CN106619161A - One-dosage type warm-molding hair perming agent and preparation method thereof - Google Patents
One-dosage type warm-molding hair perming agent and preparation method thereof Download PDFInfo
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- CN106619161A CN106619161A CN201611024510.8A CN201611024510A CN106619161A CN 106619161 A CN106619161 A CN 106619161A CN 201611024510 A CN201611024510 A CN 201611024510A CN 106619161 A CN106619161 A CN 106619161A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/04—Preparations for permanent waving or straightening the hair
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Abstract
The invention relates to a one-dosage type warm-molding hair perming agent which comprises the following raw materials in percentage by mass: 2-8% of hydrosulphite, 0.5-2% of ethanolamine, 0.05-0.5% of a p-hydroxybenzoic acid ester, 1-5% of a penetrant, 0.5-3% of air permeable oil, 2-6% of cystine and the balance of water. The one-dosage type warm-molding hair perming agent can be directly applied to aluminum foil, coiled hair is wrapped by the aluminum foil so as to enable the hair perming agent to be in contact with hair, and the hair can be permed after the aluminum foil is heated for about 10 minutes (about 1 hour if a conventional warm-molding hair perming process is used). The one-dosage type warm-molding hair perming agent is rapid in shape fixation, simple in working process, long in lasting time of coiled hair (about half a year), good in hair perming effect, high in reliability, simple in preparation process, easy to operate, high in production efficiency, high in product pass percentage and applicable to large-scale popularization and application, the hair perming time can be greatly shortened, and the hair is not damaged.
Description
Technical field
The present invention relates to heavy chemicals technical field, more particularly to a kind of one formula temperature modeling agent for permanent hair waving and preparation method thereof.
Background technology
It is a kind of common method for permanent waving hair that temperature modeling is scalded, and it mainly includes two steps:1st, using the medicament destruction head of alkalescence
The hair scale piece sent out so as to can be crimped by blanching;2nd, hair is repaired using acid medicament, when extending frizzly continuing
Between, it is to avoid hair excessively dries up.
Scalding medicament using the modeling of existing two doses of formula temperature carries out the boiling hot operation of temperature modeling, and the flow process of operation is complicated, the time is expended, to sending out
The destruction of matter is serious, and the frizzly duration is short, and hair-waving effect is poor, there is improved necessity.
The content of the invention
The present invention provides a kind of one formula temperature modeling agent for permanent hair waving and preparation method thereof to overcome drawbacks described above, one formula
Temperature modeling agent for permanent hair waving can be directly coated on aluminium foil, and then the aluminium foil is wrapped the hair for having spooled moulding, make agent for permanent hair waving
Contact with hair, then aluminium foil is heated complete by 10 minutes or so (existing temperature modeling ironing process needs to perm 1 hour or so)
Into hair-waving, sizing is quick, and work flow is simple, highly shortened the hair-waving time, hair quality is not destroyed, when frizzly lasting
Between long (or so half a year), hair-waving effect is good, and reliability is high;One formula temperature moulds the preparation method process is simple of agent for permanent hair waving, operation
Easily, production efficiency is high, and product percent of pass is high, is suitable for large-scale promotion application.
For achieving the above object, the present invention is adopted the following technical scheme that.
A kind of one formula temperature moulds agent for permanent hair waving, including the raw material of following mass percent:
Bisulfites is the inorganic salts that a class has bisulfite, and its solution is in faintly acid.
Monoethanolamine, colourless liquid is at room temperature water white thick liquid, has hygroscopicity and ammonia smelly.Monoethanolamine
The aqueous solution has extremely strong hygroscopicity in alkalescence, can absorb sour gas, again can be by the gas release for absorbing after heating.There is emulsification
And bubble.Salt can be generated with inorganic acid and organic acid, with acid anhydrides effect ester is generated.Hydrogen atom in its amino can be by acyl
Halogen, alkyl halide etc. are replaced.
P-hydroxybenzoate, white crystalline powder or colourless crystallization, are soluble in alcohol, ether and acetone, atomic to be dissolved in water, boiling
270-280 DEG C of point.Organic synthesis, food, cosmetics, the sterilization antiseptic of medicine are mainly used as, are also served as in feed anticorrosion agent.
Because it has phenolic hydroxyl structure, so bacteria resistance can be all stronger than benzoic acid, sorbic acid.Its mechanism of action is:Destroy micro- life
The cell membrane of thing, makes intracellular protein denaturation, and can suppress the breathing enzyme system and electron transmission enzyme system of microbial cell
Activity.
Bleeding agent plays osmosis, with fixed hydrophilic lipophilic group, aligns in the surface energy of solution, and can make
Surface tension is remarkably decreased.
Preferably, the bleeding agent is one or two mixture of penetrating agent JFC and fast penetrant T.
Penetrating agent JFC is AEO, belongs to nonionic surfactant, soluble in water, acidproof, alkaline-resisting, resistance to
Chlorine, heat-resisting, resistance to hard water, resistance to slaine, wetability, rewettability are good, and with emulsification and clean result.
Fast penetrant T belongs to anion surfactant, by maleic anhydride and sec-octyl alcohol in Catalyzed by p-Toluenesulfonic Acid
Under agent catalysis, it is esterified in 120-140 DEG C, then carries out sulfonation with sodium hydrogensulfite and be obtained, its permeability, wetability, breast
Agent, foaming characteristic are all preferable.
Ventilative oil is mainly used in toiletries, and its permeability is good, the effect of tool antiperspirant and skin affinity are strong, is excellent
Skin emollient, its stable performance is oxidizable or produce peculiar smell, skin can be made soft soft and without greasy feeling, good penetrability,
It is usually used in all kinds of face cream.In cosmetics as in extension agent, the joint agent of press-powder formula cosmetics and color make-up pigment it is good
Solvent.In being usually used in the formula such as vanishing cream, sunscreen productses, eye shadow, lipstick, mascara.Softening agent, dispersant are alternatively arranged as, in profit
Apply in the formula such as hair-cream, shower cream.
Preferably, the ventilative oil is isobutyl palmitate.
Cystine, white hexagon plate crystal or white crystalline powder, it has three kinds of isomers:Levo form (L- Guang ammonia
Acid), d-isomer (D- cystines), mesomer.The purposes of cystine:For biochemistry and nutrient research, pharmaceutically there is rush
Enter body cell oxidation and reduce function, increase white blood cell and prevent the effects such as pathogen development.It is mainly used in various baldness.
The acute infectious diseases such as dysentery, typhoid fever, influenza, asthma, neuralgia, eczema and various poisoning illness etc. are also used for, and have maintenance
The effect of protein configuration.Also serve as food flavor.
Preferably, a kind of one formula temperature moulds agent for permanent hair waving, including the raw material of following mass percent:
Preferably, a kind of one formula temperature moulds agent for permanent hair waving, including the raw material of following mass percent:
Wherein, one formula temperature modeling agent for permanent hair waving also includes seawater collagen with micro- extract, the seawater
Collagen accounts for the 2~6% of total raw material mass percent with micro- extract.
Seawater collagen herein is referred to by Patent No. CN201420254388 (title with micro- extract
Be the device that collagen and element are extracted with seawater) equipment from seawater the direct mixed liquor of extraction, the mixed liquor contains
Molecule is little in the seawater of the depth that sunlight cannot be reached in ocean, light weight and absorbable collagen and element.
Wherein, the one formula temperature modeling agent for permanent hair waving also includes spices, the spices account for total raw material mass percent 0.1~
0.5%.
Spices be it is a kind of fragrance can be smelt by smell or the sense of taste tastes the material of fragrance, be the raw material for preparing essence.
Wherein, the bisulfites is sodium hydrogensulfite, potassium bisulfite, bisulfite lithium, calcium bisulfite, sulfurous
One or more mixture of sour hydrogen magnesium and barium bisulfite.
Preferably, the bisulfites is sodium hydrogensulfite.
Sodium hydrogensulfite, white crystalline powder.There are the smell of sulfur dioxide, the unhappy taste of tool.Lose in exposure air
Part sulfur dioxide, simultaneous oxidation is into sulfate.3.5 parts of cold water, 2 parts of boiling water, about 70 parts of ethanol are dissolved in, its aqueous solution is in acid
Property.
Wherein, the monoethanolamine is one or more mixture of monoethanolamine, diethanol amine and triethanolamine.
Preferably, the monoethanolamine is monoethanolamine.
Monoethanolamine is a kind of organic compound, english abbreviation ETA or MEA, and chemical formula C2H7NO is that a kind of primary amine is organic
Compound.With hygroscopicity, toxicity, combustibility and corrosivity.It is present in phosphatide, and coexists with choline, therefore monoethanolamine is also referred to as
For cholamine.
Wherein, the p-hydroxybenzoate is methyl parabens, ethyl p-hydroxybenzoate, propyl group pair
One or more mixture of hydroxybenzoate and butyl parabens.
Preferably, the p-hydroxybenzoate is propyl para-hydroxybenzoate.
Wherein, the cystine is one or two mixture of CYSTINE and D- cystines.
Preferably, the cystine is CYSTINE.
CYSTINE refers to the levo form of cystine.CYSTINE be 1810 by Wollaston from vesical calculus
It was found that.1832, Betzelius was named as cystine, and it is a kind of sulfur-containing amino acid, is had in protein and is deposited on a small quantity
In being contained in the keratin of hair, paw etc. more.White hexagon platelike crystal or crystalline powder.Odorless, it is tasteless.It is dissolved in dilute
Acid and alkaline solution, it is atomic to be dissolved in water, insoluble in ethanol, ether, benzene and chloroform.
A kind of one formula temperature moulds the preparation method of agent for permanent hair waving, including following procedure of processing:
Step A, according to formula weigh appropriate material, in being placed individually into different containers;
Step B, monoethanolamine is added to into reactor, toward reactor bisulfites is added, it is stirring while adding so that sulfurous
Sour hydrogen salt is uniformly dispersed;
Step C, past reactor add p-hydroxybenzoate, stirring while adding so that p-hydroxybenzoate dispersion is equal
It is even;
Step D, past reactor add bleeding agent, stirring while adding so that bleeding agent is uniformly dispersed;
Step E, oil of breathing freely toward reactor addition, it is stirring while adding so that ventilative oil dispersed is uniform;
Step F, past reactor add cystine, stirring while adding so that cystine is uniformly dispersed;
Step G, past reactor add water, stir, and get product.
Beneficial effects of the present invention are:A kind of one formula temperature modeling agent for permanent hair waving of the present invention, one formula temperature moulds agent for permanent hair waving energy
It is enough to be directly coated on aluminium foil, then the aluminium foil is wrapped the hair for having spooled moulding, agent for permanent hair waving is contacted with hair, connect
Heat aluminium foil and complete hair-waving by (existing temperature modeling ironing process needs hair-waving 1 hour or so) in 10 minutes or so, sizing is fast
Speed, work flow is simple, highly shortened the hair-waving time, does not destroy hair quality, and (half a year is left for frizzly duration length
It is right), hair-waving effect is good, and reliability is high;One formula temperature moulds the preparation method process is simple of agent for permanent hair waving, processing ease, production effect
Rate is high, and product percent of pass is high, is suitable for large-scale promotion application.
Specific embodiment
With reference to embodiment, the present invention is further illustrated, and this is presently preferred embodiments of the present invention.
Embodiment 1.
A kind of one formula temperature modeling agent for permanent hair waving of the present embodiment, including the raw material of following mass percent:
A kind of one formula temperature moulds the preparation method of agent for permanent hair waving, including following procedure of processing:
Step A, according to formula weigh appropriate material, in being placed individually into different containers;
Step B, monoethanolamine is added to into reactor, toward reactor sodium hydrogensulfite is added, it is stirring while adding so that sub-
Niter cake is uniformly dispersed;Seawater collagen and micro- extract are added toward reactor, it is stirring while adding so that seawater
Collagen is uniformly dispersed with micro- extract;
Step C, past reactor add propyl para-hydroxybenzoate, stirring while adding so that propyl p-hydroxybenzoate
Ester is uniformly dispersed;
Step D, past reactor add bleeding agent, stirring while adding so that bleeding agent is uniformly dispersed;
Step E, oil of breathing freely toward reactor addition, it is stirring while adding so that ventilative oil dispersed is uniform;
Step F, past reactor add CYSTINE, stirring while adding so that CYSTINE is uniformly dispersed;Add toward reactor
Enter spices, it is stirring while adding so that spices is uniformly dispersed;
Step G, past reactor add water, stir, and get product.
Embodiment 2.
A kind of one formula temperature modeling agent for permanent hair waving of the present embodiment, including the raw material of following mass percent:
A kind of one formula temperature moulds the preparation method of agent for permanent hair waving, including following procedure of processing:
Step A, according to formula weigh appropriate material, in being placed individually into different containers;
Step B, diethanol amine is added to into reactor, toward reactor potassium bisulfite is added, it is stirring while adding so that sub-
Potassium acid sulfate is uniformly dispersed;Seawater collagen and micro- extract are added toward reactor, it is stirring while adding so that seawater
Collagen is uniformly dispersed with micro- extract;
Step C, past reactor add methyl parabens, stirring while adding so that methyl para hydroxy benzoic acid
Ester is uniformly dispersed;
Step D, past reactor add bleeding agent, stirring while adding so that bleeding agent is uniformly dispersed;
Step E, oil of breathing freely toward reactor addition, it is stirring while adding so that ventilative oil dispersed is uniform;
Step F, past reactor add D- cystines, stirring while adding so that D- cystines are uniformly dispersed;
Step G, past reactor add water, stir, and get product.
Embodiment 3.
A kind of one formula temperature modeling agent for permanent hair waving of the present embodiment, including the raw material of following mass percent:
A kind of one formula temperature moulds the preparation method of agent for permanent hair waving, including following procedure of processing:
Step A, according to formula weigh appropriate material, in being placed individually into different containers;
Step B, triethanolamine is added to into reactor, toward reactor bisulfite lithium is added, it is stirring while adding so that sub-
Lithium hydrogen sulfate is uniformly dispersed;
Step C, past reactor add ethyl p-hydroxybenzoate, stirring while adding so that ethyl P-hydroxybenzoic acid
Ester is uniformly dispersed;
Step D, past reactor add bleeding agent, stirring while adding so that bleeding agent is uniformly dispersed;
Step E, oil of breathing freely toward reactor addition, it is stirring while adding so that ventilative oil dispersed is uniform;
Step F, past reactor add CYSTINE, stirring while adding so that CYSTINE is uniformly dispersed;
Step G, past reactor add water, stir, and get product.
Embodiment 4.
A kind of one formula temperature modeling agent for permanent hair waving of the present embodiment, including the raw material of following mass percent:
A kind of one formula temperature moulds the preparation method of agent for permanent hair waving, including following procedure of processing:
Step A, according to formula weigh appropriate material, in being placed individually into different containers;
Step B, diethanol amine is added to into reactor, toward reactor calcium bisulfite is added, it is stirring while adding so that sub-
Calcium bisulfate is uniformly dispersed;Seawater collagen and micro- extract are added toward reactor, it is stirring while adding so that seawater
Collagen is uniformly dispersed with micro- extract;
Step C, past reactor add ethyl p-hydroxybenzoate, stirring while adding so that ethyl P-hydroxybenzoic acid
Ester is uniformly dispersed;
Step D, past reactor add bleeding agent, stirring while adding so that bleeding agent is uniformly dispersed;
Step E, oil of breathing freely toward reactor addition, it is stirring while adding so that ventilative oil dispersed is uniform;
Step F, past reactor add D- cystines, stirring while adding so that D- cystines are uniformly dispersed;Add toward reactor
Enter spices, it is stirring while adding so that spices is uniformly dispersed;
Step G, past reactor add water, stir, and get product.
Embodiment 5.
A kind of one formula temperature modeling agent for permanent hair waving of the present embodiment, including the raw material of following mass percent:
A kind of one formula temperature moulds the preparation method of agent for permanent hair waving, including following procedure of processing:
Step A, according to formula weigh appropriate material, in being placed individually into different containers;
Step B, triethanolamine is added to into reactor, toward reactor magnesium bisulfite is added, it is stirring while adding so that sub-
Magnesium bisulfate is uniformly dispersed;Seawater collagen and micro- extract are added toward reactor, it is stirring while adding so that seawater
Collagen is uniformly dispersed with micro- extract;
Step C, past reactor add methyl parabens, stirring while adding so that methyl para hydroxy benzoic acid
Ester is uniformly dispersed;
Step D, past reactor add bleeding agent, stirring while adding so that bleeding agent is uniformly dispersed;
Step E, oil of breathing freely toward reactor addition, it is stirring while adding so that ventilative oil dispersed is uniform;
Step F, past reactor add CYSTINE, stirring while adding so that CYSTINE is uniformly dispersed;Add toward reactor
Enter spices, it is stirring while adding so that spices is uniformly dispersed;
Step G, past reactor add water, stir, and get product.
Finally it should be noted that above example is only illustrating technical scheme, rather than to present invention guarantor
The restriction of shield scope, although having made to explain to the present invention with reference to preferred embodiment, one of ordinary skill in the art should
Work as understanding, technical scheme can be modified or equivalent, without deviating from the reality of technical solution of the present invention
Matter and scope.
Claims (10)
1. a kind of one formula temperature moulds agent for permanent hair waving, it is characterised in that:Including the raw material of following mass percent:
2. a kind of one formula temperature according to claim 1 moulds agent for permanent hair waving, it is characterised in that:Including following mass percent
Raw material:
3. a kind of one formula temperature according to claim 1 moulds agent for permanent hair waving, it is characterised in that:Including following mass percent
Raw material:
4. a kind of one formula temperature according to claim 1 moulds agent for permanent hair waving, it is characterised in that:Also include seawater collagen with
Micro- extract, the seawater collagen accounts for the 2~6% of total raw material mass percent with micro- extract.
5. a kind of one formula temperature according to claim 4 moulds agent for permanent hair waving, it is characterised in that:Also include spices, the spices
Account for the 0.1~0.5% of total raw material mass percent.
6. a kind of one formula temperature according to claim 1 moulds agent for permanent hair waving, it is characterised in that:The bisulfites is sulfurous
One kind or one kind of sour hydrogen sodium, potassium bisulfite, bisulfite lithium, calcium bisulfite, magnesium bisulfite and barium bisulfite with
On mixture.
7. a kind of one formula temperature according to claim 1 moulds agent for permanent hair waving, it is characterised in that:The monoethanolamine is an ethanol
One or more mixture of amine, diethanol amine and triethanolamine.
8. a kind of one formula temperature according to claim 1 moulds agent for permanent hair waving, it is characterised in that:The p-hydroxybenzoate is
Methyl parabens, ethyl p-hydroxybenzoate, propyl para-hydroxybenzoate and butyl parabens
One or more mixture.
9. a kind of one formula temperature according to claim 1 moulds agent for permanent hair waving, it is characterised in that:The cystine is CYSTINE
With one or two mixture of D- cystines.
10. a kind of one formula temperature as described in claim 1-9 any one moulds the preparation method of agent for permanent hair waving, it is characterised in that:
Including following procedure of processing:
Step A, according to formula weigh appropriate material, in being placed individually into different containers;
Step B, monoethanolamine is added to into reactor, toward reactor bisulfites is added, it is stirring while adding so that bisulfite
Salt is uniformly dispersed;
Step C, past reactor add p-hydroxybenzoate, stirring while adding so that p-hydroxybenzoate is uniformly dispersed;
Step D, past reactor add bleeding agent, stirring while adding so that bleeding agent is uniformly dispersed;
Step E, oil of breathing freely toward reactor addition, it is stirring while adding so that ventilative oil dispersed is uniform;
Step F, past reactor add cystine, stirring while adding so that cystine is uniformly dispersed;
Step G, past reactor add water, stir, and get product.
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Cited By (1)
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CN115154358A (en) * | 2022-06-13 | 2022-10-11 | 湘潭湘莱生物科技有限公司 | Permanent wave agent for reducing hair damage and hot wave method thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115154358A (en) * | 2022-06-13 | 2022-10-11 | 湘潭湘莱生物科技有限公司 | Permanent wave agent for reducing hair damage and hot wave method thereof |
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Application publication date: 20170510 |