CN106479536A - Rice straw charcoal production equipment and the technique for producing charcoal - Google Patents

Rice straw charcoal production equipment and the technique for producing charcoal Download PDF

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Publication number
CN106479536A
CN106479536A CN201610203771.XA CN201610203771A CN106479536A CN 106479536 A CN106479536 A CN 106479536A CN 201610203771 A CN201610203771 A CN 201610203771A CN 106479536 A CN106479536 A CN 106479536A
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China
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rice straw
charcoal
reaction vessel
cooler
temperature
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CN106479536B (en
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张玉虎
赵远
侯国军
杨泽平
孙辰鹏
潘韬
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Capital Normal University
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Capital Normal University
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
    • C10B53/02Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of cellulose-containing material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00Other carbonising or coking processes; Features of destructive distillation processes in general
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00Other carbonising or coking processes; Features of destructive distillation processes in general
    • C10B57/04Other carbonising or coking processes; Features of destructive distillation processes in general using charges of special composition
    • C10B57/06Other carbonising or coking processes; Features of destructive distillation processes in general using charges of special composition containing additives
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The invention discloses a kind of rice straw charcoal production equipment, including material feeding box, grinder, reaction vessel, discharging supply pipe, cracking case, stove, the first cooler, the second cooler.The present invention discloses a kind of technique for producing charcoal, first rice straw is entered material feeding box through charging aperture, enter back into grinder to be crushed, rice straw after crushing is entered through discharge valve and is processed in reaction vessel, after rice straw after process is cooled down through the first cooler, sending into cracking case by discharging supply pipe carries out Pintsch process, is then conveyed in stove and is carbonized, after rice straw after charing is cooled down through the second cooler, by discharge hole for discharge.Simple production process of the present invention, device therefor energy consumption are low, and cost is less than additive method more than 8%;With short production cycle, production process controllability is strong, and gained charcoal apparent specific gravity is big.

Description

Rice straw charcoal production equipment and the technique for producing charcoal
Technical field
The invention belongs to charcoal production equipment and process technical field, is related to a kind of life of rice straw charcoal Product equipment and the technique for producing charcoal.
Background technology
As crop yield is improved year by year, Rural Urbanization Development and life of farmers level are lifted further, Agricultural crop straw yield is dramatically increased, and at the same time, stalk progressively declines as the proportion of utilization of firewood, greatly The superfluous stalk abandoned of amount is in the edge of a field, roadside or irrigation canals and ditches, or burns in the edge of a field, to ecological environment and life, Property safety brings great hidden danger.China is main Rice Production country, produces substantial amounts of water every year Rice straw, rice straw are the byproducts that paddy rice shelling obtains gained after seed, the stalk after shelling and attachment Cured leaf becomes stalk, and most rice straw is arbitrarily abandoned and burned, and causes great environmental pollution, The quality of life of impact peasant, also results in the significant wastage of resource.
Charcoal be bio-organic materials (living beings) in anoxic or anoxybiotic environment, after high temperature pyrolysis The solid product of generation.The high-quality energy, soil conditioner is can not only be used for, also can be used as reducing agent, fertilizer Slow-released carrier and carbon dioxide sequestration agent etc., are widely used to carbon fixation and emission reduction, water source purifying, heavy metal and inhale Soil improvement etc. is echoed, can be that climate change, environmental pollution and soil function degeneration etc. is complete to a certain extent Ball hot issue deeply concerned provides solution.Charcoal can also improve agricultural productivity, reduce intensive to carbon The demand of fertilizer.The pore space structure of charcoal particle very easily assembles nutriment and beneficial microbe, so as to Make soil become fertile, beneficial to plant growth, realize while volume increase, allowing agricultural have more continuation.Still better It is that it is locked in carbon in biota, rather than allows it be discharged in the air.Biomass carbonated technology is generally acknowledged Solve the problems, such as one of possible technique measure of climate change, with raw material sources extensively, low production cost, Ecological safety, pollution-free, can the distinguishing feature such as spread.
It can be a kind of with carbon fixation and emission reduction with environmental area that the charcoal produced after biomass carbonated is applied to ecological Effectively carbon remittance technology, is combined with agriculture, forestry, it is possible to resolve agriculture and forestry organic waste material pollution and greenhouse gas emission Problem.Charcoal applies farmland, can be effectively improved soil physico-chemical property, increases crop yield, promotes agricultural Sustainable development.Charcoal is a kind of economically viable mode of fixing carbon dioxide, not only have cured trees With the carbon dioxide for having been absorbed in crop, its product " biological carbon " is stored in soil, thousand of years all without Change, while production regenerative resource, soil fertility is also improved, improve crop yield.Raw Thing charcoal can be embedded in discarded colliery, or in placing into the soil when cultivating.Charcoal landfill also helps improvement soil Earth drainage system, and 80% or so such as nitric oxide and methane isothermal chamber gas are sealed up for safekeeping in soil, resistance Stop which to be discharged in air.At present rice straw charcoal production equipment and for produce charcoal technique very Many, but high energy consumption, long the production cycle, production process poor controllability, cause gained charcoal apparent specific gravity little. Therefore work out a kind of energy consumption low, cycle is short, the big charcoal production equipment of gained charcoal apparent specific gravity and For the technique of charcoal is produced, there is important economic benefit and social value in association area.
State Intellectual Property Office's application number 200880013328.X application documents disclose one kind for producing biology The equipment of charcoal and technique, the equipment include:Reducing mechanism, heater, pressue device and cooling device, But the high energy consumption of this invention, the charcoal apparent specific gravity for obtaining are little.
Content of the invention
The technical problem to be solved:For current rice straw charcoal production equipment and for giving birth to The process energy consumption of generation charcoal is high, long the production cycle, and production process poor controllability causes charcoal to produce into This height, the drawbacks of gained charcoal apparent specific gravity is little, there is provided rice straw charcoal production equipment and be used for The technique of production charcoal, the equipment and process energy consumption are low, with short production cycle, and production process controllability is strong, Gained charcoal apparent specific gravity is big.
The present invention employs the following technical solutions realization, a kind of rice straw charcoal production equipment, including Material feeding box, grinder, reaction vessel, discharging supply pipe, cracking case, stove, the first cooler, second Cooler, the material feeding box are located above the grinder, and the material feeding box is provided with charging aperture, the crushing Disintegrating knife is provided with device, is connected by discharge valve between the grinder and reaction vessel, the reaction Container is provided with heater and pressue device, and the discharging supply pipe is connected between reaction vessel and stove, First cooler is located on the stove located at the outlet connection of the reaction vessel, the cracking case Face, the side wall of the stove are additionally provided with discharge nozzle, and second cooler is on discharge nozzle.
Preferably, pressure gauge is additionally provided with the reaction vessel.
Preferably, cracking case side wall is provided with argon inlet mouth.
Preferably, the discharging supply pipe is provided with tail gates near reaction vessel one end, and the other end is provided with brake application Door, is provided with charging quantity detection sensor in the discharging supply pipe at the upper lock gate position, described enter Doses detection sensor is used for detecting the inlet amount of cracking case, is examined with the tail gates, upper lock gate and inlet amount Survey sensor is connected and is provided with MCU, is connected with the MCU and is provided with display screen, and the MCU prestores cracking case and enters Doses preset data, the MCU is according to the inlet amount Data Control tail gates of charging quantity detection sensor collection Opening and closing with upper lock gate.
Preferably, the reaction vessel is additionally provided with temperature-detecting device, and the temperature-detecting device is arranged on instead Answer the exit of container, for detecting the reaction temperature in reaction vessel, the temperature-detecting device with described MCU is connected with heater.
Preferably, the cracking case is additionally provided with temp measuring system, and the temp measuring system includes that thermo detector and thermometric are visited Head, the temperature probe are deep in cracking case through the thermometer hole of cracking case, the outside and thermometric of temperature probe Meter connection.
Preferably, the cracking lower box part is additionally provided with tar catalyst chamber, is provided with tar in the tar catalyst chamber Catalyst.
Biological straw can produce tar in course of reaction and cracking process, and tar is piled up for a long time, can cause Pipeline blockage, the blackspot pollution environment of in addition tar gas splash, sooting, smell difficulty are smelt, and impact production is biological The quality of charcoal, it is nontoxic material that tar catalyst can convert tar.
Preferably, the stove exit is additionally provided with tar separator, is connected with the tar separator and is provided with Coke tar cracking room, is connected with the coke tar cracking room and is provided with tar exhausting waste gas pipeline.
Although being reacted through catalyst by cracking room product out, a small amount of tar is still had to deposit in stove , still affect product quality, by tar separator by tar separation out, be sent to coke tar cracking room pair Tar is made further cracking and is processed, and obtains nontoxic material.
The present invention discloses a kind of technique for producing charcoal, comprises the following steps,
1) water intaking rice straw is put in material feeding box through charging aperture, enters back into grinder, arrange rotating speed be 300~ 500r/min is crushed, and after the completion of crushing, the rice straw after crushing is introduced in reaction vessel through discharging To be reacted, obtained fused mass, pressure is 0.6~0.8Mpa in control reaction vessel, temperature is 160~ 180 DEG C, react 1~2h;
2) fused mass for obtaining is cooled to after room temperature through the first cooler, cracking is transported to by discharging supply pipe In case, at 1000~1200 DEG C, Pintsch process being carried out, while be passed through argon gas being protected, cracking 3~5h;
3) after the completion of waiting to crack, it is transported in stove, control temperature is 600~800 DEG C, carry out carbonizing 1~ 2h, is cooled to 23~25 DEG C through the second cooler, is discharged by discharge nozzle, that is, obtain rice straw charcoal.
Preferably, the technique for producing charcoal is comprised the following steps,
1) water intaking rice straw is put in material feeding box through charging aperture, enters back into grinder, and setting rotating speed is 400r/min Crushed, after the completion of crushing, the rice straw after crushing is introduced in reaction vessel through discharging, control is anti- It is 0.7Mpa to answer pressure in container, and temperature is 170 DEG C, reacts 1.5h;
2) fused mass for obtaining is cooled to after room temperature through the first cooler, cracking is transported to by discharging supply pipe In case, at 1100 DEG C, Pintsch process being carried out, while be passed through argon gas being protected, cracking 4h;
3) after the completion of waiting to crack, it is transported in stove, control temperature is 700 DEG C, carries out charing 1.5h, warp Second cooler is cooled to 24 DEG C, by discharge hole for discharge, that is, obtains rice straw charcoal.
Compared with other production active carbon method, Advantageous Effects are the present invention:
1) simple production process of the present invention, device therefor energy consumption are low, and cost is less than additive method more than 8%;
2) with short production cycle, production process controllability is strong, and gained charcoal apparent specific gravity is big.
Description of the drawings
Further illustrate with reference to the accompanying drawings and detailed description:
Fig. 1 is the structural representation of the rice straw charcoal production equipment of the embodiment of the present invention 1.
Fig. 2 is the structural representation of the rice straw charcoal production equipment of the embodiment of the present invention 2.
Fig. 3 is the structural representation of the rice straw charcoal production equipment of the embodiment of the present invention 3.
Fig. 4 is the frame principle figure that the upper and lower gate of the embodiment of the present invention 2 is opened and closed.
Specific embodiment
Embodiment 1
Fig. 1 gives one embodiment of the present invention, as shown in figure 1, a kind of life of rice straw charcoal Product equipment, including material feeding box 2, grinder 4, reaction vessel 6, discharging supply pipe 10, cracking case 11, fire Stove 12, the first cooler 9, the second cooler 13, the material feeding box 2 are located above the grinder 4, The material feeding box 2 is provided with charging aperture 1, is provided with Disintegrating knife 3 in the grinder 4, the grinder 4 with It is connected by discharge valve 5 between reaction vessel 6, the reaction vessel 6 is provided with heater 8 and pressurization Device, the discharging supply pipe 10 are connected between reaction vessel 6 and stove 12, first cooler 9 Located at the outlet connection of the reaction vessel 6, the cracking case 11 is located above the stove 12, institute The side wall for stating stove 12 is additionally provided with discharge nozzle 14, and second cooler 13 is on discharge nozzle 14.
Pressure gauge 7 is additionally provided with the reaction vessel 6.
The cracking 11 side wall of case is provided with argon inlet mouth.
Embodiment 2
Fig. 2 gives the 2nd embodiment of the present invention, as shown in Figure 2, Figure 4 shows, embodiment 2 and embodiment Unlike 1, the discharging supply pipe 10 is additionally provided with tail gates 15, the other end near 6 one end of reaction vessel Upper lock gate 16 is provided with, and inlet amount inspection is provided with the discharging supply pipe 10 at 16 position of the upper lock gate Sensor 17 is surveyed, the charging quantity detection sensor 17 is used for the inlet amount of cracking case 11 to be detected, and described Tail gates 15, upper lock gate 16 are connected with charging quantity detection sensor 17 and are provided with MCU18, with the MCU18 It is connected and display screen is provided with, the MCU18 prestores cracking 11 inlet amount preset data of case, the MCU18 root According to charging quantity detection sensor 17 gather inlet amount Data Control tail gates 15 and upper lock gate 16 open and Close.
The reaction vessel 6 is additionally provided with temperature-detecting device 19, and the temperature-detecting device 19 is arranged on reaction The exit of container 6, for detecting the reaction temperature in reaction vessel 6, the temperature-detecting device 19 with The MCU18 is connected with heater 8.
The cracking case 11 is additionally provided with temp measuring system, and the temp measuring system includes thermo detector and temperature probe, institute State temperature probe to be deep in cracking case 11 through the thermometer hole of cracking case 11, the outside and thermometric of temperature probe Meter connection.
Remaining is same as Example 1 for embodiment 2.
Embodiment 3
Fig. 3 gives the 3rd embodiment of the present invention, as shown in figure 3, embodiment 3 is with embodiment 2 not With cracking 11 bottom of case is additionally provided with tar catalyst chamber 21, is provided with the tar catalyst chamber 21 Tar catalyst.
12 exit of the stove is additionally provided with tar separator 23, is connected with the tar separator 23 and is provided with Coke tar cracking room 22, is connected with the coke tar cracking room 22 and is provided with tar exhausting waste gas pipeline.
Remaining is same as Example 2 for embodiment 3.
Embodiment 4
The present invention discloses a kind of technique for producing charcoal, comprises the following steps,
1) water intaking rice straw is put in material feeding box 2 through charging aperture 1, enters back into grinder 4, is arranged rotating speed and is 400r/min is crushed, and after the completion of crushing, the rice straw after crushing is introduced reaction vessel 6 through discharging In reacted, obtain fused mass, in control reaction vessel 6, pressure is 0.7Mpa, and temperature is 170 DEG C, Reaction 1.5h;
2) fused mass for obtaining is cooled to after room temperature through the first cooler 9, is conveyed by discharging supply pipe 10 To in cracking case 11, at 1100 DEG C, Pintsch process being carried out, while be passed through argon gas being protected, cracking 4h;
3) after the completion of waiting to crack, it is transported in stove 12, control temperature is 700 DEG C, carries out charing 1.5h, 24 DEG C are cooled to through the second cooler 13, discharge through discharge nozzle 14, that is, obtain rice straw charcoal.
Embodiment 5
A kind of technique for producing charcoal, comprises the following steps,
1) water intaking rice straw is put in material feeding box 2 through charging aperture 1, enters back into grinder 4, is arranged rotating speed and is 300r/min is crushed, and after the completion of crushing, the rice straw after crushing is introduced reaction vessel 6 through discharging In reacted, obtain fused mass, in control reaction vessel 6, pressure is 0.6Mpa, and temperature is 160 DEG C, Reaction 1h;
2) fused mass for obtaining is cooled to after room temperature through the first cooler 9, is conveyed by discharging supply pipe 10 To in cracking case 11, at 1000 DEG C, Pintsch process being carried out, while be passed through argon gas being protected, cracking 3h;
3) after the completion of waiting to crack, it is transported in stove 12, control temperature is 600 DEG C, carries out charing 1h, 23 DEG C are cooled to through the second cooler 13, discharge through discharge nozzle 14, that is, obtain rice straw charcoal.
Embodiment 6
A kind of technique for producing charcoal, comprises the following steps,
1) water intaking rice straw is put in material feeding box 2 through charging aperture 1, enters back into grinder 4, is arranged rotating speed and is 500r/min is crushed, and after the completion of crushing, the rice straw after crushing is introduced reaction vessel 6 through discharging In reacted, obtain fused mass, in control reaction vessel 6, pressure is 0.8Mpa, and temperature is 180 DEG C, Reaction 2h;
2) fused mass for obtaining is cooled to after room temperature through the first cooler 9, is conveyed by discharging supply pipe 10 To in cracking case 11, at 1200 DEG C, Pintsch process being carried out, while be passed through argon gas being protected, cracking 5h;
3) after the completion of waiting to crack, it is transported in stove 12, control temperature is 800 DEG C, carries out charing 2h, 25 DEG C are cooled to through the second cooler 13, discharge through discharge nozzle 14, that is, obtain rice straw charcoal.
Test example 1:Charcoal apparent specific gravity is determined
Charcoal that the embodiment of the present invention 4 obtain is taken respectively as experimental group and application number 200880013328.X The charcoal that obtains of invention as a control group, determine apparent specific gravity, the results are shown in Table 1.
1 charcoal apparent specific gravity of table
After measured, the apparent specific gravity of the charcoal that the present invention is obtained is 1.92-2.04, and application number The apparent specific gravity of the charcoal that the patent of invention of 200880013328.X is obtained is 1.2-1.38, and the present invention is obtained Charcoal apparent specific gravity apparently higher than the charcoal obtained with other production equipments and production method.
Test example 2:Charcoal physical characteristic is determined
The charcoal that relatively the present embodiment 4 is obtained and Wooden Biomass and the physical characteristic of coal coke, are as a result shown in Table 2.
2 charcoal physical characteristic of table and the other materials table of comparisons
Performance of the charcoal that the present invention is obtained in terms of hardness and inflammability is more superior.
By technique productions charcoal of the present invention, the charcoal of high rigidity and high heating value can be obtained, anti- Answer in container, by heating biological matter at a temperature of 160 to 180, as biomass material main become / mono- hemicellulose is pyrolyzed, and lignin keep its framework in the case of with consolidation effect phase interaction With enhancing intensity whereby.
Test example 3
Compare in the case of technique of the present invention for producing charcoal takes different parameter values and parameter value is not at this The charcoal physical characteristic obtained in the case of invention scope, the results are shown in Table 3.
3 charcoal physical characteristic of table
As can be seen from the table, change the present invention preparation technology parameter by the apparent specific gravity of charcoal and Calorific value has a huge impact, and only limits within the scope of the present invention, could obtain apparent specific gravity height, The high charcoal of calorific value.
Industrial applicibility
By using the charcoal production equipment and process of the present embodiment, efficiently can produce with high rigidity With the charcoal of golf calorific value, the charcoal can serve as the substitute of coal coke.Produced according to the present embodiment Charcoal can be used for the cupola furnace of cast iron or ironmaking or the thermal source in blast furnace, reducing agent etc., Yi Jiyong Make the material using high compression-strength charcoal.
Embodiment described above is only that the preferred embodiment of the present invention is described, not to the present invention's Scope is defined, and on the premise of without departing from design spirit of the present invention, those of ordinary skill in the art are to this Various modifications and improvement that the technical scheme of invention is made, all should fall into claims of the present invention determination In protection domain.

Claims (10)

1. a kind of rice straw charcoal production equipment, it is characterised in that including material feeding box (2), crush Device (4), reaction vessel (6), discharging supply pipe (10), cracking case (11), stove (12), First cooler (9), the second cooler (13), described material feeding box (2) are located at grinder (4) Above, described material feeding box (2) be provided with charging aperture (1), is provided with Disintegrating knife (3) in grinder (4), It is connected by discharge valve (5) between grinder (4) and reaction vessel (6), the reaction vessel (6) heater (8) and pressue device are provided with, and discharging supply pipe (10) are connected to reaction vessel (6) and stove (12) between, described first cooler (9) are located at the outlet of reaction vessel (6) Place, cracking case (11) are located at stove (12) above, and the side wall of stove (12) also sets There is discharge nozzle (14), described second cooler (13) are on discharge nozzle (14).
2. rice straw charcoal production equipment according to claim 1, it is characterised in that described anti- Answer and on container (6), be additionally provided with pressure gauge (7).
3. rice straw charcoal production equipment according to claim 1, it is characterised in that described split Solution case (11) side wall is provided with argon inlet mouth.
4. rice straw charcoal production equipment according to claim 1, it is characterised in that described go out Material conveying tube (10) is provided with tail gates (15) near reaction vessel (6) one end, and the other end is provided with upper lock gate (16), inlet amount inspection is provided with the discharging supply pipe (10) at upper lock gate (16) position Sensor (17) is surveyed, charging quantity detection sensor (17) is used for detecting the charging of cracking case (11) Amount, is connected with the tail gates (15), upper lock gate (16) and charging quantity detection sensor (17) and is provided with MCU (18), is connected with the MCU (18) and is provided with display screen (20), and MCU (18) prestore Cracking case (11) inlet amount preset data, MCU (18) are adopted according to charging quantity detection sensor (17) Inlet amount Data Control tail gates (15) of collection and the opening and closing of upper lock gate (16).
5. rice straw charcoal production equipment according to claim 4, it is characterised in that described anti- The exit of container (6) is answered to be additionally provided with temperature-detecting device (19), for detecting in reaction vessel (6) Reaction temperature, temperature-detecting device (19) are connected with the MCU (18) and heater (8).
6. rice straw charcoal production equipment according to claim 1, it is characterised in that described split Temp measuring system is additionally provided with solution case (11), the temp measuring system includes thermo detector and temperature probe, the survey The thermometer hole that temperature is popped one's head in through cracking case (11) is deep in cracking case (11), and temperature probe is outside and surveys Temperature meter connection.
7. rice straw charcoal production equipment according to claim 1, it is characterised in that described split Solution case (11) bottom is additionally provided with tar catalyst chamber (21), is provided with tar and urges in tar catalyst chamber (21) Agent.
8. rice straw charcoal production equipment according to claim 1, it is characterised in that the fire Stove (12) exit is additionally provided with tar separator (23), is connected with the tar separator (23) and is provided with Coke tar cracking room (22), is connected with coke tar cracking room (22) and is provided with tar exhausting waste gas pipeline.
9. a kind of technique for producing charcoal, it is characterised in that comprise the following steps,
1) water intaking rice straw is put in material feeding box (2) through charging aperture (1), enters back into grinder (4), if Put rotating speed to be crushed for 300~500r/min, after the completion of crushing, by the rice straw after crushing through discharging Be introduced in reaction vessel (6) and reacted, obtain fused mass, in control reaction vessel (6) pressure be 0.6~ 0.8Mpa, temperature are 160~180 DEG C, react 1~2h;
2) fused mass for obtaining is cooled to after room temperature through the first cooler (9), by discharging supply pipe (10) Be transported in cracking case (11), Pintsch process is carried out at 1000~1200 DEG C, while be passed through argon gas carrying out Protection, cracks 3~5h;
3) after the completion of waiting to crack, it is transported in stove (12), control temperature is 600~800 DEG C, carries out charcoal Change 1~2h, 23~25 DEG C are cooled to through the second cooler (13), discharged by discharge nozzle (14), obtain final product To rice straw charcoal.
10. the technique for producing charcoal according to claim 9, it is characterised in that the use Comprise the following steps in the technique of production charcoal,
1) water intaking rice straw is put in material feeding box (2) through charging aperture (1), enters back into grinder (4), if Put rotating speed to be crushed for 400r/min, after the completion of crushing, the rice straw after crushing is introduced through discharging anti- Answer in container (6), in control reaction vessel (6), pressure is 0.7Mpa, temperature is 170 DEG C, reacts 1.5h;
2) fused mass for obtaining is cooled to after room temperature through the first cooler (9), by discharging supply pipe (10) It is transported in cracking case (11), at 1100 DEG C, Pintsch process is carried out, while be passed through argon gas protected, Cracking 4h;
3) after the completion of waiting to crack, it is transported in stove (12), control temperature is 700 DEG C, carries out charing 1.5h, 24 DEG C are cooled to through the second cooler (13), are discharged by discharge nozzle (14), that is, obtain rice straw biological Charcoal.
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CN113265264A (en) * 2021-06-15 2021-08-17 河南省万禾企生物科技有限公司 Method for preparing straw biochar through low-temperature efficient carbonization

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CN110182782B (en) * 2019-06-04 2020-04-17 兰州大学 Environment-friendly device for preparing straw biochar by hydrothermal method
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