CN106472923B - The preparation method of lactoferrin high methoxy pectin speed energy drink - Google Patents

The preparation method of lactoferrin high methoxy pectin speed energy drink Download PDF

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CN106472923B
CN106472923B CN201610815656.8A CN201610815656A CN106472923B CN 106472923 B CN106472923 B CN 106472923B CN 201610815656 A CN201610815656 A CN 201610815656A CN 106472923 B CN106472923 B CN 106472923B
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lactoferrin
oil
methoxy pectin
high methoxy
speed
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CN106472923A (en
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王春维
李奥
彭凯迪
程铭
陶冶
焦文佳
夏廉臣
祝爱侠
祝家东
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Wuhan Polytechnic University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/62Clouding agents; Agents to improve the cloud-stability
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/66Proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Edible Oils And Fats (AREA)

Abstract

The invention discloses a kind of preparation method of lactoferrin high methoxy pectin speed energy drink, technical solution is with 0.05~0.6 part of lactoferrin, 0.05~0.6 part of high methoxy pectin, 78.85~94.9 parts of water phase, 0.05~0.2 part of vitamin E, 1.5~6 parts of soybean oil, 1.25~5 parts of olive oil, 1.5~6 parts of median chain triglyceride oil, 0.75~3 part of fish oil are raw material, by the way that lactoferrin is high-temperature denatured, then add high methoxy pectin and lactoferrin high methoxy pectin mixture is made;Then mix with oil phase high-speed stirred and be made after high-pressure homogeneous.Preparation method of the present invention is simple, production cost and cost of investment are low, obtained speed energy drink has good mobility and storage-stable, and can provide energy rapidly, quickly be absorbed by the body.

Description

The preparation method of lactoferrin-high methoxy pectin speed energy drink
Technical field
The present invention relates to the preparation of field of food, specifically a kind of lactoferrin-high methoxy pectin speed energy drink Method.
Background technology
Either sportsman, or postoperative patient, participate in volunteer for fighting flood and relieve victims etc., its be engaged in a large amount of movements or It is after physical extremely consumption, for fast quick-recovery physical efficiency and the energy conservation of maintenance body, all needs a large amount of and be rapidly performed by Supplement energy.And the common fat of excess intake, protein etc. are difficult to the food digested, gastric emptying is slow merely, can not only make The speed that can be converted into direct energy source substance A TP slows down, influences quickly energy supply, and it is also possible to can cause digestive discomfort, produces The reactions such as raw Nausea and vomiting;During a large amount of supplement glucide, can not all be absorbed by the body, stomach to the digestion power of sugar by To limitation, and when excessive sugar remains under one's belt, the moisture in human body can be absorbed, and at this moment stomach can produce feeling of pain, make People produces nausea.
At present, for sportsman, the physical training person of large amount of exercise, the physical efficiency such as personnel and postoperative patient of fighting flood and relieve victims pole The food that the colony of degree consumption provides supplement physical efficiency is mostly sport type beverage, and sports drink is generally by sugar, salt, mineral matter, egg White matter and polypeptide etc. and prepare;Its supplement energy is slower, with less the rapid supplement energy during movement and physical consumption Function.
In view of the above-mentioned problems, researcher wish to obtain a kind of speed can drink, can accelerate absorption of the human body to nutriment, Quick extra-nutrition material, dispelling fatigue and recovery physical efficiency, the aspiration that can be fought flood and relieve victims for sportsman, postoperative patient, participation Zhe Deng specific groups, after the extremely consumption of its muscle power, it is required quickly to be provided after moment that can be during the motion or movement Aliphatic acid and energy, make the oxidation of fat effectively to reduce fat independent of insulin and be exhaled in oxidizing process body Inhale quotient.
The content of the invention
The purpose of the present invention is to solve above-mentioned technical problem, there is provided a kind of preparation method is simple, production cost and throwing Money cost it is low, it is obtained speed can drink there is good mobility and storage-stable, and energy can be provided rapidly, can be by human body The preparation method of the lactoferrin absorbed rapidly-high methoxy pectin speed energy drink.
Technical solution includes the raw material of following parts by weight:
0.05~0.6 part of lactoferrin, 0.05~0.6 part of high methoxy pectin, 78.85~94.9 parts of water phase, vitamin E 0.05~0.2 part, 1.5~6 parts of soybean oil, 1.25~5 parts of olive oil, 1.5~6 parts of median chain triglyceride oil, fish oil 0.75~3 Part;
Preparation method comprises the following steps:
(1) lactoferrin is dissolved in water, it is 6.5~7.5 to adjust pH, high-temperature denatured, then is rapidly cooled to room temperature, is adjusted Section pH adds high methoxy pectin after being 7.5~8.3, is lactoferrin-high methoxyl in 30~50 DEG C of stirring in water bath dissolvings Pectin mixture;
(2) oil phase will be obtained after vitamin E, soybean oil, olive oil, median chain triglyceride oil and fish oil uniformly mixing;
(3) high-speed stirred mixing is carried out after the ferritin-high methoxy pectin mixed liquor is added into oil phase, then through height The thin breast that pressure homogeneous obtains is lactoferrin-high methoxy pectin speed can drink.
In the step (1), high-temperature denatured temperature is 80~95 DEG C, denaturation time 15~25 minutes.
In the step (3), it is 10 000~20 000r/min to control mixing speed, and mixing time is 5~15min.
In the step (3), high-pressure homogeneous pressure is 10~80Mpa, homogenization cycles 2~10 times.
For problem present in background technology, inventor is using lactoferrin and high methoxy pectin as raw material, using height Under the conditions of temperature, make the disulfide bond in lactoferrin and the destroyed denaturation of hydrophobic bond interaction, it is 7 then to adjust pH, then and high Methoxy group pectin key connection forms compound, and stable emulsion system (lactoferrin-high methoxy pectin mixed liquor) is made, this Kind emulsion system has excellent stability, is excellent stabilizer, wherein lactoferrin has good emulsification, more Sugared high methoxy pectin has increase system viscosity effect, and when being prepared for fast energy drink, both take compound with that can form electrostatic Thing, can reach the effect for effectively preventing water-oil phase segregation phenomenon.0.05~0.6 part of lactoferrin is controlled, polyprotein is crossed and adds System viscosity can be dramatically increased by adding, and increase cost, and the very few meeting of lactoferrin additive amount is so that emulsifying capacity deficiency;Control is high 0.05~0.6 part of methoxy group pectin, and when anion polysaccharide content is too low cannot play the role of stable milk beverage.High methoxyl Pectin additive amount can dramatically increase the viscosity of system when big, cause milk beverage coarse mouthfeel, and high methoxy pectin content is too low Shi Buneng plays the role of stable emulsion.
Further, oil phase is made of soybean oil, median chain triglyceride oil, vitamin E, olive oil and fish oil.Wherein, greatly Main component in soya-bean oil is oleic acid and linoleic acid, and containing abundant gamma-Linolenic acid and alpha-linolenic acid, nutritive value is higher, energy Enhancing development, prevention of cardiovascular disease and reduction serum cholesterol and blood fat, it plays an important role health, control Soybean oil 1.5~6 processed, can reduce the digestibility of lipid when soybean oil is excessive in oil phase, and soybean oil content deficiency can drop Low oily nutritive value;Olive oil is a kind of generally acknowledged natural green grease, containing abundant unrighted acid, in olive oil Not only also contain polyunsaturated fatty acid omega-3-fatty acids, also containing substantial amounts of liposoluble vitamin, fatty alcohol, squalene, polyphenol With sterol and various microelements of calcium, phosphorus, iron, potassium, selenium etc., nutritional ingredient is higher, thus possess and promote blood circulation, improve disappear Change systemic-function, protection skin, improve metabolic function, anticancer, radioresistance, work that is anti-aging and preventing cardiovascular and cerebrovascular disease With, 1.25~5 parts of olive oil is controlled, oxidation deterioration easily occurs when content of olive oil is excessive in oil phase, and content of olive oil is insufficient Shi Buneng reaches the function of improving digestive system;Median chain triglyceride oil (MCT) is the aliphatic acid containing 8~12 carbon atoms, It has high soluble and lower molecular wt, can also improve the discharge capacity of serum ketone and carboxylic acid, is conducive to fat Digest and assimilate, control 1.5~6 parts of median chain triglyceride oil, in oil phase median chain triglyceride oil mainly by portal vein directly into Enter liver, metabolism that can be in liver stimulates the ketogenesis, and whens too high levels is also easy to produce acid poisoning;Median chain triglyceride oil in oil phase The too low digestibility that can reduce oil phase of content.Vitamin E, also known as tocopherol, have stronger bioactivity, can suppress fat Matter peroxidating, removes free radical, increases immunity of organism, delaying human body caducity, prevention and treatment angiocardiopathy etc.;Dimension is not added Raw element E can cause oil phase that oxidation deterioration occurs rapidly.Fish oil therein is the main source of EPA and DHA, the intake of EPA and DHA The serum levels of the lipid of hyperlipidemia patient, lipoprotein and apolipoprotein can be significantly reduced;Strengthen diabetes B patient's body Inner membrance island element sensitiveness, alleviates insulin resistance, reduces plasma triglyceride, lipoid and lipoprotein levels, reduces health adult Body fat content, promote fat utilization, control 0.75~3 part of fish oil, emulsion system can be caused when fish oil content is excessive in oil phase The increase of fishlike smell smell, influences drink flavor, and the too low meeting of fish oil content causes EPA and DHA content deficiency in oil phase, reduces fat The utilization rate of fat, although above-mentioned grease has extremely excellent effect, there are fishy smell weight, is not easy the shortcomings that rapid digestion, because The complex emulsions system that the invention is considered as lactoferrin-high methoxy pectin covers the fishlike smell of fish oil and improves grease Digestibility.By soybean oil, median chain triglyceride oil, olive oil, fish oil, lactoferrin, high methoxy pectin and water according to The combination of specified quantitative and lotion processing technology, combine the fatty acid proportion containing balance in oil phase, can provide long-chain fat to human body Fat is sour and meets the needs of human body is to necessary aliphatic acid, while medium chain triglyceride can be energized quickly, and olive oil and fish oil provide Omega-3 polyunsaturated fatty acids, and the ratio of ω -6 and omega-fatty acid meets the ω -6/ omega-fatty acid ratios of recommendation, because And the characteristics of rapid complementary energy can be reached, be easy to digest and assimilate.
In step (3), it is 10 000~20 000r/min that emulsion system controls mixing speed when mixing, to reach oil The mixed uniformly purpose of water two-phase;It is 5~15min to control mixing time, and mixing time is long to cause emulsion system temperature to become Height, causes wild effect;And the too short meeting of mixing time is so that water-oil phase mixing is uneven;The high-pressure homogeneous purpose is In order to form smaller and uniform drop, increase emulsion intercalation method and the digestibility for improving grease, control is high-pressure homogeneous Pressure is 10~80Mpa, and homogenization pressure, which crosses conference, causes overpower effect, causes increasing for emulsion particle diameter, is unfavorable for breast on the contrary The stabilization of liquid;Emulsion particle diameter is larger when homogenization pressure is too low, and lamination easily occurs.
Present invention process is simple, and reaction process is easier to control, and production cost is low, lactoferrin-high methoxy of preparation Base pectin glue speed energy drink has the advantages that good fluidity, storage-stable, rapid offer energy, has a vast market prospect.
Brief description of the drawings
Fig. 1 is for embodiment 2 from different comparative examples with time external steatolysis rate change curve.
Embodiment
Embodiment 1
The preparation method of lactoferrin-high methoxy pectin mixed liquor is:0.6g lactoferrins are dissolved in 78.85g water In, it is 7 to adjust pH, and 90 DEG C of high temperature is denatured 20 minutes, is rapidly cooled to room temperature, adjusts after pH is 8 and adds 0.6g high methoxyl fruits Glue, is lactoferrin-high methoxy pectin mixture in 40 DEG C of stirring in water bath dissolvings.
Soybean oil 6.0g, olive oil 5.0g, median chain triglyceride oil 6.0g, 0.2g vitamin E, fish oil 3.0g are weighed in room The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly under temperature.Oil phase is added into lactoferrin-high methoxy High-speed stirred mixing is carried out after base pectin mixture, mixing speed 20000r/min, mixing time 15min, then uses High-pressure homogeneous to prepare thin breast, high-pressure homogeneous pressure is 80Mpa, and homogenization cycles are 10 times, both obtain lactoferrin-high methoxy pectin Fast energy lotion.
Embodiment 2
The preparation method of lactoferrin-high methoxy pectin mixed liquor is:0.4g lactoferrins are dissolved in 94.9g water In, it is 7 to adjust pH, and 90 DEG C of high temperature is denatured 20 minutes, is rapidly cooled to room temperature, adjusts after pH is 8 and adds 0.4g high methoxyl fruits Glue, is lactoferrin-high methoxy pectin mixture in 50 DEG C of stirring in water bath dissolvings.
Weigh soybean oil 1.5g, olive oil 1.25g, median chain triglyceride oil 1.5g, 0.05g vitamin E, fish oil 0.75g The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly at room temperature.Oil phase is added into lactoferrin-height Progress high-speed stirred mixing after methoxy group pectin mixture, mixing speed 15000r/min, mixing time 10min, then Thin breast is prepared using high-pressure homogeneous, high-pressure homogeneous pressure is 50Mpa, and homogenization cycles are 5 times, both obtain lactoferrin-high methoxyl Pectin speed can lotion.
Embodiment 3
The preparation method of lactoferrin-high methoxy pectin mixed liquor is:0.6g lactoferrins are dissolved in 92.28g water In, it is 7.5 to adjust pH, and 80 DEG C of high temperature is denatured 25 minutes, is rapidly cooled to room temperature, adjusts after pH is 8 and adds 0.05g high methoxyls Pectin, is lactoferrin-high methoxy pectin mixture in 40 DEG C of stirring in water bath dissolvings.
Weigh soybean oil 2.0g, olive oil 2.0g, median chain triglyceride oil 2.0g, 0.07g vitamin E, fish oil 1.0g in The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly at room temperature.Oil phase is added into lactoferrin-high first High-speed stirred mixing is carried out after epoxide pectin mixture, mixing speed 10000r/min, mixing time 5min, then uses High-pressure homogeneous to prepare thin breast, high-pressure homogeneous pressure is 10Mpa, and homogenization cycles are 2 times, both obtain lactoferrin-high methoxy pectin Fast energy lotion.
Embodiment 4
The preparation method of lactoferrin-high methoxy pectin mixed liquor is:0.05g lactoferrins are dissolved in 89.45g water In, it is 6.5 to adjust pH, and 90 DEG C of high temperature is denatured 20 minutes, is rapidly cooled to room temperature, adjusts after pH is 8.3 and adds 0.4g high methoxies Base pectin, is lactoferrin-high methoxy pectin mixture in 30 DEG C of stirring in water bath dissolvings.
Soybean oil 3.5g, olive oil 2.5g, median chain triglyceride oil 2.5g, 0.1g vitamin E, fish oil 1.5g are weighed in room The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly under temperature.Oil phase is added into lactoferrin-high methoxy High-speed stirred mixing is carried out after base pectin mixture, mixing speed 15000r/min, mixing time 10min, then uses High-pressure homogeneous to prepare thin breast, high-pressure homogeneous pressure is 40Mpa, and homogenization cycles are 6 times, both obtain lactoferrin-high methoxy pectin Fast energy lotion.
Embodiment 5
The preparation method of lactoferrin-high methoxy pectin mixed liquor is:0.5g lactoferrins are dissolved in 88.9g water In, it is 7 to adjust pH, and 95 DEG C of high temperature is denatured 15 minutes, is rapidly cooled to room temperature, adjusts after pH is 7.5 and adds 0.5g high methoxyls Pectin, is lactoferrin-high methoxy pectin mixture in 37 DEG C of stirring in water bath dissolvings
Soybean oil 3.0g, olive oil 2.5g, median chain triglyceride oil 3.0g, 0.1g vitamin E, fish oil 1.5g are weighed in room The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly under temperature.Oil phase is added into lactoferrin-high methoxy High-speed stirred mixing is carried out after base pectin mixture, mixing speed 16000r/min, mixing time 10min, then uses High-pressure homogeneous to prepare thin breast, high-pressure homogeneous pressure is 50Mpa, and homogenization cycles are 5 times, both obtain lactoferrin-high methoxy pectin Fast energy lotion.
Comparative example 6
The preparation method of lactoferrin-high methoxy pectin mixed liquor is:0.3g lactoferrins are dissolved in 89.2g water In, it is 7 to adjust pH, and 90 DEG C of high temperature is denatured 20 minutes, is rapidly cooled to room temperature, adjusts after pH is 8 and adds 0.4g high methoxyl fruits Glue, is lactoferrin-high methoxy pectin mixture in 40 DEG C of stirring in water bath dissolvings.
Soybean oil 8.0g, olive oil 1.0g, median chain triglyceride oil 0.5g, 0.1g vitamin E, fish oil 0.5g are weighed in room The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly under temperature.Oil phase is added into lactoferrin-high methoxy High-speed stirred mixing is carried out after base pectin mixture, mixing speed 15000r/min, mixing time 10min, then uses High-pressure homogeneous to prepare thin breast, high-pressure homogeneous pressure is 50Mpa, and homogenization cycles are 5 times, both obtain lactoferrin-high methoxy pectin Fast energy lotion.
Comparative example 7
The preparation method of lactoferrin-high methoxy pectin mixed liquor is:0.4g lactoferrins are dissolved in 94.16g water In, it is 7 to adjust pH, and 90 DEG C of high temperature is denatured 20 minutes, is rapidly cooled to room temperature, adjusts after pH is 8 and adds 0.4g high methoxyl fruits Glue, is lactoferrin-high methoxy pectin mixture in 40 DEG C of stirring in water bath dissolvings.
Weigh soybean oil 1.5g, olive oil 1.25g, median chain triglyceride oil 1.5g, 0.05g vitamin E, fish oil 0.75g The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly at room temperature.Oil phase is added into lactoferrin-height High-speed stirred mixing is carried out after methoxy group pectin mixture, mixing speed 15000r/min, mixing time 10min, obtains Lactoferrin-high methoxy pectin speed can lotion.
Comparative example 8
Weigh soybean oil 1.5g, olive oil 1.25g, median chain triglyceride oil 1.5g, 0.05g vitamin E, fish oil 0.75g The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly at room temperature.Carried out after oil phase is added to the water Mix, both having obtained lactoferrin-high methoxy pectin speed can lotion.
Comparative example 9
0.4g lactoferrins are dissolved in 94.16g water, add 0.4g high methoxy pectin, it is molten in 40 DEG C of stirring in water bath Solution.
Weigh soybean oil 1.5g, olive oil 1.25g, median chain triglyceride oil 1.5g, 0.05g vitamin E, fish oil 0.75g The oil phase of obtained lactoferrin-high methoxy pectin speed energy lotion is stirred evenly at room temperature.Oil phase is added into lactoferrin-height Progress high-speed stirred mixing after methoxy group pectin mixture, mixing speed 15000r/min, mixing time 10min, then Thin breast is prepared using high-pressure homogeneous, high-pressure homogeneous pressure is 50Mpa, and homogenization cycles are 5 times, both obtain lactoferrin-high methoxyl Pectin speed can lotion.
The physicochemical property of the lactoferrin prepared to embodiment 1-5 and comparative example 6-9-high methoxy pectin speed energy lotion is examined Survey the results are shown in Table 1:
The physicochemical property testing result of 1 lactoferrin of table-high methoxy pectin speed energy lotion
Conclusion:The combination and specific processing of lactoferrin, high methoxy pectin, oil phase and water according to specified quantitative in formula Technique can form good fluidity, stable in storage lactoferrin-high methoxy pectin speed energy lotion, and contrast the breast of case formation Liquid can be unstable, so that lamination occur.
Table 2:External digestion is evaluated
Conclusion:The lactoferrin prepared with case study on implementation 1-5-high methoxy pectin speed energy lotion has good fluidity, passes through Storage keeps homogeneous flowable without lamination.PH stat are the devices of the outer gastroenteric environment of an analogue body, pass through body Lipid digestion process of the outer simulated emulsion in the case of pancreatic juice and bile exist, can predict that lipid discharges lotion in the gastrointestinal tract Behavior.For this method using in the buffer system of Tris- maleic acids (Tris-maleate), the lipid in lotion can be first by pancreas fat Fat enzyme hydrolysis generates free fatty, makes the pH of system reduce, with steatolysis in certain density sodium hydroxide solution acid-base titration The free fatty gone out, makes system maintain constant pH, so that steatolysis process can continue, passes through the sodium hydroxide body of consumption Accumulated amount can calculate the speed and degree that lipid in lotion is digested indirectly, so as to obtain dietary fiber data.External digestion is real Test and show:Compared with comparative example 7,8,9, case study on implementation 2 can hydrolyze lotion rapidly at first 5 minutes in lipid, can quickly carry For energy.

Claims (3)

1. the preparation method of a kind of lactoferrin-high methoxy pectin speed energy drink, it is characterised in that including following parts by weight Raw material:
0.05~0.6 part of lactoferrin, 0.05~0.6 part of high methoxy pectin, 78.8~94.9 parts of water phase, vitamin E 0.05 ~0.2 part, 1.5~6 parts of soybean oil, 1.25~5 parts of olive oil, 1.5~6 parts of median chain triglyceride oil, 0.75~3 part of fish oil;
Preparation method comprises the following steps:
(1) lactoferrin is dissolved in water, adjusting pH is 6.5~7.5,80~95 DEG C of high-temperature denatured, denaturation times 15~25 Minute, then room temperature is rapidly cooled to, and adjust after pH is 7.5~8.3 and add high methoxy pectin, it is molten in 30~50 DEG C of stirring in water bath Solution is lactoferrin-high methoxy pectin mixture;
(2) oil phase will be obtained after vitamin E, soybean oil, olive oil, median chain triglyceride oil and fish oil uniformly mixing;
(3) high-speed stirred mixing is carried out after the ferritin-high methoxy pectin mixed liquor is added into oil phase, then it is equal through high pressure The thin breast that matter obtains is lactoferrin-high methoxy pectin speed can drink.
2. the preparation method of lactoferrin as claimed in claim 1-high methoxy pectin speed energy drink, it is characterised in that institute State in step (3), it is 10 000~20 000r/min to control mixing speed, and mixing time is 5~15min.
3. the preparation method of lactoferrin as claimed in claim 1 or 2-high methoxy pectin speed energy drink, it is characterised in that In the step (3), high-pressure homogeneous pressure is 10~80Mpa, and homogenization cycles are 2~10 times.
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US9186640B2 (en) * 2007-08-28 2015-11-17 Pepsico, Inc. Delivery and controlled release of encapsulated lipophilic nutrients
EP2292102A1 (en) * 2009-09-02 2011-03-09 Lipofoods, S.L. Microcapsules containing salts for food products
CN103876006B (en) * 2012-12-20 2016-01-20 丰益(上海)生物技术研发中心有限公司 Emulsifier combination, comprise its stable instant microemulsion, and preparation method thereof
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