CN106436275B - A kind of method for sorting of long-acting washable natural antibacterial fabric - Google Patents
A kind of method for sorting of long-acting washable natural antibacterial fabric Download PDFInfo
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- CN106436275B CN106436275B CN201610977371.4A CN201610977371A CN106436275B CN 106436275 B CN106436275 B CN 106436275B CN 201610977371 A CN201610977371 A CN 201610977371A CN 106436275 B CN106436275 B CN 106436275B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention discloses a kind of method for sorting of long-acting washable natural antibacterial fabric, includes the following steps：(1) by textile pad in antibiotic essential oil Liposomal suspensions, second dipping and rolling；(2) under conditions of partial pressure of oxygen is 0.5~0.8 atmospheric pressure, with the fabric for the treatment of with UV radiation step (1)；Wherein, UV wavelength range is 200~400nm, irradiation time is 30~60s, the ultraviolet irradiation intensity of fabric surface is 80~100mW/cm2；(3) fabric for handling step (2), carries out crosslink finishing with genipin, washes, drying.Method disclosed by the invention uses pure natural antibacterial finishing agent and auxiliary agent, greatly reduce the use of synthesis of chemicals, it is more environmentally-friendly, the biocompatibility of its textile article is more preferably, and it is greatly reduced the volatility of essential oil and release property, fastness to washing and Different Tear Test intensity are increased, its antibacterial functions is enhanced.
Description
Technical field
The present invention relates to functional textile technical fields, more particularly to a kind of arrangement of long-acting washable natural antibacterial fabric
Method.
Background technique
With the transformation of consumption idea and concept of health, people have the requirement updated to textile, have health care thus
The textile of effect gains great popularity.
More nano silver, nano zine oxide, nano-ceramic powder, TiO are studied at present2Equal inorganic antiseptics are used for cotton fabric
It arranges, preferable antibiotic health care performance can be obtained.But metal ion be easy to be changed into oxide or be reduced to simple substance and
Discoloration, influencing fabric color, especially silver ion or nano-Ag particles has genotoxic potential to reproductive system and liver.Some light
The metal oxide of catalysis, it is bad in the skin surface antibacterial effect being protected from light.In addition, metal in the fabric enters nothing after environment
Method is converted or is enriched with, it is thus possible to lead to disruption of ecological balance.There are also intrinsic defects for quaternary ammonium salt, such as：It is easy to soak from fabric
Out, incompatible with anionic surfactant etc..DC company has produced a kind of type siloxane quaternary ammonium salt antiseptic
(AEM5700), it can be covalently bound to fabric surface, there is lasting antibacterial activity.However this quarternary ammonium salt compound is anti-
Bacterium activity is also due to the absorption of dust or the microorganism that dies or positive quaternary ammonium salt and negative surfactant are washing repeatedly
It forms compound in the process and reduces performance or failure.In addition, biguanides are weaker to the antibacterial action of fungi, and to the resistance to of light
It is not strong by property.Triclosan is to the resistance of bacterium it has been reported that and attracting attention.But since it can have been generated in the sun
More chlorine Dioxins compounds of poison, therefore forbidden using in fabric and many other products by many countries.In short, big portion
Point the organic synthesis antibacterial antiplaque agent period is short, safety and poor chemical stability, be also easy to produce microorganism drug resistance, lead to them
Application range it is limited.Importantly, metal and metal oxide, organic antibacterial agent are produced by nonrenewable resources
, under the impact of crisis of resource, it is bound to cause these antibacterial agent manufacturing costs and increases substantially, be unfavorable for the hair of antibiotic finish
Exhibition.
One ideal textiles antibacterial finishing will not only kill harmful bacteria and prevent the propagation of disease, while also must satisfy
Three basic demands：Firstly, safety：Product should not have excessive toxicity to the mankind and environment, should not cause skin allergy and thorn
Swash；Secondly, compatible：Negative effect must be not present to properties of textile or appearance in product, it is necessary to flat textile product technique
It is compatible；Third, durability：Product should be able to be resistant to washing and drying, and be not easy to leach from fabric.It is final in order to reach this
Purpose, natural antibacterial agent are one of optimal selections.Because antimicrobial natural active material can be used in production safety, it is nontoxic, environmentally friendly,
The bioactivity textile non-stimulated to skin, therefore its application in the biological functional of textile fabric seems more and more heavier
It wants.And natural antibacterial agent is from a wealth of sources, and it is more to measure big type, and action target spot multiplicity, has a broad antifungal spectrum is not likely to produce drug resistance.Cause
This, it is necessary to antimicrobial natural active material is combined with modern textiles finishing technique, cotton fabric is arranged, not only
It is beneficial to prevent fabric to be stained by microorganism, it is often more important that the propagation for preventing disease ensure that the safety and comfort of human body, drop
The low cross-infection rate of public environment.This pursues health, green, the theory of environmental protection with people and fits like a glove, and has weight
Big social benefit.
Summary of the invention
A kind of in view of the deficiencies of the prior art, the present invention provides antibacterials lasting, washable long-acting washable natural antibacterial fabric
Method for sorting.
The present invention is realized by following technological means solves above-mentioned technical problem：A kind of long-acting washable natural antibacterial fabric
Method for sorting, include the following steps：
(1) by textile pad in antibiotic essential oil Liposomal suspensions, second dipping and rolling；
(2) under conditions of partial pressure of oxygen is 0.5~0.8 atmospheric pressure, with the fabric for the treatment of with UV radiation step (1)；Its
In, UV wavelength range is 200~400nm, irradiation time is 30~60s, the ultraviolet irradiation intensity of fabric surface be 80~
100mW/cm2；
(3) fabric for handling step (2), carries out crosslink finishing with genipin, washes, drying.
Preferably, the antibacterial plant essential oil is one of tea tree ethereal oil, eucalyptus quintessence oil.
Preferably, the concentration of antibacterial plant essential oil Liposomal suspensions is 10~30g/L in step (1).
It preferably, is 3~5 by bath raio by fabric:1 pads in antibiotic essential oil Liposomal suspensions, second dipping and rolling.
Preferably, nip pressure is 0.1~0.25MPa, and pick-up is 80~100%.
Preferably, the genipin is Geniposide, oleuropein, procyanidine, catechin, one in tannic acid
Kind.
Preferably, the concentration of the genipin is 15~30g/L.
Preferably, cross-linking reaction temperature is 80~90 DEG C, and the reaction time is 0.5~1h.
Preferably, washing temperature is 80~95 DEG C, and drying temperature is 100~120 DEG C.
A kind of fabric that the method for sorting using above-mentioned long-acting washable natural antibacterial fabric arranges.
The advantage of the invention is that：(1) the strong ultraviolet irradiation under oxygen atmosphere is used, the terpene in essential oil is ultraviolet and ultraviolet
Corresponding alcohol, aldehyde, ketone or carboxylic acid are oxidized in the lower ozone generated of effect.These terpene derivants have stronger antibacterial work
Property, and boiling point also accordingly increases, and such active constituent is not volatile, and fabric fungistatic effect is more longlasting.
(2) antibacterial finishing agent used is plants essential oil liposome, and also source is natural for finishing auxiliaries and crosslinking agent, right
Environment and human body are all very friendly, and environmental hazard and human body will not be caused to poison.
(3) it after ultraviolet and ozonidation, and uses genipin crosslinking curing and arranges.By terpene and its
Oxidized derivatives are crosslinked, and are crosslinked with fabric itself, form one layer of Antimicrobial preservative protective film in fabric surface.At this
Reason method improves the tearing strength and fastness to washing of fabric, and further improves the fastness to washing of antibacterial.
(4) widely used, it can be used as medical material, anti-biotic material, textile garment material, health hygienic, antibacterial nursing etc..
Specific embodiment
To further describe the present invention, it is described further below with reference to embodiment.
Fabric of the invention is cotton fabric, it is of course also possible to fine using the woven fabric of other natural fibers or synthesis
Tie up woven fabric.
Embodiment 1
The present embodiment discloses the method for sorting of natural antibacterial fabric, includes the following steps：
It (1) is 4 by bath raio by fabric:1 pads in the suspension of the liposome of eucalyptus quintessence oil containing 20g/L, and second dipping and rolling is rolled
Roller pressure is 0.2MPa, pick-up 95%；
(2) under conditions of partial pressure of oxygen is 0.75 atmospheric pressure, with the fabric for the treatment of with UV radiation step (1)；Wherein, purple
Outer wave-length coverage is 260nm, the ultraviolet irradiation intensity of irradiation time 50s, fabric surface is 90mW/cm2；
(3) fabric for handling step (2), carries out crosslink finishing with Geniposide, washes, drying；Wherein Geniposide is dense
Degree is 25g/L, and cross-linking reaction temperature is 90 DEG C, reaction time 1h；Washing temperature is 90 DEG C, and drying temperature is 120 DEG C.
Embodiment 2
The present embodiment discloses the method for sorting of natural antibacterial fabric, includes the following steps：
It (1) is 3 by bath raio by fabric:1 pads in the suspension of the liposome of tea tree ethereal oil containing 10g/L, second dipping and rolling, roll
Pressure is 0.1MPa, pick-up 80%；
(2) under conditions of partial pressure of oxygen is 0.5 atmospheric pressure, with the fabric for the treatment of with UV radiation step (1)；Wherein, purple
Outer wave-length coverage is 200nm, the ultraviolet irradiation intensity of irradiation time 30s, fabric surface is 80mW/cm2；
(3) fabric for handling step (2), carries out crosslink finishing with catechin, washes, drying；Wherein catechin is dense
Degree is 15g/L, and cross-linking reaction temperature is 80 DEG C, reaction time 0.5h；Washing temperature is 80 DEG C, and drying temperature is 100 DEG C.
Embodiment 3
The present embodiment discloses the method for sorting of natural antibacterial fabric, includes the following steps：
It (1) is 5 by bath raio by fabric:1 pads in the suspension of the liposome of eucalyptus quintessence oil containing 30g/L, and second dipping and rolling is rolled
Roller pressure is 0.25MPa, pick-up 100%；
(2) under conditions of partial pressure of oxygen is 0.8 atmospheric pressure, with the fabric for the treatment of with UV radiation step (1)；Wherein, purple
Outer wave-length coverage is 400nm, the ultraviolet irradiation intensity of irradiation time 60s, fabric surface is 100mW/cm2；
(3) fabric for handling step (2), carries out crosslink finishing with oleuropein, washes, drying；Wherein oleuropein
Concentration be 30g/L, cross-linking reaction temperature be 85 DEG C, reaction time 1h；Washing temperature is 95 DEG C, and drying temperature is 110 DEG C.
The present invention discloses a kind of suspension preparation method of plants essential oil liposome, as follows：
(1) plants essential oil is added to phosphate buffer solution, obtains plants essential oil/phosphate buffer solution；Wherein, phosphorus
The pH value of hydrochlorate buffer solution is 7；
It (2) will be 1 according to the mass ratio of the material:1.1:1.1:1.2:1:1.1 natural phospholipid, phosphatidyl choline, glycerol phosphorus
Rouge, phosphatidyl-ethanolamine, phosphatidylserine, phosphatidic acid mixing, obtain phosphatide acid blend；Cholesterol, phosphatide acid-mixed is added
Close object, the mass ratio of cholesterol is 7:1；It is dissolved in the container equipped with chloroform；It rotates at room temperature, removes solvent, hold
Wall forms lipid membrane.
(3) plants essential oil/phosphate buffer solution is preheated to 55 DEG C in 50 DEG C of ultrasonic water bath, (2) is added and are covered with
In the container of lipid membrane, sonic oscillation；Ultrasonic time is 10min, supersonic frequency 300MHz, vibration frequency be 150 turns/
min；Wherein the mass ratio of plants essential oil and film in container is 3:1；
Wherein the preparation method of liposome includes the following steps：
Natural phospholipid of the invention is selected from soybean lecithin, naturally it is also possible to select egg yolk lecithin or other existing skills
The natural phospholipid of art.
Phosphatidyl choline is selected from 1- myristoyl -2- stearyl lecithin, naturally it is also possible to be two palmityl ovum
One of phosphatide, distearyl acyl group lecithin or 1- palmityl -2- stearyl lecithin or other prior arts
Phosphatidyl choline.
Glycerophosphatide is selected from dipalmitoylphosphatidylglycerol sodium salt, naturally it is also possible to select distearoylphosphatidylglycerol sodium
Salt or other prior arts glycerophosphatide.
Phosphatidyl-ethanolamine is selected from dimyristoylphosphatidylethanolamine, naturally it is also possible to select two palmityl phosphatidyl second
The phosphatidyl-ethanolamine of hydramine or Distearoyl Phosphatidylethanolamine or other prior arts.
Phosphatidylserine is selected from two palmityl phosphatidylserine sodium salts, can also select distearoylphosphatidyl silk ammonia
The phosphatidylserine of acid sodium-salt or other prior arts.
Phosphatidic acid is selected from di-myristoyl phosphatidic acid sodium salt, naturally it is also possible to select dipalmitophosphatidic acid sodium salt or two meat
The phosphatidylserine of myristoyl phosphatide acid sodium-salt or other prior arts.
The preparation method of the suspension of certain plants essential oil liposome of the present invention is not limited to the above method, any prior art
The preparation method of the suspension of plants essential oil liposome all should be within protection scope of the present invention.
Comparative example 1：
A kind of method of plants essential oil liposome finish fabric, includes the following steps：
It (1) is 5 by bath raio by fabric:1 pads in the suspension of the liposome of tea tree ethereal oil containing 30g/L, second dipping and rolling, roll
Pressure is 0.25MPa, pick-up 100%.
(2) fabric for handling step (1), 95 DEG C of washings, 120 DEG C of drying.
Comparative example 2：
A kind of method of plants essential oil liposome finish fabric, includes the following steps：
It (1) is 3 by bath raio by fabric:1 pads in the suspension of the liposome of tea tree ethereal oil containing 10g/L, second dipping and rolling, roll
Pressure is 0.1MPa, pick-up 80%.
(2) it is with wave-length coverage in the oxygen atmosphere that partial pressure of oxygen is 0.5 atmospheric pressure by the fabric of step (1) processing
The ultraviolet irradiation of 200nm is handled, and the ultraviolet irradiation intensity of fabric surface is 80mW/cm2, irradiation time 30s.
(3) fabric for handling step (2), 80 DEG C of washings, 100 DEG C of drying.
Comparative example 3：
A kind of method of plants essential oil liposome finish fabric, includes the following steps：
It (1) is preferably 4 by bath raio by fabric:1 pads in the suspension of the liposome of eucalyptus quintessence oil containing 20g/L, two leachings two
It rolls, nip pressure 0.2MPa, pick-up 95%.
(2) fabric for handling step (1), is immersed in 25g/L genipin solution and carries out crosslink finishing, reaction temperature is
90 DEG C, reaction time 1h.Then 90 DEG C of washings, 120 DEG C of drying.
Embodiment 4
The washable number experiment of fabric：Six kinds of fabrics as obtained by above-described embodiment 1~3 and comparative example 1~3, according to
Staphylococcus aureus, Escherichia coli, white are read after its washing of AATCC100-2004 and AATCC124-2006 standard test
Pearl bacterium, pseudomonas aeruginosa, proteus, micrococcus scarlatinae fungistatic effect are shown in Table 1.
Table 1
The present invention arrange after fabric, to staphylococcus aureus, Escherichia coli, Candida albicans, P. aeruginosa
Bacterium, proteus, micrococcus scarlatinae have a significant inhibitory effect, durable antibacterial effect, after up to 50 times washings still
Keep higher broad-spectrum antibacterial rate.And in comparative example, after washing for several times, the inhibitory effect of various microorganisms is substantially reduced.
Embodiment 5
Tearing strength before and after textile finishing is measured using YG-026 type fabric strength instrument, test result is shown in Table 2.
Table 2
Compared to comparative example 1~3, the present invention arranges after fabric, tearing strength is up to 420N or more, before comparing arrangement
It increases.Especially embodiment 1 arrange after fabric, tearing strength is up to 440N, compared to improved before arrangement 4.2% with
On.Illustrate the fabric after the present invention arranges, crosslinking is sufficiently, its strength retentivity is preferable, does not have not only to fabric physical property itself
Loss, there is facilitation effect instead.
The above is only the preferred embodiments of the invention, are not intended to limit the invention creation, all in the present invention
Made any modifications, equivalent replacements, and improvements etc., should be included in the guarantor of the invention within the spirit and principle of creation
Within the scope of shield.
Claims (6)
1. a kind of fabric finishing process of long-acting washable natural antibacterial, which is characterized in that include the following steps：
(1) by textile pad in the plants essential oil Liposomal suspensions of antibacterial, it is 3~5 that fabric, which is pressed bath raio,:1 pads in plant
In essential oil Liposomal suspensions, second dipping and rolling, nip pressure is 0.1~0.25MPa, and pick-up is 80~100%；
(2) fabric that step (1) is handled is handled with ultraviolet irradiation in oxygen atmosphere, wherein in oxygen atmosphere, partial pressure of oxygen
For 0.5-0.8 atmospheric pressure；UV wavelength range is 200-400nm, and the ultraviolet irradiation intensity of fabric surface is 80-100mW/cm2,
Irradiation time is 30-60s；
(3) fabric for handling step (2), carries out crosslink finishing with genipin, washes, drying；Wherein, genipin
Working concentration be 15~30g/L, cross-linking reaction temperature be 80-90 DEG C, reaction time 0.5-1h.
2. the fabric finishing process of long-acting washable natural antibacterial according to claim 1, which is characterized in that in step (1),
The plants essential oil liposome of the antibacterial is one of tea tree ethereal oil liposome and eucalyptus quintessence oil liposome.
3. the fabric finishing process of long-acting washable natural antibacterial according to claim 1, which is characterized in that in step (1),
The concentration of essential oil liposome is 10-30g/L.
4. the fabric finishing process of long-acting washable natural antibacterial according to claim 1, which is characterized in that in step (3),
Genipin is one of Geniposide, oleuropein, procyanidine, catechin, tannic acid.
5. the fabric finishing process of long-acting washable natural antibacterial according to claim 1, which is characterized in that in step (3),
Washing temperature is 80-95 DEG C, and drying temperature is 100-120 DEG C.
6. what the fabric finishing process of long-acting washable natural antibacterial was prepared described in any one of Claims 1 to 5 knits
Object.
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| CN106948163A (en) * | 2017-03-23 | 2017-07-14 | 鑫缘茧丝绸集团股份有限公司 | A kind of preparation method of the silk fabric of antibiosis anti-acarien |
| CN110373897B (en) * | 2019-07-15 | 2021-09-10 | 南通大学 | Natural washable anti-hypha and wool fabric finishing method |
| CN110453492B (en) * | 2019-08-12 | 2021-09-24 | 南通大学 | Long-acting washable antibacterial fabric finishing method |
| WO2022121420A1 (en) * | 2020-12-09 | 2022-06-16 | 华南农业大学 | Ultraviolet sterilization synergist and sterilization method using same in combination with ultraviolet |
| CN113863004B (en) * | 2021-09-28 | 2024-01-26 | 衣拉拉集团股份有限公司 | Mosquito-repellent antibacterial plant traditional Chinese medicine essential oil composition and preparation method of mosquito-repellent antibacterial functional cotton knitted fabric |
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| CN103966847A (en) * | 2014-04-16 | 2014-08-06 | 南通大学 | Method for finishing fabric through plant essential oil thermosensitive liposomes |
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| CN1592578A (en) * | 2001-10-04 | 2005-03-09 | 以色列国家农业部富卡尼中心 | Microbiocidal formulation comprising essential oils or their derivatives |
| CN102733184A (en) * | 2012-07-18 | 2012-10-17 | 南通大学 | Finishing technology for aromatic anti-bacteria cotton textile |
| CN103147310A (en) * | 2013-03-27 | 2013-06-12 | 南通苏州大学纺织研究院 | Method for finishing cotton fabrics through spraying plant essential oil |
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Effective date of registration: 20190723 Address after: 528231 Second Floor on the Right of Gate 3, Beihai Industrial Zone, Yanbu River West Land, Dali Town, Nanhai District, Foshan City, Guangdong Province Patentee after: Foshan Nanhai Yijia Underwear Co., Ltd. Address before: 226000 Nine Road, Siyuan Road, Nantong City, Jiangsu Province Patentee before: Nantong University |