CN106398677A - 一种驱油有机硅表面活性剂及其制备方法 - Google Patents
一种驱油有机硅表面活性剂及其制备方法 Download PDFInfo
- Publication number
- CN106398677A CN106398677A CN201610785259.0A CN201610785259A CN106398677A CN 106398677 A CN106398677 A CN 106398677A CN 201610785259 A CN201610785259 A CN 201610785259A CN 106398677 A CN106398677 A CN 106398677A
- Authority
- CN
- China
- Prior art keywords
- displacement
- organic silicon
- unsaturated polyether
- reservoir oil
- silicon surfactant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000004094 surface-active agent Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims description 11
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 29
- 239000010703 silicon Substances 0.000 claims abstract description 29
- 230000000694 effects Effects 0.000 claims abstract description 7
- 229920000570 polyether Polymers 0.000 claims description 34
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 31
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 31
- 238000006073 displacement reaction Methods 0.000 claims description 30
- 239000003921 oil Substances 0.000 claims description 30
- 239000002253 acid Substances 0.000 claims description 15
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000003054 catalyst Substances 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 10
- RSNQKPMXXVDJFG-UHFFFAOYSA-N tetrasiloxane Chemical compound [SiH3]O[SiH2]O[SiH2]O[SiH3] RSNQKPMXXVDJFG-UHFFFAOYSA-N 0.000 claims description 9
- 238000010792 warming Methods 0.000 claims description 9
- OWXJKYNZGFSVRC-NSCUHMNNSA-N (e)-1-chloroprop-1-ene Chemical compound C\C=C\Cl OWXJKYNZGFSVRC-NSCUHMNNSA-N 0.000 claims description 7
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 239000001294 propane Substances 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
- 230000006837 decompression Effects 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 239000003999 initiator Substances 0.000 claims description 5
- SWGZAKPJNWCPRY-UHFFFAOYSA-N methyl-bis(trimethylsilyloxy)silicon Chemical compound C[Si](C)(C)O[Si](C)O[Si](C)(C)C SWGZAKPJNWCPRY-UHFFFAOYSA-N 0.000 claims description 5
- 238000006116 polymerization reaction Methods 0.000 claims description 5
- 238000010992 reflux Methods 0.000 claims description 5
- 230000000630 rising effect Effects 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- JECYNCQXXKQDJN-UHFFFAOYSA-N 2-(2-methylhexan-2-yloxymethyl)oxirane Chemical compound CCCCC(C)(C)OCC1CO1 JECYNCQXXKQDJN-UHFFFAOYSA-N 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000000376 reactant Substances 0.000 claims description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 239000012467 final product Substances 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- 239000000693 micelle Substances 0.000 abstract description 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 3
- -1 Siloxanes Chemical class 0.000 description 3
- 125000001539 acetonyl group Chemical group [H]C([H])([H])C(=O)C([H])([H])* 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000010668 complexation reaction Methods 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 125000003368 amide group Chemical group 0.000 description 2
- 150000002430 hydrocarbons Chemical group 0.000 description 2
- 125000001165 hydrophobic group Chemical group 0.000 description 2
- 125000001181 organosilyl group Chemical group [SiH3]* 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000013530 defoamer Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000002563 ionic surfactant Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 description 1
- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 239000004223 monosodium glutamate Substances 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 125000003698 tetramethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/58—Compositions for enhanced recovery methods for obtaining hydrocarbons, i.e. for improving the mobility of the oil, e.g. displacing fluids
- C09K8/584—Compositions for enhanced recovery methods for obtaining hydrocarbons, i.e. for improving the mobility of the oil, e.g. displacing fluids characterised by the use of specific surfactants
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
- C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/32—Polymers modified by chemical after-treatment
- C08G65/329—Polymers modified by chemical after-treatment with organic compounds
- C08G65/336—Polymers modified by chemical after-treatment with organic compounds containing silicon
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Polyethers (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Silicon Polymers (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201610785259.0A CN106398677B (zh) | 2016-08-31 | 2016-08-31 | 一种驱油有机硅表面活性剂及其制备方法 |
Applications Claiming Priority (1)
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CN201610785259.0A CN106398677B (zh) | 2016-08-31 | 2016-08-31 | 一种驱油有机硅表面活性剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN106398677A true CN106398677A (zh) | 2017-02-15 |
CN106398677B CN106398677B (zh) | 2019-04-09 |
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CN201610785259.0A Active CN106398677B (zh) | 2016-08-31 | 2016-08-31 | 一种驱油有机硅表面活性剂及其制备方法 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111019624A (zh) * | 2019-12-23 | 2020-04-17 | 郑州洁灵科技有限公司 | 一种驱油用纳米微乳液的制备及其应用 |
CN114796074A (zh) * | 2022-05-08 | 2022-07-29 | 广州市盛美化妆品有限公司 | 一种含芦荟枸杞植物精粹的保湿舒缓面霜及其制备方法 |
CN115637141A (zh) * | 2021-07-20 | 2023-01-24 | 中国石油天然气股份有限公司 | 一种碳酸盐岩气藏解水锁剂及其制备方法 |
Citations (8)
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CN101233160A (zh) * | 2005-07-26 | 2008-07-30 | 巴斯福股份公司 | 含硅氧烷基团的共聚物、其制备方法和用途 |
CN101942083A (zh) * | 2010-09-10 | 2011-01-12 | 广东标美硅氟新材料有限公司 | 一种有机硅化合物及其制备方法和应用 |
CN102527096A (zh) * | 2011-05-12 | 2012-07-04 | 湖北新四海化工股份有限公司 | 一种有机硅消泡剂及其制备方法 |
CN103417388A (zh) * | 2005-03-07 | 2013-12-04 | 戴博全球保健有限公司 | 含有有机硅表面活性剂的高醇含量发泡组合物 |
CN104312256A (zh) * | 2014-11-07 | 2015-01-28 | 北京优美特纳米材料科技有限公司 | 一种聚醚改性三硅氧烷润湿剂及其制备与应用方法 |
CN104448323A (zh) * | 2014-12-18 | 2015-03-25 | 江苏美思德化学股份有限公司 | 一种星形梳状聚醚有机硅共聚物及其制备方法 |
CN105032281A (zh) * | 2015-07-23 | 2015-11-11 | 南雄鼎成化工有限公司 | 一种抑泡的有机硅湿润剂 |
CN105669968A (zh) * | 2015-12-30 | 2016-06-15 | 中山大学惠州研究院 | 一种聚醚接枝三硅氧烷表面活性剂的制备方法 |
-
2016
- 2016-08-31 CN CN201610785259.0A patent/CN106398677B/zh active Active
Patent Citations (8)
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CN103417388A (zh) * | 2005-03-07 | 2013-12-04 | 戴博全球保健有限公司 | 含有有机硅表面活性剂的高醇含量发泡组合物 |
CN101233160A (zh) * | 2005-07-26 | 2008-07-30 | 巴斯福股份公司 | 含硅氧烷基团的共聚物、其制备方法和用途 |
CN101942083A (zh) * | 2010-09-10 | 2011-01-12 | 广东标美硅氟新材料有限公司 | 一种有机硅化合物及其制备方法和应用 |
CN102527096A (zh) * | 2011-05-12 | 2012-07-04 | 湖北新四海化工股份有限公司 | 一种有机硅消泡剂及其制备方法 |
CN104312256A (zh) * | 2014-11-07 | 2015-01-28 | 北京优美特纳米材料科技有限公司 | 一种聚醚改性三硅氧烷润湿剂及其制备与应用方法 |
CN104448323A (zh) * | 2014-12-18 | 2015-03-25 | 江苏美思德化学股份有限公司 | 一种星形梳状聚醚有机硅共聚物及其制备方法 |
CN105032281A (zh) * | 2015-07-23 | 2015-11-11 | 南雄鼎成化工有限公司 | 一种抑泡的有机硅湿润剂 |
CN105669968A (zh) * | 2015-12-30 | 2016-06-15 | 中山大学惠州研究院 | 一种聚醚接枝三硅氧烷表面活性剂的制备方法 |
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Title |
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贾赟,等: "星型羧基改性聚醚硅氧烷的合成及应用", 《印染》 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111019624A (zh) * | 2019-12-23 | 2020-04-17 | 郑州洁灵科技有限公司 | 一种驱油用纳米微乳液的制备及其应用 |
CN115637141A (zh) * | 2021-07-20 | 2023-01-24 | 中国石油天然气股份有限公司 | 一种碳酸盐岩气藏解水锁剂及其制备方法 |
CN115637141B (zh) * | 2021-07-20 | 2023-08-01 | 中国石油天然气股份有限公司 | 一种碳酸盐岩气藏解水锁剂及其制备方法 |
CN114796074A (zh) * | 2022-05-08 | 2022-07-29 | 广州市盛美化妆品有限公司 | 一种含芦荟枸杞植物精粹的保湿舒缓面霜及其制备方法 |
CN114796074B (zh) * | 2022-05-08 | 2023-08-15 | 广州市盛美化妆品有限公司 | 一种含芦荟枸杞植物精粹的保湿舒缓面霜及其制备方法 |
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Effective date of registration: 20220524 Address after: 441200 Taoyuan Road South, West Ring 4th Road West, Zaoyang City, Xiangyang City, Hubei Province Patentee after: Hubei Longsheng Sihai New Material Co.,Ltd. Address before: 441200 building 3, group 5, Nancheng Wangjiawan community neighborhood committee, Zaoyang City, Xiangfan City, Hubei Province Patentee before: HUBEI NEW SIHAI CHEMICAL INDUSTRY CO.,LTD. |
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Denomination of invention: A silicone surfactant for oil recovery and its preparation method Granted publication date: 20190409 Pledgee: Bank of China Limited Xiangyang Branch Pledgor: Hubei Longsheng Sihai New Material Co.,Ltd. Registration number: Y2024980006288 |