CN106578416A - Mycotoxin adsorbent and preparation method thereof - Google Patents

Mycotoxin adsorbent and preparation method thereof Download PDF

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Publication number
CN106578416A
CN106578416A CN201611006931.8A CN201611006931A CN106578416A CN 106578416 A CN106578416 A CN 106578416A CN 201611006931 A CN201611006931 A CN 201611006931A CN 106578416 A CN106578416 A CN 106578416A
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China
Prior art keywords
parts
mold toxin
additive
toxin sorbent
standby
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CN201611006931.8A
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Chinese (zh)
Inventor
蒲连震
马亮
马宏叙
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ANHUI HONGLIANG FEED TECHNOLOGY Co Ltd
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ANHUI HONGLIANG FEED TECHNOLOGY Co Ltd
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Priority to CN201611006931.8A priority Critical patent/CN106578416A/en
Publication of CN106578416A publication Critical patent/CN106578416A/en
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Abstract

The invention discloses a mycotoxin adsorbent and a preparation method thereof. The mycotoxin adsorbent is prepared from, by weight, 12-14 parts of ettringite, 8-10 parts of white amber, 6-9 parts of limonite, 10-14 parts of dehydrogenized xanthan gum, 1-3 parts of polyglutamic acid, 15-19 parts of resina draconis, 9-11 parts of olibanum, 2-4 parts of mongollian thyme herb, 10-13 parts of chinese knotweed herb, 6-9 parts of oroxylum indicum, 15-17 parts of lotus seeds, 11-16 parts of fish roes, 12-15 parts of fructus citri aurantii amarae, 14-17 parts of pig liver powder and 5-8 parts of snakegourd seeds. Compared with the prior art, the mycotoxin adsorbent can kill various kinds of mildew, has a good adsorption effect on various mycotoxins, and can prevent hyperplasia of mildew in the feed storage process.

Description

A kind of mold toxin sorbent and preparation method thereof
Technical field
The invention belongs to the technical field of mold toxin sorbent, and in particular to a kind of mold toxin sorbent and its preparation Method.
Background technology
To the pollution of food by the common concern of people, toxin residual in animal body jeopardizes mycotoxin To the health of the mankind.Being caused because of aflatoxin concentration over-standard in feedstuff also occurred in the Feed Enterprise having interior in recent years Duck culturing family the event be poisoned to death of duckling, all cause larger economic loss to Feed Enterprise and raiser, therefore, it is mould Harm of the verticillium toxin to animal should also cause the great attention of feedstuff and poultry farming.Give feeding of the feeding animal containing mycotoxin After material, show as gradual loss of appetite, it is thirsty, have blood in stool, poor growth, lose weight, dermatorrhagia, be overexcited, jaundice, Tic, opisthotonus etc..The performances such as the visible liver enlargement of pathological anatomy, diffusivity hyperemia, bleeding and necrosis, cardiac dilatation, lung Edema etc..Mycotoxin attacks the specific biochemical system of animal and organ, injures immune system, causes acute and chronic poisoning, And various mycotoxins coexist meeting toxic " multiplication "(" potentiation ")Effect.
In the face of the pollution of mycete, present feed factory is mainly using antifungus agent and mildew removing agent.Antifungus agent is mainly some propanoic acid Calcium, sorbic acid, benzoic acid and potassium sorbate etc., antifungus agent is only killed to mycete, dirty to mycotoxin without any effect The feedstuff of dye adds again many antifungus agents also not eliminate harm of the mycotoxin to animal.In addition, the Calcium Carbonate in feedstuff (Stone powder)And protein feedss(Semen sojae atricolor powder, fish flour etc.)Antacid effect can be played, the effect for making antifungus agent declines.On market Mildew removing agent, can be divided into many kinds such as mineral adsorbent class, yeast cell wall class, microbiology class, enzyme preparation class, mixing class. The country, the mildew removing agent utilization rate highest of mineral adsorbent class.Mineral absorption class mildew removing agent can only adsorb a certain poison mostly Element, adsorption is limited.Citing, montmorillonite adsorption of aflatoxin effect is preferable, but for vomitoxin, FT etc. The adsorption effect of toxin is not good.In addition, the feedstuff that processed of Jing mildew removing agent enters the internal of animal, be not " ten thousand none Lose ", the mycotoxin being attached to above mildew removing agent is also possible to be come off again in the larger stomach of water content, eventually enters into animal The organs such as liver and gall work the mischief.
The content of the invention
For problem present in background technology, the present invention provides one kind and can kill mycete, and with good mycete The adsorbent of toxin adsorption effect, and this adsorbent is added in feedstuff, and good palatability will not produce any toxic action.
In order to realize the purpose of the present invention, the present invention is adopted the following technical scheme that:
A kind of mold toxin sorbent, is made up of the component of following weight portion:Entringite 12-14 parts, bone amber 8-10 parts, Limonitum 6-9 parts, dehydroxanthan 10-14 parts, polyglutamic acid 1-3 parts, Sanguis Draxonis 15-19 parts, Olibanum 9-11 parts, Herba Thymi 2-4 parts, Herb Polygoni Chinensiss 10-13 parts, Semen Oroxyli 6-9 parts, Semen Nelumbinis 15-17 parts, roe 11-16 parts, FRUCTUS CITRI AURANTII AMARAE 12-15 parts, pork liver powder 14-17 part, Trichosanthes seed 5-8 parts.
Preferably, a kind of mold toxin sorbent, also including 9 parts of additive, the additive by weight by Following raw material is made:40% Poria, 30% Parmelia saxatilis Ach., 20% Auricularia Sophorae, 10% Ganoderma, are obtained using following methods:By Fu After Siberian cocklebur, Parmelia saxatilis Ach., Auricularia Sophorae, Ganoderma mixing, smash, additive is obtained.
Specifically, the preparation method of described mold toxin sorbent, comprises the following steps:
(1)After by entringite, bone amber, Limonitum mixing, 200-220 mesh is crushed to standby;
(2)Sanguis Draxonis, Olibanum are ground, dehydroxanthan, polyglutamic acid is then added thereto to, it is standby after stirring;
(3)Herba Thymi, Herb Polygoni Chinensiss, Semen Oroxyli, Semen Nelumbinis, FRUCTUS CITRI AURANTII AMARAE, trichosanthes seed are put in 50-60 DEG C of water, are soaked 12 hours Post-drying, is then crushed to 200-220 mesh, standby;
(4)By step(1), step(2), step(3)After powder and roe, pork liver powder, the additive mixing of middle gained, stirring is equal It is even, mold toxin sorbent is obtained.
As shown from the above technical solution, the invention has the beneficial effects as follows:
Compared to the mold toxin sorbent that prior art, the present invention are provided, various mycetes can not only be killed, also to various mycetes Toxin has good adsorption effect, and can also prevent the hypertrophy of feedstuff mycete during storage.Entringite is generally used for In cement, bone amber is usually used in ornament, and general people are difficult to expect both as mold toxin sorbent, and Jing test cards Bright, after both is crushed, after mixing with dehydroxanthan, polyglutamic acid, four collective effects can be with presence in adsorption feed Various mycotoxins, especially to the adsorption effect of aflatoxin more preferably, and the toxin after adsorbing, can't be in animal Come off again in vivo, animal is damaged;The mutually coordinated effect of effective ingredient in Limonitum, Sanguis Draxonis and Olibanum, to feedstuff In mycete killing effect significantly, and can also effectively press down mycostatic hypertrophy, extend the shelf-life of feedstuff;Herba Thymi, Linesless charcoal After effective ingredient collective effect in mother, Semen Oroxyli, Semen Nelumbinis, roe, FRUCTUS CITRI AURANTII AMARAE, pork liver powder, trichosanthes seed, animal can be improved Immunity, maintain animal intestinal in microecological balance, various immunocytes, digestive enzyme and protein synthesis enzyme can be activated Activity, and the function with protecting liver and detoxication, can effectively treat the injury that mycotoxin is caused to animal.It is effective in additive The mutual synergism of composition, can be good at improving the palatability of feedstuff, and can promote the growth of probioticss in animal intestinal, enter One step improves the immunity of body.
Specific embodiment
In order that those skilled in the art can be further understood that the feature and technology contents of the present invention, referring to following has Close detailed description of the invention.
Embodiment 1
A kind of mold toxin sorbent, is made up of the component of following weight portion:It is 12 parts of entringite, 8 parts of bone amber, 6 parts of Limonitum, de- 10 parts of hydrogen xanthan gum, 1 part of polyglutamic acid, 15 parts of Sanguis Draxonis, 9 parts of Olibanum, 2 parts of Herba Thymi, 10 parts of Herb Polygoni Chinensiss, 6 parts of Semen Oroxyli, Semen Nelumbinis 15 Part, 11 parts of roe, 12 parts of FRUCTUS CITRI AURANTII AMARAE, 14 parts of pork liver powder, 5 parts of trichosanthes seed.
Preferably, a kind of mold toxin sorbent, also including 9 parts of additive, the additive by weight by Following raw material is made:40% Poria, 30% Parmelia saxatilis Ach., 20% Auricularia Sophorae, 10% Ganoderma, are obtained using following methods:By Fu After Siberian cocklebur, Parmelia saxatilis Ach., Auricularia Sophorae, Ganoderma mixing, smash, additive is obtained.
Specifically, the preparation method of described mold toxin sorbent, comprises the following steps:
(1)After by entringite, bone amber, Limonitum mixing, 200 mesh are crushed to standby;
(2)Sanguis Draxonis, Olibanum are ground, dehydroxanthan, polyglutamic acid is then added thereto to, it is standby after stirring;
(3)Herba Thymi, Herb Polygoni Chinensiss, Semen Oroxyli, Semen Nelumbinis, FRUCTUS CITRI AURANTII AMARAE, trichosanthes seed are put in 50 DEG C of water, 12 hours after bake are soaked It is dry, 200 mesh are then crushed to, it is standby;
(4)By step(1), step(2), step(3)After powder and roe, pork liver powder, the additive mixing of middle gained, stirring is equal It is even, mold toxin sorbent is obtained.
Test
Feidong sow plant:There is sow 160 in, sow occurs poor appetite, poor growth or stagnation at summer, disappears It is thin;There is purpura in Visual mucous membrane xanthochromia, skin surface, and external genital swelling and mammary gland expand.On inspection, it is due to the Semen arachidis hypogaeae of feeding Caused by dregs of rice aflatoxin contamination, after add the mold toxin sorbent in embodiment 1, the addition of every kilogram of Semen arachidis hypogaeae dregs in Semen arachidis hypogaeae dregs Adsorbent 80g, after feeding 5 days, the swelling of sow external genital disappears, and appetite recovers normal, and growth recovery is normal.
Embodiment 2
A kind of mold toxin sorbent, is made up of the component of following weight portion:It is 13 parts of entringite, 9 parts of bone amber, 8 parts of Limonitum, de- 12 parts of hydrogen xanthan gum, 2 parts of polyglutamic acid, 17 parts of Sanguis Draxonis, 10 parts of Olibanum, 3 parts of Herba Thymi, 12 parts of Herb Polygoni Chinensiss, 8 parts of Semen Oroxyli, Semen Nelumbinis 16 parts, 13 parts of roe, 14 parts of FRUCTUS CITRI AURANTII AMARAE, 16 parts of pork liver powder, 7 parts of trichosanthes seed.
Preferably, a kind of mold toxin sorbent, also including 9 parts of additive, the additive by weight by Following raw material is made:40% Poria, 30% Parmelia saxatilis Ach., 20% Auricularia Sophorae, 10% Ganoderma, are obtained using following methods:By Fu After Siberian cocklebur, Parmelia saxatilis Ach., Auricularia Sophorae, Ganoderma mixing, smash, additive is obtained.
Specifically, the preparation method of described mold toxin sorbent, comprises the following steps:
(1)After by entringite, bone amber, Limonitum mixing, 210 mesh are crushed to standby;
(2)Sanguis Draxonis, Olibanum are ground, dehydroxanthan, polyglutamic acid is then added thereto to, it is standby after stirring;
(3)Herba Thymi, Herb Polygoni Chinensiss, Semen Oroxyli, Semen Nelumbinis, FRUCTUS CITRI AURANTII AMARAE, trichosanthes seed are put in 55 DEG C of water, 12 hours after bake are soaked It is dry, 210 mesh are then crushed to, it is standby;
(4)By step(1), step(2), step(3)After powder and roe, pork liver powder, the additive mixing of middle gained, stirring is equal It is even, mold toxin sorbent is obtained.
Test
Feixi breeding layer chicken field:There is laying hen more than 120,000 in, start to find that laying rate of laying hen drastically declines in August, 2016, Laying hen feed intake is reduced, and remaining many is from spice in hopper.Jing is dissected, and the mesentery nigrescence that degree differs, intestinal tube occurs in diseased chicken Placenta percreta is distributed black floccule.Spleen, liver enlargement, substantially, mainly air bag wall thickening has cloud to secrete to air bag inflammation Attachment.Follicle liquefaction, degeneration necrosis, atrophy.On inspection, Semen Maydiss go mouldy seriously.This batch of Semen Maydiss are changed, new Semen Maydiss are purchased again Grain ration, and the mold toxin sorbent in embodiment 2 is added in Semen Maydiss, feed intake is gradually recovered after three days, lays eggs after 15 days Amount recovers normal.Illustrating the mold toxin sorbent of present invention offer has reparation to the harm that mycotoxin is caused and removes work( Energy.
Embodiment 3
A kind of mold toxin sorbent, is made up of the component of following weight portion:14 parts of entringite, 10 parts of bone amber, 9 parts of Limonitum, 14 parts of dehydroxanthan, 3 parts of polyglutamic acid, 19 parts of Sanguis Draxonis, 11 parts of Olibanum, 4 parts of Herba Thymi, 13 parts of Herb Polygoni Chinensiss, 9 parts of Semen Oroxyli, lotus 17 parts of son, 16 parts of roe, 15 parts of FRUCTUS CITRI AURANTII AMARAE, 17 parts of pork liver powder, 8 parts of trichosanthes seed.
Preferably, a kind of mold toxin sorbent, also including 9 parts of additive, the additive by weight by Following raw material is made:40% Poria, 30% Parmelia saxatilis Ach., 20% Auricularia Sophorae, 10% Ganoderma, are obtained using following methods:By Fu After Siberian cocklebur, Parmelia saxatilis Ach., Auricularia Sophorae, Ganoderma mixing, smash, additive is obtained.
Specifically, the preparation method of described mold toxin sorbent, comprises the following steps:
(1)After by entringite, bone amber, Limonitum mixing, 220 mesh are crushed to standby;
(2)Sanguis Draxonis, Olibanum are ground, dehydroxanthan, polyglutamic acid is then added thereto to, it is standby after stirring;
(3)Herba Thymi, Herb Polygoni Chinensiss, Semen Oroxyli, Semen Nelumbinis, FRUCTUS CITRI AURANTII AMARAE, trichosanthes seed are put in 60 DEG C of water, 12 hours after bake are soaked It is dry, 220 mesh are then crushed to, it is standby;
(4)By step(1), step(2), step(3)After powder and roe, pork liver powder, the additive mixing of middle gained, stirring is equal It is even, mold toxin sorbent is obtained.
Feixi County broiler breeding field:There is yellow-feather broiler more than 100,000 in, from April, 2016, chicken feed intake declines, egg Chicken feed intake is reduced, and body weight increase is slow, and paralysis occurs in part chicken, dyspnea, rapid, diarrhoea, and row's black and carrying does not disappear Change the feces of feedstuff.It is containing in a large number by caused by the ageing Semen sojae atricolor powder of mycotoxin contamination in feed particulate material by confirmation.Afterwards Feedstuff is changed, fresh corn pellet is purchased, and the mold toxin sorbent in embodiment 3 is added in feedstuff, searched for food after 2 Amount is gradually recovered, and produces without black feces after 5 days, and feed intake recovers normal.Illustrate to provide mycotoxin adsorption in embodiment 3 Agent can alleviate the harm that mycotoxin is caused to broiler.
It should be noted that above example is only to illustrate technical scheme and unrestricted.Although with reference to compared with Good embodiment has been described in detail to the present invention, it will be understood by those within the art that, can be to the technology of invention Scheme is modified or equivalent, and without deviating from the scope of technical solution of the present invention, it all should cover the power in the present invention In sharp claimed range.

Claims (3)

1. a kind of mold toxin sorbent, it is characterised in that be made up of the component of following weight portion:Entringite 12-14 parts, bone amber 8-10 parts, Limonitum 6-9 parts, dehydroxanthan 10-14 parts, polyglutamic acid 1-3 parts, Sanguis Draxonis 15-19 parts, Olibanum 9-11 parts, Green pepper 2-4 parts, Herb Polygoni Chinensiss' 10-13 parts, Semen Oroxyli 6-9 parts, Semen Nelumbinis 15-17 parts, roe 11-16 parts, FRUCTUS CITRI AURANTII AMARAE 12-15 parts, Pork liver powder 14-17 part, trichosanthes seed 5-8 parts.
2. according to a kind of mold toxin sorbent described in claim 1, it is characterised in that a kind of mycotoxin adsorption Agent, also including 9 parts of additive, the additive is made up by weight of following raw material:40% Poria, 30% Parmelia saxatilis Ach., 20% Auricularia Sophorae, 10% Ganoderma, using following methods be obtained:After by Poria, Parmelia saxatilis Ach., Auricularia Sophorae, Ganoderma mixing, smash, be obtained and add Plus agent.
3. the preparation method of the mold toxin sorbent described in a kind of claim 1 and 2, it is characterised in that including following step Suddenly:
(1)After by entringite, bone amber, Limonitum mixing, 200-220 mesh is crushed to standby;
(2)Sanguis Draxonis, Olibanum are ground, dehydroxanthan, polyglutamic acid is then added thereto to, it is standby after stirring;
(3)Herba Thymi, Herb Polygoni Chinensiss, Semen Oroxyli, Semen Nelumbinis, FRUCTUS CITRI AURANTII AMARAE, trichosanthes seed are put in 50-60 DEG C of water, are soaked 12 hours Post-drying, is then crushed to 200-220 mesh, standby;
(4)By step(1), step(2), step(3)After powder and roe, pork liver powder, the additive mixing of middle gained, stirring is equal It is even, mold toxin sorbent is obtained.
CN201611006931.8A 2016-11-16 2016-11-16 Mycotoxin adsorbent and preparation method thereof Pending CN106578416A (en)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103141685A (en) * 2013-03-12 2013-06-12 北京翰赛柯生物科技有限公司 Mycotoxin detoxication agent for swine feed
CN103418347A (en) * 2012-05-24 2013-12-04 程会 Mold adsorbent
CN103583823A (en) * 2013-11-07 2014-02-19 北京大北农科技集团股份有限公司 Mold removal agent for feed and preparation method and feed additive thereof
CN103875916A (en) * 2012-12-20 2014-06-25 信宜市金方子生物科技有限公司 Chinese herbal medicine-type feed mildew inhibitor
CN104605164A (en) * 2015-02-13 2015-05-13 安徽恒源药业有限公司 Livestock feed mold-removing additive
CN105211635A (en) * 2015-10-26 2016-01-06 金华傲农生物科技有限公司 A kind of feed addictive removing mycotoxin and preparation method thereof and application
CN105639401A (en) * 2016-01-05 2016-06-08 山东中科嘉亿生物工程有限公司 Feeding mold removal agent formula and application method

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103418347A (en) * 2012-05-24 2013-12-04 程会 Mold adsorbent
CN103875916A (en) * 2012-12-20 2014-06-25 信宜市金方子生物科技有限公司 Chinese herbal medicine-type feed mildew inhibitor
CN103141685A (en) * 2013-03-12 2013-06-12 北京翰赛柯生物科技有限公司 Mycotoxin detoxication agent for swine feed
CN103583823A (en) * 2013-11-07 2014-02-19 北京大北农科技集团股份有限公司 Mold removal agent for feed and preparation method and feed additive thereof
CN104605164A (en) * 2015-02-13 2015-05-13 安徽恒源药业有限公司 Livestock feed mold-removing additive
CN105211635A (en) * 2015-10-26 2016-01-06 金华傲农生物科技有限公司 A kind of feed addictive removing mycotoxin and preparation method thereof and application
CN105639401A (en) * 2016-01-05 2016-06-08 山东中科嘉亿生物工程有限公司 Feeding mold removal agent formula and application method

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Application publication date: 20170426