CN106566188A - Flame-retardant diesel engine accessory material and preparation method thereof - Google Patents
Flame-retardant diesel engine accessory material and preparation method thereof Download PDFInfo
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- CN106566188A CN106566188A CN201610930938.2A CN201610930938A CN106566188A CN 106566188 A CN106566188 A CN 106566188A CN 201610930938 A CN201610930938 A CN 201610930938A CN 106566188 A CN106566188 A CN 106566188A
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- parts
- phenolic resin
- retardant
- diesel engine
- fire
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L61/00—Compositions of condensation polymers of aldehydes or ketones; Compositions of derivatives of such polymers
- C08L61/04—Condensation polymers of aldehydes or ketones with phenols only
- C08L61/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention discloses a flame-retardant diesel engine accessory material and a preparation method thereof. Phenol-formaldehyde resin, phenolic resin, aluminium oxide, chrysotile, copper powder, hexamethylenetetramine, antimonous oxide, zinc borate, dibutyl tin dialurate, silicone oil, trietyl tetramine, stainless metal powder, dicumyl peroxide and fluoro trichloromethane are weighed. oxygen index is 40-44%, shore hardness is 55-75A, and notch impact strength is 40-60 kJ/m<3>; permanent compression set is 25-45%, and tensile strength is 120-160 MPa; the material is resistant to high temperature of 600-700 DEG C with no fusion drop, bending strength is 60-80 MPa, and elongation at break is 300-700%; tear strength is 500-900 N/m, impact resilience is 45-65%, abrasion loss is 0.3-0.5 micron/time, and flexural modulus is 1.05-1.45 GPa.
Description
Technical field
The present invention relates to diesel engine Material Field, more particularly to a kind of fire-retardant diesel engine part materials and preparation method thereof.
Background technology
Common rail injection formula oil supply system is by high-pressure oil pump, common feeder line, fuel injector, ECU(ECU)With some pipes
Road pressure transducer composition, each fuel injector in system is connected by respective high-pressure oil pipe with common feeder line, public
Fuel feed pump plays the effect of fluid power pressure accumulation to fuel injector.During work, high-pressure oil pump delivers fuel into common feeder line with high pressure, high
Pressure oil pump, pressure transducer and ECU composition Closed loop operation, to the oil pressure in common feeder line precise control is realized, is thoroughly changed
The phenomenon that charge oil pressure changes with engine speed.
When diesel engine works, internal toggle is directly contacted with high temperature and high pressure gas, and the rotary speed of bent axle is again
Very high, the linear velocity of reciprocating motion of the pistons is quite big, while contacting with combustion mixture and burning waste gas, toggle is also
Acted on by chemical attack, and lubricating difficulties.It can be seen that, the working condition of toggle is quite severe, and it will bear height
Temperature, high pressure, high speed and chemical attack effect.
Toggle is that diesel engine realizes cycle of operation, complete energy conversion drive mechanism, for transmit power and
Change motion mode.In work, toggle is transformed into the rotation of bent axle in expansion space stroke the reciprocating motion of piston
Motion, externally exports power, and in other three strokes, i.e., again the rotary motion of bent axle in air inlet, compression, instroke
It is transformed into the linear reciprocating motion of piston.Generally speaking toggle is electromotor so as to producing and transmits the machine of power
Structure.The thermal energy sent after it is fuel combustion is mechanical energy.
It is dilute via piston ring incorporation machine oil because Diesel engine engine control is increased using the situation of multiple rear injections
The fuel quantity for releasing machine oil is continuously increased, and is so easily reduced the lubricity and viscosity of machine oil.In addition, coal smoke passes through EGR(Aerofluxuss
Recirculation)Being mixed into the amount of machine oil increases, and causes the reduction of additive effect, engine oil viscosity to raise.Due to only determining viscosity, easily receive
The impact of the two contrary factors, it is difficult to accurately grasp the deterioration degree of machine oil.
Gasoline automobile has rotating speed high(Automobile gasoline machine rotating speed may be up to 5000-6000 revs/min, goods motor petrol
Machine is up to 4000 revs/min or so)Noise is little when light weight, work, start easy, manufacture and the low feature of maintenance cost, therefore in sedan-chair
It is used widely on car and medium and small lorry and military offroad vehicle.Its weak point is that fuel consumption is higher, thus fuel oil Jing
Ji property is poor.Diesel engine automobile is high because of compression ratio, and fuel consumption average specific gasoline automobile is low by 30% or so, so fuel-economy
Property is preferable.1.7 liters of diesel-powered cars can save 2 liters of oil than 1.6 liters of spark ignition passenger car per 100 kms.General lorry mostly adopts diesel oil
Machine.The weakness of diesel engine is that rotating speed is low compared with gasoline engine(Typically up to rotating speed is at 2500-3000 revs/min or so), quality is big, system
Make high with maintenance cost(Because injection pump and fuel injector requirement on machining accuracy are high).Its range of application is in, light-duty goods
Car extends.External diesel-powered car also has development quickly, and its maximum speed is up to 5000 revs/min.With social city, science and technology
Change, the development of hommization, design high a kind of high impact strength, tensile strength height, elongation at break, hardness height and bending strength high
Fire-retardant diesel engine part materials and preparation method thereof, to meet the market demand, be very important.
The content of the invention
The technical problem of solution:
The application is for existing fire-retardant diesel engine part materials tensile strength is low, impact strength is low, elongation at break is low and bending
A kind of low technical problem of low intensity, there is provided fire-retardant diesel engine part materials and preparation method thereof.
Technical scheme:
A kind of fire-retardant diesel engine part materials, raw materials by weight portion proportioning is as follows:100 parts of phenolic resin, phenolic resin 30-50
Part, aluminium oxide 0.5-4.5 parts, chrysotile 4-8 parts, copper powder 20-40 parts, hexamethylenetetramine 12-18 parts, antimony oxide 5-25
Part, Firebrake ZB 2-6 parts, dibutyl tin laurate 0.5-4.5 parts, silicone oil 3-7 parts, trientine 0.6-1 parts, stainless steel metal
Powder 25-65 parts, cumyl peroxide 0.5-2.5 parts, fluoro trichloromethane is 10-30 parts.
As a preferred technical solution of the present invention:The raw materials by weight portion of the fire-retardant diesel engine part materials is matched somebody with somebody
Than as follows:100 parts of phenolic resin, phenolic resin 35-45 parts, aluminium oxide 1.5-3.5 parts, chrysotile 5-7 parts, copper powder 25-35 parts,
Hexamethylenetetramine 13-17 parts, antimony oxide 10-20 parts, Firebrake ZB 3-5 parts, dibutyl tin laurate 1.5-3.5 parts, silicon
Oily 4-6 parts, trientine 0.7-0.9 parts, stainless steel metal powder 35-55 parts, cumyl peroxide 1-2 parts, a fluorine trichlorine
Methane is 15-25 parts.
As a preferred technical solution of the present invention:The raw materials by weight portion of the fire-retardant diesel engine part materials is matched somebody with somebody
Than as follows:100 parts of phenolic resin, 35 parts of phenolic resin, 1.5 parts of aluminium oxide, 5 parts of chrysotile, 25 parts of copper powder, hexamethylenetetramine
13 parts, 10 parts of antimony oxide, 3 parts of Firebrake ZB, 1.5 parts of dibutyl tin laurate, 4 parts of silicone oil, 0.7 part of trientine, no
35 parts of rust steel metal powder, 1 part of cumyl peroxide, fluoro trichloromethane is 15 parts.
As a preferred technical solution of the present invention:The raw materials by weight portion of the fire-retardant diesel engine part materials is matched somebody with somebody
Than as follows:100 parts of phenolic resin, 45 parts of phenolic resin, 3.5 parts of aluminium oxide, 7 parts of chrysotile, 35 parts of copper powder, hexamethylenetetramine
17 parts, 20 parts of antimony oxide, 5 parts of Firebrake ZB, 3.5 parts of dibutyl tin laurate, 6 parts of silicone oil, 0.9 part of trientine, no
55 parts of rust steel metal powder, 2 parts of cumyl peroxide, fluoro trichloromethane is 25 parts.
As a preferred technical solution of the present invention:The raw materials by weight portion of the fire-retardant diesel engine part materials is matched somebody with somebody
Than as follows:100 parts of phenolic resin, 40 parts of phenolic resin, 2.5 parts of aluminium oxide, 6 parts of chrysotile, 30 parts of copper powder, hexamethylenetetramine
15 parts, 15 parts of antimony oxide, 4 parts of Firebrake ZB, 2.5 parts of dibutyl tin laurate, 5 parts of silicone oil, 0.8 part of trientine, no
45 parts of rust steel metal powder, 1.5 parts of cumyl peroxide, fluoro trichloromethane is 20 parts.
As a preferred technical solution of the present invention:The preparation method step of the fire-retardant diesel engine part materials is:
The first step:Weigh phenolic resin, phenolic resin, aluminium oxide, chrysotile, copper powder, hexamethylenetetramine, antimony oxide,
Firebrake ZB, dibutyl tin laurate, silicone oil, trientine, stainless steel metal powder, cumyl peroxide and the chloromethane of a fluorine three
Alkane;
Second step:Phenolic resin, phenolic resin, stainless steel metal powder and cumyl peroxide input is provided with into agitator and temperature
In the reactor of degree meter, 80-100 DEG C is warming up to, stirs 10-30min, mixing speed is 3000-5000 rev/min;
3rd step:Surplus stock is added, in input kneader, 20-40min, twin-screw extrusion barrel is mediated at 100-120 DEG C
Temperature 145-155 DEG C, 150-160 DEG C, 155-165 DEG C, 165-175 DEG C, 170-180 DEG C, 180-190 DEG C of head temperature.
Beneficial effect:
A kind of fire-retardant diesel engine part materials of the present invention and preparation method thereof are using above technical scheme and prior art phase
Than with following technique effect:1st, oxygen index (OI) 40-44%, shore hardness 55-75A, notch impact strength 40-60kJ/m3;2nd, press
Compression permanent deformation 25-45%, tensile strength 120-160MPa;3rd, resistance to 600-700 DEG C of high temperature, without melting drippage, bending strength 60-
80MPa, elongation at break 300-700%;4th, tearing strength 500-900N/m, bounce impact elasticity 45-65%, wear extent is 0.3-
0.5 μm/secondary, bending moduluses 1.05-1.45GPa, mechanical property is good, can extensively produce and constantly replace current material.
Specific embodiment
Embodiment 1:
By weight proportioning weighs 100 parts of phenolic resin, 30 parts of phenolic resin, 0.5 part of aluminium oxide, 4 parts of chrysotile, copper powder 20
Part, 12 parts of hexamethylenetetramine, 5 parts of antimony oxide, 2 parts of Firebrake ZB, 0.5 part of dibutyl tin laurate, 3 parts of silicone oil, three second
0.6 part of urotropine, 25 parts of stainless steel metal powder, 0.5 part of cumyl peroxide, fluoro trichloromethane is 10 parts.
Phenolic resin, phenolic resin, stainless steel metal powder and cumyl peroxide input is provided with into agitator and temperature
In the reactor of meter, 80 DEG C are warming up to, stir 10min, mixing speed is 3000-5000 rev/min.
Surplus stock is added, in input kneader, 20min is mediated at 100 DEG C, 145 DEG C of twin-screw extrusion barrel temperature,
150 DEG C, 155 DEG C, 165 DEG C, 170 DEG C, 180 DEG C of head temperature.
Oxygen index (OI) 40%, shore hardness 55A, notch impact strength 40kJ/m3;Compression set 45%, tensile strength
120MPa;Resistance to 600 DEG C of high temperature, without melting drippage, bending strength 60MPa, elongation at break 300%;Tearing strength 500N/m, punching
Resilience 45% is hit, wear extent is 0.5 μm/secondary, bending moduluses 1.05GPa, and mechanical property is good, can extensively produce the not division of history into periods
For current material.
Embodiment 2:
By weight proportioning weighs 100 parts of phenolic resin, 50 parts of phenolic resin, 4.5 parts of aluminium oxide, 8 parts of chrysotile, copper powder 40
Part, 18 parts of hexamethylenetetramine, 25 parts of antimony oxide, 6 parts of Firebrake ZB, 4.5 parts of dibutyl tin laurate, 7 parts of silicone oil, three second
1 part of urotropine, 65 parts of stainless steel metal powder, 2.5 parts of cumyl peroxide, fluoro trichloromethane is 30 parts.
Phenolic resin, phenolic resin, stainless steel metal powder and cumyl peroxide input is provided with into agitator and temperature
In the reactor of meter, 100 DEG C are warming up to, stir 30min, mixing speed is 5000 revs/min.
Surplus stock is added, in input kneader, 40min is mediated at 120 DEG C, 155 DEG C of twin-screw extrusion barrel temperature,
160 DEG C, 165 DEG C, 175 DEG C, 180 DEG C, 190 DEG C of head temperature.
Oxygen index (OI) 41%, shore hardness 60A, notch impact strength 45kJ/m3;Compression set 40%, tensile strength
130MPa;Resistance to 630 DEG C of high temperature, without melting drippage, bending strength 65MPa, elongation at break 400%;Tearing strength 600N/m, punching
Resilience 50% is hit, wear extent is 0.45 μm/secondary, bending moduluses 1.15GPa, and mechanical property is good, can extensively produce the not division of history into periods
For current material.
Embodiment 3:
By weight proportioning weighs 100 parts of phenolic resin, 35 parts of phenolic resin, 1.5 parts of aluminium oxide, 5 parts of chrysotile, copper powder 25
Part, 13 parts of hexamethylenetetramine, 10 parts of antimony oxide, 3 parts of Firebrake ZB, 1.5 parts of dibutyl tin laurate, 4 parts of silicone oil, three second
0.7 part of urotropine, 35 parts of stainless steel metal powder, 1 part of cumyl peroxide, fluoro trichloromethane is 15 parts.
Phenolic resin, phenolic resin, stainless steel metal powder and cumyl peroxide input is provided with into agitator and temperature
In the reactor of meter, 80 DEG C are warming up to, stir 10min, mixing speed is 3000 revs/min.
Surplus stock is added, in input kneader, 20min is mediated at 100 DEG C, 145 DEG C of twin-screw extrusion barrel temperature,
150 DEG C, 155 DEG C, 165 DEG C, 170 DEG C, 180 DEG C of head temperature.
Oxygen index (OI) 42%, shore hardness 65A, notch impact strength 50kJ/m3;Compression set 35%, tensile strength
140MPa;Resistance to 650 DEG C of high temperature, without melting drippage, bending strength 70MPa, elongation at break 500%;Tearing strength 700N/m, punching
Resilience 55% is hit, wear extent is 0.4 μm/secondary, bending moduluses 1.25GPa, and mechanical property is good, can extensively produce the not division of history into periods
For current material.
Embodiment 4:
By weight proportioning weighs 100 parts of phenolic resin, 45 parts of phenolic resin, 3.5 parts of aluminium oxide, 7 parts of chrysotile, copper powder 35
Part, 17 parts of hexamethylenetetramine, 20 parts of antimony oxide, 5 parts of Firebrake ZB, 3.5 parts of dibutyl tin laurate, 6 parts of silicone oil, three second
0.9 part of urotropine, 55 parts of stainless steel metal powder, 2 parts of cumyl peroxide, fluoro trichloromethane is 25 parts.
Phenolic resin, phenolic resin, stainless steel metal powder and cumyl peroxide input is provided with into agitator and temperature
In the reactor of meter, 100 DEG C are warming up to, stir 30min, mixing speed is 5000 revs/min.
Surplus stock is added, in input kneader, 40min is mediated at 120 DEG C, 155 DEG C of twin-screw extrusion barrel temperature,
160 DEG C, 165 DEG C, 175 DEG C, 180 DEG C, 190 DEG C of head temperature.
Oxygen index (OI) 43%, shore hardness 70A, notch impact strength 55kJ/m3;Compression set 30%, tensile strength
150MPa;Resistance to 670 DEG C of high temperature, without melting drippage, bending strength 75MPa, elongation at break 600%;Tearing strength 800N/m, punching
Resilience 60% is hit, wear extent is 0.35 μm/secondary, bending moduluses 1.35GPa, and mechanical property is good, can extensively produce the not division of history into periods
For current material.
Embodiment 5:
By weight proportioning weighs 100 parts of phenolic resin, 40 parts of phenolic resin, 2.5 parts of aluminium oxide, 6 parts of chrysotile, copper powder 30
Part, 15 parts of hexamethylenetetramine, 15 parts of antimony oxide, 4 parts of Firebrake ZB, 2.5 parts of dibutyl tin laurate, 5 parts of silicone oil, three second
0.8 part of urotropine, 45 parts of stainless steel metal powder, 1.5 parts of cumyl peroxide, fluoro trichloromethane is 20 parts.
Phenolic resin, phenolic resin, stainless steel metal powder and cumyl peroxide input is provided with into agitator and temperature
In the reactor of meter, 90 DEG C are warming up to, stir 20min, mixing speed is 4000 revs/min.
Surplus stock is added, in input kneader, 30min is mediated at 110 DEG C, 150 DEG C of twin-screw extrusion barrel temperature,
155 DEG C, 160 DEG C, 170 DEG C, 175 DEG C, 185 DEG C of head temperature.
Oxygen index (OI) 44%, shore hardness 75A, notch impact strength 60kJ/m3;Compression set 25%, tensile strength
160MPa;Resistance to 700 DEG C of high temperature, without melting drippage, bending strength 80MPa, elongation at break 700%;Tearing strength 900N/m, punching
Resilience 65% is hit, wear extent is 0.3 μm/secondary, bending moduluses 1.45GPa, and mechanical property is good, can extensively produce the not division of history into periods
For current material.
All components in above example can be with commercially available.
Above-described embodiment is only intended to be illustrated present disclosure, rather than limits, therefore with the present invention's
Any change in claims suitable implication and scope, is all considered as being included within the scope of the claims.
Claims (6)
1. a kind of fire-retardant diesel engine part materials, it is characterised in that the raw material of the fire-retardant diesel engine part materials is by weight
Number proportioning is as follows:100 parts of phenolic resin, phenolic resin 30-50 parts, aluminium oxide 0.5-4.5 parts, chrysotile 4-8 parts, copper powder 20-
40 parts, hexamethylenetetramine 12-18 parts, antimony oxide 5-25 parts, Firebrake ZB 2-6 parts, dibutyl tin laurate 0.5-4.5
Part, silicone oil 3-7 parts, trientine 0.6-1 parts, stainless steel metal powder 25-65 parts, cumyl peroxide 0.5-2.5 parts, one
Fluoro trichloromethane is 10-30 parts.
2. a kind of fire-retardant diesel engine part materials according to claim 1, it is characterised in that the fire-retardant diesel engine part
The raw materials by weight portion proportioning of materials is as follows:100 parts of phenolic resin, phenolic resin 35-45 parts, aluminium oxide 1.5-3.5 parts, temperature
Asbestos 5-7 parts, copper powder 25-35 parts, hexamethylenetetramine 13-17 parts, antimony oxide 10-20 parts, Firebrake ZB 3-5 parts, Laurel
Sour dibutyl tin 1.5-3.5 parts, silicone oil 4-6 parts, trientine 0.7-0.9 parts, stainless steel metal powder 35-55 parts, peroxidating
Diisopropylbenzene (DIPB) 1-2 parts, fluoro trichloromethane is 15-25 parts.
3. a kind of fire-retardant diesel engine part materials according to claim 1, it is characterised in that the fire-retardant diesel engine part
The raw materials by weight portion proportioning of materials is as follows:100 parts of phenolic resin, 35 parts of phenolic resin, 1.5 parts of aluminium oxide, chrysotile 5
Part, 25 parts of copper powder, 13 parts of hexamethylenetetramine, 10 parts of antimony oxide, 3 parts of Firebrake ZB, 1.5 parts of dibutyl tin laurate, silicon
4 parts of oil, 0.7 part of trientine, 35 parts of stainless steel metal powder, 1 part of cumyl peroxide, fluoro trichloromethane is 15 parts.
4. a kind of fire-retardant diesel engine part materials according to claim 1, it is characterised in that:The fire-retardant diesel engine part
The raw materials by weight portion proportioning of materials is as follows:100 parts of phenolic resin, 45 parts of phenolic resin, 3.5 parts of aluminium oxide, chrysotile 7
Part, 35 parts of copper powder, 17 parts of hexamethylenetetramine, 20 parts of antimony oxide, 5 parts of Firebrake ZB, 3.5 parts of dibutyl tin laurate, silicon
6 parts of oil, 0.9 part of trientine, 55 parts of stainless steel metal powder, 2 parts of cumyl peroxide, fluoro trichloromethane is 25 parts.
5. a kind of fire-retardant diesel engine part materials according to claim 1, it is characterised in that:The fire-retardant diesel engine part
The raw materials by weight portion proportioning of materials is as follows:100 parts of phenolic resin, 40 parts of phenolic resin, 2.5 parts of aluminium oxide, chrysotile 6
Part, 30 parts of copper powder, 15 parts of hexamethylenetetramine, 15 parts of antimony oxide, 4 parts of Firebrake ZB, 2.5 parts of dibutyl tin laurate, silicon
5 parts of oil, 0.8 part of trientine, 45 parts of stainless steel metal powder, 1.5 parts of cumyl peroxide, fluoro trichloromethane is 20
Part.
6. the preparation method of fire-retardant diesel engine part materials described in a kind of claim 1, it is characterised in that comprise the steps:
The first step:Weigh phenolic resin, phenolic resin, aluminium oxide, chrysotile, copper powder, hexamethylenetetramine, antimony oxide,
Firebrake ZB, dibutyl tin laurate, silicone oil, trientine, stainless steel metal powder, cumyl peroxide and the chloromethane of a fluorine three
Alkane;
Second step:Phenolic resin, phenolic resin, stainless steel metal powder and cumyl peroxide input is provided with into agitator and temperature
In the reactor of degree meter, 80-100 DEG C is warming up to, stirs 10-30min, mixing speed is 3000-5000 rev/min;
3rd step:Surplus stock is added, in input kneader, 20-40min, twin-screw extrusion barrel is mediated at 100-120 DEG C
Temperature 145-155 DEG C, 150-160 DEG C, 155-165 DEG C, 165-175 DEG C, 170-180 DEG C, 180-190 DEG C of head temperature.
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