionally provided with PLC control system control, make work
Make spilling or deficiency that personnel know in time material, increase the service life of equipment.
The foregoing description of the disclosed embodiments, enables professional and technical personnel in the field to realize or using the present invention.
Various modifications to these embodiments will be apparent for those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention;Therefore, the present invention
The embodiments shown herein is not intended to be limited to, and is to fit to and principles disclosed herein and features of novelty phase one
The most wide scope for causing.
Although more having used reference in figure herein:Installing rack 1, housing 2, waste gas filter layer 3, waste gas adsorption layer
4, waste air ventilation layer 5, vent passages 6, wallboard 7 of divulging information, the first linkage section 7-1, the second linkage section 7-2, the 3rd linkage section 7-3,
Storage bin 8, discharging opening 9, deflector 10, kettle 11, charging aperture 12, discharging opening 13 installs bracing frame 14, kettle cover 15, steam vent
16, reinforcement 17, discharge duct 18, trumpet type suction opeing 19, LOAD CELLS 20, terminal box 21, discharge gate 22, flexibility is unloaded
Material elephant trunk 23, material inlet valve 24 buffers filtering chamber 25, self-conveyor feed 26, motor 27, connecting tube 28, Weighing mechanism 29, weight
Quantity sensor 29-1, material tremie pipe 29-2, blanking control valve door 29-3, motor 30, bracing frame 31, shaft 32 steams
Vapor inlet 33, steam (vapor) outlet 34, steam pipe 35, hinging type stirrer paddle 36, pusher blade 37, four leaf swept-back blades 38,
Pressure sensor 39, pressure device for digit-displaying 40, thermometer boss 41, the grade term of air exhauster 42, but be not precluded from using other terms
Possibility.It is used for the purpose of more easily describing and explaining the essence of the present invention using these terms;It is construed as appointing
A kind of what additional restriction is all contrary with spirit of the invention.
Claims (10)
1. one kind for waste gas purification weigh integral type reaction kettle device, it is characterised in that:Including kettle(11), exhaust-gas treatment it is net
Makeup is put and located at kettle(11)The weighing device at top;The kettle(11)Top be provided with kettle cover(15), kettle cover(15)On
It is provided with charging aperture(12), steam vent(16)And thermometer boss(41);Exhaust gas purification device is located at kettle(11)Upper end
And by installing rack(1)It is fixed;The bottom of exhaust gas purification device is provided with the first connecting tube in trumpet type(43), first
Connecting tube(43)Bottom and steam vent(16)It is connected;The thermometer boss(41)Stretch into kettle(11)Interior and upper end is fixed on
The kettle cover(15)On, the thermometer boss(41)Inside set thermometer, kettle(11)Bottom is provided with discharging opening(13);Kettle
(11)Inside it is provided with agitating device;Kettle(11)Bottom arrange install bracing frame(14);The weighing device includes storage bin
(8);Storage bin(8)Lower end be provided with two discharging openings of tapered cavity(9);Storage bin(8)Lower end is provided with and discharging opening
(9)Corresponding LOAD CELLS(20), LOAD CELLS(20)Side is provided with connected terminal box(21);Terminal box
(21)It is installed on LOAD CELLS(20)Side wall on, two discharging openings(9)Centre position extend vertically be provided with water conservancy diversion upwards
Plate(10), deflector(10)Positioned at storage bin(8)It is interior, deflector(10)Height be storage bin(8)The 1/2 of height, storage bin
(8)Upper port be provided with material inlet valve(24), corresponding, discharging opening(9)Lower port be provided with discharge gate
(22), discharge gate(22)Bottom is connected with buffering filtering chamber(25), buffer filtering chamber(25)Bottom connect one it is soft
Property discharger slip awaing tube(23), flexible discharger slip awaing tube(23)Lower end connection reducing mechanism;The reducing mechanism includes self-conveyor feed
(26), self-conveyor feed(26)Bottom is provided with connecting tube(28), self-conveyor feed(26)Bottom be also equipped with Weighing mechanism
(29)And self-conveyor feed(26)On be provided with motor(27), self-conveyor feed(26)By connecting tube(28)With Weighing mechanism
(29)It is connected;The Weighing mechanism(29)Including being installed on connecting tube(28)On weight sensor(29-1)With material tremie pipe
(29-2);Material tremie pipe(29-2)With kettle(11)On charging aperture(12)It is connected;Material tremie pipe(29-2)Upper end peace
Equipped with material blanking control valve door(29-3);Weight sensor(29-1)With material blanking control valve door(29-3)Connection;Institute
Agitating device is stated including motor(30), bracing frame(31), shaft(32)With stirring paddle mechanism;Bracing frame(31)It is fixedly arranged on
Kettle cover(15)On, motor(30)Positioned at bracing frame(31)On, shaft(32)One end and motor(30)The company of rotation
Connect, the other end is passed through kettle(11)It is interior to be connected with stirring paddle mechanism;The exhaust gas purification device includes housing(2), be located at
Housing(2)The waste gas filter layer inside laid successively from the bottom to top(3), waste gas adsorption layer(4)With waste air ventilation layer(5);Waste gas mistake
Filtering layer(3), waste gas adsorption layer(4)With waste air ventilation layer(5)Between be respectively kept with gap;The waste gas filter layer(3)For labyrinth
Formula filter layer, the labyrinth type filter layer is waveform bilayer paper structure, and before and after the duplex paper perforate is intersected;Waste gas adsorption layer(4)
To be filled with activated carbon in activated carbon filter layer, activated carbon filter layer.
It is 2. according to claim 1 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:It is described
Waste air ventilation layer(5)Including positioned at housing(2)The interior vent passages with certain knuckle(6);The vent passages(6)By at least two
Block identical ventilation wallboard(7)It is formed by connecting;Vent passages(6)Lower end is connected with for fixed ventilation wallboard(7)Reinforcement
(17).
It is 3. according to claim 2 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:It is described
Ventilation wallboard(7)By the first linkage section(7-1), the second linkage section(7-2)With the 3rd linkage section(7-3)It is formed by fixedly connecting, one
It is body formed;First linkage section(7-1)With housing(2)Top vertically connect, the 3rd linkage section(7-3)With reinforcement(17)Vertically
Connection, the second linkage section(7-2)Obliquely, for connecting the first linkage section(7-1)With the 3rd linkage section(7-3).
It is 4. according to claim 3 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:It is described
Second linkage section(7-2)With the 3rd linkage section(7-3)Equal length;First linkage section(7-1)Length be the 3rd linkage section
(7-3)The 1/2 of length;Second linkage section(7-2)With the first linkage section(7-1)With the 3rd linkage section(7-3)In 25 °~
65 ° of angle is inclined.
It is 5. according to claim 3 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:It is described
Housing(2)Top is provided with discharge duct(18), discharge duct(18)Lower end is provided with trumpet type suction opeing(19), trumpet type takes out
Air port(19)Upper end is provided with air exhauster(42).
It is 6. according to claim 1 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:It is described
Kettle(11)Steam inlet is separately installed with the wall of side(33)And steam (vapor) outlet(34);Steam inlet(33)And steam (vapor) outlet(34)
Between be connected with steam pipe(35), steam pipe(35)Annular is laid in kettle(11)Inwall, the steam pipe(35)With paddle
Mechanism keeps certain spacing.
7. the one kind according to claim 1 or 6 for waste gas purification weigh integral type reaction kettle device, it is characterised in that:
The stirring paddle mechanism includes from top to bottom being laid in shaft successively(32)On hinging type stirrer paddle(36), push-paddle
Leaf(37)With four leaf swept-back blades(38);Hinging type stirrer paddle(36), pusher blade(37)With four leaf swept-back blades
(38)It is socketed on shaft(32)On, with shaft(32)For removable connection;The hinging type stirrer paddle(36), it is pusher
Blade(37)With four leaf swept-back blades(38)Equidistantly it is laid in shaft(32)On;The four leaves swept-back blade(38)Leaf
Piece end is in sharp portion.
It is 8. according to claim 1 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:It is described
Kettle cover(15)To kettle(11)Cavity have pressure sensor under extending to(39), pressure sensor(39)Connection temperature and pressure
Power device for digit-displaying(40), by temperature and pressure device for digit-displaying(40)Show kettle(11)Interior pressure.
It is 9. according to claim 1 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:Also wrap
PLC control system is included, the PLC control system and LOAD CELLS(20), terminal box(21)And weight sensor(29-1)Electricity
Connection.
It is 10. according to claim 1 a kind of to weigh integral type reaction kettle device for waste gas purification, it is characterised in that:Institute
State material inlet valve(24), discharge gate(22)Adopt air cylinder driven, material inlet valve(24)Also carry hand door.
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CN201611101539.1A CN106622073A (en) | 2016-12-05 | 2016-12-05 | Waste gas purifying and weighing integrated reaction kettle device |
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CN201611101539.1A CN106622073A (en) | 2016-12-05 | 2016-12-05 | Waste gas purifying and weighing integrated reaction kettle device |
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