CN106473227A - A kind of cigarette preparation method for causing fragrant extract and using method - Google Patents
A kind of cigarette preparation method for causing fragrant extract and using method Download PDFInfo
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- CN106473227A CN106473227A CN201610885354.8A CN201610885354A CN106473227A CN 106473227 A CN106473227 A CN 106473227A CN 201610885354 A CN201610885354 A CN 201610885354A CN 106473227 A CN106473227 A CN 106473227A
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- Prior art keywords
- cigarette
- extract
- preparation
- dilution
- concentrate
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
Abstract
A kind of cigarette preparation method for causing fragrant extract, is obtained using following step：(1), crush, (2), extract, (3), sedimentation, filtration, (4), pH value is adjusted, (5), concentrate, (6), alcohol precipitation, (7), refrigeration, (8), filter, (9), concentrate acquisition product.It is to dilute that described cigarette causes the using method of fragrant extract：The cigarette extract is weighed by 0.1% the 2% of pipe tobacco weight, added the dilution of water, propane diols or ethanol solution, mix, obtain dilution；Spray：The dilution is applied to the charging in flue-cured tobacco Primary Processing or perfuming link, is sprayed on pipe tobacco.Cigarette extract is applied to cigarette, is proved through sensory evaluating smoking's contrast, the interior quality of cigarette is significantly improved, increase cigarette flavor, the sweet sense of flue gas is improved, mitigate miscellaneous gas.
Description
Technical field
The present invention relates to a kind of cigarette preparation method, extract and its using method for causing fragrant extract, more particularly to one
Plant using the useless cigarette such as flue dust, fume-bar waste material production cigarette preparation method, the extract for causing perfume extract of Cigarette Industrial Enterprise
And its using method.
Background technology
Useless flue dust is present in each Cigarette Industrial Enterprise, and whole nation entirety reserves are big, but to its development and utilization level very at present
Low, only only a few enterprise has carried out utilizing simply, on a small quantity to which, is generally taken as waste process.Disclosed special pin
To Cigarette Industrial Enterprise actual conditions, the research that recycles to the useless flue dust that Cigarette processing terminal is produced has no report.At present,
It is related to the research that the cigarette such as waste/hypo-tobacco leaf waste material extracts direction, is concentrated mainly on extraction and is worth higher chemical composition, absolute oil, cigarette use
The aspects such as extract.The such as extraction of Salanesol, the extraction of nicotine, the isolating and purifying of tobacco protein, pectin extraction etc., this respect
Research belongs to laboratory basic research, and Cigarette Industrial Enterprise is realized recycling, cost efficiency meaning limited.Such as
Salanesol, lot of documents report can be realized extracting, but purity cannot generally meet the application requirement of downstream industry.Indivedual researchs
The preparation of higher degree is achieved, process procedure becomes complicated again, and production cost is too high；Tobacco protein is separated and prepares skill for another example
Art, theoretical, technically all highly developed, but for Cigarette Industrial Enterprise, high input and technical which is lost
Application prospect.See on the whole, academic research and produce reality disconnect, and " produce, grind separation " phenomenon is serious, and achievement lacks application
Property, there is no operability and Practical significance for tobacco productive corporation.Cigarette enterprise is needed using own resource and industry experience,
Work out the reutilization technology for adapting to self-growth and actual benefit being produced.
Content of the invention
In view of this, the technical problem to be solved is to provide one kind to use using useless flue dust or fume-bar processing cigarette
Preparation method, extract and its using method of fragrant extract is caused, so as to the useless flue dust for effectively Cigarette Industrial Enterprise being produced
Or fume-bar is circulated recycling, extract is prepared, and tobacco manufacture field is applied to, final acquisition improves in cigarette in product
Matter, increases cigarette flavor, improves the sweet sense of flue gas, mitigate the effect of miscellaneous gas.
The purpose of the present invention is achieved through the following technical solutions：
The method that a kind of useless flue dust of utilization Cigarette Industrial Enterprise or fume-bar produce cigarette extract, is obtained using following step
?：
1st, crush：Moisture is carried out machinery for the useless flue dust of 1%-5% or fume-bar and makes broken, be ground into particle diameter and be equal to and little
In the first powder of the flue dust of 80 mesh.
2nd, extract：First for the flue dust for crushing powder and water in mass ratio 1: 4-15 are inserted multi-function extractor (can be with super
Sonic generator and with temperature control ability) in, extract 1-4 hour at 80-100 DEG C, the Aqueous extracts of extraction standing sedimentation 12-48 again
Hour.
3rd, sedimentation, filtration：Aqueous extracts are tentatively filtered with 80 mesh gauzes (2 layers), is removed in crude opium waste residue and fume-bar and mixes
The impurity such as the shredded paper bits that enter, offal, after be transferred to sedimentation removal of impurities 12-48 hour in settling tank, the dust that goes to be mixed in smoke abatement,
The impurity such as fine sand, shredded paper bits, collect supernatant liquid.Upper liquid is filtered again with 100 mesh gauzes (6 layers) under normal temperature and pressure conditionses
Body, obtains filtered fluid after reject filter residue.
4th, pH value is adjusted：Filtered fluid pH to 3- is adjusted using hydrochloric acid or sodium hydroxide solution according to the acid-base value of filtered fluid
11.Also can be replaced with sulfuric acid, phosphoric acid or potassium hydroxide.
5th, concentrate：The filtrate for adjusting pH value is placed in concentration tank carries out reduced pressure concentration, and temperature is set as 80-110 DEG C.Dense
The volume of contracting liquid is the 1/2-1/8 for concentrating front filtrate, places and is cooled to room temperature.
6th, alcohol precipitation：Equidirectional quick stirring is carried out to concentrate, and being slowly added to mass concentration 55%-95% ethanol carries out alcohol
Heavy, alcohol precipitation terminal is containing alcohol quality 30%-80%.
7th, refrigerate：Precipitation solution is refrigerated 12-48 hour in 4-10 DEG C.
8th, filter：(4 layers) filtrations of 80 mesh gauzes of the precipitation solution of refrigeration, obtain clear liquid.Identical alcohol content can be used if necessary
Solvent sediment is eluted, so can lift object yield on a small quantity.
9th, concentrate and obtain product：Reduced pressure concentration is carried out to clear liquid, feed liquid density is concentrated into for 0.9～1.4g/ml.Obtain
Brown liquid is gained cigarette under the process conditions and causes fragrant extract.
Using technique scheme, can efficiently obtain corresponding cigarette and cause fragrant extract.Generally, the extract
For brownish red working fluid, with tobacco characteristic perfume, also while there is fruital and fragrant and sweet, water, propane diols can be dissolved in, or
The ethanol solution of certain alcohol content.Certainly, the specific technological means that is taken due to the preparation method is variant, and which is obtained
The cigarette extract for obtaining also accordingly has some differences in nature.
The present invention also provides a kind of using method of described cigarette extract, comprises the steps：
1st, dilute：The cigarette extract is weighed by the 0.1%-2% of pipe tobacco weight, adds water, propane diols or ethanol
Solution dilution, mixing, obtain dilution；
2nd, spray：The dilution is applied in the middle of charging or the perfuming technology for making tobacco threds of flue-cured tobacco, is sprayed on pipe tobacco.
Using technique scheme, cigarette extract is applied to cigarette, is proved through Experimental Comparison, significantly improve
The interior quality of cigarette, increases cigarette flavor, improves the sweet sense of flue gas, mitigate miscellaneous gas.
Specific embodiment
The invention will be further described for the preferred embodiment of the present invention below.
A kind of embodiment of the preparation method of the cigarette extract of the present invention, using useless fume-bar, drying is crushed, is added water
Extracted, cigarette extract is obtained through filtering, adjusting the steps such as pH value, concentration, alcohol precipitation, filtration, secondary concentration.Drying and crushing has
Beneficial to the yield for improving cigarette extract, but should be appropriate, can otherwise increase time and the difficulty in filtration of sedimentation removal of impurities；Using containing alcohol
The different alcohol precipitation of amount, can make opposed polarity and deliquescent material (starch, protein macromolecule etc.) be precipitated removal；Filter
The cigarette extract that finished product then be ensure that with concentration process has good state and stability.
Requirement of the present invention to the technical equipment that is related to and its technical parameter such as Extracting temperature, water consumption all belongs to conventional model
Enclose, industrial production is easily achieved, albumen, starch etc. have the macromolecular of negative effect by technical arrangement plan to cigarette sense organ,
All can be removed by appropriateness.
In conjunction with the embodiment of the preparation method of further specific cigarette extract, further detailed description is below done：
Embodiment 1：
Take the useless flue dust 100g for having trapped and 80 mesh of particle diameter is crushed to, be put in beaker, add 400g water, 85 DEG C of stirring and leaching
2 hours.Standing sedimentation 12 hours, filters to obtain clear filtrate.PH to 5 is adjusted with watery hydrochloric acid, decompression low temperature is concentrated into former filtrate body
Long-pending 1/2, adds 65% ethanol of mass concentration, and alcohol is sink to containing alcohol quality for 50%, and 10 DEG C of refrigeration was filtered after 12 hours, to filtrate
Carry out being evaporated to the brown liquid that feed liquid relative density obtained for 1.107g/ml. and be gained cigarette under the process conditions
With the fragrant extract I of cause.
Embodiment 2：
Take the useless flue dust 100g for having trapped and 80 mesh of particle diameter is crushed to, be put in beaker, add 500g water, 90 DEG C of ultrasound extractions
2 hours.Standing sedimentation 36 hours, filters to obtain clear filtrate.PH to 8 is adjusted with sodium hydroxide solution, decompression low temperature is concentrated into original
The 1/4 of filtrate volume, adds 80% ethanol, and alcohol is sink to alcohol content for 60%, and 6 DEG C of refrigeration was filtered after 36 hours, and filtrate is carried out
It is evaporated to the brown liquid that feed liquid relative density obtained for 1.242g/ml. and is gained cigarette under the process conditions and causes
Fragrant extract II.
Embodiment 3：
Useless fume-bar after delivery pressure, crosses 80 mesh sieve of particle diameter after crushing, weighs 100g, be put in beaker, adds 600g
Water, 100 DEG C of ultrasounds add stirring and leaching 4 hours.Standing sedimentation 48 hours, filters to obtain clear filtrate.Adjusted with sodium hydroxide solution
PH to 10, decompression low temperature are concentrated into the 1/5 of former filtrate volume, add 90% ethanol, and it is 75% that alcohol is sink to alcohol content, 4 DEG C of refrigerations
Filtered after 48 hours, the brown liquid that feed liquid relative density obtained for 1.292g/ml. is carried out being evaporated to filtrate and is
Gained cigarette fragrant extract II I of cause under the process conditions.
Comparative test：
By the cigarette in above-described embodiment 1,2,3 with cause fragrant extract I, II, III press respectively pipe tobacco weight 0.1%,
0.2%th, 0.5%, 1.0% adds, and is first diluted with pure water, is then uniformly sprayed in a kind of pipe tobacco of flue-cured tobacco.While not spray
The pipe tobacco for spilling the extract is control sample, and the cigarette process that subsequent treatment can be routinely is carried out, that is, spraying cigarette extract
After dilution, store 4 hours, then cigarette finished product is made through throwing and packaging process.
Obtained cigarette is carried out sensory quality assessment, as a result as shown in the table：
The useless flue dust main component that Cigarette Industrial Enterprise is produced includes a part of waster tobacco, part offal, in the air
Dust, a small amount of fine sand, broken cigarette paper scrap, a small amount of filter stick etc..For reducing volume, generally exist with the flue dust bar form after compression,
Fragrant extract is caused to fall within scope of the invention hence with fume-bar for raw material production cigarette.
Above content is further description made for the present invention with reference to specific preferred embodiment, it is impossible to assert
Being embodied as of the present invention is confined to these explanations.For general technical staff of the technical field of the invention,
On the premise of present inventive concept, some simple deduction or replace can also be made, should all be considered as belonging to the present invention's
Protection domain.
Claims (8)
1. a kind of cigarette preparation method for causing fragrant extract, is obtained using following step：
(1), crush, (2), extraction, (3), sedimentation, filtration, (4), pH value adjusted, (5), concentrate, (6), alcohol precipitation, (7), refrigeration,
(8), filter, (9), concentrate acquisition product.
2. preparation method according to claim 1, it is characterised in that：In step (1), useless flue dust or fume-bar are carried out machine
Tool is made broken, is ground into particle diameter and is equal to and the first powder of flue dust less than 80 mesh；In step (2), by the flue dust for crushing, just powder and water are put
Enter in multi-function extractor, extract at 80-100 DEG C, the Aqueous extracts of extraction standing sedimentation again.
3. preparation method according to claim 1, it is characterised in that：In step (3), Aqueous extracts are tentatively filtered, remove
The impurity such as the shredded paper bits that are mixed in crude opium waste residue and fume-bar, offal, after be transferred to sedimentation removal of impurities in settling tank, go in smoke abatement
The dust that is mixed into, fine sand, shredded paper bits impurity, collect supernatant liquid, filter supernatant liquid under normal temperature and pressure conditionses again, and reject is filtered
Filtered fluid is obtained after slag；In step (4), using hydrochloric acid or sodium hydroxide solution, filtered fluid pH to 3-11 is adjusted, it is also possible to sulphur
Acid, phosphoric acid or potassium hydroxide replace.
4. preparation method according to claim 1, it is characterised in that：In step (5), the filtrate for adjusting pH value is placed in dense
Reduced pressure concentration is carried out in contracting tank, and the volume of concentrate is the 1/2-1/8 for concentrating front filtrate, places and is cooled to room temperature.
5. preparation method according to claim 1, it is characterised in that：In step (6), concentrate is carried out equidirectional quick
Stirring, being slowly added to ethanol carries out alcohol precipitation, and alcohol precipitation terminal is containing alcohol quality 30%-80%.
6. preparation method according to claim 1, it is characterised in that：In step (7), precipitation solution is refrigerated in 4-10 DEG C；
In step (8), the precipitation solution of refrigeration is filtered, and obtains clear liquid.
7. preparation method according to claim 1, it is characterised in that：In step (9), reduced pressure concentration is carried out to clear liquid, dense
Feed liquid density is reduced to for 0.9～1.4g/ml, the liquid for obtaining is gained cigarette under the process conditions and causes fragrant extract.
8. a kind of cigarette using method for causing fragrant extract, comprises the steps：
(1), dilute：The cigarette extract is weighed by the 0.1%-2% of pipe tobacco weight, adds water, propane diols or ethanol molten
Liquid dilution, mixing, obtain dilution；
(2), spray：The dilution is applied in the middle of charging or the perfuming technology for making tobacco threds of flue-cured tobacco, is sprayed on pipe tobacco.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610885354.8A CN106473227A (en) | 2016-10-11 | 2016-10-11 | A kind of cigarette preparation method for causing fragrant extract and using method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610885354.8A CN106473227A (en) | 2016-10-11 | 2016-10-11 | A kind of cigarette preparation method for causing fragrant extract and using method |
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| Publication Number | Publication Date |
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| CN106473227A true CN106473227A (en) | 2017-03-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610885354.8A Pending CN106473227A (en) | 2016-10-11 | 2016-10-11 | A kind of cigarette preparation method for causing fragrant extract and using method |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107637858A (en) * | 2017-09-14 | 2018-01-30 | 云南中烟工业有限责任公司 | A kind of plant for improving water extraction and alcohol precipitation method extraction causes perfumery and extracting method and application |
| CN113508919A (en) * | 2020-12-31 | 2021-10-19 | 上海零诺生物科技有限公司 | Tobacco extract and preparation method and application thereof |
| CN115251454A (en) * | 2022-05-20 | 2022-11-01 | 深圳麦克韦尔科技有限公司 | Method for treating tobacco extract, aerosol-generating substrate and atomizer |
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| JPH11225731A (en) * | 1998-02-12 | 1999-08-24 | Japan Tobacco Inc | Improving agent for aroma and smoking taste of tobacco and improvement of the same |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107637858A (en) * | 2017-09-14 | 2018-01-30 | 云南中烟工业有限责任公司 | A kind of plant for improving water extraction and alcohol precipitation method extraction causes perfumery and extracting method and application |
| CN113508919A (en) * | 2020-12-31 | 2021-10-19 | 上海零诺生物科技有限公司 | Tobacco extract and preparation method and application thereof |
| CN115251454A (en) * | 2022-05-20 | 2022-11-01 | 深圳麦克韦尔科技有限公司 | Method for treating tobacco extract, aerosol-generating substrate and atomizer |
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Application publication date: 20170308 |