CN106525751A - Polluted soil sampling detection device - Google Patents

Polluted soil sampling detection device Download PDF

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Publication number
CN106525751A
CN106525751A CN201611221506.0A CN201611221506A CN106525751A CN 106525751 A CN106525751 A CN 106525751A CN 201611221506 A CN201611221506 A CN 201611221506A CN 106525751 A CN106525751 A CN 106525751A
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China
Prior art keywords
chamber
detection device
soil sampling
sampling detection
feed pipe
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Withdrawn
Application number
CN201611221506.0A
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Chinese (zh)
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不公告发明人
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Zhengzhou Information Technology Co Ltd
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Zhengzhou Information Technology Co Ltd
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Priority to CN201611221506.0A priority Critical patent/CN106525751A/en
Publication of CN106525751A publication Critical patent/CN106525751A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/33Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using ultraviolet light
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/75Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
    • G01N21/77Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/12Preparation by evaporation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/12Preparation by evaporation
    • G01N2030/126Preparation by evaporation evaporating sample

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plasma & Fusion (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a polluted soil sampling detection device. The device comprises a box, partition plates, electric heaters, metal probes, crushers, gas chromatographs, gas collection tanks, cameras, rotating shafts, impellers, a nitrogen container, color developing agent adding tubes and ultraviolet spectrophotometers; the box is internally provided with the partition plates which divide the box into multiple sealed cavities, a feed pipe is arranged at the top end of each cavity, the crushers are arranged at the inlet ends of the feed pipes, the box is internally provided with the rotating shafts, the impellers are installed on the rotating shafts, the top end of the cavity is communicated with the nitrogen container through a nitrogen conveying pipe, the metal probes are arranged inside the cavities, heat transfer plates are arranged inside the cavities, the electric heaters are arranged on the lower portions of the heat transfer plates, a timer is installed on the side wall of the box, the gas connection tanks are communicated with gas delivery pipes, the gas chromatographs are installed on the gas collection tanks, and the cavities are internally provided with the ultraviolet spectrophotometers. According to the polluted soil sampling detection device, the accuracy of the detection result is guaranteed, the contingency of testing is avoided, detection on multiple aspects is convenient, the structure is simple, use is convenient, and popularization is promoted.

Description

A kind of contaminated soil sampling Detection device
Technical field
The present invention relates to a kind of environmental protection equipment, specifically a kind of contaminated soil sampling Detection device.
Background technology
Soil pollution reparation is important in environmental protection one, and soil pollution can cause serious direct economic loss agriculture The pollution of crop, the underproduction.The soil pollution soil pollution that is detrimental to health can be such that pollutant accumulates in plant, and by food Thing chain is enriched in human body and animal body, endangers human and livestock health, cause cancer and other diseases etc..Soil pollution causes other rings After border problem soil is contaminated, easily enter in the presence of wind-force and waterpower respectively containing the higher contaminated surface soil of heavy metal concentration Enter in air and water body, cause other secondary lifes such as atmosphere pollution, surface water pollution, underground water pollution and ecosystem degradation State environmental problem.In soil pollution, an important part is organic contamination, organic pollution mainly include machine agricultural chemicals, phenols, Cyanide, oil, synthetic detergent, many BaPs and the harmful microorganism that brought by municipal sewage, sludge and barnyard manure etc..When Contain hazardous substance in soil excessive, more than the self-purification capacity of soil, composition of the soil, 26S Proteasome Structure and Function will be caused to occur to become Change, microbial activities is suppressed, gradually accumulation passes through " soil-plant-people in soil for harmful substance or its catabolite Body ", or be absorbed by the body by " soil-water-human body " indirectly, reach the degree being detrimental to health.Existing soil has Machine thing pollutant typically has volatile-type, such as agricultural chemicals, trichloroacetaldehyde, polycyclic aromatic hydrocarbon, oil, methane, different organic contaminations Need to take different soil pollution repairing and treating schemes, the most of testing results of testing equipment in the market are inaccurate, Testing result is single, it is difficult to play a role.
The content of the invention
It is an object of the invention to provide a kind of contaminated soil sampling Detection device, to solve to propose in above-mentioned background technology Problem.
For achieving the above object, the present invention provides following technical scheme:
A kind of contaminated soil sampling Detection device, including casing, dividing plate, electric heater, heat-conducting plate, metal probe, crushing Machine, feed pipe, gas chromatograph, plenum chamber, camera, rotating shaft, controller, variable frequency power source, impeller, nitrogen pot, developer add Plus manage and ultraviolet specrophotometer, described tank floor is provided with guide wheel, dividing plate is provided with casing, and casing is separated into many by dividing plate The chamber of individual sealing, chamber top are provided with feed pipe, and the feed pipe port of export is provided with threaded cap, and weighing device is installed on feed pipe, Feed pipe arrival end is provided with pulverizer, and rotating shaft is provided with casing, installs impeller in rotating shaft, chamber top by nitrogen transfer tube with Nitrogen pot is connected, and gas flowmeter is installed on nitrogen transfer tube, and within the chamber is provided with metal probe, and chamber interior is provided with heat-conducting plate, Electric heater is provided with below heat-conducting plate, heat-conducting plate lower surface is provided with temperature sensor, and wall box installs timer, and plenum chamber leads to Appendix and chamber are crossed, appendix is provided with control valve, gas chromatograph is installed on plenum chamber, chamber top top is provided with Developer adding tube, within the chamber are provided with ultraviolet specrophotometer, and developer adding tube is provided with scale, and chamber inner wall is provided with shooting Head, controller on wall box, casing are provided with variable frequency power source.
As further scheme of the invention:Described guide wheel is provided with parking brake.
As further scheme of the invention:Described rotating shaft top is connected with external motor.
As further scheme of the invention:Described metal probe be humidity sensor, metal probe appearance coating Once chlorination lithium coating.
As further scheme of the invention:Described heat-conducting plate is arranged in a mutually vertical manner with dividing plate.
As further scheme of the invention:Described camera is connected with external display device.
As further scheme of the invention:Described variable frequency power source is by being connected with electric heater by wire.
As further scheme of the invention:Microprocessor is provided with described controller, temperature sensor, metal are visited Head, camera are electrically connected with the microprocessor input in controller, and electric heater is by the microprocessor in wire and controller Device output end connects.
Compared with prior art, the invention has the beneficial effects as follows:The chamber of the multiple sealings of the present invention is measured together, it is ensured that knot The accuracy of fruit, it is to avoid the contingency of test, contaminated soil are entered from feed pipe, by pulverizer by soil breaking, are conveniently entered The operation of row next step, is stirred to soil in the dynamic lower rotary shaft of outside motor belt motor and impeller, and the carrying out of convenient detection, detection are opened Oxygen is discharged full of nitrogen within the chamber by nitrogen pot before beginning, it is to avoid the imflammable gas in soil is lighted at high temperature, Metal probe appearance coats once lithium chloride coating, and vapor conduction can be absorbed from ambient gas, and humidity is higher, lithium chloride Water absorption rate is better, and metal probe resistance is less, can pass through the humidity in its Characteristics Detection soil, then be supplied by variable frequency power source The different frequency band heating of electric heater, temperature sensor measures heating-up temperature at any time, agricultural chemicals, trichloroacetaldehyde in soil, many The pollutants such as PAH, oil, methane evaporate into gas in case of heating, are transferred in plenum chamber by appendix, lead to Cross gas chromatograph to be analyzed mixed gas plus survey, from the species and content for determining organic pollution, added by developer Plus pipe adds suitable developer, the heavy metal in soil is detected by ultraviolet specrophotometer, simple structure, use It is convenient, beneficial to popularization.
Description of the drawings
Structural representations of the Fig. 1 for contaminated soil sampling Detection device.
In figure:1st, guide wheel, 2, casing, 3, dividing plate, 4, electric heater, 5, temperature sensor, 6, heat-conducting plate, 7, timer, 8th, metal probe, 9, pulverizer, 10, feed pipe, 11, weighing device, 12, threaded cap, 13, gas chromatograph, 14, plenum chamber, 15th, appendix, 16, camera, 17, rotating shaft, 18, controller, 19, variable frequency power source, 20, impeller, 21, nitrogen pot, 22, gas stream Gauge, 23, nitrogen transfer tube, 24, developer adding tube, 25, ultraviolet specrophotometer.
Specific embodiment
The technical scheme of this patent is described in more detail with reference to specific embodiment.
Refer to Fig. 1, a kind of contaminated soil sampling Detection device, including casing 2, dividing plate 3, electric heater 4, heat-conducting plate 6, Metal probe 8, pulverizer 9, feed pipe 10, gas chromatograph 13, plenum chamber 14, camera 16, rotating shaft 17, controller 18, tune Frequency power 19, impeller 20, nitrogen pot 21, developer adding tube 24 and ultraviolet specrophotometer 25, described 2 bottom surface of casing are provided with Guide wheel 1, guide wheel 1 are provided with parking brake, are provided with dividing plate 3 in casing 2, and casing 2 is separated into dividing plate 3 chamber of multiple sealings, multiple The chamber of sealing is measured together, it is ensured that the accuracy of result, it is to avoid the contingency of test, chamber top are provided with feed pipe 10, enter 10 port of export of expects pipe is provided with threaded cap 12, and weighing device 11 is installed on feed pipe 10, and 10 arrival end of feed pipe is provided with pulverizer 9, Contaminated soil is entered from feed pipe 10, by pulverizer by soil breaking, is conveniently carried out the operation of next step, is provided with casing 2 Rotating shaft 17, installs impeller 20 in rotating shaft 17,17 top of rotating shaft is connected with external motor, in the dynamic lower rotary shaft 17 of outside motor belt motor and leaf 20 pairs of soil of wheel are stirred, and the carrying out of convenient detection, chamber top are connected with nitrogen pot 21 by nitrogen transfer tube 23, nitrogen Gas flowmeter 22 is installed on transfer tube 23, detection discharges oxygen full of nitrogen within the chamber by nitrogen pot 21 before starting, The imflammable gas in soil is avoided to light at high temperature, within the chamber is provided with metal probe 8, metal probe 8 is humidity sensor, 8 appearance of metal probe coats once lithium chloride coating, and vapor conduction can be absorbed from ambient gas, and humidity is higher, chlorination Lithium water absorption rate is better, and 8 resistance of metal probe is less, can pass through the humidity in its Characteristics Detection soil, and chamber interior is provided with to be led Hot plate 6, heat-conducting plate 6 are arranged in a mutually vertical manner with dividing plate 3, and electric heater 4 is provided with below heat-conducting plate 6, and 6 lower surface of heat-conducting plate is provided with temperature Degree sensor 5,2 side wall of casing install timer 7, and plenum chamber 14 passes through appendix 15 and chamber, and appendix 15 is provided with Control valve, is installed gas chromatograph 13, then is added by the different frequency band of the supply electric heater 4 of variable frequency power source 19 on plenum chamber 14 Heat, temperature sensor 5 measure heating-up temperature at any time, the pollution such as agricultural chemicals, trichloroacetaldehyde, polycyclic aromatic hydrocarbon, oil, methane in soil Thing evaporates into gas in case of heating, is transferred in plenum chamber 14 by appendix 15, and by gas chromatograph, 13 pairs are mixed Close gas to be analyzed plus survey, from the species and content for determining organic pollution, chamber top top is provided with developer adding tube 24, within the chamber is provided with ultraviolet specrophotometer 25, and developer adding tube 24 is provided with scale, is added by developer adding tube 24 To the heavy metal in soil, suitable developer, detects that chamber inner wall is provided with camera by ultraviolet specrophotometer 25 16, camera 16 is connected with external display device, controller 18 on 2 side wall of casing, is provided with microprocessor, casing in controller 18 2 are provided with variable frequency power source 19, variable frequency power source 19 by being connected with electric heater 4 by wire, temperature sensor 5, metal probe 8th, camera 16 is electrically connected with the microprocessor input in controller 18, and electric heater 4 is by wire and controller 18 Output end of microprocessor connects.
The present invention operation principle be:The chamber of the multiple sealings of the present invention is measured together, it is ensured that the accuracy of result, it is to avoid The contingency of test, contaminated soil are entered from feed pipe, by pulverizer by soil breaking, conveniently carry out the operation of next step, Soil is stirred in the dynamic lower rotary shaft of outside motor belt motor and impeller, the carrying out of convenient detection, detection start before by nitrogen Tank discharges oxygen full of nitrogen within the chamber, it is to avoid the imflammable gas in soil is lighted at high temperature, and metal probe appearance is applied A chlorination lithium coating is covered with, vapor conduction can be absorbed from ambient gas, humidity is higher, and lithium chloride water absorption rate is better, gold Category probe resistance is less, can pass through the humidity in its Characteristics Detection soil, then supply electric heater difference by variable frequency power source Frequency band heating, temperature sensor measures heating-up temperature at any time, agricultural chemicals, trichloroacetaldehyde, polycyclic aromatic hydrocarbon, oil in soil, The pollutants such as methane evaporate into gas in case of heating, are transferred in plenum chamber by appendix, by gas chromatograph Mixed gas are analyzed plus are surveyed, it is from the species and content for determining organic pollution, suitable by the addition of developer adding tube Developer, the heavy metal in soil is detected by ultraviolet specrophotometer.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment party Formula, in the ken that one skilled in the relevant art possesses, can be with the premise of without departing from this patent objective Make a variety of changes.

Claims (6)

1. a kind of contaminated soil sampling Detection device, including casing, dividing plate, electric heater, heat-conducting plate, metal probe, pulverizer, Feed pipe, gas chromatograph, plenum chamber, camera, rotating shaft, controller, variable frequency power source, impeller, nitrogen pot, developer adding tube And ultraviolet specrophotometer, it is characterised in that described tank floor is provided with guide wheel, is provided with dividing plate in casing, and dividing plate is by casing The chamber of multiple sealings is separated into, chamber top is provided with feed pipe, and the feed pipe port of export is provided with threaded cap, installs on feed pipe and claim Refitting is put, and feed pipe arrival end is provided with pulverizer, and rotating shaft is provided with casing, and impeller is installed in rotating shaft, and chamber top passes through nitrogen Transfer tube is connected with nitrogen pot, and gas flowmeter is installed on nitrogen transfer tube, and within the chamber is provided with metal probe, and chamber interior is provided with Heat-conducting plate, is provided with electric heater below heat-conducting plate, heat-conducting plate lower surface is provided with temperature sensor, and wall box installs timer, Plenum chamber passes through appendix and chamber, and appendix is provided with control valve, gas chromatograph, chamber top are installed on plenum chamber Top is provided with developer adding tube, and within the chamber is provided with ultraviolet specrophotometer, and developer adding tube is provided with scale, chamber inner wall Camera is provided with, controller on wall box, casing are provided with variable frequency power source, in described controller, is provided with microprocessor, temperature Degree sensor, metal probe, camera are electrically connected with the microprocessor input in controller, and electric heater is by wire and control Output end of microprocessor connection in device processed, described variable frequency power source is by being connected with electric heater by wire.
2. contaminated soil sampling Detection device according to claim 1, it is characterised in that described guide wheel is provided with hand Stop.
3. contaminated soil sampling Detection device according to claim 1, it is characterised in that described rotating shaft top with it is outside Motor connection.
4. contaminated soil sampling Detection device according to claim 1, it is characterised in that described metal probe is humidity Sensor, metal probe appearance coat once lithium chloride coating.
5. contaminated soil sampling Detection device according to claim 1, it is characterised in that described heat-conducting plate and dividing plate phase Mutually it is vertically arranged.
6. contaminated soil sampling Detection device according to claim 1, it is characterised in that described camera is shown with outside Show that equipment connects.
CN201611221506.0A 2016-12-27 2016-12-27 Polluted soil sampling detection device Withdrawn CN106525751A (en)

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Application Number Priority Date Filing Date Title
CN201611221506.0A CN106525751A (en) 2016-12-27 2016-12-27 Polluted soil sampling detection device

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Application Number Priority Date Filing Date Title
CN201611221506.0A CN106525751A (en) 2016-12-27 2016-12-27 Polluted soil sampling detection device

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106950351A (en) * 2017-04-25 2017-07-14 刘艳丹 A kind of soil detection means
CN107677755A (en) * 2017-11-14 2018-02-09 王传忠 A kind of ambient soil detection means with crushing function
CN107807123A (en) * 2017-12-04 2018-03-16 重庆市合川区农产品质量安全监督检验检测站 A kind of agricultural product heavy metal analysis mechanism
CN107884358A (en) * 2017-11-07 2018-04-06 成都恒力达科技有限公司 A kind of portable soil nutrient detection means
CN108181443A (en) * 2017-12-20 2018-06-19 成都恒力达科技有限公司 For the multi-functional device for fast detecting of ambient soil detection
CN109557255A (en) * 2018-11-15 2019-04-02 广东精科环境科技有限公司 A kind of intelligence SOIL GAS detection method and system
CN109696326A (en) * 2019-02-28 2019-04-30 曹阳 A kind of environmental protection soil sampling Detection system
CN112578000A (en) * 2020-12-14 2021-03-30 浙江海洋大学 Device based on resistance method short-term test soil oil pollution
CN114216720A (en) * 2021-12-14 2022-03-22 陈福瑞 Soil sampling device is used in construction
CN114894973A (en) * 2022-05-05 2022-08-12 中海石油(中国)有限公司 Test device and method for preventing underwater chemical agent from being polluted

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106950351A (en) * 2017-04-25 2017-07-14 刘艳丹 A kind of soil detection means
CN107884358A (en) * 2017-11-07 2018-04-06 成都恒力达科技有限公司 A kind of portable soil nutrient detection means
CN107884358B (en) * 2017-11-07 2020-04-21 重庆昆顶环保科技有限公司 Portable soil nutrient detection device
CN107677755A (en) * 2017-11-14 2018-02-09 王传忠 A kind of ambient soil detection means with crushing function
CN107807123B (en) * 2017-12-04 2024-01-19 重庆市合川区农产品质量安全监督检验检测站 Agricultural product heavy metal detection mechanism
CN107807123A (en) * 2017-12-04 2018-03-16 重庆市合川区农产品质量安全监督检验检测站 A kind of agricultural product heavy metal analysis mechanism
CN108181443A (en) * 2017-12-20 2018-06-19 成都恒力达科技有限公司 For the multi-functional device for fast detecting of ambient soil detection
CN109557255A (en) * 2018-11-15 2019-04-02 广东精科环境科技有限公司 A kind of intelligence SOIL GAS detection method and system
CN109696326A (en) * 2019-02-28 2019-04-30 曹阳 A kind of environmental protection soil sampling Detection system
CN112578000B (en) * 2020-12-14 2023-08-01 浙江海洋大学 Device based on resistance method short-term test soil oil pollutes
CN112578000A (en) * 2020-12-14 2021-03-30 浙江海洋大学 Device based on resistance method short-term test soil oil pollution
CN114216720A (en) * 2021-12-14 2022-03-22 陈福瑞 Soil sampling device is used in construction
CN114216720B (en) * 2021-12-14 2023-07-18 陈福瑞 Soil sampling device is used in construction
CN114894973A (en) * 2022-05-05 2022-08-12 中海石油(中国)有限公司 Test device and method for preventing underwater chemical agent from being polluted

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Application publication date: 20170322