CN106492501A - A kind of single-stage segregation apparatuss and its method and purposes for animal-plant material - Google Patents
A kind of single-stage segregation apparatuss and its method and purposes for animal-plant material Download PDFInfo
- Publication number
- CN106492501A CN106492501A CN201611017457.9A CN201611017457A CN106492501A CN 106492501 A CN106492501 A CN 106492501A CN 201611017457 A CN201611017457 A CN 201611017457A CN 106492501 A CN106492501 A CN 106492501A
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- Prior art keywords
- liquid
- solid
- separating
- animal
- extraction pot
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0253—Fluidised bed of solid materials
- B01D11/0257—Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Abstract
A kind of single-stage segregation apparatuss and its method and purposes for animal-plant material, belongs to animals and plants extractive technique field.Including extraction pot（1）, solid-liquid separating machine（2）And pulverizer（3）, extraction pot（1）By feed line（101）With pulverizer（3）It is connected, extraction pot（1）Discharging opening passes through pump（4）With solid-liquid separating machine（2）Charging aperture pipeline connects, solid-liquid separating machine（2）Liquid outlet be connected to separating liquid return duct（201）With separating liquid outlet tube（202）, solid-liquid separating machine（2）Liquid outlet pass through separating liquid return duct（201）With extraction pot（1）It is connected；Solid-liquid separating machine（2）The outlet of solid material pass through the first conveyer（5）With extraction pot（1）It is connected.Raw material pulverizing to powder can be carried out solid-liquid separation extraction by the single-stage segregation apparatuss for being used for animal-plant material, with higher yield and leaching efficiency, and can significantly improve the concentration of gained separating liquid, reduce the consumption of solvent, reduce production cost.
Description
Technical field
A kind of single-stage segregation apparatuss and its method and purposes for animal-plant material, belongs to animals and plants extractive technique neck
Domain.
Background technology
Animal-plant material is leached and is referred to using appropriate solvent or method, from animal-plant material（Whole or certain part）
Middle extraction processes acquisition effective ingredient（Effective ingredient can be dissolved in solvent）.In existing industrial mass production, animal-plant material
How the extracting mode of middle effective ingredient, obtain sheet-shaped material using by animal-plant material drying, tabletting, sheet-shaped material sprayed molten
Agent, obtains extracting solution, then carries out separation and purification（Such as extraction, distillation）.
Applicant has found that existing extraction element has problems with study for action：First, existing extraction element, institute
The concentration for obtaining separating liquid is low, needs to complete to extract using substantial amounts of solvent in extraction process, not only increased the cost of solvent, also
Increased later separation, the refined, energy consumption of concentrating and separating liquid.Secondly, it is found by the applicant that the yield of existing extraction element is relatively low,
By the way of tabletting, it is difficult to abolish the cell wall of animal-plant material, even if extending spray or soak time, effective ingredient is also difficult
To leach in solvent, cause to extract insufficient.
Content of the invention
The technical problem to be solved in the present invention is：Overcome the deficiencies in the prior art, there is provided a kind of for animal-plant material
Single-stage segregation apparatuss and its method and purposes, the single-stage segregation apparatuss for being used for animal-plant material can be by raw material pulverizing to powder
Shape carries out solid-liquid separation extraction, with higher yield and leaching efficiency, and can significantly improve gained separating liquid concentration,
The consumption of solvent is reduced, reduces production cost.
The technical solution adopted for the present invention to solve the technical problems is：The single-stage for being used for animal-plant material is separated and is filled
Put, it is characterised in that：Including extraction pot, solid-liquid separating machine and pulverizer, extraction pot is connected with pulverizer by feed line
Connect, extraction pot discharging opening is connected with solid-liquid separation machine inlet pipeline by pump, and the liquid outlet of solid-liquid separating machine connects respectively
The liquid outlet for having separating liquid return duct and separating liquid outlet tube, solid-liquid separating machine is connected with extraction pot by separating liquid return duct
Connect；The solid material outlet of solid-liquid separating machine is connected with extraction pot by the first conveyer.
The solid material outlet of described solid-liquid separating machine is connected with second conveyor.
Control valve is equipped with described separating liquid return duct and separating liquid outlet tube.
Described separating liquid return duct is provided with reflux pump.
The grinding particle size of described pulverizer is Centimeter Level, grade, micron order or nanoscale.
Described pulverizer is wet crushing mill, is connected with solvent delivery pipe on pulverizer.
Described pulverizer is dry grinding machine, is connected with solvent delivery pipe on extraction pot, and feed line is provided with feeding
Machine.
Described solvent delivery pipe is provided with thermoregulator.
This is used for the operational approach of the single-stage segregation apparatuss of animal-plant material, it is characterised in that comprise the steps：
a）Raw material pulverizing is powder by pulverizer, to improve effective ingredient yield and leaching efficiency in extraction pot；After crushing
Dusty raw materials and solvent by proportioning add extraction pot, in extraction pot mixing leach；The material that extraction pot is discharged, by pump
Enter solid-liquid separating machine to filter；
b）In solid-liquid separating machine filter process, separating liquid outlet tube is closed, open separating liquid return duct and the first conveyer, separated
The separating liquid for going out and solid material are recycled in extraction pot repeatedly, circulation extraction, until the separating liquid in separating liquid return duct is dense
When degree is increased to stationary value, closes separating liquid return duct, open separating liquid outlet tube, discharge separating liquid；
c）When in separating liquid outlet tube, separating liquid concentration starts continuous decrease, now the raw material in extraction pot is filled by solvent
Sub-dip is carried, supplementing solvent in stopping to extraction pot, closes the first conveyer, discharges solid material, and separating liquid is defeated by separating liquid
Outlet pipe is discharged.
This is used for the purposes of the single-stage segregation apparatuss of animal-plant material, it is characterised in that：Oils and fatss, Chinese medicine are extracted in oil plant to carry
Take the extraction of thing, spice and extract the application that volatile oil or edible animals and plants raw material extract extraction oil aspect.
For being described as follows for present invention applicant：
Animal-plant material sufficiently can be crushed by pulverizer, raw material is put in extraction pot in the form of powdery, is crushed
The grinding particle size that material powder reaches pulverizer afterwards is Centimeter Level, grade, micron order or nanoscale（10 centimetres ~ 0.1 nanometer）,
The grinding particle size of preferred pulverizer is 3 centimetres ~ 0.1 micron, and the grinding particle size of further preferred pulverizer is micro- for 5000 ~ 2
Rice, under the grinding particle size, Grin-ding energ7 is little, and filter efficiency is high；The grinding particle size of further preferred pulverizer is micro- for 600 ~ 5
Rice, can fully abolish the cell wall of most plants so that the effective ingredient in animal and plant cellss fully soaks under the grinding particle size
Go out, improve yield, the grinding particle size of further preferred pulverizer is that leaching efficiency preferably and is crushed under the grinding particle size
Efficiency and filter efficiency are higher.Therefore, compared to existing technology in by raw material tabletting spray extract or by raw material pulverizing to centimetre
Grade particles are extracted, the design that extraction pot of the present invention is connected with pulverizer by feed line so that the yield of effective ingredient
It is significantly improved with leaching efficiency.Pulverizer can be dry grinding machine or wet crushing mill, when being that wet crushing mill is crushed, pulverizer powder
Broken liquid is extraction solvent.
And applicant designs, and solid-liquid separation is carried out using solid-liquid separating machine, solve the problems, such as filtration difficulty, solid-liquid point
Disembark as decanter type, membrane filtration formula, filter-press type, spiral squeezing type, vacuum type, swinging or centrifuge formula solid-liquid separating machine.Excellent
The solid-liquid separating machine of choosing is centrifugal separator for solid from liquid, filter-press type solid-liquid separating machine or screw extruding type solid-liquid separator.
Compared with prior art, a kind of single-stage segregation apparatuss and its method and purposes for animal-plant material of the invention
Had an advantageous effect in that：
1st, raw material pulverizing to powder can be carried out solid-liquid separation extraction by the single-stage segregation apparatuss for being used for animal-plant material, tool
There are higher yield and leaching efficiency, and the concentration of gained separating liquid can be significantly improved, reduce the consumption of solvent, reduce life
Produce cost.First, applicant is devised extraction pot and is connected with pulverizer by feed line, and raw material pulverizing is by pulverizer
Powder, can abolish the cell wall and cell membrane of animal-plant material, effective ingredient is fully leached in solvent so that effectively
The yield and leaching efficiency of composition is significantly improved.Secondly, applicant devises extraction pot and is connected with solid-liquid separating machine, solid-liquid
Separating function effectively carries out solid-liquid separation, the impurity effectively removed in separating liquid, with higher extraction efficiency.Finally, apply
People devises separating liquid return duct and the first conveyer so that separating obtained separating liquid is back to extraction pot, solidss repeatedly
Material is recycled to repeatedly to extraction pot, is circulated extraction, using the single-stage segregation apparatuss of the animal-plant material of the present invention, just can
Continuous circulation extraction is carried out, so as to improve the concentration of separating liquid, solvent load is reduced.And the separating liquid of high concentration, also reduces
Energy consumption during follow-up refined, concentrating and separating liquid, in a disguised form reduces cost.
2nd, the single-stage segregation apparatuss for being used for animal-plant material further increase leaching efficiency.Applicant devises and carries
The solvent delivery pipe of thermoregulator, can adjust the temperature of solvent, improve leaching efficiency, and it is dry that applicant devises pulverizer
Pulverizer or wet crushing mill, meet different crushing requirements, improve production efficiency.
3rd, this is used for the single-stage segregation apparatuss low cost of animal-plant material and applied widely.This is used for animal-plant material
Single-stage segregation apparatuss can be used in multiple fields, can be used in oil crop and carry oil（Extracting bean oil such as from Semen sojae atricolor）, can
Extract for plant medicine raw material（Semen Cassiae extract, methanol are extracted as solvent as Ramulus Cinnamomi extracts volatile oil, ethyl acetate
Extract the glycoside in Radix Ginseng）, can be used in plant perfume and carry oil（Extraction such as volatile oil in Flos Rosae Rugosae, lavandula angustifolia）, can be used in
Edible animals and plants raw material is extracted and leaches oil（Algal oil extract in carrot oil, Sargassum as extracted in Radix Dauci Sativae）.
Description of the drawings
Fig. 1 is a kind of structural representation of the single-stage segregation apparatuss for animal-plant material of embodiment 1.
Fig. 2 is a kind of structural representation of the single-stage segregation apparatuss for animal-plant material of embodiment 2.
Wherein：1st, extraction pot 101, feed line 102, solvent delivery pipe 103, thermoregulator 2, solid-liquid separation
Machine 201, separating liquid return duct 202, separating liquid outlet tube 3, pulverizer 301, feeder 4, pump 5, the first conveyer 6,
Two conveyers 7, control valve 8, reflux pump.
Specific embodiment
Fig. 1 is highly preferred embodiment of the present invention, and with reference to Fig. 1 ~ 2, the present invention is described further.
Embodiment 1
With reference to Fig. 1, this is used for the single-stage segregation apparatuss of animal-plant material, including extraction pot 1, solid-liquid separating machine 2 and pulverizer 3,
Extraction pot 1 is connected with pulverizer 3 by feed line 101, and 1 discharging opening of extraction pot is fed with solid-liquid separating machine 2 by pump 4
Mouth pipeline connection, the liquid outlet of solid-liquid separating machine 2 are connected to separating liquid return duct 201 and separating liquid outlet tube 202, Gu
The liquid outlet of liquid separator 2 is connected with extraction pot 1 by separating liquid return duct 201；The solid material outlet of solid-liquid separating machine 2 is logical
Cross the first conveyer 5 to be connected with extraction pot 1.The solid material outlet of solid-liquid separating machine 2 is connected with second conveyor 6, the second conveying
Machine 6 is used for discharging solid material, or goes further to extract for conveying solid material.Separating liquid return duct 201 and separating liquid
Control valve 7 is equipped with outlet tube 202.The grinding particle size of pulverizer 3 is Centimeter Level, grade, micron order or nanoscale.Its
In, mixing arrangement is provided with extraction pot 1, mixing arrangement can adopt agitator or jet mixing, and extraction pot periphery is provided with heating
Device, it is also possible to be not provided with heater.
The present embodiment pulverizer 3 is wet crushing mill, is connected with solvent delivery pipe 102 on pulverizer 3.
Embodiment 2
With reference to Fig. 2, the present embodiment is distinguished as with embodiment 1：Pulverizer 3 is dry grinding machine, is connected with solvent defeated on extraction pot 1
Pipe 102, feed line 101 is sent to be provided with feeder 301.Solvent delivery pipe 102 is provided with thermoregulator 103.Separating liquid
Return duct 201 is provided with reflux pump 8.
The operational approach that this is used for the single-stage segregation apparatuss of animal-plant material is as follows：
a）Raw material pulverizing is powder by pulverizer 3, to improve effective ingredient yield and leaching efficiency in extraction pot 1；To crush
Dusty raw materials and solvent afterwards add extraction pot 1 by proportioning, and mixing in extraction pot 1 is leached；The material that extraction pot 1 is discharged,
Solid-liquid separating machine 2 is entered by pump 4 to filter；
b）In 2 filter process of solid-liquid separating machine, separating liquid outlet tube 202 is closed, open separating liquid return duct 201 and the first conveying
Machine 5, the separating liquid that isolates and solid material are recycled in extraction pot 1 repeatedly, and circulation extraction, until separating liquid return duct 201
In separating liquid concentration when being increased to stationary value, close separating liquid return duct 201, open separating liquid outlet tube 202, make separating liquid
Discharge；
c）When in separating liquid outlet tube 202, separating liquid concentration starts continuous decrease, now the raw material in extraction pot 1 is by molten
Agent is fully extracted, supplementing solvent in stopping to extraction pot 1, closes the first conveyer, discharges solid material, separating liquid（Containing effectively
Composition and solvent）Discharged by separating liquid outlet tube 202.
The above, is only presently preferred embodiments of the present invention, is not the restriction for making other forms to the present invention, appoints
What those skilled in the art changed possibly also with the technology contents of the disclosure above or be modified as equivalent variations etc.
Effect embodiment.But every without departing from technical solution of the present invention content, the technical spirit according to the present invention is to above example institute
Any simple modification, equivalent variations and the remodeling that makees, still falls within the protection domain of technical solution of the present invention.
Claims (10)
1. a kind of single-stage segregation apparatuss for animal-plant material, it is characterised in that：Including extraction pot（1）, solid-liquid separating machine（2）
And pulverizer（3）, extraction pot（1）By feed line（101）With pulverizer（3）It is connected, extraction pot（1）Discharging opening passes through
Pump（4）With solid-liquid separating machine（2）Charging aperture pipeline connects, solid-liquid separating machine（2）Liquid outlet be connected to separating liquid return
Flow tube（201）With separating liquid outlet tube（202）, solid-liquid separating machine（2）Liquid outlet pass through separating liquid return duct（201）With carry
Take tank（1）It is connected；Solid-liquid separating machine（2）The outlet of solid material pass through the first conveyer（5）With extraction pot（1）It is connected.
2. a kind of single-stage segregation apparatuss for animal-plant material according to claim 1, it is characterised in that：Described consolidates
Liquid separator（2）The outlet of solid material be connected with second conveyor（6）.
3. a kind of single-stage segregation apparatuss for animal-plant material according to claim 1, it is characterised in that：Described divides
Chaotropic return duct（201）With separating liquid outlet tube（202）On be equipped with control valve（7）.
4. a kind of single-stage segregation apparatuss for animal-plant material according to claim 1, it is characterised in that：Described divides
Chaotropic return duct（201）It is provided with reflux pump（8）.
5. a kind of single-stage segregation apparatuss for animal-plant material according to claim 1, it is characterised in that：Described powder
Broken machine（3）Grinding particle size be Centimeter Level, grade, micron order or nanoscale.
6. a kind of single-stage segregation apparatuss for animal-plant material according to claim 1, it is characterised in that：Described powder
Broken machine（3）For wet crushing mill, pulverizer（3）On be connected with solvent delivery pipe（102）.
7. a kind of single-stage segregation apparatuss for animal-plant material according to claim 1, it is characterised in that：Described powder
Broken machine（3）For dry grinding machine, extraction pot（1）On be connected with solvent delivery pipe（102）, feed line（101）It is provided with feeding
Machine（301）.
8. a kind of single-stage segregation apparatuss for animal-plant material according to claim 6 or 7, it is characterised in that：Described
Solvent delivery pipe（102）It is provided with thermoregulator（103）.
9. a kind of operational approach of the single-stage segregation apparatuss for animal-plant material described in claim 1, it is characterised in that bag
Include following steps：
a）Pulverizer（3）It is powder by raw material pulverizing, to improve extraction pot（1）Middle effective ingredient yield and leaching efficiency；Will
Dusty raw materials and solvent after crushing add extraction pot by proportioning（1）, in extraction pot（1）Middle mixing is leached；Extraction pot（1）Row
The material for going out, by pump（4）Enter solid-liquid separating machine（2）Filter；
b）Solid-liquid separating machine（2）In filter process, separating liquid outlet tube is closed（202）, open separating liquid return duct（201）With
One conveyer（5）, the separating liquid that isolates and solid material are recycled to extraction pot repeatedly（1）In, circulation extraction, until separating liquid
Return duct（201）In separating liquid concentration when being increased to stationary value, close separating liquid return duct（201）, open separating liquid output
Pipe（202）, discharge separating liquid；
c）When separating liquid outlet tube（202）When middle separating liquid concentration starts continuous decrease, now extraction pot（1）In raw material lead to
Cross solvent fully to extract, stop to extraction pot（1）Middle supplementing solvent, closes the first conveyer, discharges solid material, and separating liquid is led to
Cross separating liquid outlet tube（202）Discharge.
10. the purposes of a kind of single-stage segregation apparatuss for animal-plant material described in claim 1, it is characterised in that：In oil
Material extracts oils and fatss, the extraction of Chinese medicine extract, spice extraction volatile oil or edible animals and plants raw material and extracts answering for extraction oil aspect
With.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610883145X | 2016-10-10 | ||
| CN201610883145 | 2016-10-10 |
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| Publication Number | Publication Date |
|---|---|
| CN106492501A true CN106492501A (en) | 2017-03-15 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611017457.9A Pending CN106492501A (en) | 2016-10-10 | 2016-11-19 | A kind of single-stage segregation apparatuss and its method and purposes for animal-plant material |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107287028A (en) * | 2017-08-18 | 2017-10-24 | 刘玉通 | A kind of alcohol extracting taking technique of oil Class material Ultramicro-powder |
| CN108079618A (en) * | 2017-11-13 | 2018-05-29 | 涟源康麓生物科技有限公司 | It is atomized extraction element and extracting method |
| CN108355830A (en) * | 2018-03-08 | 2018-08-03 | 中国矿业大学 | A kind of fine sand resource recovering system and technique built in stone ore Tailings Dam |
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| CN2792589Y (en) * | 2005-05-18 | 2006-07-05 | 戴群 | Integrated membrane circulating extractor |
| CN203123614U (en) * | 2013-03-14 | 2013-08-14 | 衡阳市中一制药机械有限公司 | Hot reflux extraction and concentration unit |
| CN203281068U (en) * | 2013-06-19 | 2013-11-13 | 温州市森博轻工机械有限公司 | Multifunctional extraction concentration recycling set |
| CN206184036U (en) * | 2016-10-10 | 2017-05-24 | 王芹 | A single -stage separator for animal and plant materials |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2003068360A1 (en) * | 2002-01-24 | 2003-08-21 | Euroconstruct, S.R.O. | Method for production of plant extracts |
| CN2792589Y (en) * | 2005-05-18 | 2006-07-05 | 戴群 | Integrated membrane circulating extractor |
| CN203123614U (en) * | 2013-03-14 | 2013-08-14 | 衡阳市中一制药机械有限公司 | Hot reflux extraction and concentration unit |
| CN203281068U (en) * | 2013-06-19 | 2013-11-13 | 温州市森博轻工机械有限公司 | Multifunctional extraction concentration recycling set |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107287028A (en) * | 2017-08-18 | 2017-10-24 | 刘玉通 | A kind of alcohol extracting taking technique of oil Class material Ultramicro-powder |
| CN108079618A (en) * | 2017-11-13 | 2018-05-29 | 涟源康麓生物科技有限公司 | It is atomized extraction element and extracting method |
| CN108355830A (en) * | 2018-03-08 | 2018-08-03 | 中国矿业大学 | A kind of fine sand resource recovering system and technique built in stone ore Tailings Dam |
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Application publication date: 20170315 |