CN106596277A - Mechanical testing device and method of high-throughout membrane material - Google Patents

Mechanical testing device and method of high-throughout membrane material Download PDF

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Publication number
CN106596277A
CN106596277A CN201611058590.9A CN201611058590A CN106596277A CN 106596277 A CN106596277 A CN 106596277A CN 201611058590 A CN201611058590 A CN 201611058590A CN 106596277 A CN106596277 A CN 106596277A
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membrane material
high flux
measurement system
flux membrane
cabin
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CN106596277B (en
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张东升
张水强
刘斌
张统
张统一
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University of Shanghai for Science and Technology
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University of Shanghai for Science and Technology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • G01N3/10Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces generated by pneumatic or hydraulic pressure
    • G01N3/12Pressure testing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • G01N3/06Special adaptations of indicating or recording means
    • G01N3/068Special adaptations of indicating or recording means with optical indicating or recording means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0019Compressive
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/003Generation of the force
    • G01N2203/0042Pneumatic or hydraulic means
    • G01N2203/0044Pneumatic means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/06Indicating or recording means; Sensing means
    • G01N2203/0641Indicating or recording means; Sensing means using optical, X-ray, ultraviolet, infrared or similar detectors
    • G01N2203/0647Image analysis

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
  • Length Measuring Devices By Optical Means (AREA)

Abstract

The invention relates to a mechanical testing device and method of a high-throughout membrane material. The device comprises an electronic speckle pattern interferometry off-surface measurement system, a sealed cabin, a pneumatic pump, and a high-sensitivity baroceptor, wherein a high-throughout membrane material sampling is installed at the opening position of the sealed cabin so that a completely airtight sealed cabin is formed, the pneumatic pump is used for controlling air pressure P in the cabin, and recording and giving feedbacks on real-time pressure in the cabinet through the high-sensitivity baroceptor; when an experiments undergoes, the electronic speckle pattern interferometry off-surface measurement system and the sealed cabin are fixed on an optical vibration isolation table, and the surface of the sampling in the sealed cabin is located in field of view of the electronic speckle pattern interferometry off-surface measurement system. According to the mechanical testing device and method of the high-throughout membrane material, a function relationship among uniform pressure, membrane central point off-plane displacement, and other mechanical parameters is adopted, so that each mechanical parameter such as elasticity modulus of multiple thin-film materials is induced respectively, and thus the purpose that multiple kinds of the mechanical parameters of the thin-film materials can be obtained at mere one test is achieved.

Description

High flux membrane Material mechanics test device and method
Technical field
The present invention relates to a kind of high flux membrane Material mechanics test device and method, belongs to photodynamics detection field.
Background technology
On June 24th, 2011, US President Barack Obama are announced to start " an advanced manufacturing industry for overbalancing 500,000,000 dollars Fellowship "(Advanced Manufacturing Partnership, AMP)Plan, appeals U.S. government, colleges and universities and enterprise Between should strengthen cooperation, to strengthen US Manufacturing Industry leading position, and " material genome plan "(Materials Genome Initiative, MGI)It is the calculated important component parts of AMP.In the last few years, domestic and international high flux material was prepared and was characterized Platform technology achieves very fast development, and be proved to can effectively accelerated material research and development application process, therefore be listed in material One of three big technology essential factors of genome plan.While high flux material preparation technology is greatly developed, need high-throughout Measuring technology is matching, and high flux experimental tool is also another important technical key element in material genome plan.At present Conventional high flux experimental tool all haves the shortcomings that testing efficiency is low, and this is just badly in need of exploring a kind of new high flux test skill Art, while efficiency and measuring accuracy are taken into account, so as to effectively facilitate the enforcement of material genome plan.
Optical interference techniques are a kind of typical optical measurement mechanics method, for example, speckle interference, moire interference and cutting speckle The technologies such as interference, it has also become the important method of deformation field measurement.Their principles based on optical interference, with very high sensitive Degree, can measure displacement and the displacement derivatives of stress body surface.Simultaneously because it has, measurement of full field, light path are simple, adjust Conveniently, to the low feature of environmental requirement, therefore it is widely used in all kinds of accurate measurements.Wherein speckle interference off-surface displacement measurement System can accurately measure the surface deformation of testee, and certainty of measurement reaches nanoscale.The introducing of phase shift method improves measurement essence The signal to noise ratio of degree and result, and can measure tested in real time based on the speckle interference off-surface displacement measurement technology of real-time phase-shifting technique The surface deformation situation of object, has the advantages that measurement efficiency height, precision are good.
The content of the invention
Present invention aims to the deficiency of prior art, proposes a kind of new high flux mechanics characterization experiment side Method --- high flux membrane Material mechanics test device and method.The invention can be used in physics(Temperature), chemistry(Corrosion)Bar Sign under part to multiple film material mechanical performance, it may also be used for the sign to multiple film fatigue of materials mechanical property.Using Particular technique scheme of the invention is as follows:
A kind of high flux membrane Material mechanics test device, including ESPI off-surface displacement measurement system, sealing cabin, gas Press pump and high sensitivity baroceptor, it is characterised in that:High flux membrane testing of materials sample is arranged on the opening of sealing cabin Place, forms the closed nacelle for fully sealing, and pulsometer is used for the air pressure in control cabinet body, is remembered by high sensitivity baroceptor Record and feed back the real-time pressure in nacelle;ESPI off-surface displacement measurement system and sealing cabin are fixed on during test On optics Isolating Platform, and the specimen surface allowed on sealing cabin is located at the visual field model of ESPI off-surface displacement measurement system In enclosing.
The ESPI off-surface displacement measurement system includes computer, CCD area array cameras, piezoelectric ceramics, reference Face, spectroscope, reflecting mirror, laser instrument;The reflected mirror of laser that laser instrument sends enters the spectroscope of half-reflection and half-transmission, CCD camera Testee --- the speckle interference image of specimen surface is obtained, digital picture is input to after computer, be capable of achieving automatization In-plane displacement and acoplanarity displacement measure in real time.
The sealing cabin is an openings at one side nacelle, to install high flux membrane material substrate at opening --- examination Sample, the substrate are collectively forming a sealing cabin for fully sealing with nacelle.
The pulsometer is by inflating the pressure value in precise control sealing cabin so that various membrane material samples bear phase Same well-distributed pressure, by the air pressure in high sensitivity baroceptor real―time precision measurment and record cabin inside sealing cabin Value.
A kind of high flux membrane Material mechanics test method, adopts to be entered according to above-mentioned high flux membrane Material mechanics test device Row operation, it is characterised in that operating procedure is as follows:
1)Prepare the test sample of high flux membrane material;
2)High flux membrane testing of materials sample is arranged at sealing cabin opening;
3)Speckle interference off-surface displacement measurement system is installed, optical path is debugged;
4)Pressure in control sealing cabin;
5)Pressure and film sample position phase bar graph during record high flux membrane testing of materials in sealing cabin;
6)Obtain the mechanics parameter of various thin-film material samples;
The step 1)It is the test sample for preparing high flux membrane material first:The thin-film material of various material is adopted identical Technological process, is simultaneously arranged on one piece of substrate in the form of an array, and each membrane material is constrained all in periphery fixed, film and film it Between without being interconnected, do not produce between them and interfere, film sample is distributed on substrate with a matrix type.
The step 2)It is the sealed compartment that the substrate of the high flux membrane material sample of above-mentioned preparation is arranged on one side opening At the opening of body, a closed nacelle for fully sealing is formed.
The step 3)It is that the speckle interference off-surface displacement measurement system with real-time phase-shifting technique is fixed on into optics first In vibration isolation table, then again above-mentioned sealing cabin is fixed in optics vibration isolation table, and allows the specimen surface of sealing cabin to be located at electricity In the field range of sub- speckle interference off-surface displacement measurement system;ESPI off-surface displacement measurement system has real-time phase Shifting function, can measure the acoplanarity displacement of multiple membrane material specimen surfaces simultaneously.
The step 4)It is that pressure in sealing cabin can pass through inflator pump precise control so that various membrane material samples Identical well-distributed pressure is born, is accurately shown by high sensitivity baroceptor in real time inside nacelle and is recorded the air pressure in cabin Value.
The step 5)It is high sensitivity baroceptor and ESPI off-surface displacement measurement system synchronization record The well-distributed pressure and the surface deformation of corresponding multiple circular membrane samples that various membrane material samples bear interferes position phase bar graph.
The step 6)It is to step 5 by ESPI the poster processing soft)Multiple thin film of middle acquisition from face Deforming position phasor carries out automatization's filtering, solution phase place and phase extraction operation, obtains the acoplanarity displacement of each thin film center point;High pass The mechanical model of amount membrane material is the circular membrane structure of a periphery fixed, and between its mechanics parameter and physical dimension, correspondence is closed System is as follows:
It is wherein the elastic modelling quantity of thin-film material, is Poisson's ratio, is the radius of membrane material, be thickness, represents inside sealing cabin Pressure, namely the same well-distributed pressure that various membrane materials bear represents every kind of membrane material corresponding under well-distributed pressure effect The acoplanarity displacement of central point;According to the functional relationship between well-distributed pressure, center membrane point acoplanarity displacement and other mechanics parameters, can The mechanics parameters such as the respective elastic modelling quantity of multiple thin-film materials are derived respectively, so as to realize, by an Experiments of Machanics, obtaining The purpose of various thin film material mechanics parameters.
Description of the drawings
Fig. 1 is the measuring method flow chart of the present invention.
Fig. 2 is the light path schematic diagram of high flux membrane Material mechanics test technology of the present invention.
Fig. 3 is the mechanical simplified model of high flux membrane material of the present invention --- discuss a series of periphery fixed thin film uniform Surface deformation under pressure effect.
Fig. 4 is the schematic diagram of the high flux membrane testing of materials sample in embodiment, prepares the circle of 10 × 10 arrays altogether Film sample.
Fig. 5 is the high flux membrane obtained with the ESPI off-surface displacement measurement system with real-time phase-shifting technique Material sample represents the position phase bar graph of acoplanarity displacement under the effect of a certain well-distributed pressure.
Fig. 6 is the well-distributed pressure of high flux membrane material, circular membrane central point acoplanarity displacement curve chart.
Specific embodiment
It is as follows that the preferred embodiment of the present invention combines detailed description:
Embodiment one:
Referring to Fig. 2 and Fig. 3, this high flux membrane Material mechanics test device, including ESPI off-surface displacement measurement system, Sealing cabin, pulsometer and high sensitivity baroceptor, it is characterised in that:High flux membrane testing of materials sample is arranged on sealing At the opening of nacelle, the closed nacelle for fully sealing is formed, pulsometer is used for the air pressure in control cabinet body, by high sensitivity gas Pressure sensor is recorded and feeds back the real-time pressure in nacelle;By ESPI off-surface displacement measurement system and sealing during test Nacelle is fixed on optics Isolating Platform, and the specimen surface allowed on sealing cabin is located at ESPI off-surface displacement measurement system In the field range of system.
Embodiment two:
The ESPI off-surface displacement measurement system include computer, CCD area array cameras, piezoelectric ceramics, the plane of reference, point Light microscopic, reflecting mirror, laser instrument;The reflected mirror of laser that laser instrument sends enters the spectroscope of half-reflection and half-transmission, and CCD camera obtains quilt Object --- the speckle interference image of specimen surface is surveyed, digital picture is input to after computer, be capable of achieving in the face of automatization Displacement and acoplanarity displacement are measured in real time.
The sealing cabin is an openings at one side nacelle, to install high flux membrane material substrate at opening --- examination Sample, the substrate are collectively forming a sealing cabin for fully sealing with nacelle.
The pulsometer is by inflating the pressure value in precise control sealing cabin so that various membrane material samples bear phase Same well-distributed pressure, by the air pressure in high sensitivity baroceptor real―time precision measurment and record cabin inside sealing cabin Value.
Embodiment three:
As Fig. 2 gives the light path schematic diagram of high flux membrane Material mechanics test technology, the thin-film material of various material in sample It is fixed on test substrate in the matrix form, each thin film is in periphery fixed state.Fig. 3 is the simplified mechanics mould of membrane material Type --- a diameter of, thickness is, the surface deformation that periphery fixed circular membrane is produced in the case where well-distributed pressure effect is born.
The DCO process of this example is:
1)The test sample of high flux membrane material is prepared, the thin-film material of various material identical technological process is adopted, with 10 × 10 array formats are arranged on substrate simultaneously, and each membrane material fixes the state for supporting, nothing between film and film all in periphery Any interference.Sample is to be provided with the steel plate of identical array circular hole, a series of circular membrane material of various materials by two pieces to constitute, Plate size is 85mm × 85mm, and the Circularhole diameter on its light plate is 5 mm, is slightly less than high flux circle membrane material.First At the array circular hole that various thin-film material rules are placed on one block of steel plate, the circular hole on circular membrane and steel plate is as far as possible same The heart, then cover another block of steel plate and compress so that above-mentioned various membrane materials are in periphery fixed restrained condition, and schematic diagram is shown in Fig. 4.
2)At the opening of the sealing cabin that the substrate of above-mentioned high flux membrane material is arranged on one side opening, formation one is complete Hermetic closed nacelle, schematic diagram are shown on the right side of Fig. 2.
3)Air pressure in sealing cabin is inflated by inflator pump and causes various membrane material samples by inflator pump precise control Bear identical well-distributed pressure.Sealing cabin can be accurately shown in real time and be recorded in cabin built with high sensitivity baroceptor Pressure value.
4)ESPI off-surface displacement measurement system with real-time phase-shifting technique and above-mentioned sealing cabin are fixed In optics vibration isolation table, the specimen surface of sealing cabin is used as tested region.With ESPI off-surface displacement measurement system System can measure the acoplanarity displacement of multiple membrane material specimen surfaces simultaneously.
5)The speckle interference image of a secondary tested region is gathered before pressurising first as with reference to figure.Then filled by inflator pump Gas bears well-distributed pressure by array film material, and Real-time Collection represents the position phase bar graph of tested region acoplanarity displacement this moment, and Atmospheric pressure value in synchronous recording sealed compartment.The acoplanarity displacement position phase bar graph of array film material sample is as shown in Figure 5.
6)Automatization's filtering is carried out by software to the position phase bar graph in Fig. 5, goes parcel and phase extraction to process, can be obtained To each circular membrane as well-distributed pressure acts on the acoplanarity displacement for producing, the acoplanarity displacement value of thin film center point is paid close attention to.
7)According to the relation between the acoplanarity displacement of the well-distributed pressure and thin film center point of above-mentioned synchronous recording, draw out Cloth pressure and the three cubed curve of central point acoplanarity displacement, as shown in Figure 6.Periphery fixed thin film disk as shown in Figure 3 is equal Mechanical model under the effect of cloth pressure, then by the corresponding relation between mechanics parameter and physical dimension, you can try to achieve each thin The parameters such as the elastic modelling quantity of membrane material.
8)The high flux membrane Material mechanics test technology is can also be used in physics(Temperature), chemistry(Corrosion)Under the conditions of to many Plant the sign of membrane material mechanical property;Can be additionally used in the sign to multiple film fatigue of materials mechanical property.

Claims (11)

1. a kind of high flux membrane Material mechanics test device, including ESPI off-surface displacement measurement system, sealing cabin (5), pulsometer(6)With high sensitivity baroceptor(11), it is characterised in that:High flux membrane testing of materials sample(9)Install In sealing cabin(5)Opening at, form the closed nacelle that fully seals, pulsometer(6)For the air pressure P in control cabinet body, By high sensitivity baroceptor(11)Record and feed back the real-time pressure in nacelle;By ESPI from face during test Displacement measurement system and sealing cabin(5)It is fixed on optics Isolating Platform, and allows sealing cabin(5)On sample(9)Surface position In the field range of ESPI off-surface displacement measurement system.
2. high flux membrane Material mechanics test device according to claim 1, it is characterised in that:The ESPI Off-surface displacement measurement system includes computer(1), CCD area array cameras(2), piezoelectric ceramics(3), the plane of reference(4), spectroscope (10), reflecting mirror(7), laser instrument(8);Laser instrument(8)The reflected mirror of laser for sending(7)Into the spectroscope of half-reflection and half-transmission (10), CCD camera(2)Obtain testee --- sample(9)Digital picture is input to calculating by the speckle interference image on surface Machine(1)Afterwards, the in-plane displacement and acoplanarity displacement for being capable of achieving automatization is measured in real time.
3. high flux membrane Material mechanics test device according to claim 1, it is characterised in that:The sealing cabin(5) It is an openings at one side nacelle, to install high flux membrane material substrate at opening --- sample(9), the substrate is common with nacelle Form a sealing cabin for fully sealing(5).
4. high flux membrane Material mechanics test device according to claim 1, it is characterised in that:The pulsometer(6)It is logical Gas overcharging precise control sealing cabin(5)Interior pressure value P so that various membrane material samples(9)Identical well-distributed pressure is born, Sealing cabin(5)It is internal to pass through high sensitivity baroceptor(11)Atmospheric pressure value P in real―time precision measurment and record cabin.
5. a kind of high flux membrane Material mechanics test method, is surveyed using the high flux membrane mechanics of materials according to claim 1 Trial assembly is put and is operated, it is characterised in that operating procedure is as follows:
1)Prepare the test sample of high flux membrane material(9);
2)By high flux membrane testing of materials sample(9)Installed in sealing cabin(5)At opening;
3)Speckle interference off-surface displacement measurement system is installed, optical path is debugged;
4)Control sealing cabin(5)Interior pressure;
5)Sealing cabin during record high flux membrane testing of materials(5)Interior pressure P and film sample(9)Position phase bar graph;
6)Obtain various thin-film material samples(9)Mechanics parameter.
6. high flux membrane Material mechanics test method according to claim 5, it is characterised in that:The step 1)It is first Prepare the test sample of high flux membrane material(9):The thin-film material of various material is adopted identical technological process, with array shape Formula is arranged on one piece of substrate simultaneously, and each membrane material is constrained all in periphery fixed, and between film and film, nothing is interconnected, they Between do not produce and interfere, film sample(9)It is distributed on substrate with a matrix type.
7. high flux membrane Material mechanics test method according to claim 5, it is characterised in that:The step 2)Being will be upper State the high flux membrane material sample of preparation(9)Substrate be arranged on one side opening sealing cabin(5)Opening at, formed one The closed nacelle for fully sealing(5).
8. high flux membrane Material mechanics test method according to claim 5, it is characterised in that:The step 3)First will be Speckle interference off-surface displacement measurement system with real-time phase-shifting technique is fixed in optics vibration isolation table, then again by above-mentioned sealing Nacelle(5)It is fixed in optics vibration isolation table, and allows sealing cabin(5)Sample(9)Surface is located at ESPI from face position In the field range of shift measurement system;ESPI off-surface displacement measurement system has real-time phase shift function, can survey simultaneously Measure multiple membrane material samples(9)The acoplanarity displacement on surface.
9. high flux membrane Material mechanics test method according to claim 5, it is characterised in that:The step 4)It is sealing Nacelle(5)Interior pressure P can pass through inflator pump(6)Precise control so that various membrane material samples(9)Bear identical uniform Pressure, passes through high sensitivity baroceptor inside nacelle(11)It is accurate in real time to show and record the atmospheric pressure value P in cabin.
10. high flux membrane Material mechanics test method according to claim 5, it is characterised in that:The step 5)It is high Sensitivity baroceptor and ESPI off-surface displacement measurement system synchronization record various membrane material samples(9)Bear Well-distributed pressure and corresponding multiple circular membrane samples(9)Surface deformation interfere position phase bar graph.
11. high flux membrane Material mechanics test methods according to claim 5, it is characterised in that:The step 6)It is logical ESPI the poster processing soft is crossed to step 5)The surface deformation position phasor of multiple thin film of middle acquisition carries out automatization's filter Ripple, solution phase place and phase extraction operation, obtain the acoplanarity displacement of each thin film center point;High flux membrane material(9)Mechanical model For the circular membrane structure of a periphery fixed, between its mechanics parameter and physical dimension, corresponding relation is as follows:
Wherein it is thin-film material(9)Elastic modelling quantity, be Poisson's ratio, be the radius of membrane material, be thickness, represent sealing cabin (5)Internal pressure, namely the same well-distributed pressure that various membrane materials bear, represent every kind of membrane material under well-distributed pressure effect The acoplanarity displacement of corresponding central point;According to the function between well-distributed pressure, center membrane point acoplanarity displacement and other mechanics parameters Relation, can derive multiple thin-film materials respectively(9)The mechanics parameters such as respective elastic modelling quantity, so as to realize by a mechanics Experiment, obtains the purpose of various thin film material mechanics parameters.
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CN108414257A (en) * 2018-03-02 2018-08-17 北京空间技术研制试验中心 A kind of precision of equipment installation measurement method for spacecraft
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CN113640133A (en) * 2021-08-11 2021-11-12 中国工程物理研究院激光聚变研究中心 Sealing film mechanical property testing device based on expansion method
CN114441326A (en) * 2021-12-31 2022-05-06 天津大学 Multifunctional thin film material bulging testing device

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Publication number Priority date Publication date Assignee Title
CN108414257A (en) * 2018-03-02 2018-08-17 北京空间技术研制试验中心 A kind of precision of equipment installation measurement method for spacecraft
CN108802095A (en) * 2018-08-24 2018-11-13 上海大学 The method and system of rigid material coefficient of thermal expansion are measured using speckle-shearing interferometry
CN113640133A (en) * 2021-08-11 2021-11-12 中国工程物理研究院激光聚变研究中心 Sealing film mechanical property testing device based on expansion method
CN113640133B (en) * 2021-08-11 2024-05-07 中国工程物理研究院激光聚变研究中心 Sealing film mechanical property testing device based on expansion method
CN114441326A (en) * 2021-12-31 2022-05-06 天津大学 Multifunctional thin film material bulging testing device
CN114441326B (en) * 2021-12-31 2024-03-12 天津大学 Multifunctional film material bulging testing device

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