CN106473129A - A kind of preparation method of turmeric micro-capsule - Google Patents
A kind of preparation method of turmeric micro-capsule Download PDFInfo
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- CN106473129A CN106473129A CN201610894916.5A CN201610894916A CN106473129A CN 106473129 A CN106473129 A CN 106473129A CN 201610894916 A CN201610894916 A CN 201610894916A CN 106473129 A CN106473129 A CN 106473129A
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Abstract
The invention discloses a kind of preparation method of turmeric micro-capsule, is that dry turmeric is crushed, ethanol dissolving is added, the tween emulsifier of its quality 8 15% is added, is stirred, obtains core material solution；Will be soluble in water to sodium alginate and xanthans, wall material solution is obtained, the wherein mass ratio of sodium alginate, xanthans fat and water is 5 10:15‑20:100；Above-mentioned core material solution and wall material solution are 1 according to mass ratio:24 addition ultrasonic homogenizers carry out sterilization treatment；The slurry of gained is carried out microwave drying, the dried powder that water content is 6 8% is obtained, room temperature is cooled to, packaging, obtain final product turmeric micro-capsule.Turmeric micro-capsule prepared by this method not only can avoid its active ingredient and external environment, significantly improve the stability of turmeric, it is obviously prolonged storage period, moreover it is possible to save full nutrition and the active component of turmeric original powder very well, be easy to the technique of turmeric to process, preserve and transport.This method also has preparation process is simple, simple to operate, consume energy low, low cost and other advantages, easily realizes industrialized production.
Description
Technical field
The present invention relates to Technology of Processing Chinese Herbal Medicines field, specifically a kind of preparation method of turmeric micro-capsule.
Background technology
Turmeric（Curcuma longa L.）,Also known as root tuber of aromatic turmeric, tripod perfume, milli life, yellow ginger etc., it is that Zingiber perennial herb is planted
The rhizome of thing turmeric.Main product is in originating from the provinces and regions such as TaiWan, China, Fujian, Guangdong, Guangxi, Yunnan, Tibet.Play in turmeric main
Health-care efficacy composition is curcumin, and which has anti-oxidant, antitumor, reducing blood lipid, hypoglycemic, antiulcer, protection liver, the anti-heart
Myocardial ischemia, antidepression, antibacterial, anti-inflammatory, the effect such as antiviral and antimycotic, can be used for treating cancer, diabetes, coronary heart disease, pass
Section inflammation, Alzheimer's and other chronic diseases.Additionally, turmeric can also make flavouring, pigment, spices, fuel, desinsection
Agent etc., its application are extremely wide.
Turmeric is simply simply dried by prior art to the deep processing of turmeric medicinal material, and disintegrating process is obtained turmeric dry powder.
But turmeric dry powder does not have the protection of other media, it is easy to oxidative degradation in the presence of illumination, high temperature and oxygen, causes
The loss of nutrition and quality decline.Microcapsule technology be with the macromolecular material of natural or synthesis as wall material, by liquid, solid or
The core substances such as gas carry out packing, form a kind of technology of the microencapsulation with semi permeability or sealing cyst membrane.Because micro-capsule
Changing to improve the physical propertys such as the color for being wrapped material, outward appearance, apparent density, dissolubility；Improve stablizing for core substance
Property, improve reactivity, durability, thermal sensitivity and the light sensitivity for being wrapped material, have been widely used medical, agriculture, chemical
In the industry such as product, food processing, cosmetics, cause the extensive concern in the world.Therefore, microencapsulation be improve curcuma powder stability,
Extend the effective way of storage period.
Content of the invention
The present invention is easy to asking for oxidative degradation presence for turmeric dry powder in the presence of illumination, high temperature and oxygen
Topic, provides a kind of preparation method of turmeric micro-capsule.Turmeric micro-capsule prepared by this method can increase its dispersiveness and to heat, light etc.
Tolerance, significantly improves stability, is difficult mouldy, hence it is evident that extend storage period.
In order to realize object above, the technical solution used in the present invention is as follows:
A kind of preparation method of turmeric micro-capsule, comprises the following steps：
（1）Prepare core：Dry turmeric is crushed, is added its quality for 5-7 times of ethanol dissolving, adds as turmeric quality
The tween emulsifier of 8-15%, stirs, and obtains core material solution；
（2）Prepare wall material：Will be soluble in water to sodium alginate and xanthans, obtain wall material solution, wherein sodium alginate, xanthans fat and
The mass ratio of water is 5-10:15-20:100；
（3）Ultrasonic wave homogeneous：Above-mentioned core material solution and wall material solution are 1 according to mass ratio:2-4 adds ultrasonic homogenizer to enter
Row sterilization treatment 30-60min；
（4）Microwave drying：By step（3）The slurry of gained carries out microwave drying, obtains dried powder of the water content for 6-8%, cooling
To room temperature, pack, obtain final product turmeric micro-capsule.
Preferably, above step（1）Described crushing is that turmeric is crushed to 200-250 mesh.
Preferably, the mass concentration of the above ethanol is 90-95%.
Preferably, the above tween emulsifier is Tween 80 or the one kind in polysorbate60.
Preferably, during the above ultrasonic wave sterilization treatment, the power of ultrasonic wave is 200-250W, and temperature is 50-60 DEG C.
Preferably, the above microwave drying is dry at temperature is for 60-80 DEG C.
Compared with prior art, advantages of the present invention and have the beneficial effect that:
1st, turmeric micro-capsule prepared by the inventive method not only can avoid its active ingredient and external environment, not receive thermal source, light
Source, air etc. affect, and significantly improve the stability of turmeric, hence it is evident that extend storage period, moreover it is possible to save the complete of turmeric original powder very well
Valency Ingredient, is easy to the technique of turmeric to process, preserve and transport.
2nd, this method selects beta-schardinger dextrin and soybean lecithin as wall material, improves the compactness of micro-capsule, and which is to turmeric
Full rate is high, and micro-capsule product property is stable.
3rd, compared with turmeric original powder, its water solubility is significantly improved turmeric micro-capsule prepared by this method, and with good in water
Good dispersiveness, can be digested and assimilated completely by human body, at utmost play the drug effect of turmeric.
4th, the present invention is by carrying out sterilization treatment using ultrasonic technology, as the cavitation of ultrasonic wave causes homogeneous to imitate
Fruit is more preferable than high-pressure homogeneous, and when the turmeric micro-capsule that ultrasonic wave homogeneous is obtained is dissolved in water, nothing precipitation is produced.
5th, the inventive method adopts microwave K cryogenic treatment, and compared with conventional spray drying, temperature is lower, can be to greatest extent
Minimizing heat-sensitive substance loss.
6th, this method preparation process is simple, simple to operate, the low, low cost of power consumption, easily realize industrialized production.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is further described, but is not limited to protection scope of the present invention.
Embodiment 1
A kind of preparation method of turmeric micro-capsule, comprises the following steps：
（1）Prepare core：The turmeric that 100kg is dry is crushed, and adds the ethanol dissolving that 500kg mass concentration is 90%, adds
10kg Tween 80 emulsifying agent, stirs, obtains core material solution；
（2）Prepare wall material：Will be soluble in water to sodium alginate and xanthans, obtain wall material solution, wherein sodium alginate, xanthans fat and
The mass ratio of water is 8:15:100；
（3）Ultrasonic wave homogeneous：Above-mentioned core material solution and wall material solution are 1 according to mass ratio:3 add ultrasonic homogenizer,
Temperature is 50 DEG C, power is sterilization treatment 60min under 200W；
（4）Microwave drying：By step（3）The slurry of gained is microwave drying at 70 DEG C in temperature, obtains the drying that water content is 6%
Powder, is cooled to room temperature, packaging, obtains final product turmeric micro-capsule.
Embodiment 2
A kind of preparation method of turmeric micro-capsule, comprises the following steps：
（1）Prepare core：The turmeric that 100kg is dry is crushed, and adds the ethanol dissolving that 600kg mass concentration is 95%, adds
8kg Tween 80 emulsifying agent, stirs, obtains core material solution；
（2）Prepare wall material：Will be soluble in water to sodium alginate and xanthans, obtain wall material solution, wherein sodium alginate, xanthans fat and
The mass ratio of water is 5:20:100；
（3）Ultrasonic wave homogeneous：Above-mentioned core material solution and wall material solution are 1 according to mass ratio:2 add ultrasonic homogenizer,
Temperature is 60 DEG C, power is sterilization treatment 30min under 250W；
（4）Microwave drying：By step（3）The slurry of gained is microwave drying at 80 DEG C in temperature, obtains the drying that water content is 6%
Powder, is cooled to room temperature, packaging, obtains final product turmeric micro-capsule.
Embodiment 3
A kind of preparation method of turmeric micro-capsule, comprises the following steps：
（1）Prepare core：The turmeric that 100kg is dry is crushed, and adds the ethanol dissolving that 700kg mass concentration is 95%, adds
12kg polysorbate60 emulsifying agent, stirs, obtains core material solution；
（2）Prepare wall material：Will be soluble in water to sodium alginate and xanthans, obtain wall material solution, wherein sodium alginate, xanthans fat and
The mass ratio of water is 10:18:100；
（3）Ultrasonic wave homogeneous：Above-mentioned core material solution and wall material solution are 1 according to mass ratio:2 add ultrasonic homogenizer,
Temperature is 55 DEG C, power is sterilization treatment 40min under 200W；
（4）Microwave drying：By step（3）The slurry of gained is microwave drying at 70 DEG C in temperature, obtains the drying that water content is 7%
Powder, is cooled to room temperature, packaging, obtains final product turmeric micro-capsule.
Embodiment 4
A kind of preparation method of turmeric micro-capsule, comprises the following steps：
（1）Prepare core：The turmeric that 100kg is dry is crushed, and adds the ethanol dissolving that 500kg mass concentration is 95%, adds
15kg polysorbate60 emulsifying agent, stirs, obtains core material solution；
（2）Prepare wall material：Will be soluble in water to sodium alginate and xanthans, obtain wall material solution, wherein sodium alginate, xanthans fat and
The mass ratio of water is 10:15:100；
（3）Ultrasonic wave homogeneous：Above-mentioned core material solution and wall material solution are 1 according to mass ratio:3 add ultrasonic homogenizer,
Temperature is 60 DEG C, power is sterilization treatment 30min under 250W；
（4）Microwave drying：By step（3）The slurry of gained is microwave drying at 60 DEG C in temperature, obtains the drying that water content is 8%
Powder, is cooled to room temperature, packaging, obtains final product turmeric micro-capsule.
The preferred embodiments of the present invention are the foregoing is only, the present invention is not limited to, for those skilled in the art
For member, the present invention can have various modifications and variations.All any modifications that within the spirit and principles in the present invention, is made,
Equivalent, improvement etc., should be included within the scope of the present invention.
Claims (6)
1. a kind of preparation method of turmeric micro-capsule, it is characterised in that:Comprise the following steps：
（1）Prepare core：Dry turmeric is crushed, is added its quality for 5-7 times of ethanol dissolving, adds as turmeric quality
The tween emulsifier of 8-15%, stirs, and obtains core material solution；
（2）Prepare wall material：Will be soluble in water to sodium alginate and xanthans, obtain wall material solution, wherein sodium alginate, xanthans fat and
The mass ratio of water is 5-10:15-20:100；
（3）Ultrasonic wave homogeneous：Above-mentioned core material solution and wall material solution are 1 according to mass ratio:2-4 adds ultrasonic homogenizer to enter
Row sterilization treatment 30-60min；
（4）Microwave drying：By step（3）The slurry of gained carries out microwave drying, obtains dried powder of the water content for 6-8%, cooling
To room temperature, pack, obtain final product turmeric micro-capsule.
2. the preparation method of turmeric micro-capsule according to claim 1, it is characterised in that:Step（1）Described crushing be by ginger
Bloom is broken to 200-250 mesh.
3. the preparation method of turmeric micro-capsule according to claim 1, it is characterised in that:The mass concentration of the ethanol is 90-
95%.
4. the preparation method of turmeric micro-capsule according to claim 1, it is characterised in that:The tween emulsifier be Tween 80 or
One kind in polysorbate60.
5. the preparation method of turmeric micro-capsule according to claim 1, it is characterised in that:Ultrasound during the ultrasonic wave sterilization treatment
The power of ripple is 200-250W, and temperature is 50-60 DEG C.
6. the preparation method of turmeric micro-capsule according to claim 1, it is characterised in that:The microwave drying is to be in temperature
Dry at 60-80 DEG C.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468669A (en) * | 2017-09-27 | 2017-12-15 | 右江民族医学院 | A kind of preparation method of Gastrodin microcapsule granule |
| CN107648197A (en) * | 2017-09-27 | 2018-02-02 | 右江民族医学院 | The microencapsulation method of flax lignan |
| CN107789335A (en) * | 2017-09-27 | 2018-03-13 | 右江民族医学院 | The preparation method of qinghaosu microcapsules |
| CN110051550A (en) * | 2019-05-30 | 2019-07-26 | 佛山市康伲爱伦生物技术有限公司 | A kind of ar-turmerone inclusion compound and preparation method thereof with sterilization anti-inflammatory effect |
| CN110269166A (en) * | 2019-07-04 | 2019-09-24 | 北京九前健康科技有限公司 | A kind of preparation method of relieving alcoholism and protecting liver composition and drink and drink |
| CN111481524A (en) * | 2020-03-31 | 2020-08-04 | 右江民族医学院 | Curcumin microencapsulation method |
| CN111494334A (en) * | 2020-03-31 | 2020-08-07 | 右江民族医学院 | Method for preparing linarin microcapsule particles |
| CN112753766A (en) * | 2020-12-29 | 2021-05-07 | 光明乳业股份有限公司 | Turmeric yoghourt beverage and preparation method thereof |
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| CN101214046A (en) * | 2007-12-30 | 2008-07-09 | 夏建伟 | Method for preparing ginkgo biloba oil powder |
| CN104173395A (en) * | 2014-09-05 | 2014-12-03 | 南京泽朗生物科技有限公司 | Preparation method of lysimachia christinae hance flavonoids microcapsule |
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| CN101032683A (en) * | 2006-03-10 | 2007-09-12 | 郑亚津 | Xanthin micro-capsule and the preparing method |
| CN101214046A (en) * | 2007-12-30 | 2008-07-09 | 夏建伟 | Method for preparing ginkgo biloba oil powder |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468669A (en) * | 2017-09-27 | 2017-12-15 | 右江民族医学院 | A kind of preparation method of Gastrodin microcapsule granule |
| CN107648197A (en) * | 2017-09-27 | 2018-02-02 | 右江民族医学院 | The microencapsulation method of flax lignan |
| CN107789335A (en) * | 2017-09-27 | 2018-03-13 | 右江民族医学院 | The preparation method of qinghaosu microcapsules |
| CN107648197B (en) * | 2017-09-27 | 2020-04-03 | 右江民族医学院 | Microencapsulation method of secoisolariciresinol diglucoside |
| CN107789335B (en) * | 2017-09-27 | 2020-04-03 | 右江民族医学院 | Preparation method of artemisinin microcapsules |
| CN107468669B (en) * | 2017-09-27 | 2020-04-03 | 右江民族医学院 | Preparation method of gastrodin micro-capsule granules |
| CN110051550A (en) * | 2019-05-30 | 2019-07-26 | 佛山市康伲爱伦生物技术有限公司 | A kind of ar-turmerone inclusion compound and preparation method thereof with sterilization anti-inflammatory effect |
| CN110269166A (en) * | 2019-07-04 | 2019-09-24 | 北京九前健康科技有限公司 | A kind of preparation method of relieving alcoholism and protecting liver composition and drink and drink |
| CN111481524A (en) * | 2020-03-31 | 2020-08-04 | 右江民族医学院 | Curcumin microencapsulation method |
| CN111494334A (en) * | 2020-03-31 | 2020-08-07 | 右江民族医学院 | Method for preparing linarin microcapsule particles |
| CN112753766A (en) * | 2020-12-29 | 2021-05-07 | 光明乳业股份有限公司 | Turmeric yoghourt beverage and preparation method thereof |
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Application publication date: 20170308 |