CN106577814A - Novel pharmaceutical composition for controlling black rot of citrus gonggan - Google Patents
Novel pharmaceutical composition for controlling black rot of citrus gonggan Download PDFInfo
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- CN106577814A CN106577814A CN201610933365.9A CN201610933365A CN106577814A CN 106577814 A CN106577814 A CN 106577814A CN 201610933365 A CN201610933365 A CN 201610933365A CN 106577814 A CN106577814 A CN 106577814A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/74—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,3
- A01N43/78—1,3-Thiazoles; Hydrogenated 1,3-thiazoles
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- A01N49/00—Biocides, pest repellants or attractants, or plant growth regulators, containing compounds containing the group, wherein m+n>=1, both X together may also mean —Y— or a direct carbon-to-carbon bond, and the carbon atoms marked with an asterisk are not part of any ring system other than that which may be formed by the atoms X, the carbon atoms in square brackets being part of any acyclic or cyclic structure, or the group, wherein A means a carbon atom or Y, n>=0, and not more than one of these carbon atoms being a member of the same ring system, e.g. juvenile insect hormones or mimics thereof
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- A01N59/08—Alkali metal chlorides; Alkaline earth metal chlorides
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- A01N59/12—Iodine, e.g. iodophors; Compounds thereof
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- A—HUMAN NECESSITIES
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
Abstract
The invention discloses a novel pharmaceutical composition for controlling black rot of citrus gonggan. The pharmaceutical composition comprises the following raw materials: paulownia leaf, tripterygium wilfordii, folium artemisiae argyi, wasabia japonica, weeping willow leaf, piper methysticum, tea tree leaf, anabasis aphylla, potassium salts, phosphor salts, nitrogen salts, calcium salts, magnesium salts, iodine salts, boron salts, molybdenum salts, zinc salts, manganese salts, copper salts, iron salts, vitamins, amino acids, indolebutyric acid, gibberellin, 6-benzyl adenine, naphthylacetic acid, agar, kinetin, N-methyl pyrrolidone, sodium dinonyl naphthalene sulfonate, American Dupont EEA2112AC compatibilizer, earthworm powder, potassium alkyl sulfate, trimethylol propane triacrylate, 3-aminopropyl triethoxysilane, carrageenan, mancozeb, carbendazim, prochloraz, wetting osmotic agent, synergist, and ethanol. The provided novel pharmaceutical composition can control black rot of citrus gonggan, and improve yield and sugar content. The taste of cultured citrus gonggan is good, and the quality is high. The using effect of provided pharmaceutical composition is better than that of common pharmaceutical compositions.
Description
【Technical field】
The invention belongs to tribute Citrus chachiensis Hort. diseases prevention technical field, and in particular to a kind of newtype drug combination of preventing and treating tribute Citrus chachiensis Hort. black rot
Thing.
【Background technology】
Tribute Citrus chachiensis Hort. is that Hezhou City Zhongshan County has much one of mandarin orange improved seeds of local characteristic, especially pure sweet, in good taste with taste
The market competitiveness is had much with there are the merits such as special fragrance.
Tribute Citrus chachiensis Hort. fruit shape is beautiful, fruit coloured gold Huang, few thin skin core, fragile muscle slugging, fresh and sweet fragrant honey, high sugar are low sour, with rich flavor, it
Orange class beautiful outline form and mandarin orange fine and tender taste, the two-fold advantage of easy peeling are concentrated, has been that other citrus varieties hardly match, is described as
The king of mandarin orange.90-145 gram of tribute Citrus chachiensis Hort. mean fruit weight, fruit footpath 60-65mm, soluble solid (mainly sugar) is up to 9.0-
12.5%, edible rate about 78%, per 100 milliliters of fruit juice sugar contents 8.5-11.0 gram, acid content 0.3-0.5%.Fruit is in November
The last ten-days period to late December is ripe, is the splendid fruit in the Spring Festival holidays.The fruit is nutritious, rich in multivitamin, trace element, ore deposit
Material, organic acid etc., autumn and winter season, the great stagnation that disappears was acted on yearningly, can effectively supplement needed by human body nutrient and moisture, by fruit industry
Boundary is referred to as the fruit upstart of current health.
The disease that Citrus black rot is mainly produced by fruit such as the microbial Citrus of Citrus rod method, with evil mind type,
Citrus fruits are caused certain harm by black rotten type, the base of a fruit corruption type such as type and dry scar type.Cause the main danger of black rot
Evil microorganism is alternaric bacteria, prevents and treats black rot at present and is mainly biological pesticide, and effective drug duration is short, frequently gos and buy Chinese medicine
The burden of orchard worker, also increases labor cost, also causes tribute Citrus chachiensis Hort. alternaric bacteria that a large amount of pesticide are generated with Drug resistance, sterilization effect
Fruit declines obvious.It is the task of top priority to find additive method prevention and control Citrus black rot.
Additionally, other it is existing preventing and treating tribute Citrus chachiensis Hort. black rot medicines using it is rear exist improve tribute Citrus chachiensis Hort. yield and sugar content rate it is low,
The problems such as mouthfeel and general appearance color and luster.
【The content of the invention】
The present invention provides a kind of new pharmaceutical composition of preventing and treating tribute Citrus chachiensis Hort. black rot, to solve present biological pesticide, medicine
The effect time is short, effect is poor, and the medicine of existing preventing and treating tribute Citrus chachiensis Hort. black rot using it is rear exist improve tribute Citrus chachiensis Hort. yield and sugar content rate
The problems such as low, mouthfeel and general appearance color and luster.The present invention new pharmaceutical composition preventing and treating tribute Citrus chachiensis Hort. black rot, can improve yield and
Sugar content, and tribute Citrus chachiensis Hort. is in good taste, appearance color and luster is mellow and full, and quality is high, higher than conventional control tribute Citrus chachiensis Hort. black rot new pharmaceutical composition
Using effect.
To solve above technical problem, the present invention is employed the following technical solutions：
A kind of new pharmaceutical composition of preventing and treating tribute Citrus chachiensis Hort. black rot, in units of weight portion, including following raw material：Folium paulowniae
104-130 parts, Radix Tripterygii Wilfordii 83-100 parts, Folium Artemisiae Argyi 73-90 parts, Wasabia japonic (Euterma Wasabi) 75-90 parts, Salix babylonica L. leaf 52-80 parts, piper methysticum 46-75
Part, leaf of tea tree 40-65 parts, Herba Anabasis aphyllae 35-60 parts, potassium salt 2-3 parts, microcosmic salt 1-3 parts, nitrogen salt 1-2 parts, calcium salt 0.6-0.9
Part, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron salt 0.2-0.4 part, molybdenum salt 0.2-0.4 parts, zinc salt 0.2-0.4 parts, manganese salt
0.2-0.4 parts, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts, vitamin 0.2-0.4 parts, aminoacid 0.2-0.3 parts, indole fourth
Sour 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyl gland fat purine 0.06-0.08 parts, naphthalene acetic acid 0.04-0.06 parts, fine jade
Fat 0.1-0.3 parts, kinetins 0.04-0.06 parts, N-Methyl pyrrolidone 0.7-2.3 parts, dinonylnaphthalene sulfonic acid sodium 0.6-1.5
Part, Dupont EEA2112AC compatilizer 1-1.6 parts, Lumbricus powder 0.6-1.4 parts, alkyl sulfate potassium 0.5-1.2 parts, three hydroxyls
Propane tri 0.5-0.9 parts, 3- aminopropyl triethoxysilane 0.6-1.3 parts, carrageenan 0.5-1.2 parts, generation
Gloomy MnZn 0.4-0.7 parts, carbendazim 0.3-0.6 parts, Prochloraz 0.5-0.8 parts, wetting and penetrating agent 0.9-1.6 parts, synergist
1.5-2.5 part, ethanol 2000-6000 parts；
The preparation method of the new pharmaceutical composition of the preventing and treating tribute Citrus chachiensis Hort. black rot, comprises the following steps：
S1：By Folium paulowniae, Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, Wasabia japonic (Euterma Wasabi), Salix babylonica L. leaf, piper methysticum, leaf of tea tree, Herba Anabasis aphyllae mixed powder
It is broken, mixture I is obtained, mixture I is added in ethanol, be 1 in solid-liquid ratio:14-16, ultrasonic power are 200-300W,
Concentration of alcohol is 65%-80%, and Extracting temperature is that medicinal liquid 17-23min is extracted at 64-76 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed into 3000-5000 mesh sieve, filtrate is obtained；
S3：By filtrate addition potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc obtained in step S2
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, N-Methyl pyrrolidone, dinonylnaphthalene sulfonic acid sodium, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate potassium,
Trimethylolpropane trimethacrylate, 3- aminopropyl triethoxysilanes, carrageenan, Mancozeb, carbendazim, Prochloraz, profit
Wet penetrating agent, synergist, are 40-53 DEG C in temperature, and rotating speed is stirring and dissolving 18-32min under 100-300r/min, and mixing is obtained
Liquid；
S4：Mixed liquor obtained in step S3 is concentrated into into water content≤22% in the case where temperature is for 60-80 DEG C, mixture is obtained
Ⅱ；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed,
120-260 mesh sieve is crossed, gained powder adopts pulse vacuum pressure steam sterilizer in temperature for 134-136 DEG C, and pressure is
Sterilize under 210-230KPa 3-4min, and preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition is obtained.
Further, the wetting and penetrating agent is sodium alkyl benzene sulfonate；The synergist in units of weight portion, including with
Lower raw material：Wood vinegar 20-40 parts, glycerol 10-18 parts, Portugal's ethamine 8-16 parts, ammonium citrate 6-12 parts, tween 20 5-10 parts,
Fulvic acid 4-6 parts, laurel alcohol ether phosphate 3-5 part.
Further, the potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, nitric acid
Potassium 0.4-0.6 parts, potassium carbonate 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts.
Further, the microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, phosphoric acid
Ferrum 0.2-0.7 parts, zinc phosphate 0.2-0.7 parts.
Further, the nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, chlorine
Change ammonium 0.3-0.6 parts.
Further, the calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulfur
Sour Asia calcium 0.1-0.2 parts.
Further, the magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulfur
Sour Asia magnesium 0.1-0.2 parts.
Further, the iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride.
Further, the vitamin is composed of the following components：Raw element A 0.08-0.14 parts, vitamin B10.08-0.12
Part, vitamin B20.02-0.08 parts, vitamin C 0.02-0.06 parts.
Further, the aminoacid is composed of the following components：Glycine 0.08-0.1 parts, isoleucine 0.06-0.08
Part, proline 0.04-0.07 parts, Phenylalanine 0.02-0.05 part.
The invention has the advantages that：
(1) preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition of the invention preventing and treating tribute Citrus chachiensis Hort. black rot, can improve yield and contain
Sugar amount, and tribute Citrus chachiensis Hort. is in good taste, appearance color and luster is mellow and full, and quality is high, makes higher than conventional control tribute Citrus chachiensis Hort. black rot new pharmaceutical composition
Use effect；
(2) preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition production method of the invention is simple, and low cost is easy to use,
, up to 3-6 month, application effect is good, is conducive to popularization and application for effective drug duration.
【Specific embodiment】
For ease of more fully understanding the present invention, it is illustrated by following examples, these embodiments belong to the present invention's
Protection domain, but do not limit the scope of the invention.
In embodiment, the new pharmaceutical composition of the preventing and treating tribute Citrus chachiensis Hort. black rot, in units of weight portion, including following
Raw material：Folium paulowniae 104-130 parts, Radix Tripterygii Wilfordii 83-100 parts, Folium Artemisiae Argyi 73-90 parts, Wasabia japonic (Euterma Wasabi) 75-90 parts, Salix babylonica L. leaf 52-80 parts, card
Watt Fructus Piperiss 46-75 parts, leaf of tea tree 40-65 parts, Herba Anabasis aphyllae 35-60 parts, potassium salt 2-3 parts, microcosmic salt 1-3 parts, nitrogen salt 1-2 parts,
Calcium salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron salt 0.2-0.4 part, molybdenum salt 0.2-0.4 parts, zinc salt
0.2-0.4 parts, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts, vitamin 0.2-0.4 parts, aminoacid
0.2-0.3 parts, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyl gland fat purine 0.06-0.08 parts, naphthalene second
Sour 0.04-0.06 parts, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, N-Methyl pyrrolidone 0.7-2.3 parts, dinonyl
Sodium naphthalene sulfonate 0.6-1.5 parts, Dupont EEA2112AC compatilizer 1-1.6 parts, Lumbricus powder 0.6-1.4 parts, alkyl sulfate potassium
0.5-1.2 parts, trimethylolpropane trimethacrylate 0.5-0.9 parts, 3- aminopropyl triethoxysilane 0.6-1.3 parts, OK a karaoke club
Glue 0.5-1.2 parts, Mancozeb 0.4-0.7 parts, carbendazim 0.3-0.6 parts, Prochloraz 0.5-0.8 parts, wetting and penetrating agent 0.9-
1.6 parts, synergist 1.5-2.5 parts, ethanol 2000-6000 parts；
The wetting and penetrating agent is sodium alkyl benzene sulfonate；
Synergist in units of weight portion, including following raw material：Wood vinegar 20-40 parts, glycerol 10-18 parts, Portugal's ethamine
8-16 parts, ammonium citrate 6-12 parts, tween 20 5-10 parts, fulvic acid 4-6 parts, laurel alcohol ether phosphate 3-5 part；
The potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6
Part, potassium carbonate 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts；
The microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7
Part, zinc phosphate 0.2-0.7 parts；
The nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3-
0.6 part；
The calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1-
0.2 part；
The magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1-
0.2 part；
The iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A 0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin
B20.02-0.08 parts, vitamin C 0.02-0.06 parts；
The aminoacid is composed of the following components：Glycine 0.08-0.1 parts, isoleucine 0.06-0.08 parts, proline
0.04-0.07 parts, Phenylalanine 0.02-0.05 part；
The preparation method of described preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, comprises the following steps：
S1：By Folium paulowniae, Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, Wasabia japonic (Euterma Wasabi), Salix babylonica L. leaf, piper methysticum, leaf of tea tree, Herba Anabasis aphyllae mixed powder
It is broken, mixture I is obtained, mixture I is added in ethanol, be 1 in solid-liquid ratio:14-16, ultrasonic power are 200-300W,
Concentration of alcohol is 65%-80%, and Extracting temperature is that medicinal liquid 17-23min is extracted at 64-76 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed into 3000-5000 mesh sieve, filtrate is obtained；
S3：By filtrate addition potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc obtained in step S2
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, N-Methyl pyrrolidone, dinonylnaphthalene sulfonic acid sodium, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate potassium,
Trimethylolpropane trimethacrylate, 3- aminopropyl triethoxysilanes, carrageenan, Mancozeb, carbendazim, Prochloraz, profit
Wet penetrating agent, synergist, are 40-53 DEG C in temperature, and rotating speed is stirring and dissolving 18-32min under 100-300r/min, and mixing is obtained
Liquid；
S4：Mixed liquor obtained in step S3 is concentrated into into water content≤22% in the case where temperature is for 60-80 DEG C, mixture is obtained
Ⅱ；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed,
120-260 mesh sieve is crossed, gained powder adopts pulse vacuum pressure steam sterilizer in temperature for 134-136 DEG C, and pressure is
Sterilize under 210-230KPa 3-4min, and preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition is obtained.
The using method of the new pharmaceutical composition preventing and treating tribute Citrus chachiensis Hort. black rot of the present invention is as follows：By preventing to tribute Citrus chachiensis Hort. young sprout
The new pharmaceutical composition of spray the present embodiment in time is noted before 2-3 time, particularly rain after rain.
It is illustrated below by more specifically embodiment.
Embodiment 1
A kind of new pharmaceutical composition of preventing and treating tribute Citrus chachiensis Hort. black rot, in units of weight portion, including following raw material：Folium paulowniae
115 parts, it is 90 parts of Radix Tripterygii Wilfordii, 80 parts of Folium Artemisiae Argyi, 80 parts of Wasabia japonic (Euterma Wasabi), 65 parts of Salix babylonica L. leaf, 60 parts of piper methysticum, 55 parts of leaf of tea tree, false without leaf
50 parts of Herba Equiseties Hiemalis, 2.5 parts of potassium salt, 2 parts of microcosmic salt, 1.5 parts of nitrogen salt, 0.8 part of calcium salt, 0.8 part of magnesium salt, 0.3 part of iodine salt, 0.3 part of boron salt,
0.3 part of molybdenum salt, 0.3 part of zinc salt, 0.3 part of manganese salt, 0.3 part of mantoquita, 0.3 part of iron salt, 0.3 part of vitamin, 0.2 part of aminoacid, Yin
0.08 part of diindyl butanoic acid, 0.08 part of gibberellins, 0.07 part of 6- benzyl gland fats purine, 0.05 part of naphthalene acetic acid, 0.2 part of agar, kinetins
0.05 part, 1.5 parts of N-Methyl pyrrolidone, 1 part of dinonylnaphthalene sulfonic acid sodium, 1.4 parts of Dupont EEA2112AC compatilizers, earthworm
1 part of earthworm powder, 0.9 part of alkyl sulfate potassium, 0.8 part of trimethylolpropane trimethacrylate, 3- aminopropyl triethoxysilanes 0.9
Part, 0.8 part of carrageenan, 0.6 part of Mancozeb, 0.5 part of carbendazim, 0.7 part of Prochloraz, 1.2 parts of wetting and penetrating agent, synergist 2
Part, 4000 parts of ethanol；
The wetting and penetrating agent is sodium alkyl benzene sulfonate；
Synergist in units of weight portion, including following raw material：30 parts of wood vinegar, 15 parts of glycerol, 12 parts of Portugal's ethamine, lemon
Lemon 9 parts of ammonium of acid, 8 parts of tween 20,5 parts of fulvic acid, 4 parts of laurel alcohol ether phosphate；
The potassium salt is composed of the following components：0.7 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, potassium carbonate 0.5
Part, 0.4 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.6 part of calcium phosphate, 0.6 part of magnesium phosphate, 0.5 part of iron phosphate, zinc phosphate 0.3
Part；
The nitrogen salt is composed of the following components：0.6 part of ammonium hydrogen carbonate, 0.5 part of ammonium carbonate, 0.4 part of ammonium chloride；
The calcium salt is composed of the following components：0.3 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.3 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.2 part of sodium iodide, 0.1 part of potassium iodate；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：0.1 part of raw element A, vitamin B10.1 part, vitamin B20.05 part, dimension life
0.05 part of plain C；
The aminoacid is composed of the following components：0.08 part of glycine, 0.06 part of isoleucine, 0.04 part of proline, benzene
0.02 part of alanine；
The preparation method of described preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, comprises the following steps：
S1：By Folium paulowniae, Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, Wasabia japonic (Euterma Wasabi), Salix babylonica L. leaf, piper methysticum, leaf of tea tree, Herba Anabasis aphyllae mixed powder
It is broken, mixture I is obtained, mixture I is added in ethanol, be 1 in solid-liquid ratio:15, ultrasonic power is 250W, concentration of alcohol
For 75%, Extracting temperature is that medicinal liquid 20min is extracted at 70 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed into 4000 mesh sieve, filtrate is obtained；
S3：By filtrate addition potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc obtained in step S2
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, N-Methyl pyrrolidone, dinonylnaphthalene sulfonic acid sodium, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate potassium,
Trimethylolpropane trimethacrylate, 3- aminopropyl triethoxysilanes, carrageenan, Mancozeb, carbendazim, Prochloraz, profit
Wet penetrating agent, synergist, are 48 DEG C in temperature, and rotating speed is stirring and dissolving 25min under 200r/min, and mixed liquor is obtained；
S4：It is 22% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 70 DEG C, and mixture II is obtained；
S5：It is 6% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 86 DEG C, is then crushed, mistake
200 mesh sieve, gained powder adopt pulse vacuum pressure steam sterilizer in temperature for 135 DEG C, and pressure is to sterilize under 220KPa
3.5min, is obtained preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition.
The using method of the new pharmaceutical composition preventing and treating tribute Citrus chachiensis Hort. black rot of the present invention is as follows：By preventing to tribute Citrus chachiensis Hort. young sprout
The new pharmaceutical composition of spray the present embodiment in time is noted before 1 time, particularly rain after rain.
Embodiment 2
A kind of new pharmaceutical composition of preventing and treating tribute Citrus chachiensis Hort. black rot, in units of weight portion, including following raw material：Folium paulowniae
104 parts, it is 83 parts of Radix Tripterygii Wilfordii, 73 parts of Folium Artemisiae Argyi, 75 parts of Wasabia japonic (Euterma Wasabi), 52 parts of Salix babylonica L. leaf, 46 parts of piper methysticum, 40 parts of leaf of tea tree, false without leaf
35 parts of Herba Equiseties Hiemalis, 2 parts of potassium salt, 1 part of microcosmic salt, 1 part of nitrogen salt, 0.6 part of calcium salt, 0.6 part of magnesium salt, 0.2 part of iodine salt, 0.2 part of boron salt, molybdenum salt
0.2 part, 0.2 part of zinc salt, 0.2 part of manganese salt, 0.2 part of mantoquita, 0.2 part of iron salt, 0.2 part of vitamin, 0.2 part of aminoacid, indole fourth
Acid 0.06 part, 0.06 part of gibberellins, 0.06 part of 6- benzyl gland fats purine, 0.04 part of naphthalene acetic acid, 0.1 part of agar, 0.04 part of kinetins,
0.7 part of N-Methyl pyrrolidone, 0.6 part of dinonylnaphthalene sulfonic acid sodium, 1 part of Dupont EEA2112AC compatilizers, Lumbricus powder 0.6
Part, 0.5 part of alkyl sulfate potassium, 0.5 part of trimethylolpropane trimethacrylate, 0.6 part of 3- aminopropyl triethoxysilanes, card
Draw 0.5 part of glue, 0.4 part of Mancozeb, 0.3 part of carbendazim, 0.5 part of Prochloraz, 0.9 part of wetting and penetrating agent, 1.5 parts of synergist,
2000 parts of ethanol；
The wetting and penetrating agent is sodium alkyl benzene sulfonate；
Synergist in units of weight portion, including following raw material：20 parts of wood vinegar, 10 parts of glycerol, 8 parts of Portugal's ethamine, lemon
Lemon 6 parts of ammonium of acid, 5 parts of tween 20,4 parts of fulvic acid, 3 parts of laurel alcohol ether phosphate；
The potassium salt is composed of the following components：0.6 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, potassium carbonate 0.3
Part, 0.2 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.3 part of calcium phosphate, 0.3 part of magnesium phosphate, 0.2 part of iron phosphate, zinc phosphate 0.2
Part；
The nitrogen salt is composed of the following components：0.4 part of ammonium hydrogen carbonate, 0.3 part of ammonium carbonate, 0.3 part of ammonium chloride；
The calcium salt is composed of the following components：0.3 part of calcium glycine, 0.2 part of calcium chloride, 0.1 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.3 part of magnesium glycinate, 0.2 part of magnesium chloride, 0.1 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.1 part of sodium iodide, 0.1 part of potassium iodate；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.08 parts, vitamin B10.08 part, vitamin B20.02 part, dimension
Raw element C0.02 parts；
The aminoacid is composed of the following components：0.08 part of glycine, 0.06 part of isoleucine, 0.04 part of proline, benzene
0.02 part of alanine；
The preparation method of described preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, comprises the following steps：
S1：By Folium paulowniae, Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, Wasabia japonic (Euterma Wasabi), Salix babylonica L. leaf, piper methysticum, leaf of tea tree, Herba Anabasis aphyllae mixed powder
It is broken, mixture I is obtained, mixture I is added in ethanol, be 1 in solid-liquid ratio:14, ultrasonic power is 200W, concentration of alcohol
For 65%, Extracting temperature is that medicinal liquid 23min is extracted at 64 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed into 3000 mesh sieve, filtrate is obtained；
S3：By filtrate addition potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc obtained in step S2
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, N-Methyl pyrrolidone, dinonylnaphthalene sulfonic acid sodium, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate potassium,
Trimethylolpropane trimethacrylate, 3- aminopropyl triethoxysilanes, carrageenan, Mancozeb, carbendazim, Prochloraz, profit
Wet penetrating agent, synergist, are 40 DEG C in temperature, and rotating speed is stirring and dissolving 32min under 100r/min, and mixed liquor is obtained；
S4：It is 20% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 60 DEG C, and mixture II is obtained；
S5：It is 5% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 84 DEG C, is then crushed, mistake
120 mesh sieve, gained powder adopt pulse vacuum pressure steam sterilizer in temperature for 134 DEG C, and pressure is to sterilize under 210KPa
4min, is obtained preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition.
The using method of the new pharmaceutical composition preventing and treating tribute Citrus chachiensis Hort. black rot of the present invention is as follows：By preventing to tribute Citrus chachiensis Hort. young sprout
The new pharmaceutical composition of spray the present embodiment in time is noted before 2 times, particularly rain after rain.
Embodiment 3
A kind of new pharmaceutical composition of preventing and treating tribute Citrus chachiensis Hort. black rot, in units of weight portion, including following raw material：Folium paulowniae
130 parts, 100 parts of Radix Tripterygii Wilfordii, 90 parts of Folium Artemisiae Argyi, 90 parts of Wasabia japonic (Euterma Wasabi), Salix babylonica L. leaf 50-80 parts, 75 parts of piper methysticum, 65 parts of leaf of tea tree, nothing
Leaf vacation 60 parts of Herba Equiseties Hiemalis, 3 parts of potassium salt, 3 parts of microcosmic salt, 2 parts of nitrogen salt, 0.9 part of calcium salt, 0.9 part of magnesium salt, 0.4 part of iodine salt, 0.4 part of boron salt,
0.4 part of molybdenum salt, 0.4 part of zinc salt, 0.4 part of manganese salt, 0.4 part of mantoquita, 0.4 part of iron salt, 0.4 part of vitamin, 0.3 part of aminoacid, Yin
0.09 part of diindyl butanoic acid, 0.09 part of gibberellins, 0.08 part of 6- benzyl gland fats purine, 0.06 part of naphthalene acetic acid, 0.3 part of agar, kinetins
0.06 part, 2.3 parts of N-Methyl pyrrolidone, 1.5 parts of dinonylnaphthalene sulfonic acid sodium, 1.6 parts of Dupont EEA2112AC compatilizers,
1.4 parts of Lumbricus powder, 1.2 parts of alkyl sulfate potassium, 0.9 part of trimethylolpropane trimethacrylate, 3- aminopropyl-triethoxy silicon
1.3 parts of alkane, 1.2 parts of carrageenan, 0.7 part of Mancozeb, 0.6 part of carbendazim, 0.8 part of Prochloraz, 1.6 parts of wetting and penetrating agent, increasing
2.5 parts of agent of effect, 6000 parts of ethanol；
The wetting and penetrating agent is sodium alkyl benzene sulfonate；
Synergist in units of weight portion, including following raw material：40 parts of wood vinegar, 18 parts of glycerol, 16 parts of Portugal's ethamine, lemon
Lemon 12 parts of ammonium of acid, 10 parts of tween 20,6 parts of fulvic acid, 5 parts of laurel alcohol ether phosphate；
The potassium salt is composed of the following components：0.8 part of potassium chloride, 0.6 part of potassium sulfate, 0.6 part of potassium nitrate, potassium carbonate 0.5
Part, 0.5 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.8 part of calcium phosphate, 0.8 part of magnesium phosphate, 0.7 part of iron phosphate, zinc phosphate 0.7
Part；
The nitrogen salt is composed of the following components：0.8 part of ammonium hydrogen carbonate, 0.6 part of ammonium carbonate, 0.6 part of ammonium chloride；
The calcium salt is composed of the following components：0.4 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.4 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.2 part of sodium iodide, 0.2 part of potassium iodate；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.14 parts, vitamin B10.12 part, vitamin B20.08 part, dimension
Raw element C0.06 parts；
The aminoacid is composed of the following components：0.1 part of glycine, 0.08 part of isoleucine, 0.07 part of proline, phenylpropyl alcohol
0.05 part of propylhomoserin；
The preparation method of described preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, comprises the following steps：
S1：By Folium paulowniae, Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, Wasabia japonic (Euterma Wasabi), Salix babylonica L. leaf, piper methysticum, leaf of tea tree, Herba Anabasis aphyllae mixed powder
It is broken, mixture I is obtained, mixture I is added in ethanol, be 1 in solid-liquid ratio:16, ultrasonic power is 300W, concentration of alcohol
For 80%, Extracting temperature is that medicinal liquid 17min is extracted at 76 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed into 5000 mesh sieve, filtrate is obtained；
S3：By filtrate addition potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc obtained in step S2
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, N-Methyl pyrrolidone, dinonylnaphthalene sulfonic acid sodium, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate potassium,
Trimethylolpropane trimethacrylate, 3- aminopropyl triethoxysilanes, carrageenan, Mancozeb, carbendazim, Prochloraz, profit
Wet penetrating agent, synergist, are 53 DEG C in temperature, and rotating speed is stirring and dissolving 18min under 300r/min, and mixed liquor is obtained；
S4：It is 16% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 80 DEG C, and mixture II is obtained；
S5：It is 4% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 88 DEG C, is then crushed, mistake
260 mesh sieve, gained powder adopt pulse vacuum pressure steam sterilizer in temperature for 136 DEG C, and pressure is to sterilize under 230KPa
3min, is obtained preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition.
The using method of the new pharmaceutical composition preventing and treating tribute Citrus chachiensis Hort. black rot of the present invention is as follows：By preventing to tribute Citrus chachiensis Hort. young sprout
The new pharmaceutical composition of spray the present embodiment in time is noted before 1 time, particularly rain after rain.
(1) test group：Using the new pharmaceutical composition preventing and treating tribute Citrus chachiensis Hort. black rot of embodiment 1-3；(2) matched group 1：Using
The spray pattern preventing and treating tribute Citrus chachiensis Hort. black rot of embodiment 1-3 is (using conventional preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition：With
80% Mancozeb (complex state) wettable powder 600-800 extraordinarily 59.7% hundred work((includes 13.5% carbendazim, 46.2% miaow
Fresh amine) 1500-2000 times, consumption is consistent with test group), if it is 0 that matched group increases sugared rate, as a result see the table below.
From upper table, the new pharmaceutical composition preventing and treating tribute Citrus chachiensis Hort. black rot of embodiment of the present invention 1-3, can improve yield and
Sugar content, and tribute Citrus chachiensis Hort. is in good taste, appearance color and luster is mellow and full, and quality is high, higher than conventional control tribute Citrus chachiensis Hort. black rot new pharmaceutical composition
Using effect.
Above content it cannot be assumed that the present invention is embodied as being confined to these explanations, for the technical field of the invention
Those of ordinary skill for, under the premise of without departing from present inventive concept, some simple deduction or replace can also be made, all answered
When being considered as belonging to the scope of patent protection that determined by the claims submitted to of the present invention.
Claims (10)
1. it is a kind of preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that in units of weight portion, including following original
Material：Folium paulowniae 104-130 parts, Radix Tripterygii Wilfordii 83-100 parts, Folium Artemisiae Argyi 73-90 parts, Wasabia japonic (Euterma Wasabi) 75-90 parts, Salix babylonica L. leaf 52-80 parts, slips
Fructus Piperiss 46-75 parts, leaf of tea tree 40-65 parts, Herba Anabasis aphyllae 35-60 parts, potassium salt 2-3 parts, microcosmic salt 1-3 parts, nitrogen salt 1-2 parts, calcium
Salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron salt 0.2-0.4 part, molybdenum salt 0.2-0.4 parts, zinc salt 0.2-
0.4 part, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts, vitamin 0.2-0.4 parts, aminoacid 0.2-0.3
Part, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyl gland fat purine 0.06-0.08 parts, naphthalene acetic acid 0.04-
0.06 part, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, N-Methyl pyrrolidone 0.7-2.3 parts, dinonylnaphthalene sulfonic acid sodium
0.6-1.5 parts, Dupont EEA2112AC compatilizer 1-1.6 parts, Lumbricus powder 0.6-1.4 parts, alkyl sulfate potassium 0.5-1.2
Part, trimethylolpropane trimethacrylate 0.5-0.9 parts, 3- aminopropyl triethoxysilane 0.6-1.3 parts, carrageenan 0.5-
1.2 parts, Mancozeb 0.4-0.7 parts, carbendazim 0.3-0.6 parts, Prochloraz 0.5-0.8 parts, wetting and penetrating agent 0.9-1.6 parts,
Synergist 1.5-2.5 parts, ethanol 2000-6000 parts；
The preparation method of the new pharmaceutical composition of the preventing and treating tribute Citrus chachiensis Hort. black rot, comprises the following steps：
S1：By Folium paulowniae, Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, Wasabia japonic (Euterma Wasabi), Salix babylonica L. leaf, piper methysticum, leaf of tea tree, Herba Anabasis aphyllae co-grinding, obtain
To mixture I, mixture I is added in ethanol, is 1 in solid-liquid ratio:14-16, ultrasonic power is 200-300W, and ethanol is dense
Spend for 65%-80%, Extracting temperature is that medicinal liquid 17-23min is extracted at 64-76 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed into 3000-5000 mesh sieve, filtrate is obtained；
S3：By filtrate addition potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese obtained in step S2
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, kinetins, N-
Methyl pyrrolidone, dinonylnaphthalene sulfonic acid sodium, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate potassium, three hydroxyls
Propane tri, 3- aminopropyl triethoxysilanes, carrageenan, Mancozeb, carbendazim, Prochloraz, moistening are oozed
Agent, synergist, are 40-53 DEG C in temperature thoroughly, and rotating speed is stirring and dissolving 18-32min under 100-300r/min, and mixed liquor is obtained；
S4：Mixed liquor obtained in step S3 is concentrated into into water content≤22% in the case where temperature is for 60-80 DEG C, mixture II is obtained；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed, mistake
120-260 mesh sieve, gained powder adopt pulse vacuum pressure steam sterilizer in temperature for 134-136 DEG C, and pressure is 210-
Sterilize under 230KPa 3-4min, and preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition is obtained.
2. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the moistening is oozed
Agent thoroughly is sodium alkyl benzene sulfonate；The synergist in units of weight portion, including following raw material：Wood vinegar 20-40 parts, glycerol
10-18 parts, Portugal's ethamine 8-16 parts, ammonium citrate 6-12 parts, tween 20 5-10 parts, fulvic acid 4-6 parts, laurel alcohol ether phosphate
3-5 parts.
3. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the potassium salt by
Following components is constituted：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6 parts, potassium carbonate 0.3-0.5 parts,
Potassium bicarbonate 0.2-0.5 parts.
4. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the microcosmic salt by
Following components is constituted：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7 parts, zinc phosphate 0.2-0.7 parts.
5. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the nitrogen salt by
Following components is constituted：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3-0.6 parts.
6. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the calcium salt by
Following components is constituted：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1-0.2 parts.
7. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the magnesium salt by
Following components is constituted：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1-0.2 parts.
8. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the iodine salt by
Following components is constituted：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride.
9. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the vitamin
It is composed of the following components：Raw element A 0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin B20.02-0.08 parts, dimension life
Plain C 0.02-0.06 parts.
10. it is according to claim 1 preventing and treating tribute Citrus chachiensis Hort. black rot new pharmaceutical composition, it is characterised in that the amino
Acid is composed of the following components：Glycine 0.08-0.1 parts, isoleucine 0.06-0.08 parts, proline 0.04-0.07 parts, phenylpropyl alcohol
Propylhomoserin 0.02-0.05 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610933365.9A CN106577814A (en) | 2016-10-31 | 2016-10-31 | Novel pharmaceutical composition for controlling black rot of citrus gonggan |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610933365.9A CN106577814A (en) | 2016-10-31 | 2016-10-31 | Novel pharmaceutical composition for controlling black rot of citrus gonggan |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106577814A true CN106577814A (en) | 2017-04-26 |
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| CN201610933365.9A Pending CN106577814A (en) | 2016-10-31 | 2016-10-31 | Novel pharmaceutical composition for controlling black rot of citrus gonggan |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103708887A (en) * | 2013-12-20 | 2014-04-09 | 成都新朝阳作物科学有限公司 | Fruit sweetener and application thereof |
| CN105272741A (en) * | 2015-10-26 | 2016-01-27 | 广西农垦国有立新农场 | Biological organic pesticide-containing fertilizer and preparation method thereof |
| CN105272619A (en) * | 2015-10-30 | 2016-01-27 | 广西金神农生态农业科技开发有限公司 | Foliar fertilizer for hybrid oranges |
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| CN103708887A (en) * | 2013-12-20 | 2014-04-09 | 成都新朝阳作物科学有限公司 | Fruit sweetener and application thereof |
| CN105272741A (en) * | 2015-10-26 | 2016-01-27 | 广西农垦国有立新农场 | Biological organic pesticide-containing fertilizer and preparation method thereof |
| CN105272619A (en) * | 2015-10-30 | 2016-01-27 | 广西金神农生态农业科技开发有限公司 | Foliar fertilizer for hybrid oranges |
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Application publication date: 20170426 |