CN106566664A - 一种高效低泡型羊毛洗涤剂及其制备方法 - Google Patents

一种高效低泡型羊毛洗涤剂及其制备方法 Download PDF

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CN106566664A
CN106566664A CN201610906942.5A CN201610906942A CN106566664A CN 106566664 A CN106566664 A CN 106566664A CN 201610906942 A CN201610906942 A CN 201610906942A CN 106566664 A CN106566664 A CN 106566664A
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范恒功
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Abstract

本发明公开了一种高效低泡型羊毛洗涤剂及其制备方法,涉及养殖业技术领域,由如下重量份数的原料制成:预糊化淀粉15‑20份、微晶纤维素10‑15份、聚氧化乙烯6‑11份、冷溶型聚乙烯醇4‑8份、糯米粉3‑6份、聚乙二醇4000 3‑6份、聚季铵盐2‑4份、茶枯粉2‑4份、吸附助剂2‑4份、聚乙烯醇树脂1‑2份、氢化棕榈油1‑2份、米糠蜡1‑2份、田菁胶0.5‑1份、小苏打粉0.5‑1份、磷酸氢二钠0.5‑1份、水100‑200份。本发明洗涤剂通过润湿、吸附、絮凝以及沉降作用,来对羊毛进行高效清洗,清洗效果好,且无毒无害,增强羊毛白度的同时不影响羊毛的使用安全性;该洗涤剂还具有杀菌效果,能对羊毛进行初步杀菌处理。

Description

一种高效低泡型羊毛洗涤剂及其制备方法
技术领域:
本发明涉及养殖业技术领域,具体涉及一种高效低泡型羊毛洗涤剂及其制备方法。
背景技术:
羊毛,即羊毛原毛,在纺织前需要经过洗毛。洗毛的目的是要洗去羊毛纤维上的羊毛脂、羊汗、沙土和污垢等,而其中关键是对羊毛脂的洗涤,采用的普遍方法是加入含有洗涤剂的洗液,使其渗透到羊毛脂污垢层的缝隙中,降低污垢层和毛纤维的结合力,使污垢层脱离羊毛表面转移到洗液中。常用洗涤剂主要是皂碱和合成洗涤剂,还需利用机械作用对羊毛产生推动和挤压,以提高去污效率。这种方法虽然洗涤效果好,但容易对羊毛造成损伤,从而影响其纺织和保暖效果。
发明内容:
本发明所要解决的技术问题在于提供一种清洗效果好且不会对羊毛造成损伤的高效低泡型羊毛洗涤剂及其制备方法。
本发明所要解决的技术问题采用以下的技术方案来实现:
一种高效低泡型羊毛洗涤剂,由如下重量份数的原料制成:
预糊化淀粉15-20份、微晶纤维素10-15份、聚氧化乙烯6-11份、冷溶型聚乙烯醇4-8份、糯米粉3-6份、聚乙二醇4000 3-6份、聚季铵盐2-4份、茶枯粉2-4份、吸附助剂2-4份、聚乙烯醇树脂1-2份、氢化棕榈油1-2份、米糠蜡1-2份、田菁胶0.5-1份、小苏打粉0.5-1份、磷酸氢二钠0.5-1份、水100-200份。
所述吸附助剂的制备方法为:向10-15份氢化松香甘油酯加入2-3份氯化聚乙烯和1-2份松节油,充分混合后于微波频率2450MHz、功率700W下微波处理3min,静置1h后再次微波处理5min,然后趁热加入3-5份沸石粉和0.2-0.5份二茂铁,并于超声频率40kHz、功率50W下超声处理30min,再加入1-2份聚乙烯醇缩丁醛和0.5-1份茶籽粉,所得混合物置于-5-0℃环境中冷冻5-8h,最后经超微粉碎机制成粉末。
一种高效低泡型羊毛洗涤剂的制备方法,包括如下步骤:
(1)将糯米粉加热至70-80℃保温混合3-5min,再加入微晶纤维素、茶枯粉、米糠蜡和田菁胶,继续加热至100-110℃保温混合10-15min,所得混合物置于-5-0℃环境中冷冻3-5h,然后经超微粉碎机制成粉末,即得粉料I;
(2)向聚氧化乙烯中加入冷溶型聚乙烯醇和聚乙二醇4000,充分混合后于微波频率2450MHz、功率700W下微波处理3-5min,再加入聚乙烯醇树脂和氢化棕榈油,混合均匀后继续微波处理2-3min,即得粉料II;
(3)向水中加入预糊化淀粉和聚季铵盐,混合使其完全溶解,然后加入粉料I和粉料II,并加热至回流状态保温混合15-30min,最后加入吸附助剂、小苏打粉和磷酸氢二钠,充分混合后送入球磨机中,球磨至细度小于50μm。
本发明的有益效果是:本发明以预糊化淀粉为主要原料,辅以微晶纤维素及多种助剂制得羊毛洗涤剂,该洗涤剂属于低泡型,经该洗涤剂清洗后的羊毛只需用水冲洗一次即可进入烘干工序,从而节约用水量;该洗涤剂通过润湿、吸附、絮凝以及沉降作用,来对羊毛进行高效清洗,清洗效果好,且无毒无害,增强羊毛白度的同时不影响羊毛的使用安全性;该洗涤剂还具有杀菌效果,能对羊毛进行初步杀菌处理。
具体实施方式:
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解,下面结合具体实施例,进一步阐述本发明。
实施例1
(1)将3份糯米粉加热至70-80℃保温混合5min,再加入10份微晶纤维素、2份茶枯粉、1份米糠蜡和1份田菁胶,继续加热至100-110℃保温混合15min,所得混合物置于-5-0℃环境中冷冻5h,然后经超微粉碎机制成粉末,即得粉料I;
(2)向8份聚氧化乙烯中加入4份冷溶型聚乙烯醇和3份聚乙二醇4000,充分混合后于微波频率2450MHz、功率700W下微波处理5min,再加入2份聚乙烯醇树脂和1份氢化棕榈油,混合均匀后继续微波处理3min,即得粉料II;
(3)向200份水中加入15份预糊化淀粉和2份聚季铵盐,混合使其完全溶解,然后加入粉料I和粉料II,并加热至回流状态保温混合30min,最后加入4份吸附助剂、0.5份小苏打粉和0.5份磷酸氢二钠,充分混合后送入球磨机中,球磨至细度小于50μm。
吸附助剂的制备:向10份氢化松香甘油酯加入2份氯化聚乙烯和1份松节油,充分混合后于微波频率2450MHz、功率700W下微波处理3min,静置1h后再次微波处理5min,然后趁热加入3份沸石粉和0.2份二茂铁,并于超声频率40kHz、功率50W下超声处理30min,再加入2份聚乙烯醇缩丁醛和0.5份茶籽粉,所得混合物置于-5-0℃环境中冷冻8h,最后经超微粉碎机制成粉末。
实施例2
(1)将3份糯米粉加热至70-80℃保温混合5min,再加入15份微晶纤维素、2份茶枯粉、2份米糠蜡和0.5份田菁胶,继续加热至100-110℃保温混合15min,所得混合物置于-5-0℃环境中冷冻5h,然后经超微粉碎机制成粉末,即得粉料I;
(2)向10份聚氧化乙烯中加入4份冷溶型聚乙烯醇和5份聚乙二醇4000,充分混合后于微波频率2450MHz、功率700W下微波处理5min,再加入1份聚乙烯醇树脂和1份氢化棕榈油,混合均匀后继续微波处理3min,即得粉料II;
(3)向200份水中加入20份预糊化淀粉和2份聚季铵盐,混合使其完全溶解,然后加入粉料I和粉料II,并加热至回流状态保温混合30min,最后加入4份吸附助剂、1份小苏打粉和0.5份磷酸氢二钠,充分混合后送入球磨机中,球磨至细度小于50μm。
吸附助剂的制备:向15份氢化松香甘油酯加入2份氯化聚乙烯和1份松节油,充分混合后于微波频率2450MHz、功率700W下微波处理3min,静置1h后再次微波处理5min,然后趁热加入5份沸石粉和0.2份二茂铁,并于超声频率40kHz、功率50W下超声处理30min,再加入1份聚乙烯醇缩丁醛和0.5份茶籽粉,所得混合物置于-5-0℃环境中冷冻8h,最后经超微粉碎机制成粉末。
实施例3
将实施例1和2所制洗涤剂用于羊毛洗涤,对洗涤后的羊毛进行质量检测,并对比市售WPYM-987羊毛洗涤剂,结果如表1所示。
表1洗涤后羊毛的质量结果
由表1可知,本发明实施例1和2所制洗涤剂对羊毛的清洗效果明显优于市售WPYM-987羊毛洗涤剂,含油脂量、含土杂率和含毡并率较低,白度高,松散性好且无异味。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解,本发明不受上述实施例的限制,上述实施例和说明书中描述的只是说明本发明的原理,在不脱离本发明精神和范围的前提下,本发明还会有各种变化和改进,这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (3)

1.一种高效低泡型羊毛洗涤剂,其特征在于,由如下重量份数的原料制成:预糊化淀粉15-20份、微晶纤维素10-15份、聚氧化乙烯6-11份、冷溶型聚乙烯醇4-8份、糯米粉3-6份、聚乙二醇40003-6份、聚季铵盐2-4份、茶枯粉2-4份、吸附助剂2-4份、聚乙烯醇树脂1-2份、氢化棕榈油1-2份、米糠蜡1-2份、田菁胶0.5-1份、小苏打粉0.5-1份、磷酸氢二钠0.5-1份、水100-200份。
2.一种高效低泡型羊毛洗涤剂的制备方法,其特征在于,包括如下步骤:
(1)将糯米粉加热至70-80℃保温混合3-5min,再加入微晶纤维素、茶枯粉、米糠蜡和田菁胶,继续加热至100-110℃保温混合10-15min,所得混合物置于-5-0℃环境中冷冻3-5h,然后经超微粉碎机制成粉末,即得粉料I;
(2)向聚氧化乙烯中加入冷溶型聚乙烯醇和聚乙二醇4000,充分混合后于微波频率2450MHz、功率700W下微波处理3-5min,再加入聚乙烯醇树脂和氢化棕榈油,混合均匀后继续微波处理2-3min,即得粉料II;
(3)向水中加入预糊化淀粉和聚季铵盐,混合使其完全溶解,然后加入粉料I和粉料II,并加热至回流状态保温混合15-30min,最后加入吸附助剂、小苏打粉和磷酸氢二钠,充分混合后送入球磨机中,球磨至细度小于50μm。
3.根据权利要求1或2所述的高效低泡型羊毛洗涤剂,其特征在于,所述吸附助剂的制备方法为:向10-15份氢化松香甘油酯加入2-3份氯化聚乙烯和1-2份松节油,充分混合后于微波频率2450MHz、功率700W下微波处理3min,静置1h后再次微波处理5min,然后趁热加入3-5份沸石粉和0.2-0.5份二茂铁,并于超声频率40kHz、功率50W下超声处理30min,再加入1-2份聚乙烯醇缩丁醛和0.5-1份茶籽粉,所得混合物置于-5-0℃环境中冷冻5-8h,最后经超微粉碎机制成粉末。
CN201610906942.5A 2016-10-18 2016-10-18 一种高效低泡型羊毛洗涤剂及其制备方法 Pending CN106566664A (zh)

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CN108078273A (zh) * 2018-01-22 2018-05-29 孙旭锋 一种马尾毛弹簧床垫
CN108078273B (zh) * 2018-01-22 2024-04-02 孙旭锋 一种马尾毛弹簧床垫
CN110987734A (zh) * 2019-12-11 2020-04-10 湖南千金湘江药业股份有限公司 一种干法激光粒度分析仪的固体洗料及其清洗方法

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