CN106436275A - Settling method for long-acting washable natural antibacterial fabric - Google Patents
Settling method for long-acting washable natural antibacterial fabric Download PDFInfo
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- CN106436275A CN106436275A CN201610977371.4A CN201610977371A CN106436275A CN 106436275 A CN106436275 A CN 106436275A CN 201610977371 A CN201610977371 A CN 201610977371A CN 106436275 A CN106436275 A CN 106436275A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
Abstract
The invention discloses a settling method for a long-acting washable natural antibacterial fabric. The method comprises the following steps: (1) padding the fabric in an antibacterial essential oil liposome suspension, soaking for two times and padding for two times; (2) treating the fabric acquired in the step (1) with ultraviolet radiation under the condition of oxygen partial pressure at 0.5-0.8 Pa, wherein the scope of ultraviolet wavelength is 200-400nm, the radiation time is 30-60s, and the strength of ultraviolet radiation on the fabric surface is 80-100mW/cm<2>; and (3) adopting a natural cross-linking agent for cross-linking the fabric treated in the step (2), washing with water and then drying. According to the method disclosed by the invention, the natural antibacterial settling agent and auxiliaries are adopted, so that the use of compound chemicals is greatly reduced, the settling method is more environment-friendly, the biocompatibility of the fabric products is better, the volatility and release property of essential oil are greatly reduced, the fastness to washing and the tearing strength of the fabric are increased, and the antibacterial function of the fabric is enhanced.
Description
Technical field
The present invention relates to functional textile technical field, more particularly to a kind of arrangement of long-acting washable natural antibacterial fabric
Method.
Background technology
With the transformation of consumption idea and concept of health, people have, to textile, the requirement for updating, have health care for this
The textile of effect gains great popularity.
More nanometer silver, nano zine oxide, nano-ceramic powder, TiO are studied at present2It is used for bafta Deng inorganic antiseptic
Arrange, be obtained in that preferable antibiotic health care performance.But metal ion be easily changed into oxide or be reduced to simple substance and
Discoloration, impact fabric color, particularly silver ion or nano-Ag particles have genotoxic potential to reproductive system and liver.Some light
The metal-oxide of catalysis, not good in the skin surface antibacterial effect of lucifuge.In addition, after the metal in fabric enters environment no
Method is converted or is enriched with, it is thus possible to cause disruption of ecological balance.Quaternary ammonium salt also has some intrinsic defects, such as：Easily soak from fabric
Go out, incompatible with anion surfactant etc..DC company has produced a kind of type siloxane quaternary ammonium salt antiseptic
(AEM5700), fabric face can be covalently bound to, with lasting antibacterial activity.But this quarternary ammonium salt compound is anti-
Bacterium activity is also due to the absorption or positive quaternary ammonium salt of dust or microorganism of dying and negative surfactant are in cyclic washing
During formed complex and reduce performance or failure.In addition, biguanideses are weaker to the antibacterial action of funguses, and to the resistance to of light
Not strong by property.Triclosan has had document report to the resistance of antibacterial, and receives publicity.But as which can produce in the sun
Many chlorine Dioxins compound of poison, is therefore forbidden used in fabric and many other products by many countries.In a word, big portion
Organic synthesiss antibacterial antiplaque agent cycle is short, safety and the poor chemical stability that divides, is also easy to produce microorganism drug resistance, causes them
Range of application be limited.Importantly, metal and metal-oxide, organic antibacterial agent are produced by nonrenewable resources
, under the impact of crisis of resource, these antibacterial manufacturing costs certainly will be caused to increase substantially, be unfavorable for sending out for antibiotic finish
Exhibition.
One preferable textiles antibacterial finishing will not only kill harmful bacteria and prevent transmission of disease, while must also being fulfilled for
Three basic demands：First, safety：Product should not have excessive toxicity to the mankind and environment, should not cause skin allergy and thorn
Swash；Secondly, compatibility：Must there is no negative effect to properties of textile or outward appearance in product, it is necessary to flat textile product technique
Compatible；3rd, durability：Product should be able to tolerate washing and dry, and be not easy to leach from fabric.Final in order to reach this
Purpose, natural antibacterial agent is one of optimum selection.Because antimicrobial natural active substance can be used in production safety, nontoxic, environmental protection,
The biological activity textile non-stimulated to skin, therefore its application in the biological functional of textile fabric seems more and more heavier
Will.And natural antibacterial agent wide material sources, measure that big species is many, action target spot is various, has a broad antifungal spectrum, is not likely to produce drug resistance.Cause
This, it is necessary to antimicrobial natural active substance is combined with modern textiles finishing technique, bafta is arranged, not only
Fabric is desirably prevented to be stained by microorganism, it is often more important that to prevent transmission of disease, it is ensured that the safety and comfort of human body, drop
The low cross-infection rate of public environment.This pursues healthy, green, environmental protection theory with people and fits like a glove, with weight
Big social benefit.
Content of the invention
The present invention is directed to the deficiencies in the prior art, provides a kind of antibacterial lasting, washable long-acting washable natural antibacterial fabric
Method for sorting.
The present invention realizes solving above-mentioned technical problem by following technological means：A kind of long-acting washable natural antibacterial fabric
Method for sorting, comprise the steps：
(1) by textile pad in antibiotic essential oil Liposomal suspensions, two leachings two are rolled；
(2) under conditions of partial pressure of oxygen is 0.5～0.8 atmospheric pressure, with the fabric for the treatment of with uv radiation step (1)；Its
In, UV wavelength range is 200～400nm, exposure time is 30～60s, the ultraviolet irradiation intensity of fabric face be 80～
100mW/cm2；
(3) fabric for processing step (2), carries out crosslink finishing with genipin, washing, dries.
Preferably, the antibacterial plant quintessence oil be tea tree ethereal oil, the one kind in eucalyptus quintessence oil.
Preferably, in step (1), the concentration of antibacterial plant quintessence oil Liposomal suspensions is 10～30g/L.
Preferably, it is 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～5 3～:1 pads in antibiotic essential oil Liposomal suspensions, and two leachings two are rolled.
Preferably, nip pressure is 0.1～0.25MPa, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is 80～100%, and pick-up is.
Preferably, the genipin be genipin, oleuropein, procyanidin, catechin, in tannic acid one
Kind.
Preferably, the concentration of the genipin is 15～30g/L.
Preferably, it is 0.5～1h in 80～90 DEG C, response time that cross-linking reaction temperature is.
Preferably, washing temperature is that 80～95 DEG C, drying temperature is 100～120 DEG C.
The fabric that a kind of method for sorting using above-mentioned long-acting washable natural antibacterial fabric is arranged.
It is an advantage of the current invention that：(1) using the strong ultraviolet irradiation under oxygen atmosphere, the terpenoid in quintessence oil is ultraviolet and ultraviolet
Corresponding alcohol, aldehyde, ketone or carboxylic acid are oxidized in the lower ozone for generating of effect.These terpene derivants have higher antibacterial work
Property, and boiling point also accordingly raises, and such active component is not volatile, and fabric fungistatic effect is more longlasting.
(2) antibacterial finishing agent for adopting be plants essential oil liposome, and finishing auxiliarieses and cross-linking agent also originate natural, right
Environment and human body are all very friendly, and environmental hazard and human body will not be caused to poison.
(3) after ultraviolet and ozonidation, the arrangement of genipin crosslinking curing is employed again.By terpenoid and its
Oxidized derivatives are crosslinked, and are crosslinked with fabric in itself, form one layer of Antimicrobial preservative protecting film in fabric face.At this
Reason method improves the tearing strength of fabric and fastness to washing, and further increases the fastness to washing of antibacterial.
(4) of many uses, can be used as medical material, anti-biotic material, textile garment material, health hygienic, antibacterial nursing etc..
Specific embodiment
For further describing the present invention, with reference to embodiment, which is described further.
The fabric of the present invention is bafta, it is of course also possible to fine using the woven fabric of other natural fibers or synthesis
Tie up woven fabric.
Embodiment 1
The present embodiment discloses the method for sorting of natural antibacterial fabric, comprises the steps：
(1) it is 4:1 pads in the suspension of the liposome of eucalyptus quintessence oil containing 20g/L, and two leachings two are rolled, and roll
Roller pressure is 0.2MPa, and pick-up is 95%；
(2) under conditions of partial pressure of oxygen is 0.75 atmospheric pressure, with the fabric for the treatment of with uv radiation step (1)；Wherein, purple
Outer wave-length coverage is 260nm, exposure time is 50s, the ultraviolet irradiation intensity of fabric face is 90mW/cm2；
(3) fabric for processing step (2), carries out crosslink finishing with genipin, washing, dries；Wherein genipin is dense
Spend for 25g/L, it is 1h in 90 DEG C, response time that cross-linking reaction temperature is；Washing temperature is 90 DEG C, and drying temperature is 120 DEG C.
Embodiment 2
The present embodiment discloses the method for sorting of natural antibacterial fabric, comprises the steps：
(1) it is 3:1 pads in the suspension of the liposome of tea tree ethereal oil containing 10g/L, and two leachings two are rolled, roll
Pressure is 0.1MPa, and pick-up is 80%；
(2) under conditions of partial pressure of oxygen is 0.5 atmospheric pressure, with the fabric for the treatment of with uv radiation step (1)；Wherein, purple
Outer wave-length coverage is 200nm, exposure time is 30s, the ultraviolet irradiation intensity of fabric face is 80mW/cm2；
(3) fabric for processing step (2), carries out crosslink finishing with catechin, washing, dries；Wherein catechin is dense
Spend for 15g/L, it is 0.5h in 80 DEG C, response time that cross-linking reaction temperature is；Washing temperature is 80 DEG C, and drying temperature is 100 DEG C.
Embodiment 3
The present embodiment discloses the method for sorting of natural antibacterial fabric, comprises the steps：
(1) it is 5:1 pads in the suspension of the liposome of eucalyptus quintessence oil containing 30g/L, and two leachings two are rolled, and roll
Roller pressure is 0.25MPa, and pick-up is 100%；
(2) under conditions of partial pressure of oxygen is 0.8 atmospheric pressure, with the fabric for the treatment of with uv radiation step (1)；Wherein, purple
Outer wave-length coverage is 400nm, exposure time is 60s, the ultraviolet irradiation intensity of fabric face is 100mW/cm2；
(3) fabric for processing step (2), carries out crosslink finishing with oleuropein, washing, dries；Wherein oleuropein
Concentration be 30g/L, cross-linking reaction temperature be 85 DEG C, the response time be 1h；Washing temperature is 95 DEG C, and drying temperature is 110 DEG C.
The present invention discloses a kind of suspension preparation method of plants essential oil liposome, as follows：
(1) plants essential oil is added to phosphate buffered solution, obtains plants essential oil/phosphate buffered solution；Wherein, phosphorus
The pH value of hydrochlorate buffer solution is 7；
(2) by the amount ratio according to material be 1:1.1:1.1:1.2:1:1.1 natural phospholipid, phosphatidylcholine, glycerol phosphorus
Fat, PHOSPHATIDYL ETHANOLAMINE, Phosphatidylserine, phosphatidic acid mixing, obtain phospholipid acid blend；Cholesterol is added, phosphatidic acid is mixed
Compound, the mass ratio of cholesterol are 7:1；It is dissolved in the container equipped with chloroform；Revolving under conditions of room temperature, removes solvent, holds
Wall forms lipid membrane.
(3) 55 DEG C are preheated in 50 DEG C of ultrasonic water bath, plants essential oil/phosphate buffered solution, add (2) to be covered with
In the container of lipid membrane, sonic oscillation；Ultrasonic time be 10min, supersonic frequency be 300MHz, frequency of vibration be 150 turns/
min；Wherein plants essential oil is 3 with the mass ratio of thin film in container:1；
The preparation method of wherein liposome is comprised the following steps：
The natural phospholipid of the present invention is selected from soybean lecithin, naturally it is also possible to from Egg Yolk Lecithin (PC-98T) or other existing skills
The natural phospholipid of art.
Phosphatidylcholine is selected from 1- myristoyl -2- stearyl lecithin, naturally it is also possible to for two palmityl ovum
One kind in phospholipid, distearyl acyl group lecithin or 1- palmityl -2- stearyl lecithin, or other prior arts
Phosphatidylcholine.
Phosphoglyceride is selected from DPPG sodium salt, naturally it is also possible to select Distearoyl Phosphatidyl Glycerol-Na Salt
Salt or or other prior arts phosphoglyceride.
PHOSPHATIDYL ETHANOLAMINE is selected from DMPEA, naturally it is also possible to from two palmityl phosphatidyl second
Hydramine or the PHOSPHATIDYL ETHANOLAMINE of DSPE or other prior arts.
Phosphatidylserine is selected from two palmityl Phosphatidylserine sodium salts, it is also possible to from distearoylphosphatidyl silk ammonia
Acid sodium-salt or the Phosphatidylserine of other prior arts.
Phosphatidic acid is selected from two myristoyl phospholipid acid sodium-salts, naturally it is also possible to from DPPA sodium salt or two meat
Myristoyl phospholipid acid sodium-salt or the Phosphatidylserine of other prior arts.
Certainly the preparation method of the suspension of plants essential oil liposome of the present invention is not limited to said method, any prior art
The preparation method of the suspension of plants essential oil liposome all should be within protection scope of the present invention.
Comparative example 1：
A kind of method of plants essential oil liposome finish fabric, comprises the steps：
(1) it is 5:1 pads in the suspension of the liposome of tea tree ethereal oil containing 30g/L, and two leachings two are rolled, roll
Pressure is 0.25MPa, and pick-up is 100%.
(2) fabric that step (1) is processed, 95 DEG C of washings, 120 DEG C of drying.
Comparative example 2：
A kind of method of plants essential oil liposome finish fabric, comprises the steps：
(1) it is 3:1 pads in the suspension of the liposome of tea tree ethereal oil containing 10g/L, and two leachings two are rolled, roll
Pressure is 0.1MPa, and pick-up is 80%.
(2) fabric that step (1) is processed, in the oxygen atmosphere that partial pressure of oxygen is 0.5 atmospheric pressure, with wave-length coverage be
The ultraviolet irradiation of 200nm is processed, and the ultraviolet irradiation intensity of fabric face is 80mW/cm2, exposure time is 30s.
(3) fabric that step (2) is processed, 80 DEG C of washings, 100 DEG C of drying.
Comparative example 3：
A kind of method of plants essential oil liposome finish fabric, comprises the steps：
(1) it is preferably 4 fabric to be pressed bath raio:1 pads in the suspension of the liposome of eucalyptus quintessence oil containing 20g/L, two leachings two
Roll, it is 95% that nip pressure is 0.2MPa, pick-up.
(2) fabric for processing step (1), being immersed in 25g/L genipin solution carries out crosslink finishing, and reaction temperature is
90 DEG C, the response time is 1h.Then 90 DEG C of washings, 120 DEG C of drying.
Embodiment 4
The washable number of times experiment of fabric：Six kinds of fabrics obtained by above-described embodiment 1～3 and comparative example 1～3, according to
After its washing of AATCC100-2004 and AATCC124-2006 standard test, staphylococcus aureuses, escherichia coli, white are read
Pearl bacterium, Pseudomonas aeruginosa, Bacillus proteuss, micrococcus scarlatinae fungistatic effect are shown in Table 1.
Table 1
The present invention arranged after fabric, to staphylococcus aureuses, escherichia coli, Candida albicans, P. aeruginosa
Bacterium, Bacillus proteuss, micrococcus scarlatinae all have a significant inhibition, durable antibacterial effect, after up to 50 times washings still
Keep higher broad-spectrum antibacterial rate.And in comparative example, after washing for several times, the inhibition of various microorganisms is substantially reduced.
Embodiment 5
Tearing strength before and after textile finishing is determined using YG-026 type fabric strength instrument, test result is shown in Table 2.
Table 2
Compare comparative example 1～3, the present invention arranged after fabric, its tearing strength be up to more than 420N, compare arrangement before
Increase.Fabric after especially embodiment 1 is arranged, its tearing strength is up to 440N, improve before comparing arrangement 4.2% with
On.Fabric after arranging through the present invention is described, crosslinking fully, its strength retentivity preferably, fabric physical property itself not only not
Loss, has facilitation effect on the contrary.
The preferred embodiment of the invention is these are only, not in order to limit the invention, all in the present invention
Any modification, equivalent and improvement that is made within the spirit and principle of creation etc., should be included in the guarantor of the invention
Within the scope of shield.
Claims (10)
1. a kind of method for sorting of long-acting washable natural antibacterial fabric, it is characterised in that comprise the steps：
(1) by textile pad in antibiotic essential oil Liposomal suspensions, two leachings two are rolled；
(2) under conditions of partial pressure of oxygen is 0.5～0.8 atmospheric pressure, with the fabric for the treatment of with uv radiation step (1)；Wherein, purple
Outer wave-length coverage is 200～400nm, exposure time is 30～60s, the ultraviolet irradiation intensity of fabric face is 80～100mW/
cm2；
(3) fabric for processing step (2), carries out crosslink finishing with genipin, washing, dries.
2. the method for sorting of long-acting washable natural antibacterial fabric according to claim 1, it is characterised in that the antibacterial is planted
Thing quintessence oil is tea tree ethereal oil, the one kind in eucalyptus quintessence oil.
3. the method for sorting of long-acting washable natural antibacterial fabric according to claim 1, it is characterised in that in step (1)
The concentration of antibacterial plant quintessence oil Liposomal suspensions is 10～30g/L.
4. the method for sorting of long-acting washable natural antibacterial fabric according to claim 1, it is characterised in that by fabric by bath
Than for 3～5:1 pads in antibiotic essential oil Liposomal suspensions, and two leachings two are rolled.
5. the method for sorting of long-acting washable natural antibacterial fabric according to claim 4, it is characterised in that nip pressure is
0.1～0.25MPa, pick-up is 80～100%.
6. the method for sorting of long-acting washable natural antibacterial fabric according to claim 1, it is characterised in that the natural friendship
Connection agent is genipin, oleuropein, procyanidin, catechin, the one kind in tannic acid.
7. the method for sorting of long-acting washable natural antibacterial fabric according to claim 1, it is characterised in that the natural friendship
The concentration of connection agent is 15～30g/L.
8. the method for sorting of long-acting washable natural antibacterial fabric according to claim 1, it is characterised in that cross-linking reaction temperature
Spend for 80～90 DEG C, the response time is 0.5～1h.
9. the method for sorting of long-acting washable natural antibacterial fabric according to claim 1, it is characterised in that washing temperature is
80～95 DEG C, drying temperature is 100～120 DEG C.
10. a kind of method for sorting of long-acting washable natural antibacterial fabric of use as described in any one of claim 1～9 is arranged
Fabric.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106948163A (en) * | 2017-03-23 | 2017-07-14 | 鑫缘茧丝绸集团股份有限公司 | A kind of preparation method of the silk fabric of antibiosis anti-acarien |
| CN110373897A (en) * | 2019-07-15 | 2019-10-25 | 南通大学 | A kind of natural washable antibacterial silk, woolen method for sorting |
| CN110453492A (en) * | 2019-08-12 | 2019-11-15 | 南通大学 | A kind of fabric finishing method of long-acting washable antibacterial |
| CN113863004A (en) * | 2021-09-28 | 2021-12-31 | 衣拉拉集团股份有限公司 | Mosquito-repelling antibacterial plant traditional Chinese medicine essential oil composition and preparation method of cotton knitted fabric with mosquito-repelling antibacterial function |
| WO2022121420A1 (en) * | 2020-12-09 | 2022-06-16 | 华南农业大学 | Ultraviolet sterilization synergist and sterilization method using same in combination with ultraviolet |
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| CN102733184A (en) * | 2012-07-18 | 2012-10-17 | 南通大学 | Finishing technology for aromatic anti-bacteria cotton textile |
| CN103147310A (en) * | 2013-03-27 | 2013-06-12 | 南通苏州大学纺织研究院 | Method for finishing cotton fabrics through spraying plant essential oil |
| CN103966847A (en) * | 2014-04-16 | 2014-08-06 | 南通大学 | Method for finishing fabric through plant essential oil thermosensitive liposomes |
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| CN106948163A (en) * | 2017-03-23 | 2017-07-14 | 鑫缘茧丝绸集团股份有限公司 | A kind of preparation method of the silk fabric of antibiosis anti-acarien |
| CN110373897A (en) * | 2019-07-15 | 2019-10-25 | 南通大学 | A kind of natural washable antibacterial silk, woolen method for sorting |
| CN110373897B (en) * | 2019-07-15 | 2021-09-10 | 南通大学 | Natural washable anti-hypha and wool fabric finishing method |
| CN110453492A (en) * | 2019-08-12 | 2019-11-15 | 南通大学 | A kind of fabric finishing method of long-acting washable antibacterial |
| CN110453492B (en) * | 2019-08-12 | 2021-09-24 | 南通大学 | Long-acting washable antibacterial fabric finishing method |
| WO2022121420A1 (en) * | 2020-12-09 | 2022-06-16 | 华南农业大学 | Ultraviolet sterilization synergist and sterilization method using same in combination with ultraviolet |
| CN113863004A (en) * | 2021-09-28 | 2021-12-31 | 衣拉拉集团股份有限公司 | Mosquito-repelling antibacterial plant traditional Chinese medicine essential oil composition and preparation method of cotton knitted fabric with mosquito-repelling antibacterial function |
| CN113863004B (en) * | 2021-09-28 | 2024-01-26 | 衣拉拉集团股份有限公司 | Mosquito-repellent antibacterial plant traditional Chinese medicine essential oil composition and preparation method of mosquito-repellent antibacterial functional cotton knitted fabric |
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