CN106509801A - Making method of extract base powder, and method for making novel agalloch eaglewood vegetal condiment from extract base powder - Google Patents
Making method of extract base powder, and method for making novel agalloch eaglewood vegetal condiment from extract base powder Download PDFInfo
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- 239000000284 extract Substances 0.000 title claims abstract description 124
- 239000000843 powder Substances 0.000 title claims abstract description 92
- 241000271309 Aquilaria crassna Species 0.000 title claims abstract description 75
- 238000000034 method Methods 0.000 title claims abstract description 38
- 235000013409 condiments Nutrition 0.000 title abstract description 4
- 239000012141 concentrate Substances 0.000 claims abstract description 86
- 239000000796 flavoring agent Substances 0.000 claims abstract description 48
- 235000019634 flavors Nutrition 0.000 claims abstract description 48
- 230000007062 hydrolysis Effects 0.000 claims abstract description 46
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 46
- 244000068988 Glycine max Species 0.000 claims abstract description 45
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 45
- 238000000605 extraction Methods 0.000 claims abstract description 37
- 235000019764 Soybean Meal Nutrition 0.000 claims abstract description 35
- 239000004455 soybean meal Substances 0.000 claims abstract description 35
- 241000512259 Ascophyllum nodosum Species 0.000 claims abstract description 11
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 69
- 238000005406 washing Methods 0.000 claims description 45
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- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 43
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 41
- 239000004365 Protease Substances 0.000 claims description 30
- 239000012634 fragment Substances 0.000 claims description 29
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- 238000004519 manufacturing process Methods 0.000 claims description 15
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- 239000000084 colloidal system Substances 0.000 claims description 5
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- KYOBSHFOBAOFBF-UHFFFAOYSA-N UMP Natural products OC1C(O)C(COP(O)(O)=O)OC1N1C(=O)NC(=O)C=C1C(O)=O KYOBSHFOBAOFBF-UHFFFAOYSA-N 0.000 description 1
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- RQFCJASXJCIDSX-UUOKFMHZSA-N guanosine 5'-monophosphate Chemical compound C1=2NC(N)=NC(=O)C=2N=CN1[C@@H]1O[C@H](COP(O)(O)=O)[C@@H](O)[C@H]1O RQFCJASXJCIDSX-UUOKFMHZSA-N 0.000 description 1
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- XKVWLLRDBHAWBL-UHFFFAOYSA-N imperatorin Natural products CC(=CCOc1c2OCCc2cc3C=CC(=O)Oc13)C XKVWLLRDBHAWBL-UHFFFAOYSA-N 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to a making method of extract base powder. The making method comprises the following steps of (1) treating raw materials: including (1-a) preparing agalloch eaglewood leaf extraction concentrate; (1-b) preparing kelp extraction concentrate; (1-c) preparing shiitake mushroom extraction concentrate; and (1-d) preparing defatted soybean soybean meal hydrolysis concentrate; (2) taking the agalloch eaglewood leaf extraction concentrate, the kelp extraction concentrate, the shiitake mushroom extraction concentrate and the defatted soybean soybean meal hydrolysis concentrate in proportion, and performing uniform mixing so as to obtain mixed liquor; and (3) performing spray drying on the mixed liquor so as to obtain the extract base powder. The extract base powder made by the making method disclosed by the invention has rich palatable taste ingredients, flavor development capacity has complexity effects, and the extract base powder presents high flavor development capacity. The invention also provides a method for making novel agalloch eaglewood vegetal condiment from the extract base powder. The made novel agalloch eaglewood vegetal condiment has the fragrance of agalloch eaglewood and the fragrance and the taste of amino acids, and is rich and pure in taste, palatable and healthy.
Description
Technical field
The present invention relates to food processing technology field, and in particular to a kind of manufacture method of extract original washing powder, and with should
The method that extract original washing powder manufactures new agalloch eaglewood vegetalitas flavouring.
Background technology
Flavouring refers to the color that can increase dish, promotes appetite, is beneficial to the accesary foods of health, its master
Want function to be to promote vegetable quality, meet the sense organ needs of consumer, so as to stimulate appetite, promote health.With economy
Development and living standards of the people raising, composition and quality requirement more and more higher of the people to flavouring." people to eat are
My god ", it is seen that flavouring lives closely bound up with people, is related to huge numbers of families.
The composition that delicate flavour flavouring common at present has monosodium glutamate, chickens' extract, shrimp sauce, fish sauce, oyster sauce etc., wherein monosodium glutamate is mainly
Sodium glutamate, flavour mouthfeel are more single；Chickens' extract, shrimp sauce, fish sauce, oyster sauce etc. are using animal raw materials as primary raw material, product
It is unfavorable for the composition of health containing cholesterol etc..
The content of the invention
The technical problem to be solved is to provide a kind of manufacture method of extract original washing powder and uses the extract
The method that original washing powder manufactures new agalloch eaglewood vegetalitas flavouring, with vegetalitas materials such as eaglewood leaf, sea-tangle, mushroom and defatted soybean dregs of beans
Expect to make extract original washing powder for raw material, this extract original washing powder has abundant delicate flavour composition, and there is flavor ability plyability to imitate
Really, very strong flavor ability is shown, new agalloch eaglewood vegetalitas flavouring has made by based on this extract original washing powder
Agalloch eaglewood fragrance and amino acid fragrance and flavour, flavour are strong pure, more agreeable to the taste, more healthy.Using technical scheme it is as follows：
A kind of manufacture method of extract original washing powder, it is characterised in that comprise the steps：
（1）Feedstock treating, including：
（1-a）Eaglewood leaf extracts the preparation of concentrate
30-40 mesh sieves are crossed after eaglewood leaf is crushed, eaglewood leaf powder is obtained；Then percent by volume is added in eaglewood leaf powder
Concentration carries out refluxing extraction for the ethanol solution of 65-85%, and the quality of ethanol solution used is 6-10 times of eaglewood leaf powder, is carried
Temperature is taken for 75-85 DEG C, extraction time is 3-5 hours；After refluxing extraction terminates, Jing is filtered（The filter cloth of available 160-200 mesh enters
Row is filtered）Agalloch eaglewood leaf extract is obtained, agalloch eaglewood leaf extract is reclaimed into ethanol then and Brix 20-30 ° are concentrated into, is sunk
Spiceleaf extracts concentrate；
（1-b）Sea-tangle extracts the preparation of concentrate
Sea-tangle is shredded, sea-tangle fragment is obtained；Then mass percent concentration is added for the bicarbonate of 1-3% in sea-tangle fragment
Sodium water solution, soaks 30-45 minutes, and the quality of sodium bicarbonate aqueous solution used is 6-10 times of sea-tangle fragment；Drain bicarbonate
After sodium water solution, then sea-tangle fragment is cleaned with water, it is in alkalescent to clean to the cleaning waste liquid discharged（Generally clean to row
The pH value of the cleaning waste liquid for going out is 7.5-8.0）；Then the water that quality is 5-10 times of sea-tangle fragment is added in sea-tangle fragment,
2-4 hours are extracted at 90-100 DEG C；After extraction terminates, Jing is filtered（The filter cloth of available 160-200 mesh is filtered）Obtain sea-tangle
Then kelp extract is concentrated into Brix 10-20 ° by extract, is obtained sea-tangle and is extracted concentrate；
（1-c）Mushroom extracts the preparation of concentrate
30-40 mesh sieves are crossed after mushroom is crushed, mushroom powder is obtained；Then quality is added for mushroom powder in mushroom powder
6-10 times of water is simultaneously well mixed, and adds the first complex enzyme and is hydrolyzed, and hydrolysis temperature is 35-50 DEG C, and hydrolysis time is 5-
10 hours；After hydrolysis terminates, Jing is filtered（The filter cloth of available 160-200 mesh is filtered）Mushroom hydrolyzate is obtained, then by perfume (or spice)
Mushroom hydrolyzate is concentrated into Brix 25-35 °, obtains mushroom and extracts concentrate；
First complex enzyme is made up of cellulase and flavor protease, and the quality of cellulase used is the 1- of mushroom powder
3%, the quality of flavor protease used is the 2-4% of mushroom powder；
（1-d）Defatted soybean dregs of beans hydrolyzes the preparation of concentrate
To in defatted soybean dregs of beans, addition quality is 6-10 times of defatted soybean dregs of beans of water, crosses colloid mill, obtain after being well mixed
To soybean meal slurry；Then in soybean meal slurry the second complex enzyme is added to be hydrolyzed, hydrolysis temperature is 30-45 DEG C, hydrolysis time
For 4-8 hours；After hydrolysis terminates, Jing is filtered and is obtained soybean meal hydrolysate, and soybean meal hydrolysate is concentrated into Brix 30-40 ° then,
Obtain defatted soybean dregs of beans hydrolysis concentrate；
Second complex enzyme is made up of papain and flavor protease, and the quality of papain used is defatted soybean
The 2-5% of dregs of beans, the quality of flavor protease used are the 2-4% of defatted soybean dregs of beans；
（2）Allotment
By volume, take eaglewood leaf and extract concentrate 8-12 parts, sea-tangle extraction concentrate 32-48 parts, mushroom extraction concentrate
120-180 parts, defatted soybean dregs of beans hydrolysis concentrate 320-480 parts；Then eaglewood leaf is extracted into concentrate, sea-tangle and extracts concentration
Liquid, mushroom extract concentrate and defatted soybean dregs of beans hydrolysis concentrate is well mixed, and obtain mixed liquor；
（3）It is spray-dried
Step（2）The spray-dried device of mixed liquor for obtaining is spray-dried, and obtains extract original washing powder.
Above-mentioned Brix is called Brix degree, refers to the content of the soluble solid in product.
Preferred steps（1-d）In, filtration is carried out in two steps, and first carries out coarse filtration to hydrolysate with the filter cloth of 100-160 mesh,
Refined filtration is carried out with the filter cloth of 200-300 mesh again, soybean meal hydrolysate is obtained.
Preferred steps（1-a）In, agalloch eaglewood leaf extract is carried out reclaiming ethanol and concentrating using reduced pressure concentration method.
Preferred steps（1-d）In, soybean meal hydrolysate is concentrated using reduced pressure concentration method.
Step（3）In, the EAT of spray dryer is 140-155 DEG C, leaving air temp is 120-130 DEG C, pressure is
3-3.5MPa, flow velocity are 10-12 ml/mins.
Eaglewood leaf（Such as whitewood's eaglewood leaf）In containing amino acid, polysaccharide, flavones and its glycoside, Polyphenols and volatile oil.It is heavy
Spiceleaf Jing alcohol refluxs extract the extract for obtaining to be had significant antibacterial anti-inflammatory, analgesia, promotes intestinal motility, anti-cerebral anoxia to lack
Blood, hypoglycemic, antitumor etc. are acted on.Add appropriate agalloch eaglewood leaf extract（Eaglewood leaf extracts concentrate）, not only improve lifting and adjust
The local flavor of taste product, can play a part of natural bacteriostatic agent to product again.
Sea-tangle is a kind of nutritious maritime vegetables, containing carbohydrate, protein, dietary fiber, aliphatic acid,
Iodine in the multiple nutritional components such as vitamin, mineral matter, iodine, particularly sea-tangle, determines according to analysis, per in 100 grams of sea-tangle dry products
240mg is up to containing iodine, be 13 times of seaweed, deliver vegetables 20 times, 2500 times of egg, tens to the hundred times of general marine animal,
Freshwater fish and thousand of times of vegetables, so sea-tangle is otherwise known as " champion containing iodine "；And 80% iodine is directly to utilize in sea-tangle
Active organic iodine.Sea-tangle contains abundant inosinicacid, per hectogram dry product content in more than 1000mg, is natural flavour volatile
Matter.
Mushroom contains abundant taste compound, predominantly delicious amino acid and nucleotides, and total amino acid content reaches 5.6%
（Wherein content highest is glutamic acid, accounts for the 18.4% of total amino acid content, secondly accounts for total amino acid content for asparatate
9.2%）, and containing abundant flavour nucleotide：IMP, GMP, UMP and AMP.Glutamic acid is that most important one kind is in mushroom
Taste amino acid, it forms sodium glutamate in the presence of salt（MSG）, present stronger delicate flavour.Asparatate
Sodium salt has special sense of taste, and alanine can improve sweet sense, strengthens the honest degree of sweet sense, alleviates bitter taste, with glutamic acid, guanylic acid
Coordinate the synergism that can play delicate flavour Deng delicate flavour material.Cap, the stem of mushroom or the whole mushroom conduct of mushroom can be adopted
Raw material.
Defatted soybean dregs of beans（I.e. soybean Jing oil expression after dregs of beans）, main component is protein, and enzyme is obtained Jing after enzyme hydrolysis
Hydrolyzed vegetable protein（EVP）, containing substantial amounts of delicious amino acid, integrate color and nutrition.And adopt enzyme hydrolysis
Production, is compared with acid-hydrolysis method and is had the characteristics that：1 hydrolysising condition is gently, to sensitive amino acid without destruction；2 can be maximum
Reservation raw material local flavor；3 produce without chloropropyl alcohol；4 hydrolysates except containing in addition to amino acid, also a large amount of small molecular weight titaniums.
Said extracted thing original washing powder also can be deployed into flavouring after mixing with other raw materials directly as flavouring.
The present invention also provides a kind of method that above-mentioned extract original washing powder manufactures new agalloch eaglewood vegetalitas flavouring, its feature
It is to comprise the steps：
（1’）By mass, it is equipped with following material：The extract original washing powder 32-48%, salt 32-48%, white granulated sugar 8-12%, ferment
Female extract 4-6%, I+G 2-3%, dextrin 2-3%；
（2’）By step（1’）The extract original washing powder of outfit, salt, white granulated sugar, yeast extract, I+G and dextrin are well mixed,
Obtain the new agalloch eaglewood vegetalitas flavouring.
Above-mentioned I+G is that two kinds of flavor enhancements combine the abbreviation for taking away an English alphabet, i.e. 5 ' Sodium Inosinate IMP
(Disodiuminosine5 ' monophosphate) and 5 ' bird sodium nucleinate GMP (Disodium guanosine5 '
Monophosphate) combine.
The raw materials such as above-mentioned salt, white granulated sugar, yeast extract, I+G, dextrin are commercially available.
In said extracted thing original washing powder and new agalloch eaglewood vegetalitas flavouring, contained agalloch eaglewood leaf extract（Eaglewood leaf extracts dense
Contracting liquid）In containing amino acid, polysaccharide, flavones and its glycoside, Polyphenols and volatile oil, not only improve the local flavor for lifting flavouring,
Natural bacteriostatic agent can be played a part of to product again；Thallus Laminariae (Thallus Eckloniae) extract（Sea-tangle extracts concentrate）In contain substantial amounts of iodine（Wherein
80% iodine is the active organic iodine that directly can be utilized）, and containing abundant inosinicacid, be natural taste compound, can improving product
Delicate flavour；Shitake Mushroom P.E（Mushroom extracts concentrate）With defatted soybean soybean meal extractive（Defatted soybean dregs of beans hydrolyzes concentrate）Remove
Outside containing natural delicious amino acid and flavour nucleotide, also contain the delicate flavour materials such as small-molecular peptides, ammonia propylhomoserin, nucleotides
Cooperation can play the synergism of delicate flavour, and this causes product to have strong delicate flavour, and small-molecular peptides have to body immunity
Significantly castering action.
The present invention makes extract base as raw material with vegetable matters such as eaglewood leaf, sea-tangle, mushroom and defatted soybean dregs of beans
Powder, this extract original washing powder have abundant delicate flavour composition, and flavor ability has plyability effect, shows very strong flavor energy
Power；New agalloch eaglewood vegetalitas flavouring made by based on this extract original washing powder have agalloch eaglewood fragrance and amino acid fragrance and
Flavour, flavour are strong pure, more agreeable to the taste.Due to product do not contain Animal components and do not contain cholesterol, and in sea-tangle containing compared with
High iodine, Lignum Aquilariae Resinatum extract itself have bacteriostasis and without adding other preservatives again, therefore are a kind of more healthy natural
Vegetalitas condiment.The existing seasoning effect of extract original washing powder and new agalloch eaglewood vegetalitas flavouring of the present invention, has again
Unsoundness health-care effect, will progressively replace monosodium glutamate, chickens' extract etc., become flavouring of new generation.
Specific embodiment
Embodiment 1
In the present embodiment, the manufacture method of extract original washing powder comprises the steps：
（1）Feedstock treating, including：
（1-a）Eaglewood leaf extracts the preparation of concentrate
30 mesh sieves are crossed after eaglewood leaf is crushed, eaglewood leaf powder is obtained；Then in eaglewood leaf powder add percent by volume dense
Spending carries out refluxing extraction for 80% ethanol solution, 8 times for eaglewood leaf powder of the quality of ethanol solution used, and Extracting temperature is
80 DEG C, extraction time is 3 hours；After refluxing extraction terminates, Jing is filtered（Filtered with the filter cloth of 200 mesh）Obtain eaglewood leaf to carry
Liquid is taken, agalloch eaglewood leaf extract is reclaimed into ethanol then and 20 ° of Brix is concentrated into（Eaglewood leaf is extracted using reduced pressure concentration method
Liquid is carried out reclaiming and ethanol is concentrated, during reduced pressure concentration vacuum be -0.095MPa, temperature be 50 DEG C）, obtain eaglewood leaf and extract dense
Contracting liquid；
（1-b）Sea-tangle extracts the preparation of concentrate
Sea-tangle is shredded, sea-tangle fragment is obtained；Then in sea-tangle fragment, addition mass percent concentration is 1.5% bicarbonate
Sodium water solution, soaks 45 minutes, and the quality of sodium bicarbonate aqueous solution used is 8 times of sea-tangle fragment；Drain sodium acid carbonate water-soluble
After liquid, then sea-tangle fragment is cleaned with water, it is in alkalescent to clean to the cleaning waste liquid discharged（Generally clean to what is discharged clear
The pH value for washing waste liquid is 7.8）；Then the water that quality is 6 times of sea-tangle fragment is added in sea-tangle fragment, extract 3 little at 100 DEG C
When；After extraction terminates, Jing is filtered（Filtered with the filter cloth of 160 mesh）Kelp extract is obtained, it is then that kelp extract is dense
15 ° of Brix is reduced to, sea-tangle is obtained and is extracted concentrate；
（1-c）Mushroom extracts the preparation of concentrate
30 mesh sieves are crossed after mushroom is crushed, mushroom powder is obtained；Then quality is added for 8 times of mushroom powder in mushroom powder
Water and be well mixed, add the first complex enzyme and be hydrolyzed, hydrolysis temperature be 50 DEG C, hydrolysis time be 5 hours；Hydrolysis knot
Shu Hou, Jing are filtered（The filter cloth of available 200 mesh is filtered）Mushroom hydrolyzate is obtained, mushroom hydrolyzate is concentrated into into Brix then
25 °, obtain mushroom and extract concentrate；
First complex enzyme is made up of cellulase and flavor protease, and the quality of cellulase used is mushroom powder
1%, the quality of flavor protease used is the 3% of mushroom powder；
（1-d）Defatted soybean dregs of beans hydrolyzes the preparation of concentrate
To in defatted soybean dregs of beans, addition quality is 7.5 times of defatted soybean dregs of beans of water, crosses colloid mill, obtain after being well mixed
Soybean meal slurry；Then in soybean meal slurry the second complex enzyme is added to be hydrolyzed, hydrolysis temperature is 45 DEG C, hydrolysis time is 5 little
When；After hydrolysis terminates, Jing is filtered and is obtained soybean meal hydrolysate（Filtration is carried out in two steps, and first hydrolysate is entered with the filter cloth of 100 mesh
Row coarse filtration, then refined filtration is carried out with the filter cloth of 200 mesh, obtain soybean meal hydrolysate）, soybean meal hydrolysate is concentrated into into 35 ° of Brix then
（Soybean meal hydrolysate is concentrated using reduced pressure concentration method, during reduced pressure concentration vacuum be -0.096MPa, temperature be 55
℃）, obtain defatted soybean dregs of beans hydrolysis concentrate；
Second complex enzyme is made up of papain and flavor protease, and the quality of papain used is defatted soybean
The 3% of dregs of beans, the quality of flavor protease used is the 3% of defatted soybean dregs of beans；
（2）Allotment
By volume, take eaglewood leaf 10 parts of concentrate of extraction, sea-tangle to extract 35 parts of concentrate, mushroom and extract 160 parts of concentrate, take off
Fat soybean meal hydrolyzes 380 parts of concentrate；Then eaglewood leaf is extracted into concentrate, sea-tangle and extracts concentrate, mushroom extraction concentration
Liquid and defatted soybean dregs of beans hydrolysis concentrate are well mixed, and obtain mixed liquor；
（3）It is spray-dried
Step（2）The spray-dried device of mixed liquor for obtaining is spray-dried（The EAT of spray dryer is 145 DEG C, air-out
Temperature is 125 DEG C, pressure is 3.2MPa, flow velocity is 11 ml/mins）, obtain extract original washing powder.
The method that new agalloch eaglewood vegetalitas flavouring is manufactured with above-mentioned extract original washing powder comprises the steps：
（1’）By mass, it is equipped with following material：The extract original washing powder 40%, salt 38%, white granulated sugar 11%, yeast extract
6%, I+G 2.5%, dextrin 2.5%；
（2’）By step（1’）The extract original washing powder of outfit, salt, white granulated sugar, yeast extract, I+G and dextrin are well mixed,
Obtain the new agalloch eaglewood vegetalitas flavouring.
Embodiment 2
In the present embodiment, the manufacture method of extract original washing powder comprises the steps：
（1）Feedstock treating, including：
（1-a）Eaglewood leaf extracts the preparation of concentrate
40 mesh sieves are crossed after eaglewood leaf is crushed, eaglewood leaf powder is obtained；Then in eaglewood leaf powder add percent by volume dense
Spending carries out refluxing extraction for 65% ethanol solution, 10 times for eaglewood leaf powder of the quality of ethanol solution used, and Extracting temperature is
85 DEG C, extraction time is 3.5 hours；After refluxing extraction terminates, Jing is filtered（Filtered with the filter cloth of 160 mesh）Obtain eaglewood leaf
Then agalloch eaglewood leaf extract is reclaimed ethanol and is concentrated into 25 ° of Brix by extract（Eaglewood leaf is carried using reduced pressure concentration method
Take liquid and carry out reclaiming and ethanol concentrate, during reduced pressure concentration vacuum be -0.09MPa, temperature be 50 DEG C）, obtain eaglewood leaf extraction
Concentrate；
（1-b）Sea-tangle extracts the preparation of concentrate
Sea-tangle is shredded, sea-tangle fragment is obtained；Then in sea-tangle fragment, addition mass percent concentration is 3% sodium acid carbonate
The aqueous solution, soaks 30 minutes, and the quality of sodium bicarbonate aqueous solution used is 6 times of sea-tangle fragment；Drain sodium bicarbonate aqueous solution
Afterwards, then with water sea-tangle fragment is cleaned, it is in alkalescent to clean to the cleaning waste liquid discharged（Clean to the cleaning waste liquid discharged
PH value be 8.0）；Then quality is added in sea-tangle fragment for the water of 10 times of sea-tangle fragment, extraction 4 hours at 90 DEG C；Carry
After taking end, Jing is filtered（Filtered with the filter cloth of 200 mesh）Kelp extract is obtained, then kelp extract is concentrated into
10 ° of Brix, obtains sea-tangle and extracts concentrate；
（1-c）Mushroom extracts the preparation of concentrate
40 mesh sieves are crossed after mushroom is crushed, mushroom powder is obtained；Then quality is added for 6 times of mushroom powder in mushroom powder
Water and be well mixed, add the first complex enzyme and be hydrolyzed, hydrolysis temperature be 35 DEG C, hydrolysis time be 10 hours；Hydrolysis
After end, Jing is filtered（The filter cloth of available 160 mesh is filtered）Mushroom hydrolyzate is obtained, then mushroom hydrolyzate is concentrated into
35 ° of Brix, obtains mushroom and extracts concentrate；
First complex enzyme is made up of cellulase and flavor protease, and the quality of cellulase used is mushroom powder
2%, the quality of flavor protease used is the 2% of mushroom powder；
（1-d）Defatted soybean dregs of beans hydrolyzes the preparation of concentrate
To in defatted soybean dregs of beans, addition quality is 10 times of defatted soybean dregs of beans of water, crosses colloid mill, obtain after being well mixed
Soybean meal slurry；Then in soybean meal slurry the second complex enzyme is added to be hydrolyzed, hydrolysis temperature is 30 DEG C, hydrolysis time is 8 little
When；After hydrolysis terminates, Jing is filtered and is obtained soybean meal hydrolysate（Filtration is carried out in two steps, and first hydrolysate is entered with the filter cloth of 160 mesh
Row coarse filtration, then refined filtration is carried out with the filter cloth of 300 mesh, obtain soybean meal hydrolysate）, soybean meal hydrolysate is concentrated into into 30 ° of Brix then
（Soybean meal hydrolysate is concentrated using reduced pressure concentration method, during reduced pressure concentration vacuum be -0.09MPa, temperature be 55 DEG C）,
Obtain defatted soybean dregs of beans hydrolysis concentrate；
Second complex enzyme is made up of papain and flavor protease, and the quality of papain used is defatted soybean
The 5% of dregs of beans, the quality of flavor protease used is the 2% of defatted soybean dregs of beans；
（2）Allotment
By volume, take eaglewood leaf 8 parts of concentrate of extraction, sea-tangle to extract 48 parts of concentrate, mushroom and extract 120 parts of concentrate, take off
Fat soybean meal hydrolyzes 470 parts of concentrate；Then eaglewood leaf is extracted into concentrate, sea-tangle and extracts concentrate, mushroom extraction concentration
Liquid and defatted soybean dregs of beans hydrolysis concentrate are well mixed, and obtain mixed liquor；
（3）It is spray-dried
Step（2）The spray-dried device of mixed liquor for obtaining is spray-dried（The EAT of spray dryer is 140 DEG C, air-out
Temperature is 120 DEG C, pressure is 3MPa, flow velocity is 10 ml/mins）, obtain extract original washing powder.
The method that new agalloch eaglewood vegetalitas flavouring is manufactured with above-mentioned extract original washing powder comprises the steps：
（1’）By mass, it is equipped with following material：The extract original washing powder 48%, salt 32%, white granulated sugar 12%, yeast extract
4%, I+G 2%, dextrin 2%；
（2’）By step（1’）The extract original washing powder of outfit, salt, white granulated sugar, yeast extract, I+G and dextrin are well mixed,
Obtain the new agalloch eaglewood vegetalitas flavouring.
Embodiment 3
In the present embodiment, the manufacture method of extract original washing powder comprises the steps：
（1）Feedstock treating, including：
（1-a）Eaglewood leaf extracts the preparation of concentrate
35 mesh sieves are crossed after eaglewood leaf is crushed, eaglewood leaf powder is obtained；Then in eaglewood leaf powder add percent by volume dense
Spending carries out refluxing extraction for 85% ethanol solution, 6 times for eaglewood leaf powder of the quality of ethanol solution used, and Extracting temperature is
75 DEG C, extraction time is 5 hours；After refluxing extraction terminates, Jing is filtered（Filtered with the filter cloth of 180 mesh）Obtain eaglewood leaf to carry
Liquid is taken, agalloch eaglewood leaf extract is reclaimed into ethanol then and 30 ° of Brix is concentrated into（Eaglewood leaf is extracted using reduced pressure concentration method
Liquid is carried out reclaiming and ethanol is concentrated, during reduced pressure concentration vacuum be -0.092MPa, temperature be 50 DEG C）, obtain eaglewood leaf and extract dense
Contracting liquid；
（1-b）Sea-tangle extracts the preparation of concentrate
Sea-tangle is shredded, sea-tangle fragment is obtained；Then in sea-tangle fragment, addition mass percent concentration is 1% sodium acid carbonate
The aqueous solution, soaks 40 minutes, and the quality of sodium bicarbonate aqueous solution used is 10 times of sea-tangle fragment；Drain sodium bicarbonate aqueous solution
Afterwards, then with water sea-tangle fragment is cleaned, it is in alkalescent to clean to the cleaning waste liquid discharged（Clean to the cleaning waste liquid discharged
PH value be 7.5）；Then quality is added in sea-tangle fragment for the water of 8 times of sea-tangle fragment, extraction 3.5 hours at 95 DEG C；Carry
After taking end, Jing is filtered（Filtered with the filter cloth of 180 mesh）Kelp extract is obtained, then kelp extract is concentrated into
20 ° of Brix, obtains sea-tangle and extracts concentrate；
（1-c）Mushroom extracts the preparation of concentrate
35 mesh sieves are crossed after mushroom is crushed, mushroom powder is obtained；Then quality is added for the 10 of mushroom powder in mushroom powder
Water again is simultaneously well mixed, and adds the first complex enzyme and is hydrolyzed, and hydrolysis temperature is 45 DEG C, and hydrolysis time is 8 hours；Hydrolysis
After end, Jing is filtered（The filter cloth of available 180 mesh is filtered）Mushroom hydrolyzate is obtained, then mushroom hydrolyzate is concentrated into
30 ° of Brix, obtains mushroom and extracts concentrate；
First complex enzyme is made up of cellulase and flavor protease, and the quality of cellulase used is mushroom powder
3%, the quality of flavor protease used is the 4% of mushroom powder；
（1-d）Defatted soybean dregs of beans hydrolyzes the preparation of concentrate
To in defatted soybean dregs of beans, addition quality is 6 times of defatted soybean dregs of beans of water, crosses colloid mill, obtain beans after being well mixed
Dregs of rice slurry；Then in soybean meal slurry the second complex enzyme is added to be hydrolyzed, hydrolysis temperature is 40 DEG C, hydrolysis time is 6 hours；
After hydrolysis terminates, Jing is filtered and is obtained soybean meal hydrolysate（Filtration is carried out in two steps, and first hydrolysate is carried out with the filter cloth of 120 mesh
Coarse filtration, then refined filtration is carried out with the filter cloth of 250 mesh, obtain soybean meal hydrolysate）, soybean meal hydrolysate is concentrated into into 40 ° of Brix then
（Soybean meal hydrolysate is concentrated using reduced pressure concentration method, during reduced pressure concentration vacuum be -0.095MPa, temperature be 55
℃）, obtain defatted soybean dregs of beans hydrolysis concentrate；
Second complex enzyme is made up of papain and flavor protease, and the quality of papain used is defatted soybean
The 2% of dregs of beans, the quality of flavor protease used is the 4% of defatted soybean dregs of beans；
（2）Allotment
By volume, take eaglewood leaf 12 parts of concentrate of extraction, sea-tangle to extract 32 parts of concentrate, mushroom and extract 180 parts of concentrate, take off
Fat soybean meal hydrolyzes 320 parts of concentrate；Then eaglewood leaf is extracted into concentrate, sea-tangle and extracts concentrate, mushroom extraction concentration
Liquid and defatted soybean dregs of beans hydrolysis concentrate are well mixed, and obtain mixed liquor；
（3）It is spray-dried
Step（2）The spray-dried device of mixed liquor for obtaining is spray-dried（The EAT of spray dryer is 155 DEG C, air-out
Temperature is 130 DEG C, pressure is 3.5MPa, flow velocity is 12 ml/mins）, obtain extract original washing powder.
The method that new agalloch eaglewood vegetalitas flavouring is manufactured with above-mentioned extract original washing powder comprises the steps：
（1’）By mass, it is equipped with following material：The extract original washing powder 33%, salt 48%, white granulated sugar 8%, yeast extract
5%, I+G 3%, dextrin 3%；
（2’）By step（1’）The extract original washing powder of outfit, salt, white granulated sugar, yeast extract, I+G and dextrin are well mixed,
Obtain the new agalloch eaglewood vegetalitas flavouring.
Claims (7)
1. a kind of manufacture method of extract original washing powder, it is characterised in that comprise the steps：
（1）Feedstock treating, including：
（1-a）Eaglewood leaf extracts the preparation of concentrate
30-40 mesh sieves are crossed after eaglewood leaf is crushed, eaglewood leaf powder is obtained；Then percent by volume is added in eaglewood leaf powder
Concentration carries out refluxing extraction for the ethanol solution of 65-85%, and the quality of ethanol solution used is 6-10 times of eaglewood leaf powder, is carried
Temperature is taken for 75-85 DEG C, extraction time is 3-5 hours；After refluxing extraction terminates, Jing is filtered and is obtained agalloch eaglewood leaf extract, then
Agalloch eaglewood leaf extract is reclaimed into ethanol and Brix 20-30 ° are concentrated into, eaglewood leaf is obtained and is extracted concentrate；
（1-b）Sea-tangle extracts the preparation of concentrate
Sea-tangle is shredded, sea-tangle fragment is obtained；Then mass percent concentration is added for the bicarbonate of 1-3% in sea-tangle fragment
Sodium water solution, soaks 30-45 minutes, and the quality of sodium bicarbonate aqueous solution used is 6-10 times of sea-tangle fragment；Drain bicarbonate
After sodium water solution, then sea-tangle fragment is cleaned with water, it is in alkalescent to clean to the cleaning waste liquid discharged；Then it is broken to sea-tangle
Add quality for the water of 5-10 times of sea-tangle fragment in piece, 2-4 hours are extracted at 90-100 DEG C；After extraction terminates, Jing is filtered
To kelp extract, kelp extract is concentrated into into Brix 10-20 ° then, obtains sea-tangle and extract concentrate；
（1-c）Mushroom extracts the preparation of concentrate
30-40 mesh sieves are crossed after mushroom is crushed, mushroom powder is obtained；Then quality is added for mushroom powder in mushroom powder
6-10 times of water is simultaneously well mixed, and adds the first complex enzyme and is hydrolyzed, and hydrolysis temperature is 35-50 DEG C, and hydrolysis time is 5-
10 hours；After hydrolysis terminates, Jing is filtered and is obtained mushroom hydrolyzate, mushroom hydrolyzate is concentrated into Brix 25-35 ° then, is obtained
Mushroom extracts concentrate；
First complex enzyme is made up of cellulase and flavor protease, and the quality of cellulase used is the 1- of mushroom powder
3%, the quality of flavor protease used is the 2-4% of mushroom powder；
（1-d）Defatted soybean dregs of beans hydrolyzes the preparation of concentrate
To in defatted soybean dregs of beans, addition quality is 6-10 times of defatted soybean dregs of beans of water, crosses colloid mill, obtain after being well mixed
To soybean meal slurry；Then in soybean meal slurry the second complex enzyme is added to be hydrolyzed, hydrolysis temperature is 30-45 DEG C, hydrolysis time
For 4-8 hours；After hydrolysis terminates, Jing is filtered and is obtained soybean meal hydrolysate, and soybean meal hydrolysate is concentrated into Brix 30-40 ° then,
Obtain defatted soybean dregs of beans hydrolysis concentrate；
Second complex enzyme is made up of papain and flavor protease, and the quality of papain used is defatted soybean
The 2-5% of dregs of beans, the quality of flavor protease used are the 2-4% of defatted soybean dregs of beans；
（2）Allotment
By volume, take eaglewood leaf and extract concentrate 8-12 parts, sea-tangle extraction concentrate 32-48 parts, mushroom extraction concentrate
120-180 parts, defatted soybean dregs of beans hydrolysis concentrate 320-480 parts；Then eaglewood leaf is extracted into concentrate, sea-tangle and extracts concentration
Liquid, mushroom extract concentrate and defatted soybean dregs of beans hydrolysis concentrate is well mixed, and obtain mixed liquor；
（3）It is spray-dried
Step（2）The spray-dried device of mixed liquor for obtaining is spray-dried, and obtains extract original washing powder.
2. the manufacture method of extract original washing powder according to claim 1, it is characterised in that：Step（1-a）In, using decompression
Method for concentration carries out reclaiming ethanol and concentrating to agalloch eaglewood leaf extract.
3. the manufacture method of extract original washing powder according to claim 1, it is characterised in that：Step（1-b）In, it is broken to sea-tangle
It is 7.5-8.0 that piece is cleaned to the pH value of cleaning waste liquid.
4. the manufacture method of extract original washing powder according to claim 1, it is characterised in that：Step（1-d）In, using decompression
Method for concentration is concentrated to soybean meal hydrolysate.
5. the manufacture method of extract original washing powder according to claim 1, it is characterised in that：Step（1-d）In, filtration is divided to two
Step is carried out, and coarse filtration is carried out to hydrolysate with the filter cloth of 100-160 mesh first, then carries out refined filtration with the filter cloth of 200-300 mesh, obtained
Soybean meal hydrolysate.
6. the manufacture method of extract original washing powder according to claim 1, it is characterised in that：Step（3）In, spray dryer
EAT be 140-155 DEG C, leaving air temp be 120-130 DEG C, pressure be 3-3.5mPa, flow velocity be 10-12 ml/mins
Clock.
7. the method for manufacturing new agalloch eaglewood vegetalitas flavouring with extract original washing powder obtained in any one of claim 1-6, which is special
Levy is to comprise the steps：
（1’）By mass, it is equipped with following material：The extract original washing powder 32-48%, salt 32-48%, white granulated sugar 8-12%, ferment
Female extract 4-6%, I+G 2-3%, dextrin 2-3%；
（2’）By step（1’）The extract original washing powder of outfit, salt, white granulated sugar, yeast extract, I+G and dextrin are well mixed,
Obtain the new agalloch eaglewood vegetalitas flavouring.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021057266A1 (en) * | 2019-09-26 | 2021-04-01 | 广东天企生物科技有限公司 | High-clarity soybean flavor peptide, preparation method therefor, and use thereof |
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