CN106490038A - A kind of green Chinese medicine composite bactericide and preparation method thereof - Google Patents
A kind of green Chinese medicine composite bactericide and preparation method thereof Download PDFInfo
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- CN106490038A CN106490038A CN201610932981.2A CN201610932981A CN106490038A CN 106490038 A CN106490038 A CN 106490038A CN 201610932981 A CN201610932981 A CN 201610932981A CN 106490038 A CN106490038 A CN 106490038A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
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Abstract
The present invention relates to bactericide compounded technical field, discloses a kind of green Chinese medicine composite bactericide and preparation method thereof.The active ingredient of the bactericide is mainly made up of Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut, Herba Andrographitis, defoamer, drier, lubricant and water, and the bactericide key step includes cleaning, filter and the step such as preparation.Bactericide of the present invention has the effect of good controlling disease to the common green plants disease blossom rot in city, withes broom, epidemic disease etc., in addition main component used by the present invention is the Chinese herbal medicine to human body and environmental beneficial, proportioning effect is good, friendly to urban ecology, without any side effects to people and animals, safe to use, the preparation method of the bactericide facilitates easy to operate, capable of circulation come into operation, be therefore suitable in urban greening project promote operation.
Description
Technical field
The present invention relates to bactericide compounded technical field, discloses a kind of green Chinese medicine composite bactericide and its preparation side
Method.
Background technology
Traditional chemical bactericide mechanism of action is that a part is attached on plant after bactericide is applied, or penetrates into strain
Left behind in vivo, this can be so that green plants therefore suffer from polluting；Another part is scattered on soil（Sometimes it is then direct
Impose in soil）Or evaporate, be emitted in air, or flow in urban river with rainwater and agricultural drain, pollute urban water-body
With littoral aquatile.The residual of bactericide chemical composition is eventually entered into human body, is caused by air, water body, soil, food
Various chronic or acute disease.However as the continuous development of urbanization process, municipal works afforestation project also inevitable constantly with
Enter, urban greenery plantses also can be more and more, a part of treehole can be produced, all kinds of green plants Common Diseases inside can be grown
Raw, such as process not in time, disease can gradually spread and come, and existing use chemical sterilization agent formulation preventive effect is limited, Er Qieyi
Develop immunity to drugs, dosage is conducive to the breeding of disease on the contrary using effect is not only had.
As the disease drug resistance of urban greenery plantses increases, this causes disease to increase once again and original and non-hazardous
Potential disease has the trend for gradually growing in intensity, due to chemical bactericide directly using harm people and animals, or bactericide residual and
Worked the mischief by food chain.
CN201210307913.9 one kind prevents and treats rice sheath blight disease mancozeb Chinese herbal medicine complex bactericide, is related to anti-harnessing the river
Sheath and culm blight of rice mancozeb Chinese herbal medicine complex bactericide, is wherein prepared by the raw materials in per 100 parts of built agents：Dai Sen
MnZn 8-12, Celastrus angulatus 9-11, chameajasme 9-11, kuh-seng 9-11, Herba Andrographitis 4-6, rhizome of cyrtomium 4-6, datura flower 4-6, Phytolacca acinosa 4-6,
Root of large-flowered skullcap 4-6, monkshood 4-6, betel nut 2-3, frutus cnidii 2-3, dayflower 2-3, kaladana 2-3, honeycomb 2-3, pine needle 2-3, chaulmoogra
2-3, thunder godvine 2-3, black false hellebore 4-6, remaining are auxiliary material, every kind of Chinese herbal medicine using the extract of its water extract or organic solvent as
Raw material, the built agent production cost and raw material sources of the present invention are extensive, with efficient, low toxicity and safe, the spy of environmental protection
Point, will not develop immunity to drugs, and have special efficacy rice sheath blight disease pest and disease damage is prevented and treated.The patent of invention is by vegetable Chinese herbal medicine and Dai Sen
Mixture serve the effect of Synergistic to rice sheath blight disease, but need to be used for multiple times and can be only achieved effect, be also easy to produce anti-
The property of medicine, while as Mancozeb is used in increment, the metabolic breakdown ability of the bactericide may weaken, and can hence speed up Dai Sen
People and animals are had a negative impact by accumulation of the MnZn on paddy rice.
In sum, for the problem that above urban afforestation disease and chemical bactericide are used, it has been realized that
Research and development are a kind of using safety, and the vegetable Chinese herbal medicine composite bactericide of noresidue has become trend, will also have wide market and send out
Exhibition prospect, but at present due to various reasons such as benefit, preventive effects.Composite bactericide containing vegetable Chinese herbal medicine was being promoted the use of
Unsatisfactory in journey.
Content of the invention
It is an object of the invention to provide a kind of green Chinese medicine composite bactericide.
Present invention also offers a kind of preparation method for landscape tree disease control bactericide.
A kind of green Chinese medicine composite bactericide that the present invention is provided, is made up of following parts by weight raw material：Phytolacca acinosa, rheum officinale,
Radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut, Herba Andrographitis, defoamer, drier and water；
Specifically, the bactericide is made up of following parts by weight raw material：Phytolacca acinosa 32-43 parts, rheum officinale 28-39 parts, radix scutellariae 32-45
Part, honeysuckle 28-40 parts, chaulmoogra 28-41 parts, nidus vespae 20-31 parts, bark of official magnolia 29-39 part, betel nut 18-26 parts, Herba Andrographitis
15-26 parts, defoamer 18-29 parts, drier 18-29 parts, lubricant 12-18 parts and water 90-120 parts.
Preferably, the bactericide is made up of following parts by weight raw material：Phytolacca acinosa 34-40 parts, rheum officinale 30-36 parts, radix scutellariae
35-39 parts, honeysuckle 32-37 parts, chaulmoogra 32-37 parts, nidus vespae 23-28 parts, bark of official magnolia 33-38 part, betel nut 21-24 parts, wear
Heart lotus 18-23 parts, defoamer 20-27 parts, drier 20-27 parts, lubricant 13-16 parts and water 100-110 parts.
Further preferably, the bactericide is made up of following parts by weight raw material：36 parts of Phytolacca acinosa, 33 parts of rheum officinale, radix scutellariae 37
Part, 35 parts of honeysuckle, 36 parts of chaulmoogra, 26 parts of nidus vespae, 36 parts of the bark of official magnolia, 22 parts of betel nut, 20 parts of Herba Andrographitis, 25 parts of defoamer,
107 parts of 24 parts of drier, 15 parts of lubricant and water.
Most preferably, the bactericide is made up of following parts by weight raw material：35 parts of Phytolacca acinosa, 32 parts of rheum officinale, 37 parts of radix scutellariae,
35 parts of honeysuckle, 35 parts of chaulmoogra, 26 parts of nidus vespae, 35 parts of the bark of official magnolia, 22 parts of betel nut, 20 parts of Herba Andrographitis, 25 parts of defoamer, drying
105 parts of 23 parts of agent, 14 parts of lubricant and water.
In above-mentioned bactericide：
The defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；
The drier is that soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina press 1：1：2：2 ratio mixing and
Into；
The lubricant is that polyethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
Present invention also offers the preparation method of above-mentioned bactericide, the method is comprised the following steps：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 40-60min, after will immersion mixture
40-50min is boiled in 100-120 DEG C；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 25-35 DEG C, to be cooled complete backward concentrate
In add defoamer, drier and lubricant by required ratio and also have water, uniform stirring 30-40min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 45-55 DEG C
20-30h.Bactericide needed for obtaining by after the completion of waiting to ferment.
The each raw material of above-mentioned bactericide is described as follows：
Phytolacca acinosa：（Phytolacca acinosaRoxb）It is widely distributed in Red soil low-hilly land mound area on the south the Changjiang river.Root is used as medicine, with white
Loose person is preferred, and red root has severe toxicity, is only for external application.Logical two just, relieves oedema or abdominal distension through diuresis or purgation, dissipating bind, controls oedema, turgor, tinea pedis, larynx numbness, and external application is controlled
Carbuncle sore tumefacting virus.Veterinary drug and agricultural chemicals can also be made.Fruit can obtain through refining tannin extract containing tannin.Young stem and leaf is available for cooked food.Phytolacca acinosa red root is poisonous not
It is beneficial to eat, but uses it for making bactericide and not only can turn harm into good, while with uniqueness after Phytolacca acinosa and rheum officinale mixture
The mechanism of action suppress Phytolacca acinosa red root on toxicity.
Rheum officinale：（Rheum palmatum L.）In China, rheum officinale mainly make medicinal, Chinese herb rhubarb have attack stagnant, wet clearly
The effects such as heat, purging intense heat, cool blood, dissolving stasis, removing toxic substances.Rheum officinale also makes general's medicine, the property of medicine therefore effectively can make rapidly than stronger
Pathogenic cell decomposes, and rheum officinale and Phytolacca acinosa are in the toxicity for effectively suppressing Phytolacca acinosa red root to stay after ratio of the present invention mixing in addition.
Radix scutellariae：（Scutellaria lateriflora）Radix scutellariae contains abundant active mineral matter, can stimulate, strong
Nerve, therefore now often as drugs for nervous used by people.It can effectively alleviate often has in busy life
The moods such as nervous, nervousness, hysteria, neurasthenia, depression, sense of crisis.Radix scutellariae has anti-inflammatory, antiallergic action simultaneously
Effect；Hepatic cholagogic is acted on；Step-down, diuresis, calmness, refrigeration function.Clinic is mainly used in catarrhal jaundice, acute biliary tract sense
Dye, lead poisoning are clearing heat and detoxicating, evil of vomitting uncomfortable in chest, cough with lung heat, tumour sore fetal irritability.Radix scutellariae is added in the present invention to be had surely
Determine the effect of bactericide chemical property, prevent the present invention be subject to external environment impact and produce property change thus affect medicine
Effect.
Honeysuckle：（Lonicera japonica）Honeysuckle is described as clearing heat and detoxicating good medicine from ancient times.The sweet cold air virtue of its property
Perfume (or spice), clear heat with drugs of sweet flavour and cold nature and do not injure one's stomach, fragrance is thoroughly up to again can eliminating evil.Honeysuckle is cold in nature, sweet, enters lung, the heart, stomach, with heat-clearing solution
Poison, anti-inflammatory, qi-restoratives treat effect of wind, cure mainly the diseases such as disease under turgor, warm disease heating, heat toxin large carbuncle and tumour.Which is for dizzy head
Dizzy, dry make thirsty, hidrosis unhappiness, enteritis, bacillary dysentery, measles, pneumonia, encephalitis, epidemic meningitis, acute mastitis, septicemia, appendicitis,
The illnesss such as skin infection, ulcer furunculosis, erysipelas, parotitis, suppurative tonsillitis have certain curative effect.Traditional chemical sterilization
Agent is to easily damaging to plant epidermis tissue after green plants administration so that ornamental value reduces, and in the present invention
The pro rata addition of honeysuckle can prevent plant epidermis tissue from being injured by the property of medicine, maintain the attractive in appearance of greening environment.
Chaulmoogra：（Hydnocarpus anthelminticaPierre）Chaulmoogra is distributed in the ground such as Hainan, Guangxi.Tool
Dispel pathogenic wind and remove dampness, the effect of detoxicating and destroying parasites.It is usually used in leprosy, syphilis, mange, wine nose, acne.Indication leprosy, poplar
Plum sore, mange, wine nose, acne are wet with but wind-dryness, and work(kills effect of worm.Chaulmoogra toxicity is strong, on the person only preferably
External application, does not take orally.After in present component, rheum officinale and chaulmoogra mix in proportion, the property of medicine of rheum officinale has suppressed chaulmoogra
Toxicity, but both bactericidal actions can still play the effect of Synergistic.
Nidus vespae：（Polistes mandarinusSaussure）Indication children's disease, brothers' wandering arthritis, wind decayed tooth
Bitterly, laryngalgia swell and ache, bleeding on tongue, metrorrhagia and metrostaxis, infantile cough, two just do not like, tapeworm, roundworm disease.Nidus vespae has analgesia drop
The effect of temperature, but nidus vespae toxicity is stronger, therefore will use with caution in the environment with human contact.Nidus vespae and rheum officinale press than
The toxicity of nidus vespae is effectively inhibited after example is mixed.
The bark of official magnolia：（Magnolia officinalisRehd.et Wils.）Main product is in Sichuan, Hubei, Zhejiang.Outside the bark of official magnolia
Surface taupe brown or taupe, coarse, sometimes in flakey, it is easier to peel off, has substantially ellipse hole skin and vertical wrinkle, scrapes off thick
Skin person shows yellowish-brown.Inner surface purple brown or dark purple brown, smoother, have fine and closely woven longitudinal grin, the aobvious oil trace that draws.Matter is hard, is difficult
Fracture, section graininess, outer layer taupe brown, internal layer puce or brown have oiliness, the visible most little bright stars having.Gas is fragrant, taste
Pungent, slight bitter.There is eliminating dampness dissolving phlegm, lower gas removes full.Bark of official magnolia gas consumption hinders Tianjin, and people is used should not be excessive, but for
Green plants disease but has different mechanism.The consumption of pathogenic cells is excited after the bark of official magnolia is mixed with Phytolacca acinosa, accelerates pathogeny
The death of cell, reaches bactericidal effect faster.
Betel nut（Areca catechu L.）In the torrid areas such as Chinese main distribution Yunnan, Hainan and Taiwan, Asia heat
Extensively cultivate in band area.Betel nut has the effect of " desinsection, breaks product, and sending down abnormally ascending row is stagnant, water-filling dampness elimination ", be once used to treat tapeworm,
Hookworm, roundworm, around parasitic infections such as worm, fasciolopsis.Betel nut is bad to digestive system, can stimulate coat of the stomach, but betel nut for
The stimulation of disease cell is conducive to disease material to disintegrate rapidly.
Herba Andrographitis（Andrographis paniculata(Burm. f.) Nees）China Fujian, Guangdong, Hainan,
Guangxi, the common cultivation in Yunnan, Jiangsu, Shaanxi are also introduced a fine variety.There is Herba Andrographitis eliminating inflammation and expelling toxin to act on, and clinically once be applied to multiple
Infectious diseases, including trauma infection contamination, furuncle, carbuncle, erysipelas, the infection of the upper respiratory tract, acute and chronic tonsillitis, acute and chronic pharyngitis,
Acute/chronic bronchitis, acute bacillary dysentery, acute gastroenteritis, urinary tract infections, endometritis, pelvic infecton, tympanitis, periodontitis
Deng there is different degrees of curative effect.Herba Andrographitis serves the effect of protective nature in the present invention, prevents extraneous other harmful substances
The interference of the drug effect of the present invention of verifying and denaturation.
In sum, as a result of above-mentioned technical proposal, the invention has the beneficial effects as follows：
（1）Mechanism is novel, effect is efficient：Although the Chinese herbal medicine selected by bactericide of the present invention is common mostly,
According to beat all effect can be reached after required ratio mixture of the present invention, produce the mechanism of action of novel and unique.Phytolacca acinosa
Red root toxic, chopping dissolving after can not evade its toxicity completely, but after mixing in ratio of the present invention with rheum officinale
The strong solution toxicity of rheum officinale effectively can suppress.Chaulmoogra and nidus vespae there is also same toxicity problem in the present invention, but
It is to be obtained for clear up by toxicity after mixed in proportion with rheum officinale.Herba Andrographitis and radix scutellariae can replace traditional chemical substance
Play a part of stabilizer, it is ensured that bactericide of the present invention will not be affected generation denaturation by external substance and affect drug effect.?
In the present invention, honeysuckle not only acts as the effect of Synergistic, while can prevent plant epidermis cell from being injured by the property of medicine,
So as to affect ornamental value.The bark of official magnolia and betel nut excite the loss of pathogenic cells, so as to accelerate the death of pathogenic cells.This
Bright bactericide understands this by the effect for serving good Synergistic after required ratio mixing according to experimental data of the present invention
Invention bactericide has reached 86.39% to the average preventive effect of the disease of common green plants, and tradition to be higher by uses chemical bactericide
27.75%, its prevention effect is with the obvious advantage.
（2）Turn harm into good, science environmental protection：In the present invention, although Phytolacca acinosa, chaulmoogra and nidus vespae have certain poison
Property, can not all take orally typically on the person, so playing scope to their drug effects is rather limited, even if directly in plant table
Applying on face to avoid its toxicity direct contagion from giving people class or surrounding useful animals.And by Phytolacca acinosa, chaulmoogra and reveal honeybee
Room in proportion with rheum officinale mixture after toxicity obtained effective suppression, prevent the adverse effect that toxicity is brought, reach and turn harm into good
Effect, expand such use range with toxicity Chinese herbal medicine.Honeysuckle is also added in the present invention, and honeysuckle is to target
Mark green plants serve protective effect, protect plant epidermis histocyte, prevent from being injured by the property of medicine, affect greening to plant
The ornamental value of thing, but honeysuckle is used alone and does not but have similar protective effect on green plants, it is necessary to by this
Bright ratio mixture can be only achieved property of medicine reasonable mixture ratio, play the effect of protection.Environmental protection friendly effect has been reached in sum.
（3）Stable in properties, use is saved：Rice sheath blight disease is prevented and treated compared to Chinese patent CN201210307913.9 one kind
Mancozeb Chinese herbal medicine complex bactericide, although which has reached each herbal component Synergistic during continuous dosage
Effect, but the invention monthly will at least be sprayed three times, and a protection period will at least be sprayed ten times, so be easy for making disease
Develop immunity to drugs, while Chinese herbal medicine each component is easily accumulated on green plants, it is possible to create other injurious effects.Compare therewith
Compared with, in bactericide of the present invention, Herba Andrographitis and radix scutellariae serve the effect of stabilizer, and the chemicals for using different from the past
The mankind will not have a negative impact by matter, the chemical property of the Simultaneous Stabilization present invention, prevent interference by such as insect and
Produce denaturation and then affect drug effect.In addition, also contain betel nut magnolia obovata in the present invention, both are caused after using with proportion
Pathogenic cells loss increases, and has further speeded up that pathogenic cells are dead, and this proportioning causes synergy rapidly substantially, and in the present invention three
Apply in individual month, method of application is extremely saved, prevent the waste of raw material.
Specific embodiment
Following examples are used for the present invention to be described, but are not limited to protection scope of the present invention.
Embodiment 1：A kind of green Chinese medicine composite bactericide
1st, raw material composition and parts by weight：Phytolacca acinosa 32kg, rheum officinale 39kg, radix scutellariae 32kg, honeysuckle 40kg, chaulmoogra 28kg, dew
Honeycomb 31kg, bark of official magnolia 29kg, betel nut 26kg, Herba Andrographitis 15kg, defoamer 29kg, drier 18kg, lubricant 18kg and water
90kg.
Wherein defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；Drier
1 is pressed for soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina：1：2：2 ratio is mixed；Lubricant is poly-
Ethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
2nd, preparation method：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 40min, after by immersion mixture in
120 DEG C boil 40min；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 35 DEG C, to be cooled complete in backward concentrate by
Required ratio is added defoamer, drier and lubricant and also has water, uniform stirring 30min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 55 DEG C
20h.Bactericide needed for obtaining by after the completion of waiting to ferment.
Embodiment 2：A kind of green Chinese medicine composite bactericide
1st, raw material composition and parts by weight：Phytolacca acinosa 43kg, rheum officinale 28kg, radix scutellariae 45kg, honeysuckle 28kg, chaulmoogra 41kg, dew
Honeycomb 20kg, bark of official magnolia 39kg, betel nut 18kg, Herba Andrographitis 26kg, defoamer 18kg, drier 29kg, lubricant 12kg and water
120kg.
Wherein defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；Drier
1 is pressed for soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina：1：2：2 ratio is mixed；Lubricant is poly-
Ethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
2nd, preparation method：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 60min, after by immersion mixture in
100 DEG C boil 50min；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 25 DEG C, to be cooled complete in backward concentrate by
Required ratio is added defoamer, drier and lubricant and also has water, uniform stirring 40min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 45 DEG C
30h.Bactericide needed for obtaining by after the completion of waiting to ferment..
Embodiment 3：A kind of green Chinese medicine composite bactericide
1st, raw material composition and parts by weight：Phytolacca acinosa 34kg, rheum officinale 36kg, radix scutellariae 35kg, honeysuckle 37kg, chaulmoogra 32kg, dew
Honeycomb 28kg, bark of official magnolia 33kg, betel nut 24kg, Herba Andrographitis 18kg, defoamer 27kg, drier 20kg, lubricant 16kg and water
100kg.
Wherein defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；Drier
1 is pressed for soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina：1：2：2 ratio is mixed；Lubricant is poly-
Ethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
2nd, preparation method：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 40min, after by immersion mixture in
100 DEG C boil 40min；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 25 DEG C, to be cooled complete in backward concentrate by
Required ratio is added defoamer, drier and lubricant and also has water, uniform stirring 30min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 45 DEG C
20h.Bactericide needed for obtaining by after the completion of waiting to ferment.
Embodiment 4：A kind of green Chinese medicine composite bactericide
1st, raw material composition and parts by weight：Phytolacca acinosa 40kg, rheum officinale 30kg, radix scutellariae 39kg, honeysuckle 32kg, chaulmoogra 37kg, dew
Honeycomb 23kg, bark of official magnolia 38kg, betel nut 21kg, Herba Andrographitis 23kg, defoamer 20kg, drier 27kg, lubricant 13kg and water
110kg.
Wherein defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；Drier
1 is pressed for soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina：1：2：2 ratio is mixed；Lubricant is poly-
Ethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
2nd, preparation method：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 60min, after by immersion mixture in
120 DEG C boil 50min；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 35 DEG C, to be cooled complete in backward concentrate by
Required ratio is added defoamer, drier and lubricant and also has water, uniform stirring 40min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 55 DEG C
30h.Bactericide needed for obtaining by after the completion of waiting to ferment.
Embodiment 5：A kind of green Chinese medicine composite bactericide
1st, raw material composition and parts by weight：Phytolacca acinosa 36kg, rheum officinale 33kg, radix scutellariae 37kg, honeysuckle 35kg, chaulmoogra 36kg, dew
Honeycomb 26kg, bark of official magnolia 36kg, betel nut 22kg, Herba Andrographitis 20kg, defoamer 25kg, drier 24kg, lubricant 15kg and water
107kg.
Wherein defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；Drier
1 is pressed for soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina：1：2：2 ratio is mixed；Lubricant is poly-
Ethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
2nd, preparation method：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 45min, after by immersion mixture in
105 DEG C boil 43min；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 32 DEG C, to be cooled complete in backward concentrate by
Required ratio is added defoamer, drier and lubricant and also has water, uniform stirring 37min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 52 DEG C
27h.Bactericide needed for obtaining by after the completion of waiting to ferment.
Embodiment 6：A kind of green Chinese medicine composite bactericide
1st, raw material composition and parts by weight：Phytolacca acinosa 35kg, rheum officinale 32kg, radix scutellariae 37kg, honeysuckle 35kg, chaulmoogra 35kg, dew
Honeycomb 26kg, bark of official magnolia 35kg, betel nut 22kg, Herba Andrographitis 20kg, defoamer 25g, drier 23kg, lubricant 14kg and water
105kg.
Wherein defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；Drier
1 is pressed for soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina：1：2：2 ratio is mixed；Lubricant is poly-
Ethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
2nd, preparation method：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 50min, after by immersion mixture in
110 DEG C boil 45min；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 30 DEG C, to be cooled complete in backward concentrate by
Required ratio is added defoamer, drier and lubricant and also has water, uniform stirring 35min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 50 DEG C
25h.Bactericide needed for obtaining by after the completion of waiting to ferment.
Application example：
The above embodiment of the present invention 1-6 is diluted 300～500 times, while it is commonly used in afforestation project to purchase tradition
45% lime sulfur of bactericide crystallizes 300～500 times of liquid of 300～500 times of liquid and the mixture of sulphur more than 40%, respectively as 1 He of reference examples
Reference examples 2, are spraying on emphasis disease happening part on green plants, are contrasting prevention effect with this.The target that this experiment is used
Mark disease is blossom rot, withes broom and epidemic disease, and concrete prevention effect index is shown in Table 1, table 2 and table 3 respectively：
This experiment is located at Nanning City South Lake Park southwest region piece green plants close quarters, and experimental design is 8 cells, per
About 15 square metres of individual cell, does not set repetition.Investigation bactericide is in the situation of change for spraying before and after's disease twice.
Table 1：Bactericide of the present invention and contrast preventive effect of the conventional sterilants to blossom rot
It is known that bactericide of the present invention has reached 87.62% to the average preventive effect of blossom rot by 1 data of observation table, its effect
The average preventive effect 60.52% of two reference examples is better than, 27.1% is higher by, this explanation bactericide of the present invention is to common green plants
Contrasting traditional chemical agent for using in the preventing and treating of disease blossom rot has prominent effect, and this experiment is in the trimestral time
Inside once sprayed, illustrated that comparing traditional chemical bactericide preventive effect of the present invention stablizes, the resistance to the action of a drug to blossom rot is little.
Table 2：Bactericide of the present invention and contrast preventive effect of the conventional sterilants to withes broom
It is known that bactericide of the present invention has reached 88.39% to the average preventive effect of withes broom by 1 data of observation table, its effect
The average preventive effect 60.65% of two reference examples is better than, 27.75% is higher by, this explanation bactericide of the present invention is being planted to common greening
Contrasting traditional chemical agent for using in the preventing and treating of thing disease withes broom has prominent effect, and this experiment is when trimestral
In once sprayed, illustrate to compare traditional chemical bactericide preventive effect of the present invention stably, the resistance to the action of a drug to withes broom is little.
Table 3：Bactericide of the present invention and contrast preventive effect of the conventional sterilants to epidemic disease
It is known that bactericide of the present invention has reached 88.52% to the average preventive effect of epidemic disease by 1 data of observation table, its effect will
It is better than the average preventive effect 62.23% of two reference examples, is higher by 26.29%, this explanation bactericide of the present invention is to common green plants
Contrasting the chemical agent that uses of tradition in the preventing and treating of disease epidemic disease has a prominent effect, and this experiment is within the trimestral time
Once sprayed, illustrated that comparing traditional chemical bactericide preventive effect of the present invention stablizes, the resistance to the action of a drug to epidemic disease is little.
From the point of view of the experimental data of comprehensive three above list, the embodiment of the present invention 6 is prevented to blossom rot, withes broom and epidemic disease
Effect is the peak value of respective list preventive effect, and this can illustrate that embodiment 6 is highly preferred technical scheme of the invention.The present invention is not
Only it is limited to have preventive effect to powdery mildew, anthracnose and rust etc., to common disease such as blossom rot in other afforestation projects, coal is dirty
Disease has the similar effect for being usually used in green plants chemical bactericide better than tradition with withes broom etc..
Although, general explanation, specific embodiment and test has above been used, the present invention has been made to retouch in detail
State, but on the basis of the present invention, it can be made some modifications or improvements, this is apparent to those skilled in the art
's.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, belong to claimed
Scope.
Claims (6)
1. a kind of green Chinese medicine composite bactericide, it is characterised in that the bactericide is made up of following raw material：Phytolacca acinosa, rheum officinale, Huang
Siberian cocklebur, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut, Herba Andrographitis, defoamer, drier, lubricant and water；
The defoamer is that natural oil, modified polyorganosiloxane and higher alcohols press 1：2：1 ratio is mixed；
The drier is that soda lime, anhydrous cupric sulfate, phosphorus pentoxide and activated alumina press 1：1：2：2 ratio mixing and
Into；
The lubricant is that polyethylene glycol and sldium lauryl sulfate press 1：1 ratio is mixed.
2. a kind of green Chinese medicine composite bactericide according to claim 1, it is characterised in that the bactericide is by following heavy
Amount number raw material is made：Phytolacca acinosa 32-43 parts, rheum officinale 28-39 parts, radix scutellariae 32-45 part, honeysuckle 28-40 parts, chaulmoogra 28-41
Part, nidus vespae 20-31 parts, bark of official magnolia 29-39 part, betel nut 18-26 parts, Herba Andrographitis 15-26 parts, defoamer 18-29 parts, drier
18-29 parts, lubricant 12-18 parts and water 90-120 parts.
3. a kind of green Chinese medicine composite bactericide according to claim 1, it is characterised in that the bactericide is by following heavy
Amount number raw material is made：Phytolacca acinosa 34-40 parts, rheum officinale 30-36 parts, radix scutellariae 35-39 part, honeysuckle 32-37 parts, chaulmoogra 32-37
Part, nidus vespae 23-28 parts, bark of official magnolia 33-38 part, betel nut 21-24 parts, Herba Andrographitis 18-23 parts, defoamer 20-27 parts, drier
20-27 parts, lubricant 13-16 parts and water 100-110 parts.
4. a kind of green Chinese medicine composite bactericide according to claim 1, it is characterised in that the bactericide is by following heavy
Amount number raw material is made：36 parts of Phytolacca acinosa, 33 parts of rheum officinale, 37 parts of radix scutellariae, 35 parts of honeysuckle, 36 parts of chaulmoogra, 26 parts of nidus vespae, thickness
107 parts of 36 parts of Piao, 22 parts of betel nut, 20 parts of Herba Andrographitis, 25 parts of defoamer, 24 parts of drier, 15 parts of lubricant and water.
5. a kind of green Chinese medicine composite bactericide according to claim 1, it is characterised in that the bactericide is by following heavy
Amount number raw material is made：35 parts of Phytolacca acinosa, 32 parts of rheum officinale, 37 parts of radix scutellariae, 35 parts of honeysuckle, 35 parts of chaulmoogra, 26 parts of nidus vespae, thickness
105 parts of 35 parts of Piao, 22 parts of betel nut, 20 parts of Herba Andrographitis, 25 parts of defoamer, 23 parts of drier, 14 parts of lubricant and water.
6. a kind of preparation method of green Chinese medicine composite bactericide according to any one of claim 1-5, it is characterised in that bag
Include following steps：
（1）Pretreatment of raw material：Gather fresh Phytolacca acinosa, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae, the bark of official magnolia, betel nut and wear
Heart lotus, is cleaned removal of impurities；
（2）Crush, mixing：By step（1）Through the Phytolacca acinosa of over cleaning removal of impurities, rheum officinale, radix scutellariae, honeysuckle, chaulmoogra, nidus vespae,
The bark of official magnolia, betel nut and Herba Andrographitis fine crushing, then mixing for standby use；
（3）Soak, boil：By step（2）Obtained mixed powder minces and soaks 40-60min, after will immersion mixture
40-50min is boiled in 100-120 DEG C；
（4）Cooling, filtration：Will（4）In boil the concentrate of rear gained and be cooled to 25-35 DEG C, to be cooled complete backward concentrate
In add defoamer, drier and lubricant by required ratio and also have water, uniform stirring 30-40min；
（5）Filter, ferment：Will（5）Middle gained mixed liquor is filtered, and removes filter residue, and then filtered fluid ferments in 45-55 DEG C
20-30h, after the completion of waiting to ferment by needed for bactericide.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107549217A (en) * | 2017-09-26 | 2018-01-09 | 安徽徽大农业有限公司 | A kind of vegetable cultivation green composite bactericide and preparation method thereof |
| CN108633928A (en) * | 2018-04-24 | 2018-10-12 | 弘大鼎业(武汉)科技有限公司 | One Plant Extracts sterilization bacteriostat stoste and preparation method thereof |
| CN111631232A (en) * | 2020-07-07 | 2020-09-08 | 南京慧博生物科技有限公司 | Plant bactericide containing coptis chinensis and rheum officinale and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1045908A (en) * | 1989-03-31 | 1990-10-10 | 周厚德 | The Chinese herbal medicine and the production method thereof of control orange tree foot rot and gummosis |
| CN1433694A (en) * | 2002-01-25 | 2003-08-06 | 田险峰 | Nuisance-free/Lufeng ecological pesticide |
| CN105145664A (en) * | 2014-05-29 | 2015-12-16 | 天津市蓟县江源红苗木种植专业合作社 | Nursery stock biopesticide and preparation method thereof |
-
2016
- 2016-11-01 CN CN201610932981.2A patent/CN106490038A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1045908A (en) * | 1989-03-31 | 1990-10-10 | 周厚德 | The Chinese herbal medicine and the production method thereof of control orange tree foot rot and gummosis |
| CN1433694A (en) * | 2002-01-25 | 2003-08-06 | 田险峰 | Nuisance-free/Lufeng ecological pesticide |
| CN105145664A (en) * | 2014-05-29 | 2015-12-16 | 天津市蓟县江源红苗木种植专业合作社 | Nursery stock biopesticide and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107549217A (en) * | 2017-09-26 | 2018-01-09 | 安徽徽大农业有限公司 | A kind of vegetable cultivation green composite bactericide and preparation method thereof |
| CN108633928A (en) * | 2018-04-24 | 2018-10-12 | 弘大鼎业(武汉)科技有限公司 | One Plant Extracts sterilization bacteriostat stoste and preparation method thereof |
| CN111631232A (en) * | 2020-07-07 | 2020-09-08 | 南京慧博生物科技有限公司 | Plant bactericide containing coptis chinensis and rheum officinale and preparation method thereof |
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