CN106614827A - Mosquito-repelling combination and preparation method thereof and application - Google Patents
Mosquito-repelling combination and preparation method thereof and application Download PDFInfo
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- CN106614827A CN106614827A CN201611243366.7A CN201611243366A CN106614827A CN 106614827 A CN106614827 A CN 106614827A CN 201611243366 A CN201611243366 A CN 201611243366A CN 106614827 A CN106614827 A CN 106614827A
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- oil
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- repellent composition
- mosquito
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention relates to the technical field of daily chemical products, in particular to a mosquito-repelling combination and a preparation method thereof and application. The mosquito-repelling combination comprises, by weight parts, 10-30 parts of citronella oil, 5-20 parts of eucalyptus oil, 2-15 parts of clove essential oil, 2-15 parts of mint essential oil and 0.5-10 parts of chamomile essential oil. Each raw material ingredient is reasonable in compatibility, and the mosquito-repelling combination is convenient to prepare and extensive in use. The obtained mosquito-repelling combination is good in mosquito-repelling effect and does not make people and livestock allergic or have other toxic and side effects.
Description
Technical field
The present invention relates to cosmetics of everyday use technical field, and in particular to a kind of mosquito repellent composition and its preparation method and application.
Background technology
At present conventional mosquito repellent product is mainly so that containing based on Metadelphene and dimethyl phthalate product, these products are by directly sprinkling
Realize in environment, clothing or igniting mosquito-repellent incense or by Electric heating.Both products are chemical synthesis insecticide, and mosquito repellent is former
The tactile and chemocepter for directly acting on mosquito for medicine is managed, so as to expelling mosquito.Such product uses for a long time meeting
The drug resistance of mosquito is caused, using effect is reduced, while its security also treats further evaluation.Due to such product production and
Use, can also cause the environmental pollution of water body, soil.
Just there is a tradition using natural plants mosquito repellent in China from ancient times, such as argy wormwood, peppermint, cloves natural plants etc., so
And, because natural plants mosquito component content is less, repelling effect is often notable, and also complex using process, and
Be not suitable for the house custom of modern.With the development of chemical science, people start to extract active ingredient from natural plants, and
The essential oil with identity function is formed, and is combined with chemical solvent, to carry out mosquito repellent.Mosquito-repellent essential oil in currently available technology
Usually contain chemical reagent, or even farm chemical ingredients, and need to be powered or heat when working, for mosquito repellent method, used
Journey is complex, and easily produces harmful material.Additionally, the essential oil mosquito repellent effect of many single components and blending constituent
Rate is not high, it is difficult to reach the purpose of popularization.
As can be seen here, deficiency of the prior art can be based on, there is provided one kind makes each with plant extracts as raw material components
Raw material reasonable compatibility, with using health, environmental protection, adult mosquito is had very strong prevention suck blood effect and will not to human body produce it is any
Side effect, becomes those skilled in the art's technical barrier urgently to be resolved hurrily.
The content of the invention
The present invention is in order to solve above-mentioned technical problem, there is provided a kind of mosquito repellent composition and its preparation method and application.Have
Composition of raw materials rationally, and is natural plant extract, while effective mosquito repellent, will not produce any side effect to human body.
In order to reach above-mentioned technique effect, the present invention includes technical scheme below：
A kind of mosquito repellent composition, including the raw material components of following parts by weight：10～30 parts of citronella oil, 5～20 portions of eucalyptus
Leaf oil, 2～15 parts of clove oil, 2～15 parts of Peppermint essential oil and 0.5～10 part of chamomile essential oil.
The each raw material components of mosquito repellent composition reasonable compatibility of the application, with good repelling effect, and to equal to people, animal
Without allergy, or other toxic and side effects.By citronella oil and clove oil, eucalyptus oil, Peppermint essential oil, chamomile essential oil reasonable compatibility
Afterwards, its anophelifuge activity is more preferably.
Further, including following parts by weight raw material components：15～20 parts of citronella oil, 10～15 parts of eucalyptus oils, 5
～10 parts of clove oil, 5～10 parts of Peppermint essential oil and 2～5 parts of chamomile essential oil.
The present invention further obtains the raw material components of above-mentioned each parts by weight through substantial amounts of screening experiment, makes mosquito repellent group
The anophelifuge activity of compound does further optimization.
Further, also including the paraffin oil that parts by weight are 20～50 parts.
When using mosquito repellent composition of the present invention, mosquito repellent composition can be placed in PVC sacks, the present invention is fully
Using the high boiling characteristics of each feedstock oil, the fine pore of the PVC bag materials that can pass through sealing slowly comes out, and reaches
To the effect of long-time mosquito repellent.And by the reasonable compatibility paraffin oil in mosquito repellent composition, the spy that essential oil corrodes PVC can be solved
Property, and obtain with slow release effect thing mosquito repellent medicine.Allotment solves contradiction characteristic of the essential oil to PVC material high corrosion.
Further, also including the paraffin oil that parts by weight are 35～45 parts.
The present invention obtains the optimum weight number value of paraffin oil through a large amount of screening experiments.
Further, the mosquito repellent composition is also including the raw material components of following parts by weight：2～15 parts of You Jiali is smart
Oil, 1～10 part of camphorated oil, 2～15 parts of wide fennel essential oil and 1～10 part of lemon grass (Cymbopogon citratus) essential oil.
The present invention is through further screening, the above-mentioned raw material components of compatibility, so as to get mosquito repellent composition repelling effect more
It is good, and lasting effect is more preferable.
A kind of preparation method of above-mentioned mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint are taken respectively
And chamomile, extracted using soxhlet extraction and respectively obtain citronella oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essence
Oil, the citronella oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essential oil are mixed as raw material components with paraffin oil
Obtain mosquito repellent composition.
Further, described soxhlet extraction adds 150～250ml ethyl acetate solvent Jing to take 5～15g of raw material
5h is extracted in vacuum distillation.
Under the reasonable determination of above-mentioned numerical value, the present invention extract citronella oil, eucalyptus oil, clove oil, Peppermint essential oil and
Chamomile essential oil is in hgher efficiency, more convenient to operate, is adapted to the preparation and production of industrialization.
Further, the raw material components are also included in eucalyptus quintessence oil, camphorated oil, wide fennel essential oil and lemon grass (Cymbopogon citratus) essential oil
One or more.
A kind of mosquito repellent composition is preparing mosquito-driving liquid, mosquito expelling plaster, mosquito repelling bracelet, mosquito repellent bag, mosquito-repellent spray or mosquito repellent incense
In application.
Mosquito repellent composition is made for preparing mosquito expelling plaster, mosquito repelling bracelet and mosquito repellent bag, the mosquito expelling plaster, mosquito repelling bracelet and drive
The material of mosquito bag is PVC material.
Using above-mentioned technical proposal, including following beneficial effect：A kind of mosquito repellent composition and its preparation that the present invention is provided
Methods and applications.Rationally, it is convenient and of many uses to prepare for each material composition compatibility.The mosquito repellent composition repelling effect for obtaining is good,
And to people, animal without allergy, or other toxic and side effects.
Specific embodiment
The present invention is described in further detail below by specific embodiment.
Embodiment one：A kind of mosquito repellent composition, including the raw material components of following parts by weight：10 parts of citronella oil, 20 parts
Eucalyptus oil, 2 parts of clove oil, 15 parts of Peppermint essential oil and 0.50 part of chamomile essential oil.
The present embodiment mosquito repellent composition toxicology test：
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment one, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of embodiment one in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment one, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of embodiment one belongs to actual nontoxic level.
Embodiment two：A kind of mosquito repellent composition, including the raw material components of following parts by weight：12 parts of citronella oil, 18 parts
Eucalyptus oil, 4 parts of clove oil, 12 parts of Peppermint essential oil, 1 part of chamomile essential oil, 45 parts of paraffin oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint and ocean are taken respectively
Camomile, is extracted using soxhlet extraction and respectively obtains citronella oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essential oil, will
The citronella oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essential oil are mixed to get drive as raw material components and paraffin oil
Mosquito composition.
The present embodiment mosquito repellent composition toxicology test：
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment two, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of embodiment two in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment two, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of embodiment two belongs to actual nontoxic level.
Embodiment three：A kind of mosquito repellent composition, including the raw material components of following parts by weight：15 parts of citronella oil, 15 parts
Eucalyptus oil, 5 parts of clove oil, 10 parts of Peppermint essential oil, 2 parts of chamomile essential oil and 50 parts of paraffin oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint and ocean are taken respectively
Camomile is separately added into 250ml ethyl acetate solvent Jing vacuum distillations extraction 5h and respectively obtains perfume (or spice) as each raw material 5g of raw material components
Thatch oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essential oil, by the citronella oil, eucalyptus oil, clove oil, peppermint essence
Oil, chamomile essential oil and paraffin oil are mixed to get mosquito repellent composition as raw material components and paraffin oil.
The present embodiment mosquito repellent composition toxicology test：
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment three, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of embodiment three in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment three, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of embodiment three belongs to actual nontoxic level.
Example IV：A kind of mosquito repellent composition, including the raw material components of following parts by weight：15 parts of citronella oil, 15 parts
Eucalyptus oil, 5 parts of clove oil, 10 parts of Peppermint essential oil, 2 parts of chamomile essential oil, 45 parts of paraffin oil, 2 parts of You Jiali
Essential oil, 10 parts of camphorated oil, 2 parts of wide fennel essential oil and 10 parts of lemon grass (Cymbopogon citratus) essential oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint, ocean are taken respectively
Camomile, You Jiali, camphor, wide fennel and lemon grass (Cymbopogon citratus) are separately added into 180ml ethyl acetate solvents as each raw material 8 of raw material components
It is smart that Jing vacuum distillations extraction 5h respectively obtains citronella oil, eucalyptus oil, clove oil, Peppermint essential oil, chamomile essential oil, You Jiali
Each raw material components and paraffin oil are mixed to get mosquito repellent by oil, camphorated oil, wide fennel essential oil and lemon grass (Cymbopogon citratus) essential oil as raw material components
Composition.
The present embodiment mosquito repellent composition toxicology test：
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment four, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of embodiment three in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of example IV, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of embodiment three belongs to actual nontoxic level.
Embodiment five：A kind of mosquito repellent composition, including the raw material components of following parts by weight：18 parts of citronella oil, 13 parts
Eucalyptus oil, 8 parts of clove oil, 8 parts of Peppermint essential oil, 3 parts of chamomile essential oil and 42 parts of paraffin oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint and ocean are taken respectively
Camomile is separately added into 200ml ethyl acetate solvent Jing vacuum distillations extraction 5h and respectively obtains perfume (or spice) as each raw material 12g of raw material components
Thatch oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essential oil mix each raw material components and paraffin oil as raw material components
Conjunction obtains mosquito repellent composition.
The present embodiment mosquito repellent composition toxicology test：
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment five, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of example IV in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment five, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of example IV belongs to actual nontoxic level.
Embodiment six：A kind of mosquito repellent composition, including the raw material components of following parts by weight：18 parts of citronella oil, 13 parts
Eucalyptus oil, 8 parts of clove oil, 8 parts of Peppermint essential oil, 3 parts of chamomile essential oil, 42 parts of paraffin oil, 8 parts of You Jiali are smart
Oil, 5 parts of camphorated oil, 8 parts of wide fennel essential oil and 5 parts of lemon grass (Cymbopogon citratus) essential oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint, ocean are taken respectively
Camomile, You Jiali, camphor, wide fennel and lemon grass (Cymbopogon citratus) are separately added into 150～250ml second as each 5～15g of raw material of raw material components
Acetoacetic ester solvent Jing vacuum distillations extract 5h respectively obtain citronella oil, eucalyptus oil, clove oil, Peppermint essential oil, chamomile essential oil,
Eucalyptus quintessence oil, camphorated oil, wide fennel essential oil and lemon grass (Cymbopogon citratus) essential oil mix each raw material components with paraffin oil as raw material components
Obtain mosquito repellent composition.
The present embodiment mosquito repellent composition toxicology test：
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment six, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of example IV in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment six, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of example IV belongs to actual nontoxic level.
Embodiment seven：A kind of mosquito repellent composition, including the raw material components of following parts by weight：20 parts of citronella oil, 10 parts
Eucalyptus oil, 10 parts of clove oil, 5 parts of Peppermint essential oil, 5 parts of chamomile essential oil, 35 parts of paraffin oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint and ocean are taken respectively
Camomile is separately added into 220ml ethyl acetate solvent Jing vacuum distillations extraction 5h and respectively obtains perfume (or spice) as each raw material 13g of raw material components
Thatch oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essential oil mix each raw material components and paraffin oil as raw material components
Conjunction obtains mosquito repellent composition.
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment seven, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of embodiment five in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment seven, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of embodiment five belongs to actual nontoxic level.
Embodiment eight：A kind of mosquito repellent composition, including the raw material components of following parts by weight：20 parts of citronella oil, 10 parts
Eucalyptus oil, 10 parts of clove oil, 5 parts of Peppermint essential oil, 5 parts of chamomile essential oil, 35 parts of paraffin oil, 15 parts of You Jiali
Essential oil, 1 part of camphorated oil, 15 parts of wide fennel essential oil and 10 parts of lemon grass (Cymbopogon citratus) essential oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint, ocean are taken respectively
Camomile, You Jiali, camphor, wide fennel and lemon grass (Cymbopogon citratus) are separately added into 190ml ethyl acetate molten as each raw material 14g of raw material components
It is smart that agent Jing vacuum distillations extraction 5h respectively obtains citronella oil, eucalyptus oil, clove oil, Peppermint essential oil, chamomile essential oil, You Jiali
Each raw material components and paraffin oil are mixed to get mosquito repellent by oil, camphorated oil, wide fennel essential oil and lemon grass (Cymbopogon citratus) essential oil as raw material components
Composition.
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment eight, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of embodiment five in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment eight, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of embodiment five belongs to actual nontoxic level.
Embodiment nine：A kind of mosquito repellent composition, including the raw material components of following parts by weight：30 parts of citronella oil, 5 portions of eucalyptus
Leaf oil, 15 parts of clove oil, 2 parts of Peppermint essential oil, 10 parts of chamomile essential oil, 20 parts of paraffin oil.
A kind of preparation method of mosquito repellent composition, comprises the following steps：Lemon-grass, folium eucalypti, cloves, peppermint and ocean are taken respectively
Camomile is separately added into 150ml ethyl acetate solvent Jing vacuum distillations extraction 5h and respectively obtains perfume (or spice) as each raw material 15g of raw material components
Thatch oil, eucalyptus oil, clove oil, Peppermint essential oil and chamomile essential oil mix each raw material components and paraffin oil as raw material components
Conjunction obtains mosquito repellent composition.
Toxicology test is carried out using the mosquito repellent composition described in the present embodiment nine, front 24h is tested by family's rabbit back both sides
Hair is cut, unhairing scope or so Ge Yue 6cm2.By the mosquito repellent composition uniform application of embodiment six in left side trial zone during experiment
On skin, with two layers of gauze (2.5cm × 2.5cm), one layer of glassine paper is covered, and immobilization with adhesive tape sticks 4h, and right side skin of unhairing is applied
Distilled water is compared, and after off-test, removes covering, and removing residue is cleaned with warm water.1 after tested material of going out, 24,48h
Position dermoreaction is smeared in observation respectively.Press《Cosmetics health specification》Middle pertinent regulations, carry out skin wound repair and score simultaneously
Carry out skin irritatin strength grading.
Result of the test：After Skin Irritation Test 1h, 24h and 48h of embodiment nine, rabbit trial zone and check plot are equal
Without erythema and redness, the reaction without any discomfort.Therefore Jing tests, the mosquito repellent composition of embodiment six belongs to actual nontoxic level.
Embodiment ten：
A kind of mosquito repellent composition is preparing mosquito-driving liquid, mosquito expelling plaster, mosquito repellent bag, mosquito repelling bracelet, mosquito-repellent spray or mosquito repellent incense
In application.
Described mosquito repellent composition can be the mosquito repellent composition described in embodiment one to any embodiment of embodiment nine.
If mosquito repellent composition is prepared into into mosquito repellent bag, mosquito repellent composition can be placed in PVC sacks, it is originally busy to make full use of
The high boiling characteristics of each feedstock oil, the fine pore of the PVC bag materials that can pass through sealing slowly comes out, and reaches length
The effect of time mosquito repellent.And by the reasonable compatibility paraffin oil in mosquito repellent composition, the characteristic that essential oil corrodes PVC can be solved,
And obtain with slow release effect thing mosquito repellent medicine.Allotment solves contradiction characteristic of the essential oil to PVC material high corrosion.
Embodiment 11：A kind of mosquito repellent bag, including PVC material bag, the PVC material bag is built with mosquito repellent composition, institute
Mosquito repellent composition is stated for the mosquito repellent composition described in embodiment one to embodiment nine.
Respectively Example one is put in PVC material bag to mosquito repellent composition prepared by embodiment nine, used as experimental group one
To experimental group nine, as a control group one is put in PVC material bag with commercially available culicifuge, the commercially available spray brand is village minister
Radar Europe shield adult's mosquito-repellent spray, takes a kind of culicifuge that application publication number is CN103875731A, according to the patent of invention institute
Disclosed composition of raw materials prepares culicifuge as a control group two, take equivalent experimental group respectively and control group be put into equal-volume,
In the PVC material bag of equal thickness, after sealing, after observing one day respectively, after three days and after seven days, the situation of PVC material bag, experiment
As a result it is as shown in table 1.
The mosquito repellent bag quality testing experimental result of table 1
From the data in table 1, it can be seen that the mosquito repellent bag described in the embodiment of the present invention 11, implements for PVC material bag reasonable compatibility
Mosquito repellent composition described in example one to embodiment nine, will not cause corrosion, and mosquito repellent composition of the present invention for height to PVC material bag
Volatility, the fine pore of the PVC bag materials that can pass through sealing slowly comes out, and reaches the effect of long-time mosquito repellent
Really.
Mosquito repellent composition described in Example one to embodiment nine carries out walking quickly and keeping away experiment detection：
Experiment component：Example one to embodiment nine is experimental group one to experimental group nine, and taking commercially available Mosquito-repellant spray is
Control group one, the commercially available spray brand is minister radar Europe, village shield adult's mosquito-repellent spray；Taking application publication number is
A kind of culicifuge of CN103875731A, the composition of raw materials according to the patent of invention prepares culicifuge as control
Group two；Take citronella oil control group three the most.Experimental group is taken respectively and control group is once walked quickly and kept away experiment.
Walk quickly and keep away experiment：
Experimental technique：(should not drink before experiment and during test per the qualified tester of group selection 3 and above attack
Wine, tea or coffee, should not use the medicine containing essence class), the skin area of 50mm × 50mm is respectively drawn in its both hands back, often
The mosquito repellent product of the consumption of hand uniform application 15mg/cm, uniform application experimental group to be measured and control group, experimental group and control
Examination mosquito is provided by northwest University of Science and Technology needed for the mosquito repellent product of group.By the 40mm × 40mm skins in exposure the back of the hand, tight masking
Remainder.Another hand is blank.The mosquito repellent product 1h of experimental group and control group is smeared, hand is stretched into and is placed with attack
2min in qualified mosquito cage, observation whether there is mosquito is come to stop to fall to sucking blood.Test once every 1h afterwards, as long as there is a mosquito
Come to suck blood sentence and make mosquito repellent composition failure.The effective protecting time (h) of the mosquito repellent product of record experimental group and control group, pin
Mean value is calculated to the effective protecting time of three personnel of per group of experiment.
Advanced line blank control test when being tested every time, the qualified test worm of attack can continue test, and test worm is attacked
Power is unqualified, needs to change qualified test worm and is tested.Experimental result is shown in Table 2.
Table 2 walks quickly and keeps away experimental result
From the data in table 2, it can be seen that the experimental group of the present invention is the complete guard time of embodiment one to embodiment nine being all higher than
Control group, wherein most preferred embodiment are embodiment six.More preferably embodiment is example IV, embodiment five and embodiment
Eight.The preferred embodiments of the present invention are the foregoing is only, the present invention is not limited to, for those skilled in the art
For, the present invention can have various modifications and variations.All any modifications within the spirit and principles in the present invention, made, etc.
With replacement, improvement etc., should be included within the scope of the present invention.
Claims (10)
1. a kind of mosquito repellent composition, it is characterised in that including the raw material components of following parts by weight：10～30 parts of citronella oil, 5
～20 parts of eucalyptus oils, 2～15 parts of clove oil, 2～15 parts of Peppermint essential oil and 0.5～10 part of chamomile essential oils.
2. mosquito repellent composition according to claim 1, it is characterised in that including the raw material components of following parts by weight：15
～20 parts of citronella oil, 10～15 parts of eucalyptus oils, 5～10 parts of clove oil, 5～10 parts of Peppermint essential oil and 2～5 parts of oceans
Camomile essential oil.
3. the mosquito repellent composition according to any one of claim 1 or 2, it is characterised in that also including parts by weight be 20～
50 parts of paraffin oil.
4. mosquito repellent composition according to claim 3, it is characterised in that also including the paraffin that parts by weight are 35～45 parts
Oil.
5. the mosquito repellent composition according to any one of claim 1 or 2, it is characterised in that also including following parts by weight
Raw material components：2～15 parts of eucalyptus quintessence oil, 1～10 part of camphorated oil, 2～15 parts of wide fennel essential oil and 1～10 part of lemon
Lemon grass essential oil.
6. the preparation method of the mosquito repellent composition described in a kind of any one of Claims 1 to 5, it is characterised in that including following step
Suddenly：Lemon-grass, folium eucalypti, cloves, peppermint and chamomile are taken respectively, are extracted using soxhlet extraction and are respectively obtained citronella oil, folium eucalypti
Oil, clove oil, Peppermint essential oil and chamomile essential oil, the citronella oil, eucalyptus oil, clove oil, Peppermint essential oil and ocean is sweet
Chrysanthemum essential oil is mixed to get mosquito repellent composition as raw material components and paraffin oil.
7. the preparation method of mosquito repellent composition according to claim 6, it is characterised in that described soxhlet extraction is to take
5～15g of raw material, adds 150～250ml ethyl acetate solvent Jing vacuum distillations to extract 5h.
8. the preparation method of mosquito repellent composition according to claim 6, it is characterised in that the raw material components also include outstanding
Plus one or more in sharp essential oil, camphorated oil, wide fennel essential oil and lemon grass (Cymbopogon citratus) essential oil.
9. the mosquito repellent composition described in a kind of any one of Claims 1 to 5 is preparing mosquito-driving liquid, mosquito expelling plaster, mosquito repellent bag, mosquito repellent hand
Application in ring, mosquito-repellent spray or mosquito repellent incense.
10. a kind of mosquito repellent bag, it is characterised in that including PVC material bag, the PVC material bag is described built with mosquito repellent composition
Mosquito repellent composition is the mosquito repellent composition described in any one of Claims 1 to 5.
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| CN201611243366.7A CN106614827A (en) | 2016-12-28 | 2016-12-28 | Mosquito-repelling combination and preparation method thereof and application |
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| CN201611243366.7A CN106614827A (en) | 2016-12-28 | 2016-12-28 | Mosquito-repelling combination and preparation method thereof and application |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107149567A (en) * | 2017-05-11 | 2017-09-12 | 娇时日化（杭州）股份有限公司 | Plant mosquito-repellent spray and its preparation technology for baby |
| CN109090109A (en) * | 2018-06-06 | 2018-12-28 | 钱龙风 | A kind of mosquito repellent pastes with oneself |
| CN110859783A (en) * | 2019-11-11 | 2020-03-06 | 广州环亚化妆品科技有限公司 | Lipstick for repelling mosquitoes and preparation method and application thereof |
| CN114699341A (en) * | 2022-04-02 | 2022-07-05 | 杭州声能科技有限公司 | Long-acting mosquito repellent and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102512609A (en) * | 2011-12-27 | 2012-06-27 | 浙江景岳堂药业有限公司 | Essential oil with anti-inflammatory, analgesic, cooling, itching-relieving and mosquito-dispelling functions |
| CN102579288A (en) * | 2012-04-06 | 2012-07-18 | 厦门鼎嘉奇投资管理有限公司 | Natural plant essential oil composition capable of directly serving as mosquito repellent |
| CN103865428A (en) * | 2014-04-03 | 2014-06-18 | 苏州华周胶带有限公司 | Fragrant masking tape |
| CN106074268A (en) * | 2016-07-07 | 2016-11-09 | 青岛艾派克生物科技有限公司 | A kind of plant type perfume |
-
2016
- 2016-12-28 CN CN201611243366.7A patent/CN106614827A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102512609A (en) * | 2011-12-27 | 2012-06-27 | 浙江景岳堂药业有限公司 | Essential oil with anti-inflammatory, analgesic, cooling, itching-relieving and mosquito-dispelling functions |
| CN102579288A (en) * | 2012-04-06 | 2012-07-18 | 厦门鼎嘉奇投资管理有限公司 | Natural plant essential oil composition capable of directly serving as mosquito repellent |
| CN103865428A (en) * | 2014-04-03 | 2014-06-18 | 苏州华周胶带有限公司 | Fragrant masking tape |
| CN106074268A (en) * | 2016-07-07 | 2016-11-09 | 青岛艾派克生物科技有限公司 | A kind of plant type perfume |
Non-Patent Citations (3)
| Title |
|---|
| 万树青 等: "《生物农药及使用技术》", 31 January 2003, 金盾出版社 * |
| 夏征农: "《辞海 农业分册》", 30 November 1988, 上海辞书出版社 * |
| 福建人民出版社: "《生活小常识 第二集》", 30 September 1958, 福建人民出版社 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107149567A (en) * | 2017-05-11 | 2017-09-12 | 娇时日化（杭州）股份有限公司 | Plant mosquito-repellent spray and its preparation technology for baby |
| CN107149567B (en) * | 2017-05-11 | 2021-01-12 | 虞琼斐 | Plant mosquito-repellent spray for infants and preparation process thereof |
| CN109090109A (en) * | 2018-06-06 | 2018-12-28 | 钱龙风 | A kind of mosquito repellent pastes with oneself |
| CN110859783A (en) * | 2019-11-11 | 2020-03-06 | 广州环亚化妆品科技有限公司 | Lipstick for repelling mosquitoes and preparation method and application thereof |
| CN110859783B (en) * | 2019-11-11 | 2022-08-23 | 广州环亚化妆品科技股份有限公司 | Lipstick for repelling mosquitoes and preparation method and application thereof |
| CN114699341A (en) * | 2022-04-02 | 2022-07-05 | 杭州声能科技有限公司 | Long-acting mosquito repellent and preparation method thereof |
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