CN106480740A - A kind of mosquito-proof antibacterial fabric fabric and preparation method thereof - Google Patents
A kind of mosquito-proof antibacterial fabric fabric and preparation method thereof Download PDFInfo
- Publication number
- CN106480740A CN106480740A CN201610873001.6A CN201610873001A CN106480740A CN 106480740 A CN106480740 A CN 106480740A CN 201610873001 A CN201610873001 A CN 201610873001A CN 106480740 A CN106480740 A CN 106480740A
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- Prior art keywords
- fiber
- fabric
- mosquito
- microcapsule
- proof
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000004744 fabric Substances 0.000 title claims abstract description 100
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title abstract description 5
- 239000000835 fiber Substances 0.000 claims abstract description 115
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 72
- 239000003094 microcapsule Substances 0.000 claims abstract description 71
- 238000000034 method Methods 0.000 claims abstract description 67
- 230000008569 process Effects 0.000 claims abstract description 61
- 150000001450 anions Chemical group 0.000 claims abstract description 29
- 229920000297 Rayon Polymers 0.000 claims abstract description 25
- 239000004753 textile Substances 0.000 claims abstract description 21
- 238000005406 washing Methods 0.000 claims abstract description 21
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 17
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 17
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 17
- 239000011425 bamboo Substances 0.000 claims abstract description 17
- 229920000049 Carbon (fiber) Polymers 0.000 claims abstract description 16
- 229920002101 Chitin Polymers 0.000 claims abstract description 16
- 239000004917 carbon fiber Substances 0.000 claims abstract description 16
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 15
- 210000002268 wool Anatomy 0.000 claims abstract description 15
- 239000003814 drug Substances 0.000 claims abstract description 14
- 244000068988 Glycine max Species 0.000 claims abstract description 13
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 13
- 244000082204 Phyllostachys viridis Species 0.000 claims abstract 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 81
- 238000003756 stirring Methods 0.000 claims description 45
- 239000003921 oil Substances 0.000 claims description 44
- 239000000203 mixture Substances 0.000 claims description 43
- 239000000341 volatile oil Substances 0.000 claims description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 108010010803 Gelatin Proteins 0.000 claims description 27
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 27
- 239000008273 gelatin Substances 0.000 claims description 27
- 229920000159 gelatin Polymers 0.000 claims description 27
- 235000019322 gelatine Nutrition 0.000 claims description 27
- 235000011852 gelatine desserts Nutrition 0.000 claims description 27
- 239000000843 powder Substances 0.000 claims description 26
- 244000166124 Eucalyptus globulus Species 0.000 claims description 22
- 229910021536 Zeolite Inorganic materials 0.000 claims description 22
- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 22
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 22
- 239000010457 zeolite Substances 0.000 claims description 22
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 21
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 21
- 229920000742 Cotton Polymers 0.000 claims description 18
- 239000004902 Softening Agent Substances 0.000 claims description 18
- 239000002131 composite material Substances 0.000 claims description 18
- 230000001804 emulsifying effect Effects 0.000 claims description 18
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 15
- 230000001112 coagulating effect Effects 0.000 claims description 14
- 239000000725 suspension Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 13
- 239000003599 detergent Substances 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- 239000004793 Polystyrene Substances 0.000 claims description 9
- 239000011230 binding agent Substances 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 239000002270 dispersing agent Substances 0.000 claims description 9
- 239000006185 dispersion Substances 0.000 claims description 9
- 239000012153 distilled water Substances 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 9
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- 229920002223 polystyrene Polymers 0.000 claims description 9
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- 230000001442 anti-mosquito Effects 0.000 claims description 4
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- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 2
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- 239000004490 capsule suspension Substances 0.000 claims 2
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 240000007594 Oryza sativa Species 0.000 claims 1
- 235000007164 Oryza sativa Nutrition 0.000 claims 1
- 239000000077 insect repellent Substances 0.000 claims 1
- 235000009566 rice Nutrition 0.000 claims 1
- 241000255925 Diptera Species 0.000 abstract description 16
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- 238000005516 engineering process Methods 0.000 abstract description 4
- 206010067482 No adverse event Diseases 0.000 abstract description 3
- 230000000172 allergic effect Effects 0.000 abstract description 3
- 208000010668 atopic eczema Diseases 0.000 abstract description 3
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 239000002775 capsule Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 33
- 241001330002 Bambuseae Species 0.000 description 13
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 8
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 8
- 239000002245 particle Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 229920000768 polyamine Polymers 0.000 description 7
- 239000004698 Polyethylene Substances 0.000 description 5
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- 206010003399 Arthropod bite Diseases 0.000 description 4
- 241000699670 Mus sp. Species 0.000 description 4
- 108010073771 Soybean Proteins Proteins 0.000 description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 4
- 150000004767 nitrides Chemical class 0.000 description 4
- 229920000728 polyester Polymers 0.000 description 4
- 235000019710 soybean protein Nutrition 0.000 description 4
- 229910052719 titanium Inorganic materials 0.000 description 4
- 239000010936 titanium Substances 0.000 description 4
- 239000004408 titanium dioxide Substances 0.000 description 4
- 239000011787 zinc oxide Substances 0.000 description 4
- 235000004692 Eucalyptus globulus Nutrition 0.000 description 3
- 241000283898 Ovis Species 0.000 description 2
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
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- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
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Abstract
The present invention relates to a kind of mosquito-proof antibacterial fabric fabric and preparation method thereof, it is 10 15% viscose anion function fibers, 10 15% soybean fibers, 20 30% flaxen fibers, 5 10% wool fibers, 5 10% nanometer bamboo carbon fibers, 10 15% chitin fibers, 2 5% nano-silver ionic fibers, 4 6% anti UV finishing agent and 2 4% anophelifuge finishing agents that described textile fabric includes percentage by weight；Preparation technology flow process is：Using microcapsule technology by anophelifuge capsule of nano, textile fabric mosquito proof arranges, forms mosquito proof medicine film by low temperature sticking agent in fabric face, is dehydrated, bakes, finally obtaining mosquito-proof antibacterial fabric fabric.Mosquito-proof antibacterial fabric fabric through present invention application, has to mosquito and quickly knocks down the effect of killing, mosquito-proof effect reaches 99%；To the outward appearance of fabric, strongly, the physical index such as hygroscopicity has no adverse effects；After washing 30 times, still there is good mosquito proof effect；Mosquito proof finish fabric is non-stimulated to skin, no allergic phenomena, safe to the human body, nontoxic, comfortable and easy to wear.
Description
Technical field
The present invention relates to field of fabric producing technology, more particularly, to a kind of mosquito-proof antibacterial fabric fabric and preparation method thereof.
Background technology
Textile fabric is mainly used for making home textile and clothing or medical textile, and its species is a lot.Need with market
The variation asked, the feature of fabric is also increasingly subject to people's attention.Improve constantly with living standard, people are to clothing
The functional requirement more and more higher of fabric, in addition to requiring clothing and having normal heat-preserving function, also will require to have to prevent mosquito
The effect bitten, with the summer being in sweltering heat, mosquito bite phenomenon has allowed child adult to be caught unprepared.After mosquito bite
Light then red swelling of the skin, heavy then infect disease, have a strong impact on daily life.Thus develop a kind of woven face preventing mosquito bite
Material is the engineering of a kind of great market and social benefit.
According to data introduction, World Health Organization (WHO) advocates with insecticide Impregnated Mosquito Nets, and fabric can be made to have parasite killing or anthelmintic
Function.Through for many years it was verified that typically all obtaining good effect.But after processing, the persistency of anophelifuge is weaker,
Therefore, a kind of research and development textile that is mosquito-proof and having bacteriostasis that mosquito-proof effect is good and effect is lasting has become at present urgently
The problem solving.
Content of the invention
For solving above-mentioned technical problem, the invention provides a kind of mosquito-proof antibacterial fabric fabric and preparation method thereof.Warp
The mosquito-proof antibacterial fabric fabric of present invention application, has to mosquito and quickly knocks down the effect of killing, mosquito-proof effect reaches 99%；Right
The outward appearance of fabric, strongly, the physical index such as hygroscopicity has no adverse effects；After washing 30 times, still there is good mosquito proof effect；
Mosquito proof finish fabric is non-stimulated to skin, no allergic phenomena, safe to the human body, nontoxic, comfortable and easy to wear.
For reaching this purpose, present invention employs technical scheme below：
In a first aspect, the invention provides a kind of mosquito-proof antibacterial fabric fabric, described textile fabric includes weight hundred
Divide ratio for 10-15% viscose anion function fiber, 10-15% soybean fiber, 20-30% flaxen fiber, 5-10% Pilus Caprae seu Oviss
Fiber, 5-10% nanometer bamboo carbon fiber, 10-15% chitin fiber, 2-5% nano-silver ionic fiber, 4-6% anti UV finishing
Agent and 2-4% anophelifuge finishing agent；
The mosquito-proof medicine of described antimosquito finishing agent is Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and to Meng alkane -3,
8- glycol presses 1-5:3-10:1-5:3-7:The mixture of the mass ratio of 8-12.
According to the present invention, content in textile fabric for the described viscose anion function fiber is 10-15%, for example may be used
To be 10%, 11%, 12%, 13%, 14% or 15%；Content in textile fabric for the described soybean fiber is 10-
15%, can be for example 10%, 11%, 12%, 13%, 14% or 15%；Content in textile fabric for the described flaxen fiber
For 20-30%, for example, can be 20%, 21%, 22%, 23%, 24%, 25%, 26%, 28% or 30%；Described Pilus Caprae seu Oviss are fine
Content in textile fabric for the dimension is 5-10%, for example, can be 5%, 6%, 7%, 8%, 9% or 10%；Described nano bamboo
Content in textile fabric for the Carbon fibe is 5-10%, for example, can be 5%, 6%, 7%, 8%, 9% or 10%；Described first
Content in textile fabric for the shell cellulose fiber be 10-15%, can be for example 10%, 11%, 12%, 13%, 14% or
15%；Content in textile fabric for the described nano-silver ionic fiber be 2-5%, can be for example 2%, 3%, 4% or
5%；Content in textile fabric for the described anti UV finishing agent is 4-6%, for example, can be 4%, 4.5%, 5% or 6%；
Content in textile fabric for the described anophelifuge finishing agent is 2-4%, for example, can be 2%, 2.5%, 3% or 4%.
According to the present invention, described mosquito-proof medicine is Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and to Meng alkane -3,8-
Glycol presses 1-5:3-10:1-5:3-7:The mixture of the mass ratio of 8-12；Described Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and the mass ratio to Meng's alkane -3,8- glycol are 1-5:3-10:1-5:3-7:8-12, for example, can be 1:3:1:3:8、2:4:3:
6:9、4:3:1:5:10、5:5:1:7:12、2:6:2:7:8、2:4:2:3:8、1:7:2:7:11、3:6:2:5:9、2:4:3:6:
12、2:7:2:5:8、1:4:1:7:8、5:10:2:4:8、1:6:5:7:9 or 5:10:1:7:12, preferably 1-3:5-8:1-4:5-
7:10-12, more preferably 1:3:1:3:8.
The present invention is by using by Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder with Meng's alkane -3,8- glycol formed
Mosquito-proof medicine, it is compared using for single each component, and said composition each group has synergistic function between dividing, its energy
Enough make textile fabric have preferably mosquito-proof effect, and persistency is higher.
Second aspect, present invention also offers a kind of preparation side of mosquito-proof as described in relation to the first aspect antibacterial fabric fabric
Method, methods described comprises the steps：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously,
Add dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming,
High speed doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40-45 DEG C,
Washing 10-15min；
(6) anti UV finishing agent, anophelifuge finishing agent is added to be dipped through the cloth 30-70 minute that step (5) was processed, so
Bake at 70-80 DEG C more afterwards, last heat treatment；
(7) check whether fabric is qualified, qualified is then finished product.
According to the present invention, the preparation method of described anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, molten in 50 DEG C of water-baths
Solution completely, prepares gelatin, glycerol, beta-schardinger dextrin-solution；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and 1-3 is pressed to Meng's alkane -3,8- glycol:5-8:1-4:5-7:The mixture of the mass ratio of 10-12, in high shear force dispersion and emulsion
Machine is emulsified, and rotating speed is 4000r/min, and emulsification times are 10min；Emulsifying terminates the acetum regulation system of rear Deca 10%
PH value be 4.5-5.0, rotating speed be 2500r/min under the conditions of again coagulate 15min, formed microcapsule suspensions；After the completion of coagulating again, will
Microcapsule suspensions are placed in -20 DEG C of constant temperature low-temp reaction bath, lower the temperature while stirring, and mixing speed is 2500r/min, treats molten
When liquid temp is down to 5 DEG C, adding 10% sodium hydroxide solution to adjust to pH is 9.0, stir process 20min；Add the many second of 5-9ml
Alkene polyamines, stir process 20-25min, then move on in 45-48 DEG C of water-bath, stir process 2h, is then 7000- in rotating speed
It is centrifuged 5min under the conditions of 7500r/min, take and dry under precipitation, room temperature, obtain composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
25-35g microcapsule is dissolved in 1L purified water, adds polystyrene 2-4g, make being dispersed in of uniform microcapsule whole
In reason liquid, add 50-150g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
Specifically, the preparation method of mosquito-proof antibacterial fabric fabric of the present invention comprises the following steps：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously,
Add dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming,
High speed doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40-45 DEG C,
Washing 10-15min；
(6) anti UV finishing agent, anophelifuge finishing agent is added to be dipped through the cloth 30-70 minute that step (5) was processed, so
Bake at 70-80 DEG C more afterwards, last heat treatment；
The preparation method of wherein said anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, molten in 50 DEG C of water-baths
Solution completely, prepares gelatin, glycerol, beta-schardinger dextrin-solution；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and 1-3 is pressed to Meng's alkane -3,8- glycol:5-8:1-4:5-7:The mixture of the mass ratio of 10-12, in high shear force dispersion and emulsion
Machine is emulsified, and rotating speed is 4000r/min, and emulsification times are 10min；Emulsifying terminates the acetum regulation system of rear Deca 10%
PH value be 4.5-5.0, rotating speed be 2500r/min under the conditions of again coagulate 15min, formed microcapsule suspensions；After the completion of coagulating again, will
Microcapsule suspensions are placed in -20 DEG C of constant temperature low-temp reaction bath, lower the temperature while stirring, and mixing speed is 2500r/min, treats molten
When liquid temp is down to 5 DEG C, adding 10% sodium hydroxide solution to adjust to pH is 9.0, stir process 20min；Add the many second of 5-9ml
Alkene polyamines, stir process 20-25min, then move on in 45-48 DEG C of water-bath, stir process 2h, is then 7000- in rotating speed
It is centrifuged 5min under the conditions of 7500r/min, take and dry under precipitation, room temperature, obtain composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
25-35g microcapsule is dissolved in 1L purified water, adds polystyrene 2-4g, make being dispersed in of uniform microcapsule whole
In reason liquid, add 50-150g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
(7) check whether fabric is qualified, qualified is then finished product.
Exemplarily, the preparation method of described mosquito-proof antibacterial fabric fabric is：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously,
Add dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming,
High speed doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40-45 DEG C,
Washing 10-15min；
(6) add anti UV finishing agent, anophelifuge finishing agent to be dipped through cloth that step (5) processed 70 minutes, then
Bake at 80 DEG C again, last heat treatment；
The preparation method of wherein said anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, molten in 50 DEG C of water-baths
Solution completely, prepares gelatin, glycerol, beta-schardinger dextrin-solution；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and to Meng's alkane -3,8- glycol press 1:3:1:3:The mixture of 8 mass ratio, emulsified in high shear force dispersion emulsifying machine, turn
Speed is 4000r/min, and emulsification times are 10min；The pH value that emulsifying terminates the acetum regulation system of rear Deca 10% is
5.0, rotating speed, for coagulating 15min again under the conditions of 2500r/min, forms microcapsule suspensions；After the completion of coagulating again, by microcapsule suspensions
It is placed in -20 DEG C of constant temperature low-temp reaction bath, lowers the temperature while stirring, mixing speed is 2500r/min, treats that solution temperature is down to 5
DEG C when, add 10% sodium hydroxide solution adjust to pH be 9.0, stir process 20min；Add 5-9ml polyethylene polyamine, stirring
Process 25min, then move on in 48 DEG C of water-baths, stir process 2h, then under the conditions of rotating speed is for 7500r/min, it is centrifuged 5min,
Take and dry under precipitation, room temperature, obtain composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
25g microcapsule is dissolved in 1L purified water, adds polystyrene 4g, make uniform microcapsule is dispersed in dressing liquid
In, add 150g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
(7) check whether fabric is qualified, qualified is then finished product.
Compared with prior art, the present invention at least has the advantages that：
Mosquito-proof antibacterial fabric fabric through present invention application, has to mosquito and quickly knocks down the effect of killing, mosquito-proof effect
Reach 99%；To the outward appearance of fabric, strongly, the physical index such as hygroscopicity has no adverse effects；Still have good after washing 30 times
Mosquito proof effect；Mosquito proof finish fabric is non-stimulated to skin, no allergic phenomena, safe to the human body, nontoxic, comfortable and easy to wear.
Specific embodiment
For ease of understanding the present invention, it is as follows that the present invention enumerates embodiment.Those skilled in the art are it will be clearly understood that described enforcement
Example is only to aid in understanding the present invention, is not construed as the concrete restriction to the present invention.
Embodiment 1
A kind of mosquito-proof antibacterial fabric fabric, including percentage by weight be 10% viscose anion function fiber, 10% big
Soybean protein fiber, 30% flaxen fiber, 10% wool fiber, 10% nanometer bamboo carbon fiber, 10% chitin fiber, 2% nanometer silver
Ion fiber, 4% anti UV finishing agent, 2% anophelifuge finishing agent；Wherein viscose anion function fiber adopts the multifilament of 120 denier,
And anion powder addition is 5% in viscose anion function fiber；The particle diameter of the nitride titanium of nanometer is 70nm；Anti UV finishing
Agent be by 40% zinc oxide, 40% titanium dioxide, 20% polyester master particle mix；Anophelifuge finishing agent is Bulbus Allii quintessence oil, eucalyptus globuluss
Leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and to Meng's alkane -3,8- glycol press 1:3:1:3:The mixture of 8 mass ratio.
Described mosquito-proof antibacterial fabric fabric, comprises the following steps：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously,
Add dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming,
High speed doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40 DEG C, washing
15min；
(6) add anti UV finishing agent, anophelifuge finishing agent to be dipped through cloth that step (5) processed 30 minutes, then
Bake at 70 DEG C again, last heat treatment；
The preparation method of described anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, molten in 50 DEG C of water-baths
Solution completely, prepares gelatin, glycerol, beta-schardinger dextrin-solution；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and to Meng's alkane -3,8- glycol press 1:3:1:3:The mixture of 8 mass ratio, emulsified in high shear force dispersion emulsifying machine, turn
Speed is 4000r/min, and emulsification times are 10min；The pH value that emulsifying terminates the acetum regulation system of rear Deca 10% is
4.5-5.0, rotating speed, for coagulating 15min again under the conditions of 2500r/min, forms microcapsule suspensions；After the completion of coagulating again, microcapsule is hanged
Supernatant liquid is placed in -20 DEG C of constant temperature low-temp reaction bath, lowers the temperature while stirring, and mixing speed is 2500r/min, treats that solution temperature drops
During to 5 DEG C, adding 10% sodium hydroxide solution to adjust to pH is 9.0, stir process 20min；Add 5ml polyethylene polyamine, stir
Mix process 20min, then move on in 45 DEG C of water-baths, stir process 2h, then it is centrifuged under the conditions of rotating speed is for 7500r/min
5min, takes and dries under precipitation, room temperature, obtains composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
25g microcapsule is dissolved in 1L purified water, adds polystyrene 4g, make uniform microcapsule is dispersed in dressing liquid
In, add 150g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
(7) check whether fabric is qualified, qualified is then finished product.
Embodiment 2
A kind of mosquito-proof antibacterial fabric fabric, including percentage by weight be 12% viscose anion function fiber, 12% big
Soybean protein fiber, 25% flaxen fiber, 8% wool fiber, 7% nanometer bamboo carbon fiber, 12% chitin fiber, 4% nanometer silver from
Subbundle, 5% anti UV finishing agent and 3% anophelifuge finishing agent；Wherein viscose anion function fiber adopts the multifilament of 120 denier,
And anion powder addition is 5% in viscose anion function fiber；The particle diameter of the nitride titanium of nanometer is 85nm；Anti UV finishing
Agent be by 40% zinc oxide, 40% titanium dioxide, 20% polyester master particle mix；Anophelifuge finishing agent is Bulbus Allii quintessence oil, eucalyptus globuluss
Leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and to Meng's alkane -3,8- glycol press 2:6:2:7:The mixture of 8 mass ratio.
Described mosquito-proof antibacterial fabric fabric, comprises the following steps：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously,
Add dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming,
High speed doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40 DEG C, washing
15min；
(6) add anti UV finishing agent, anophelifuge finishing agent to be dipped through cloth that step (5) processed 30 minutes, then
Bake at 70 DEG C again, last heat treatment；
The preparation method of described anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, molten in 50 DEG C of water-baths
Solution completely, prepares gelatin, glycerol, beta-schardinger dextrin-solution；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and to Meng's alkane -3,8- glycol press 2:6:2:7:The mixture of 8 mass ratio, emulsified in high shear force dispersion emulsifying machine, turn
Speed is 4000r/min, and emulsification times are 10min；The pH value that emulsifying terminates the acetum regulation system of rear Deca 10% is
5.0, rotating speed, for coagulating 15min again under the conditions of 2500r/min, forms microcapsule suspensions；After the completion of coagulating again, by microcapsule suspensions
It is placed in -20 DEG C of constant temperature low-temp reaction bath, lowers the temperature while stirring, mixing speed is 2500r/min, treats that solution temperature is down to 5
DEG C when, add 10% sodium hydroxide solution adjust to pH be 9.0, stir process 20min；Add 5ml polyethylene polyamine, at stirring
Reason 20min, then move on in 45 DEG C of water-baths, stir process 2h, then under the conditions of rotating speed is for 7500r/min, it is centrifuged 5min, take
Precipitation, dries under room temperature, obtains composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
28g microcapsule is dissolved in 1L purified water, adds polystyrene 4g, make uniform microcapsule is dispersed in dressing liquid
In, add 100g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
(7) check whether fabric is qualified, qualified is then finished product.
Embodiment 3
A kind of mosquito-proof antibacterial fabric fabric, including percentage by weight be 15% viscose anion function fiber, 15% big
Soybean protein fiber, 20% flaxen fiber, 5% wool fiber, 5% nanometer bamboo carbon fiber, 15% chitin fiber, 5% nanometer silver from
Subbundle, 6% anti UV finishing agent and 4% anophelifuge finishing agent；Wherein viscose anion function fiber adopts the multifilament of 120 denier,
And anion powder addition is 5% in viscose anion function fiber；The particle diameter of the nitride titanium of nanometer is 105nm；Uvioresistant is whole
Reason agent be by 40% zinc oxide, 40% titanium dioxide, 20% polyester master particle mix；Anophelifuge finishing agent be Bulbus Allii quintessence oil,
Eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and to Meng's alkane -3,8- glycol press 1:4:1:7:The mixture of 8 mass ratio.
Described mosquito-proof antibacterial fabric fabric, comprises the following steps：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously,
Add dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming,
High speed doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40 DEG C, washing
15min；
(6) add anti UV finishing agent, anophelifuge finishing agent to be dipped through cloth that step (5) processed 30 minutes, then
Bake at 70 DEG C again, last heat treatment；
The preparation method of described anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, molten in 50 DEG C of water-baths
Solution completely, prepares gelatin, glycerol, beta-schardinger dextrin-solution；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and to Meng's alkane -3,8- glycol press 1:4:1:7:The mixture of 8 mass ratio, emulsified in high shear force dispersion emulsifying machine, turn
Speed is 4000r/min, and emulsification times are 10min；The pH value that emulsifying terminates the acetum regulation system of rear Deca 10% is
4.5-5.0, rotating speed, for coagulating 15min again under the conditions of 2500r/min, forms microcapsule suspensions；After the completion of coagulating again, microcapsule is hanged
Supernatant liquid is placed in -20 DEG C of constant temperature low-temp reaction bath, lowers the temperature while stirring, and mixing speed is 2500r/min, treats that solution temperature drops
During to 5 DEG C, adding 10% sodium hydroxide solution to adjust to pH is 9.0, stir process 20min；Add 5ml polyethylene polyamine, stir
Mix process 20min, then move on in 45 DEG C of water-baths, stir process 2h, then it is centrifuged under the conditions of rotating speed is for 7500r/min
5min, takes and dries under precipitation, room temperature, obtains composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
25g microcapsule is dissolved in 1L purified water, adds polystyrene 4g, make uniform microcapsule is dispersed in dressing liquid
In, add 100g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
(7) check whether fabric is qualified, qualified is then finished product.
Embodiment 4
A kind of mosquito-proof antibacterial fabric fabric, including percentage by weight be 15% viscose anion function fiber, 15% big
Soybean protein fiber, 20% flaxen fiber, 10% wool fiber, 10% nanometer bamboo carbon fiber, 10% chitin fiber, 2% nanometer silver
Ion fiber, 4% anti UV finishing agent, 2% anophelifuge finishing agent；Wherein viscose anion function fiber adopts the multifilament of 120 denier,
And anion powder addition is 5% in viscose anion function fiber；The particle diameter of the nitride titanium of nanometer is 90nm；Anti UV finishing
Agent be by 40% zinc oxide, 40% titanium dioxide, 20% polyester master particle mix；Anophelifuge finishing agent is Bulbus Allii quintessence oil, eucalyptus globuluss
Leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and to Meng's alkane -3,8- glycol press 1:7:2:7:The mixture of 11 mass ratio.
Described mosquito-proof antibacterial fabric fabric, comprises the following steps：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously,
Add dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming,
High speed doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40 DEG C, washing
15min；
(6) add anti UV finishing agent, anophelifuge finishing agent to be dipped through cloth that step (5) processed 30 minutes, then
Bake at 70 DEG C again, last heat treatment；
The preparation method of described anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, molten in 50 DEG C of water-baths
Solution completely, prepares gelatin, glycerol, beta-schardinger dextrin-solution；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite
Powder and to Meng's alkane -3,8- glycol press 1:7:2:7:The mixture of 11 mass ratio, emulsified in high shear force dispersion emulsifying machine, turn
Speed is 4000r/min, and emulsification times are 10min；The pH value that emulsifying terminates the acetum regulation system of rear Deca 10% is
4.5, rotating speed, for coagulating 15min again under the conditions of 2500r/min, forms microcapsule suspensions；After the completion of coagulating again, by microcapsule suspensions
It is placed in -20 DEG C of constant temperature low-temp reaction bath, lowers the temperature while stirring, mixing speed is 2500r/min, treats that solution temperature is down to 5
DEG C when, add 10% sodium hydroxide solution adjust to pH be 9.0, stir process 20min；Add 5ml polyethylene polyamine, at stirring
Reason 20min, then move on in 45 DEG C of water-baths, stir process 2h, then under the conditions of rotating speed is for 7500r/min, it is centrifuged 5min, take
Precipitation, dries under room temperature, obtains composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
35g microcapsule is dissolved in 1L purified water, adds polystyrene 3g, make uniform microcapsule is dispersed in dressing liquid
In, add 50g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
(7) check whether fabric is qualified, qualified is then finished product.
Comparative example 1
Compared with Example 1, mosquito-proof medicine is only Bulbus Allii quintessence oil, other same as Example 1.
Comparative example 2
Compared with Example 1, mosquito-proof medicine is only eucalyptus leaf essential oil, other same as Example 1.
Comparative example 3
Compared with Example 1, mosquito-proof medicine is only Herba Artemisiae Annuae oil, other same as Example 1.
Comparative example 4
Compared with Example 1, mosquito-proof medicine is only zeolite powder, other same as Example 1.
Comparative example 5
Compared with Example 1, mosquito-proof medicine is only to Meng alkane -3,8- glycol, and other is same as Example 1.
Comparative example 6
Compared with Example 1, for Bulbus Allii quintessence oil with to Meng alkane -3,8- glycol presses 1 to mosquito-proof medicine:8 mass ratio is mixed
Close, other same as Example 1.
Comparative example 7
Compared with Example 1, mosquito-proof medicine is that eucalyptus leaf essential oil, Herba Artemisiae Annuae oil and zeolite powder press 3:1:3 mass ratio is mixed
Close, other same as Example 1.
The anophelifuge preparing fabric is cut the size of 1m × 1m, be divided into 7 equal portions, 1 part carries out mosquito-proof experiment, 2 parts
Hang respectively and be placed under room temperature condition, place 1,30 days respectively, carry out mosquito-proof experiment afterwards, 2 parts of anophelifuge fabric is existed respectively
The vent of air output 3m/s places 10 days (being equivalent to 2 years), 30 days (being equivalent to 5 years), carries out mosquito-proof experiment afterwards；2 parts points
Do not carry out clear water rinsing and detergent (10% sodium dodecyl benzene sulfonate aqueous solution) rinsing, carry out mosquito-proof experiment afterwards；
Mosquito-proof experiment be：
Fabric is through with white mice, the white mice of anti-mosquito cloth will have been worn and worn the fabric being to carry out mosquito-proof process
White mice be loaded on 24h in the same mosquito cage containing 30 mosquitoes and tested；Calculate mosquito-proof effect afterwards：(1- wears S=
Mosquito bite vestige A with anti-mosquito cloth white mice1The mosquito with the white mice of plant that/dress does not carry out mosquito-proof process
Bite vestige A0) × 100%.
Test result is as shown in table 1.
Table 1
By the above results as can be seen that the present invention is using by Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and right
Meng's alkane -3,8- glycol presses 1-5:3-10:1-5:3-7:As mosquito-proof medicine, it compares using single the mixture of the mass ratio of 8-12
For only each component, said composition each group has synergistic function between dividing, and it can make textile fabric have more preferably
Mosquito-proof effect, and persistency is higher.
Applicant states, the present invention illustrates detailed process equipment and the technological process of the present invention by above-described embodiment,
But the invention is not limited in above-mentioned detailed process equipment and technological process, that is, do not mean that the present invention has to rely on above-mentioned detailed
Process equipment and technological process could be implemented.Person of ordinary skill in the field it will be clearly understood that any improvement in the present invention,
The interpolation of the equivalence replacement to each raw material of product of the present invention and auxiliary element, selection of concrete mode etc., all fall within the present invention's
Within the scope of protection domain and disclosure.
Claims (6)
1. a kind of mosquito-proof antibacterial fabric fabric is it is characterised in that it is 10-15% that described textile fabric includes percentage by weight
Viscose anion function fiber, 10-15% soybean fiber, 20-30% flaxen fiber, 5-10% wool fiber, 5-10% receive
Rice bamboo carbon fiber, 10-15% chitin fiber, 2-5% nano-silver ionic fiber, 4-6% anti UV finishing agent and 2-4% anophelifuge
Finishing agent；
The mosquito-proof medicine of described antimosquito finishing agent is Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and to Meng alkane -3,8- two
1-5 pressed by alcohol:3-10:1-5:3-7:The mixture of the mass ratio of 8-12.
2. as claimed in claim 1 mosquito-proof antibacterial fabric fabric it is characterised in that described mosquito-proof medicine be Bulbus Allii quintessence oil,
Eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and 1-3 is pressed to Meng's alkane -3,8- glycol:5-8:1-4:5-7:The mixing of the mass ratio of 10-12
Thing.
3. as claimed in claim 1 or 2 the preparation method of mosquito-proof antibacterial fabric fabric it is characterised in that methods described bag
Include following steps：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously, add
Dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming, at a high speed
Doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40-45 DEG C, washing
10-15min；
(6) anti UV finishing agent, anophelifuge finishing agent is added to be dipped through the cloth 30-70 minute that step (5) was processed, Ran Houzai
Bake at 70-80 DEG C, last heat treatment；
(7) check whether fabric is qualified, qualified is then finished product.
4. method as claimed in claim 3 is it is characterised in that the preparation method of described anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, dissolved in 50 DEG C of water-baths
Entirely, gelatin, glycerol, beta-schardinger dextrin-solution are prepared；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and
1-3 is pressed to Meng's alkane -3,8- glycol:5-8:1-4:5-7:The mixture of the mass ratio of 10-12, under high shear force dispersion emulsifying machine
Emulsifying, rotating speed is 4000r/min, and emulsification times are 10min；Emulsifying terminates the pH of the acetum regulation system of rear Deca 10%
It is worth for 4.5-5.0, rotating speed is to coagulate 15min again under the conditions of 2500r/min, forms microcapsule suspensions；After the completion of coagulating again, by micro- glue
Capsule suspension is placed in -20 DEG C of constant temperature low-temp reaction bath, lowers the temperature while stirring, and mixing speed is 2500r/min, treats solution temperature
When degree is down to 5 DEG C, adding 10% sodium hydroxide solution to adjust to pH is 9.0, stir process 20min；Add the many ethylene of 5-9ml many
Amine, stir process 20-25min, then move on in 45-48 DEG C of water-bath, stir process 2h, is then 7000-7500r/ in rotating speed
It is centrifuged 5min under the conditions of min, take and dry under precipitation, room temperature, obtain composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
25-35g microcapsule is dissolved in 1L purified water, adds polystyrene 2-4g, make uniform microcapsule is dispersed in dressing liquid
In, add 50-150g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
5. the method according to claim 3 or 4 is it is characterised in that the method comprising the steps of：
(1) by viscose anion function fiber, wool fiber, nanometer bamboo carbon fiber, nano-silver ionic fiber mix homogeneously, add
Dispersant, binding agent, softening agent, through stirring, dry process；
(2) by soybean fiber, flaxen fiber, chitin fiber respectively hang oneself scutching cotton, dredge cotton process；
(3) the fiber drafting that will process through step (1) and (2), more successively through rove, spun yarn, automatic winding, yarn steaming, at a high speed
Doubling, double twisting process and obtain the imitative yarn of essence；
(4) using on plain weave, two, once twill or cassimere twill are weaved；
(5) 3% detergent and 2% softening agent is added to carry out washing process to clothes, water temperature controls at 40-45 DEG C, washing
10-15min；
(6) anti UV finishing agent, anophelifuge finishing agent is added to be dipped through the cloth 30-70 minute that step (5) was processed, Ran Houzai
Bake at 70-80 DEG C, last heat treatment；
The preparation method of wherein said anophelifuge finishing agent is：
The first step：Prepare microcapsule：
By 10.0g gelatin, 4.5g glycerol and 6g beta-schardinger dextrin-, add in 1000ml distilled water, dissolved in 50 DEG C of water-baths
Entirely, gelatin, glycerol, beta-schardinger dextrin-solution are prepared；
Take out 100-250ml gelatin, glycerol, beta-schardinger dextrin-solution, add Bulbus Allii quintessence oil, eucalyptus leaf essential oil, Herba Artemisiae Annuae oil, zeolite powder and
1-3 is pressed to Meng's alkane -3,8- glycol:5-8:1-4:5-7:The mixture of the mass ratio of 10-12, under high shear force dispersion emulsifying machine
Emulsifying, rotating speed is 4000r/min, and emulsification times are 10min；Emulsifying terminates the pH of the acetum regulation system of rear Deca 10%
It is worth for 4.5-5.0, rotating speed is to coagulate 15min again under the conditions of 2500r/min, forms microcapsule suspensions；After the completion of coagulating again, by micro- glue
Capsule suspension is placed in -20 DEG C of constant temperature low-temp reaction bath, lowers the temperature while stirring, and mixing speed is 2500r/min, treats solution temperature
When degree is down to 5 DEG C, adding 10% sodium hydroxide solution to adjust to pH is 9.0, stir process 20min；Add the many ethylene of 5-9ml many
Amine, stir process 20-25min, then move on in 45-48 DEG C of water-bath, stir process 2h, is then 7000-7500r/ in rotating speed
It is centrifuged 5min under the conditions of min, take and dry under precipitation, room temperature, obtain composite essential oil microcapsule；
Second step：Prepare composite essential oil microcapsule dressing agent：
25-35g microcapsule is dissolved in 1L purified water, adds polystyrene 2-4g, make uniform microcapsule is dispersed in dressing liquid
In, add 50-150g polyvinyl acetate, mix homogeneously obtains microcapsule dressing agent.
(7) check whether fabric is qualified, qualified is then finished product.
6. mosquito-prevention mosquito-repellent textile fabric according to claim 1 and 2 home textile articles for use, hygienic article, sports goods or
Application in health care.
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| CN201610873001.6A CN106480740A (en) | 2016-09-30 | 2016-09-30 | A kind of mosquito-proof antibacterial fabric fabric and preparation method thereof |
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|---|---|---|---|
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| CN106987961A (en) * | 2017-05-09 | 2017-07-28 | 南通薇星纺织科技有限公司 | A kind of fabric of antistatic ultraviolet light irradiation and preparation method thereof |
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| CN107435237A (en) * | 2017-08-23 | 2017-12-05 | 深睡（天津）科技发展有限公司 | A kind of preparation method of mosquito-proof antibacterial weaving face fabric |
| CN108221122B (en) * | 2018-01-13 | 2021-04-20 | 江苏业勤服饰有限公司 | Garment lining cloth with aromatic function and production method thereof |
| CN108221122A (en) * | 2018-01-13 | 2018-06-29 | 江苏业勤服饰有限公司 | A kind of dress lining cloth and its production method with aromatic function |
| CN109594333A (en) * | 2018-11-19 | 2019-04-09 | 湖州织里瑞茜服饰有限公司 | A kind of mosquito-proof antibacterial fabric fabric and preparation method thereof |
| CN111519309A (en) * | 2019-02-01 | 2020-08-11 | 普宁市国兴实业有限公司 | Moisture-absorbing sweat-releasing clean cotton fabric |
| CN112252041A (en) * | 2019-07-22 | 2021-01-22 | 新乡市护神特种织物有限公司 | Anti-mosquito knitted fabric and manufacturing method thereof |
| CN110656505A (en) * | 2019-09-03 | 2020-01-07 | 无锡德冠生物科技有限公司 | Biomass anti-mosquito and anti-mite finishing agent and preparation method thereof |
| CN110670362A (en) * | 2019-10-14 | 2020-01-10 | 苏州市韦普精纺科技有限公司 | Green nontoxic mosquito-proof fabric and preparation method thereof |
| CN112779644A (en) * | 2020-12-24 | 2021-05-11 | 陕西元丰纺织技术研究有限公司 | Temperature-adjusting antibacterial mosquito-proof yarn and fabric and preparation method thereof |
| CN113174759A (en) * | 2021-04-22 | 2021-07-27 | 南通欣颐家纺有限公司 | Preparation method of plant-derived slow-release mosquito-proof microcapsule |
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