CN106620415A - Disease-prevention oriental cockroach medicament and preparation method thereof - Google Patents
Disease-prevention oriental cockroach medicament and preparation method thereof Download PDFInfo
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Abstract
The invention provides a disease-prevention oriental cockroach medicament and a preparation method thereof, belonging to the technical field of breeding of oriental cockroaches. The medicament is prepared from the following raw materials in parts by weight: 30-40 parts of pine needle, 8-12 parts of cortex mori, 6-10 parts of barley leaves, 10-15 parts of semen raphani, 10-15 parts of clove, 12-18 parts of root of caragana sinica, 20-30 parts of goosegrass herb, 5-10 parts of hyacinth beans, 5-6 parts of caraway and 8-12 parts of an active agent, wherein the active agent is grey white powder prepared by the steps of acidizing sepiolite clay, and modifying the sepiolite clay through sodium bicarbonate and myristic acid. The disease-prevention oriental cockroach medicament, namely a traditional Chinese medicine composition has a certain anti-expelling effect; and by virtue of pharmacological functions of killing bacteria and mites, clearing away the heat and toxic materials and regulating the spleen and the stomach, the gastrointestinal diseases such as appetite loss, slow action, diarrhea, weak physique and the like of the oriental cockroaches are prevented, and the death of the oriental cockroaches caused by mildewing is prevented, so that the breeding yield of the oriental cockroaches and the pesticide effect are guaranteed.
Description
【Technical field】
The present invention relates to OPISTHOPLATIA cultural technique field, and in particular to a kind of OPISTHOPLATIA diseases prevention medicament and its preparation side
Method.
【Background technology】
OPISTHOPLATIA, is arthropod, belongs to Ji Lianke, light sickle subfamily.Also known as eastern Lian, Pharmaceutical name is golden-rimmed native
Unit.Shi Ji Lian sections insect Chi Bianshui's is dried female adult, and main product is in the coastal various places of the provinces such as Guangdong, Guangxi, Fujian and Taiwan.It is golden-rimmed
The effects such as ground beetle has broken heavily fortified point knot, lactagogue of stimulating the menstrual flow, Removing Blood Stasis, alleviating pain and detumescence, cure mainly knife wound bruise, the fracture stasis of blood swell, women's hematocele
The diseases such as stomachache, Amenorrhea, are a kind of conventional Chinese medicines.Medicine source always catches by field.In recent years, due to scientific research new product
Exploitation increases pharmacy industry consumption, adds the pollution of wild ground bettle living environment, causes OPISTHOPLATIA source of goods wretched insufficiency, valency
Lattice raise up successively.Therefore domestic, the wide market of OPISTHOPLATIA is developed at present.
OPISTHOPLATIA harmful ability against the enemy is poor, has many animals and insect often with ground beetle as food.Common harmful animal has：Ant
Ant, mouse, gecko, toad and poultry etc., wherein it is ant to be most difficult to anti-harmful animal.Because the domestic technology of OPISTHOPLATIA develops
Time is shorter, and raiser uses some insecticides, insecticide often relatively to have toxicity, often result in the same of termiticide when ant evil occurs
When, ground beetle also Mortality, yield is greatly decreased, and also has harmful effect to the drug effect of ground beetle.In addition, also often there is stomach in ground beetle
Disease, its symptom is that loss of appetite, activity are slow, has loose bowels (normal fecal stools are granular), has bad physiques, and female soft-shelled turtle miscarriage occurs or has difficult labour
And it is dead.
In view of this, it is necessary to which the diseases prevention technology of OPISTHOPLATIA is further studied, so as to ensure the yield of ground beetle
And drug effect.
【The content of the invention】
The present invention goal of the invention be：For above-mentioned problem, there is provided a kind of OPISTHOPLATIA diseases prevention medicament and its
Preparation method, the diseases prevention medicament is nontoxic to human body and ground beetle, has functions that necessarily to drive away ant, and by sterilized, heat-clearing solution
It is slow that poison, the pharmacological function effect of function of spleen and stomach regulating prevent ground beetle from loss of appetite, activity occurring, the stomach disease such as have loose bowels, have bad physiques
Disease, prevention OPISTHOPLATIA goes mouldy death；So as to ensure the yield and drug effect of OPISTHOPLATIA for raiser.
To achieve these goals, the technical solution used in the present invention is as follows：
A kind of OPISTHOPLATIA diseases prevention medicament, is made up of the raw material of following weight portion：Pine needle 30-40 parts, root bark of white mulberry 8-12
Part, barley young leaf 6-10 parts, radish seed 10-15 parts, cloves 10-15 parts, Chinese peashrub root 12-18 parts, eleusine indica 20-30 parts, French beans
5-10 parts, caraway 5-6 parts, activating agent 8-12 parts；
The activating agent is obtained by the following method：By weight, sepiolite clay 80-100 parts are taken, quality is dense
The nitric acid 150-200 parts for 18-25% are spent, concentration is acetic acid 65-78 parts of 0.2-0.3mol/L, first by sepiolite clay and nitre
After acid mixing, the stirring reaction 1.5-2 hour at a temperature of 80-90 DEG C is subsequently adding acetic acid and stirs at a temperature of 50-60 DEG C
Reaction 1-1.5 hours；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 2-3 time, Ran Houjing
First drying obtains the sepiolite clay after acid treatment, and the sepiolite clay after acid treatment and sodium acid carbonate 8-10 parts are mixed,
Another rising adds and is suspended in 200-300 part triethanolamines, after stirring, adds 30-45 part myristic acids, Ran Hou
At a temperature of 70-80 DEG C, stirring reaction 15-20 minute, then use filter paper suction filtration, the solid portion for obtaining is washed into 2- with ethanol
3 times, most after 150-200 mesh be crushed to Jing after secondary drying obtain the activating agent.
It is further preferred that the OPISTHOPLATIA diseases prevention medicament is made up of the raw material of following weight portion：35 parts of pine needle, mulberry
White 10 parts of skin, 8 parts of barley young leaf, 12 parts of radish seed, 13 parts of cloves, 16 parts of Chinese peashrub root, 25 parts of eleusine indica, 7 parts of French beans, caraway 5
Part, 10 parts of activating agent.
It is further preferred that the first drying and secondary temperature are 95-100 DEG C.
It is further preferred that the pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans,
Caraway is dry product.
It is further preferred that the sepiolite clay is 100-120r/min with mixing speed during nitric acid reaction, add
Mixing speed after acetic acid is also 100-120r/min.
It is further preferred that the sepiolite clay after the acid treatment and sodium acid carbonate, triethanolamine, myristic acid are stirred
Speed is mixed for 700-1000r/min.
The preparation method of above-mentioned OPISTHOPLATIA diseases prevention medicament, comprises the following steps：Weigh by weight pine needle, the root bark of white mulberry,
Barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway, activating agent, by pine needle, the root bark of white mulberry, barley young leaf, Lay
Fu, cloves, Chinese peashrub root, eleusine indica, French beans, caraway wear into the powder of 100-120 mesh after being respectively dried, then mixed with activating agent
Close uniform, then place 5-10 minutes at a temperature of 100-120 DEG C and carry out disinfection, obtain final product the diseases prevention medicament.
Raw materials used effect is as follows in the present invention：
Pine needle, taste acid is pained, warm in nature, nontoxic.Enter the heart, spleen, Liver Channel.Can dispel pathogenic wind and remove dampness, desinsection is antipruritic.Cure mainly rheumatism impotence
Numbness, wet sore mange etc..《Compendium of Materia Medica》Speech, pine needle long-term taking controls all kinds of diseases and ailments, five viscera settling, piliation, resistance to cold and heat, the rain of resistance to wind
Beat, beneficial gas of making light of one's life by commiting suicide ward off paddy macrobiosis in keeping.Pine needle based on remove pathogenic factor, do not give birth to by Xie Quze Zhengan County, disease, not hungry so as to obtain
The actual effect of macrobiosis.
The root bark of white mulberry, sweet and slightly bitter taste has hypoglycemic, diuresis, human body AIDS virus HIV, the effect such as antibacterial.The root bark of white mulberry is decocted
Agent has stronger inhibitory action to staphylococcus aureus；Also there is slight suppression to make to typhoid bacillus and shigella flexneri
With.Mulberry skin furans A has stronger bacteriostatic activity to staphylococcus aureus, mycobacterium.Cyclomorusin also has antimycotic work
With.
Barley young leaf, is seedling of the barley growth to 20-30 centimetres, and various nutrients contained by the seedling in this period are the richest
Richness, it contains various natural complex and mineral matter (being different from synthetic) vitamin, mineral matter, can participate in life entity
Energetic supersession, the reparation of cell, the balance of soda acid.
Radish seed, the active material contained by it has significant inhibitory action to staphylococcus and Escherichia coli etc., to same
Disposition trichophyta, oidium schoenleinii, Du's Ang Shi sporidiole bacterias difficult to understand, the little gemma tinea bacterium of rust, the little gemma tinea bacterium of ulotrichy and
Star nocardia also has different degrees of inhibitory action.
Cloves, can alleviate abdominal bloating, strengthen digestion power, also act on antibacterial, worm-expelling, and Jing the applicant checking is fitted
The cloves of amount is harmless to ground bettle.
Chinese peashrub root, enters lung channel, the spleen channel.With clearing lung-heat benefit spleen, effect of blood circulation and channel invigorating.Cure mainly the weak leukorrhea of spleen kidney deficiency, consumptive disease wound
Wind formation from blood deficiency, damp and hot itch.
Eleusine indica, it is sweet, put down, it is nontoxic.Effect with heat-clearing, dampness removing.Cure mainly and hinder heat heating, acute infantile convulsion, jaundice, dysentery
Disease, gonorrhoea, difficult urination, and encephalitis can be prevented and treated.The pan-fried water of this grass, informal dress takes in a large number, poison when having epidemic prevention, anti-seasonal febrile diseases is passed on from one to another from ancient times strange
Effect.
French beans, it is sweet, mild-natured, return, stomach, gas delicate fragrance and do not go here and there, it is warm in nature and and light yellow complexion, most close with temperament.Have invigorating the spleen,
With in, beneficial gas, dampness elimination, the effect of relieve summer heat.Insufficiency of the spleen and wet, anorexia and loose stool is cured mainly, wet turbid bet, women's under band is excessive, summer-heat and damp wound
In, the card such as convulsion of vomiting and diarrhoea.
Caraway, property and flavor of peppery and warm perfume (or spice) is altered, interior logical heart spleen, outward up to four limbs, can whet the appetite disappear it is strongly fragrant can also analgesic antidotal.For in we
Also there is the effect for driving away ant.
Activating agent, is first passed through after acidification by sepiolite clay, then is obtained with sodium acid carbonate and myristic acid are modified
Pale powder, the effect with sterilized and except mite, being used together with other raw materials can produce synergy, can strengthen other
The drug effect of raw material.
The method for carrying out disease prevention and cure using above-mentioned OPISTHOPLATIA diseases prevention medicament is：The each two moon is all using the medicine of the present invention
Agent is sprayed in OPISTHOPLATIA culturing pool or basin and is once prevented epidemic, every time continuous sprinkling 3-6 days, once a day, sprinkling every time
Amount is every square metre of cultured area sprinkling 80-100g, is mixed thoroughly with compost after sprinkling.
In sum, as a result of above-mentioned technical proposal, the invention has the beneficial effects as follows：The OPISTHOPLATIA of the present invention is prevented
Sick medicament is with pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway, activating agent
Made by, pine needle can uncharm Zhengan County；Chinese peashrub root, French beans energy strengthening the spleen and stomach；The root bark of white mulberry, radish seed can sterilized detoxification, eleusine indica energy
The anti-seasonal febrile diseases of heat-clearing；Cloves, caraway can drive away ant and acarid；Barley young leaf can adjust the internal metabolism of ground bettle；Activating agent energy
Soil ph is adjusted, and can disinfecting mite-removing and the drug effect for strengthening other raw materials；10 kinds of raw materials act synergistically together, with certain
Drive away ant, sterilized effect prevented or cure a disease, and prevent ground beetle generation loss of appetite, activity slow by common pharmacological function effect
Slowly, the gastrointestinal disease such as have loose bowels, have bad physiques, prevention OPISTHOPLATIA goes mouldy death；So as to ensure the product of OPISTHOPLATIA for raiser
Amount and drug effect.
【Specific embodiment】
In order to more clearly express the present invention, below by way of specific embodiment, the invention will be further described.
Embodiment 1
A kind of OPISTHOPLATIA diseases prevention medicament, is made up of the raw material of following weight portion：30 parts of pine needle, 8 parts of the root bark of white mulberry, barley
If 6 parts of leaf, 10 parts of radish seed, 10 parts of cloves, 12 parts of Chinese peashrub root, 20 parts of eleusine indica, 5 parts of French beans, 5 parts of caraway, 8 parts of activating agent；
Pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are dry product.
The preparation method of above-mentioned OPISTHOPLATIA diseases prevention medicament, comprises the following steps：
(1) activating agent is prepared：By weight, 80 parts of sepiolite clay is taken, mass concentration is 18% 200 parts of nitric acid,
Concentration is 78 parts of the acetic acid of 0.2mol/L, is 100r/min in 80 DEG C, mixing speed after first sepiolite clay is mixed with nitric acid
Under conditions of stirring reaction 2 hours, be subsequently adding stirring reaction under conditions of acetic acid is 100r/min in 50 DEG C, mixing speed
1.5 hour；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 3 times, then in 95 DEG C of baking ovens
The middle sepiolite clay Jing after first drying obtains acid treatment, by the 8 parts of mixings of the sepiolite clay after acid treatment and sodium acid carbonate,
Another rising adds and is suspended in 200 parts of triethanolamines, after stirring, 30 parts of myristic acids is added, then at 70-80 DEG C
At a temperature of, mixing speed be stirring reaction 20 minutes under conditions of 700r/min, filter paper suction filtration is then used, by the solid part for obtaining
Divide and washed with ethanol 2 times, be crushed to 150 mesh after finally drying in 95-100 DEG C of baking oven and obtain the activating agent.
(2) pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, perfume (or spice) are weighed by weight
Dish, activating agent, pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are respectively dried
The powder of 100 mesh is worn into afterwards, is then well mixed with activating agent, then placed at a temperature of 100 DEG C and carry out disinfection for 10 minutes, i.e.,
Obtain the diseases prevention medicament.
Embodiment 2
A kind of OPISTHOPLATIA diseases prevention medicament, is made up of the raw material of following weight portion：35 parts of pine needle, 10 parts of the root bark of white mulberry, greatly
8 parts of Mai Ruoye, 12 parts of radish seed, 13 parts of cloves, 16 parts of Chinese peashrub root, 25 parts of eleusine indica, 7 parts of French beans, 5 parts of caraway, activating agent 10
Part；Pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are dry product.
The preparation method of above-mentioned OPISTHOPLATIA diseases prevention medicament, comprises the following steps：
(1) activating agent is prepared：By weight, 85 parts of sepiolite clay is taken, mass concentration is 20% 160 parts of nitric acid,
Concentration is 76 parts of the acetic acid of 0.22mol/L, is 105r/ in 82 DEG C, mixing speed after first sepiolite clay is mixed with nitric acid
Stirring reaction 1.8 hours under conditions of min, are subsequently adding under conditions of acetic acid is 105r/min in 55 DEG C, mixing speed and stir
Reaction 1.2 hours；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 3 times, then at 98 DEG C
Sepiolite clay in baking oven Jing after first drying obtains acid treatment, by 9 parts of the sepiolite clay after acid treatment and sodium acid carbonate
Mix, another rising adds and be suspended in 210 parts of triethanolamines, after stirring, 32 parts of myristic acids are added, then in 70-
At a temperature of 80 DEG C, mixing speed be stirring reaction 18 minutes under conditions of 750r/min, filter paper suction filtration is then used, by what is obtained
Solid portion ethanol is washed 3 times, is crushed to 200 mesh after finally drying in 98 DEG C of baking ovens and is obtained the activating agent；
(2) pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, perfume (or spice) are weighed by weight
Dish, activating agent, pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are respectively dried
The powder of 120 mesh is worn into afterwards, is then well mixed with activating agent, then placed at a temperature of 120 DEG C and carry out disinfection for 6 minutes, i.e.,
Obtain the diseases prevention medicament.
Embodiment 3
A kind of OPISTHOPLATIA diseases prevention medicament, is made up of the raw material of following weight portion：32 parts of pine needle, 9 parts of the root bark of white mulberry, barley
If 7 parts of leaf, 11 parts of radish seed, 12 parts of cloves, 15 parts of Chinese peashrub root, 22 parts of eleusine indica, 6 parts of French beans, 5 parts of caraway, 8 parts of activating agent；
Pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are dry product.
The preparation method of above-mentioned OPISTHOPLATIA diseases prevention medicament, comprises the following steps：
(1) activating agent is prepared：By weight, 95 parts of sepiolite clay is taken, mass concentration is 22% 180 parts of nitric acid,
Concentration is 70 parts of the acetic acid of 0.28mol/L, is 108r/ in 88 DEG C, mixing speed after first sepiolite clay is mixed with nitric acid
Stirring reaction 1.8 hours under conditions of min, are subsequently adding under conditions of acetic acid is 108r/min in 55 DEG C, mixing speed and stir
Reaction 1.2 hours；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 2 times, then at 98 DEG C
Sepiolite clay in baking oven Jing after first drying obtains acid treatment, by 10 parts of the sepiolite clay after acid treatment and sodium acid carbonate
Mix, another rising adds and be suspended in 260 parts of triethanolamines, after stirring, 42 parts of myristic acids are added, then at 75 DEG C
At a temperature of, mixing speed be stirring reaction 18 minutes under conditions of 800r/min, filter paper suction filtration is then used, by the solid for obtaining
Part is washed 2 times with ethanol, is crushed to 150 mesh after finally drying in 96 DEG C of baking ovens and is obtained the activating agent；
(2) pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, perfume (or spice) are weighed by weight
Dish, activating agent, pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are respectively dried
The powder of 120 mesh is worn into afterwards, is then well mixed with activating agent, then placed at a temperature of 105 DEG C and carry out disinfection for 9 minutes, i.e.,
Obtain the diseases prevention medicament.
Embodiment 4
A kind of OPISTHOPLATIA diseases prevention medicament, is made up of the raw material of following weight portion：36 parts of pine needle, 10 parts of the root bark of white mulberry, greatly
8 parts of Mai Ruoye, 12 parts of radish seed, 12 parts of cloves, 15 parts of Chinese peashrub root, 23 parts of eleusine indica, 7 parts of French beans, 6 parts of caraway, activating agent 11
Part；Pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are dry product.
The preparation method of above-mentioned OPISTHOPLATIA diseases prevention medicament, comprises the following steps：
(1) activating agent is prepared：By weight, 95 parts of sepiolite clay is taken, mass concentration is 22% 180 parts of nitric acid,
Concentration is 70 parts of the acetic acid of 0.28mol/L, is 108r/ in 88 DEG C, mixing speed after first sepiolite clay is mixed with nitric acid
Stirring reaction 1.8 hours under conditions of min, are subsequently adding under conditions of acetic acid is 108r/min in 55 DEG C, mixing speed and stir
Reaction 1.2 hours；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 2 times, then at 98 DEG C
Sepiolite clay in baking oven Jing after first drying obtains acid treatment, by 10 parts of the sepiolite clay after acid treatment and sodium acid carbonate
Mix, another rising adds and be suspended in 260 parts of triethanolamines, after stirring, 42 parts of myristic acids are added, then at 75 DEG C
At a temperature of, mixing speed be stirring reaction 18 minutes under conditions of 800r/min, filter paper suction filtration is then used, by the solid for obtaining
Part is washed 2 times with ethanol, is crushed to 150 mesh after finally drying in 96 DEG C of baking ovens and is obtained the activating agent；
(2) pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, perfume (or spice) are weighed by weight
Dish, activating agent, pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are respectively dried
The powder of 120 mesh is worn into afterwards, is then well mixed with activating agent, then placed at a temperature of 110 DEG C and carry out disinfection for 8 minutes, i.e.,
Obtain the diseases prevention medicament.
Embodiment 5
A kind of OPISTHOPLATIA diseases prevention medicament, is made up of the raw material of following weight portion：38 parts of pine needle, 9 parts of the root bark of white mulberry, barley
If 9 parts of leaf, 12 parts of radish seed, 11 parts of cloves, 17 parts of Chinese peashrub root, 28 parts of eleusine indica, 8 parts of French beans, 6 parts of caraway, 11 parts of activating agent；
Pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are dry product.
The preparation method of above-mentioned OPISTHOPLATIA diseases prevention medicament, comprises the following steps：
(1) activating agent is prepared：By weight, 98 parts of sepiolite clay is taken, mass concentration is 20% 180 parts of nitric acid,
Concentration is 75 parts of the acetic acid of 0.22mol/L, is 100r/ in 90 DEG C, mixing speed after first sepiolite clay is mixed with nitric acid
Stirring reaction 1.5 hours under conditions of min, are subsequently adding under conditions of acetic acid is 120r/min in 50 DEG C, mixing speed and stir
Reaction 1 hour；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 2 times, then in 95 DEG C of bakings
Sepiolite clay in case Jing after first drying obtains acid treatment, by 8.5 parts of the sepiolite clay after acid treatment and sodium acid carbonate
Mix, another rising adds and be suspended in 290 parts of triethanolamines, after stirring, 42 parts of myristic acids are added, then at 75 DEG C
At a temperature of, mixing speed be stirring reaction 16 minutes under conditions of 950r/min, filter paper suction filtration is then used, by the solid for obtaining
Part is washed 2 times with ethanol, is crushed to 200 mesh after finally drying in 100 DEG C of baking ovens and is obtained the activating agent；
(2) pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, perfume (or spice) are weighed by weight
Dish, activating agent, pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are respectively dried
The powder of 100 mesh is worn into afterwards, is then well mixed with activating agent, then placed at a temperature of 120 DEG C and carry out disinfection for 5 minutes, i.e.,
Obtain the diseases prevention medicament.
Embodiment 6
A kind of OPISTHOPLATIA diseases prevention medicament, is made up of the raw material of following weight portion：40 parts of pine needle, 12 parts of the root bark of white mulberry, greatly
10 parts of Mai Ruoye, 15 parts of radish seed, 15 parts of cloves, 18 parts of Chinese peashrub root, 30 parts of eleusine indica, 10 parts of French beans, 6 parts of caraway, activating agent
12 parts；Pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are dry product.
The preparation method of above-mentioned OPISTHOPLATIA diseases prevention medicament, comprises the following steps：
(1) activating agent is prepared：By weight, 100 parts of sepiolite clay is taken, mass concentration is 25% 200 parts of nitric acid,
Concentration is 65 parts of the acetic acid of 0.3mol/L, is 120r/min in 90 DEG C, mixing speed after first sepiolite clay is mixed with nitric acid
Under conditions of stirring reaction 1.5 hours, be subsequently adding stirring reaction under conditions of acetic acid is 120r/min in 60 DEG C, mixing speed
1 hour；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 2 times, then in 100 DEG C of baking ovens
The middle sepiolite clay Jing after first drying obtains acid treatment, 10 parts of the sepiolite clay after acid treatment and sodium acid carbonate are mixed
Even, another rising adds and is suspended in 300 parts of triethanolamines, after stirring, 45 parts of myristic acids is added, then at 80 DEG C
At a temperature of, mixing speed be stirring reaction 15 minutes under conditions of 1000r/min, filter paper suction filtration is then used, by the solid for obtaining
Part is washed 3 times with ethanol, is crushed to 150 mesh after finally drying in 100 DEG C of baking ovens and is obtained the activating agent；
(2) pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, perfume (or spice) are weighed by weight
Dish, activating agent, pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are respectively dried
The powder of 110 mesh is worn into afterwards, is then well mixed with activating agent, then placed at a temperature of 100 DEG C and carry out disinfection for 10 minutes, i.e.,
Obtain the diseases prevention medicament.
The method for carrying out disease prevention and cure using above-mentioned OPISTHOPLATIA diseases prevention medicament is：The each two moon is all using the medicine of the present invention
Agent is sprayed in OPISTHOPLATIA culturing pool or basin and is once prevented epidemic, every time continuous sprinkling 3-6 days, once a day, sprinkling every time
Amount is every square metre of cultured area sprinkling 80-100g, is mixed thoroughly with compost after sprinkling.
In order to preferably state beneficial effects of the present invention, now illustrated by test.
1st, subjects：Using the Breeding container of 6 formed objects, identical number is thrown in by same feed method in every basin
Amount, the OPISTHOPLATIA in identical worm age, each Breeding container is used as a test group.
2nd, test method：The each two moon is sprayed in OPISTHOPLATIA cultivation pot with diseases prevention medicament and is once prevented epidemic, every time
The continuous sprinkling of epidemic prevention 4 days, sprays daily once, and each fountain height is each basin sprinkling 60g, mixes thoroughly with compost after sprinkling.Support
The sick situation of record ground beetle during growing, records the quantity of the OPISTHOPLATIA of death of going mouldy, and adult ground beetle, cultivation 8 are collected in time
After individual month, the yield of ground beetle dry product is counted.
Test group 1-3：Prevented and treated using the medicament made by the embodiment of the present invention 1,2,6 respectively.
Contrast groups 1：Activating agent is not contained in medicament used；It is by 35 parts of pine needle, 10 parts of the root bark of white mulberry, 8 parts of barley young leaf, Lay
12 parts of Fu, 13 parts of cloves, 16 parts of Chinese peashrub root, 25 parts of eleusine indica, 7 parts of French beans, 5 parts of caraway is pulverized and mixed and disappears after drying
Poison is obtained.
Contrast groups 2：Barley young leaf, cloves, activating agent are not contained in medicament used, are 10 parts of the root bark of white mulberry by 35 parts of pine needle,
12 parts of radish seed, 16 parts of Chinese peashrub root, 25 parts of eleusine indica, 7 parts of French beans, 5 parts of caraway, be pulverized and mixed and sterilize system after drying
.
Contrast groups 3：Medicament used is by being by 35 parts of pine needle, 10 parts of the root bark of white mulberry, 8 parts of barley young leaf, 12 parts of radish seed, fourth
Fragrant 13 parts, 16 parts of Chinese peashrub root, 25 parts of eleusine indica, 7 parts of French beans, 5 parts of caraway is pulverized and mixed and the system of sterilizing after 10 parts of drying of activating agent
, but activating agent is sepiolite clay.
3rd, result of the test：It is shown in Table 1.
The OPISTHOPLATIA protection effect of table 1
From the results shown in Table 1, the embodiment of the present invention is as a result of the more preferable anti-disease medicines of effect, gained ground beetle
Yield and quality be superior to contrast groups.And from contrast groups 1 as can be seen that increasing to the dead number of elements that goes mouldy without activating agent
Plus, yield declines, and ground beetle quality illustrates to add the effect that activating agent serves the drug effect of medicine synergy also not as the present invention.
From contrast groups 1 and contrast groups 3 it can also be seen that when activating agent is without peracid and modification, the number of elements of death of going mouldy with
The contrast groups 1 for being not added with activating agent are more or less the same, and illustrate that the activating agent after activation just has obvious synergistic effect to medicament.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this
Bright patent claim, the equal change completed under the technical spirit suggested by all present invention or modification change, all should belong to
Cover the scope of the claims in the present invention.
Claims (7)
1. a kind of OPISTHOPLATIA diseases prevention medicament, it is characterised in that be made up of the raw material of following weight portion：Pine needle 30-40 parts, mulberry
White skin 8-12 parts, barley young leaf 6-10 parts, radish seed 10-15 parts, cloves 10-15 parts, Chinese peashrub root 12-18 parts, eleusine indica 20-30
Part, French beans 5-10 parts, caraway 5-6 parts, activating agent 8-12 parts；
The activating agent is obtained by the following method：By weight, sepiolite clay 80-100 parts are taken, mass concentration is
Nitric acid 150-200 parts of 18-25%, concentration is acetic acid 65-78 parts of 0.2-0.3mol/L, first mixes sepiolite clay with nitric acid
After conjunction, the stirring reaction 1.5-2 hour at a temperature of 80-90 DEG C is subsequently adding acetic acid stirring reaction at a temperature of 50-60 DEG C
1-1.5 hour；Reaction uses filter paper suction filtration after terminating, and the solid portion for obtaining is washed with deionized 2-3 time, and then Jing is once
Drying obtains the sepiolite clay after acid treatment, the sepiolite clay after acid treatment and sodium acid carbonate 8-10 parts is mixed, further
Rise and add and be suspended in 200-300 part triethanolamines, after stirring, 30-45 part myristic acids are added, then in 70-80
At a temperature of DEG C, stirring reaction 15-20 minute, then use filter paper suction filtration, the solid portion for obtaining is washed 2-3 time with ethanol,
150-200 mesh is crushed to after most Jing after secondary drying obtain the activating agent.
2. a kind of OPISTHOPLATIA diseases prevention medicament according to claim 1, it is characterised in that be by the raw material of following weight portion
Make：35 parts of pine needle, 10 parts of the root bark of white mulberry, 8 parts of barley young leaf, 12 parts of radish seed, 13 parts of cloves, 16 parts of Chinese peashrub root, eleusine indica 25
Part, 7 parts of French beans, 5 parts of caraway, 10 parts of activating agent.
3. a kind of OPISTHOPLATIA diseases prevention medicament according to claim 1, it is characterised in that：The first drying and secondary
Temperature is 95-100 DEG C.
4. a kind of OPISTHOPLATIA diseases prevention medicament according to claim 1, it is characterised in that：The pine needle, the root bark of white mulberry, barley
If leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are dry product.
5. a kind of OPISTHOPLATIA diseases prevention medicament according to claim 1, it is characterised in that：The sepiolite clay and nitric acid
Mixing speed during reaction is 100-120r/min, adds the mixing speed after acetic acid to be also 100-120r/min.
6. a kind of OPISTHOPLATIA diseases prevention medicament according to claim 1, it is characterised in that：Sepiolite after the acid treatment
Clay is 700-1000r/min with the mixing speed of sodium acid carbonate, triethanolamine, myristic acid.
7. the preparation method of the OPISTHOPLATIA diseases prevention medicament according to any one of claim 1-6, it is characterised in that include
Following steps：Pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, perfume (or spice) are weighed by weight
Dish, activating agent, pine needle, the root bark of white mulberry, barley young leaf, radish seed, cloves, Chinese peashrub root, eleusine indica, French beans, caraway are respectively dried
The powder of 100-120 mesh is worn into afterwards, is then well mixed with activating agent, then place 5-10 minutes at a temperature of 100-120 DEG C
Carry out disinfection, obtain final product the diseases prevention medicament.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611197370.4A CN106620415A (en) | 2016-12-22 | 2016-12-22 | Disease-prevention oriental cockroach medicament and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197609A (en) * | 1997-04-29 | 1998-11-04 | 么向和 | Feed mildew preventive |
| CN105028973A (en) * | 2015-05-27 | 2015-11-11 | 桐城市杨清土元养殖有限公司 | Ground beetle yield increasing breeding feed |
-
2016
- 2016-12-22 CN CN201611197370.4A patent/CN106620415A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197609A (en) * | 1997-04-29 | 1998-11-04 | 么向和 | Feed mildew preventive |
| CN105028973A (en) * | 2015-05-27 | 2015-11-11 | 桐城市杨清土元养殖有限公司 | Ground beetle yield increasing breeding feed |
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