CN106398005A - Processing technology of rubber product - Google Patents

Processing technology of rubber product Download PDF

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Publication number
CN106398005A
CN106398005A CN201610789653.1A CN201610789653A CN106398005A CN 106398005 A CN106398005 A CN 106398005A CN 201610789653 A CN201610789653 A CN 201610789653A CN 106398005 A CN106398005 A CN 106398005A
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CN
China
Prior art keywords
rubber
parts
time
processing technique
temperature
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Pending
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CN201610789653.1A
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Chinese (zh)
Inventor
朱新洁
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Individual
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Individual
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Priority to CN201610789653.1A priority Critical patent/CN106398005A/en
Publication of CN106398005A publication Critical patent/CN106398005A/en
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/18Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
    • C08L23/20Homopolymers or copolymers of hydrocarbons having four or more carbon atoms having four to nine carbon atoms
    • C08L23/22Copolymers of isobutene; Butyl rubber ; Homo- or copolymers of other iso-olefins
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/011Nanostructured additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

The invention discloses a processing technology of a rubber product. The processing technology comprises the following steps: (1) mixing raw materials, and performing primary blending, wherein the raw materials are as follows: 100 parts of rubber, 2 to 4 parts of an activator, 3 to 4 parts of a promoter, 2 to 3 parts of an antiaging agent, 20 to 25 parts of a filler and 1 to 4 parts of a softener, and are blended at the blending temperature of 80 to 85 DEG C for 27 to 30 seconds, and the rubber is polyurethane rubber and butyl rubber; (2) adding 1 part of the softener and 3 parts of the activator again for secondary blending at the temperature of 85 to 90 DEG C for 20 to 25 seconds, then performing third blending and adding 1 part of the activator again, keeping the third blending for 10 seconds, cooling and discharging rubber; (3) adding 16 to 18 parts of a vulcanizing agent into the rubber for refining. The technology is simple, and the prepared rubber is long in service life, heat-resistant, oil-resistant, ozone-resistant and high in tensile strength.

Description

The processing technique of rubber
Technical field
The present invention relates to a kind of processing technique of rubber.
Background technology
In power system, electrician usually needs live line work, for avoiding staff to have the danger of electric shock in the course of the work Danger, people are set with the rubber with insulating properties on the handle of electrician's used tool, but current such rubber is frequently run onto and makes With short life, heat-resisting, oil resistant, resistance to ozone, the low problem of tensile strength, one kind is therefore provided to have long service life, heat-resisting, resistance to Comfortable feel that what oily, resistance to ozone, tensile strength were high the have and rubber with high-insulativity is that those skilled in the art need badly The problem solving.
Content of the invention
The present invention has designed and developed a kind of processing technique of rubber, obtained rubber long service life, heat-resisting, resistance to Oil, resistance to ozone, tensile strength is high.
The present invention provide technical scheme be:
A kind of processing technique of rubber, comprises the following steps:
Step (1), by each raw material mixing based on following parts by weight, carries out kneading for the first time, and wherein, each raw material is rubber 100 parts of glue, 2~4 parts of activating agent, 3~4 parts of accelerator, 2~3 parts of age resistor, 20~25 parts of filler, 1~4 part of softening agent, mixes Refining temperature is 80~85 DEG C, and the persistent period is 27~30s;Described rubber is polyurethane rubber and butyl rubber, polyurethane rubber With the weight of butyl rubber than for 1:11;
Step (2) adds 1 part of softening agent and 3 parts of activating agent carries out second mixing, and the time is 20~25s, and temperature is 85~90 DEG C, carry out third time afterwards again and knead, add 1 part of activating agent, the time is 10s, cool down dumping afterwards;
Add 16~18 parts of vulcanizing agent in the glue that step (3) obtains to step (2), turned refining, the time is 90~93s, Temperature is 90~95 DEG C.
Preferably, in the processing technique of described rubber, in described step (3), vulcanizing agent is 18 parts.
Preferably, in the processing technique of described rubber, in described step (2), the time is 22s, and temperature is 86 ℃.
Preferably, in the processing technique of described rubber, in described step (3), the time is 90s, and temperature is 94 ℃.
Preferably, in the processing technique of described rubber, in described step (1), melting temperature is 81 DEG C, continues Time is 27s.
Preferably, in the processing technique of described rubber, described activating agent is zinc oxide, and described accelerator is two Thiocarbamate;Described age resistor is p-phenylenediamine age resistor;Described filler is nanoclay;Described softening agent is stone Wax;Described vulcanizing agent is curing resin.
The processing technique process is simple of rubber of the present invention, obtained rubber long service life, heat-resisting, resistance to Oil, resistance to ozone, tensile strength is high.
Specific embodiment
The present invention is described in further detail below, with make those skilled in the art with reference to specification word being capable of evidence To implement.
The present invention provides a kind of processing technique of rubber, comprises the following steps:
Step (1), by each raw material mixing based on following parts by weight, carries out kneading for the first time, and wherein, each raw material is rubber 100 parts of glue, 2~4 parts of activating agent, 3~4 parts of accelerator, 2~3 parts of age resistor, 20~25 parts of filler, 1~4 part of softening agent, mixes Refining temperature is 80~85 DEG C, and the persistent period is 27~30s;Described rubber is polyurethane rubber and butyl rubber, polyurethane rubber With the weight of butyl rubber than for 1:11.
Step (2) adds 1 part of softening agent and 3 parts of activating agent carries out second mixing, and the time is 20~25s, and temperature is 85~90 DEG C, carry out third time afterwards again and knead, add 1 part of activating agent, the time is 10s, cool down dumping afterwards.At second During mixing, add a small amount of softening agent and activating agent, this will be helpful to reduce the time required for vulcanization reaction again.In order to improve The effect of mixing, has also carried out third time mixing, and has wherein added minimal amount of activating agent, and the time controlling this mixing is 10s, begins to dumping afterwards.
Add 16~18 parts of vulcanizing agent in the glue that step (3) obtains to step (2), turned refining, the time is 90~93s, Temperature is 90~95 DEG C.
The present invention adopts polyurethane rubber and butyl rubber, and the careful design ratio of the two, the rubber that finally synthesizes Glue has good insulating properties, resistance to ozone, ageing-resistant, thermostability, and have have good wearability, oil resistivity and high intensity, High resiliency.
And, the sulfiding process temperature of the present invention is low, cure time is short, the rubber anti-tensile that obtains, surely stretch, wear-resisting Performance is good.
Preferably, in the processing technique of described rubber, in described step (3), vulcanizing agent is 18 parts.
Preferably, in the processing technique of described rubber, in described step (2), the time is 22s, and temperature is 86 ℃.
Preferably, in the processing technique of described rubber, in described step (3), the time is 90s, and temperature is 94 ℃.
Preferably, in the processing technique of described rubber, in described step (1), melting temperature is 81 DEG C, continues Time is 27s.
Preferably, in the processing technique of described rubber, described activating agent is zinc oxide, and described accelerator is two Thiocarbamate;Described age resistor is p-phenylenediamine age resistor;Described filler is nanoclay;Described softening agent is stone Wax;Described vulcanizing agent is curing resin.
Although embodiment of the present invention is disclosed as above, it is not restricted to listed in description and embodiment With, it can be applied to various suitable the field of the invention completely, for those skilled in the art, can be easily Realize other modification, therefore under the general concept being limited without departing substantially from claim and equivalency range, the present invention does not limit In specific details.

Claims (6)

1. a kind of processing technique of rubber is it is characterised in that comprise the following steps:
Step (1), by each raw material mixing based on following parts by weight, carries out kneading for the first time, and wherein, each raw material is rubber 100 Part, 2~4 parts of activating agent, 3~4 parts of accelerator, 2~3 parts of age resistor, 20~25 parts of filler, 1~4 part of softening agent, mixing temperature Spend for 80~85 DEG C, the persistent period is 27~30s;Described rubber is polyurethane rubber and butyl rubber, polyurethane rubber and fourth The weight of base rubber is than for 1:11;
Step (2) adds 1 part of softening agent and 3 parts of activating agent carries out second mixing, and the time is 20~25s, and temperature is 85~ 90 DEG C, carry out third time afterwards again and knead, add 1 part of activating agent, the time is 10s, cool down dumping afterwards;
Add 16~18 parts of vulcanizing agent in the glue that step (3) obtains to step (2), turned refining, the time is 90~93s, temperature For 90~95 DEG C.
2. the processing technique of rubber as claimed in claim 1 is it is characterised in that in described step (3), vulcanizing agent is 18 Part.
3. it is characterised in that in described step (2), the time is 22s to the processing technique of rubber as claimed in claim 1, Temperature is 86 DEG C.
4. it is characterised in that in described step (3), the time is 90s to the processing technique of rubber as claimed in claim 1, Temperature is 94 DEG C.
5. the processing technique of rubber as claimed in claim 1 is it is characterised in that in described step (1), melting temperature is 81 DEG C, the persistent period is 27s.
6. the processing technique of rubber as claimed in claim 1 is it is characterised in that described activating agent is zinc oxide, described Accelerator is dithiocar-bamate;Described age resistor is p-phenylenediamine age resistor;Described filler is nanoclay;Described Softening agent is paraffin;Described vulcanizing agent is curing resin.
CN201610789653.1A 2016-08-31 2016-08-31 Processing technology of rubber product Pending CN106398005A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610789653.1A CN106398005A (en) 2016-08-31 2016-08-31 Processing technology of rubber product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610789653.1A CN106398005A (en) 2016-08-31 2016-08-31 Processing technology of rubber product

Publications (1)

Publication Number Publication Date
CN106398005A true CN106398005A (en) 2017-02-15

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107400300A (en) * 2017-08-25 2017-11-28 江苏菲勒电气有限公司 A kind of high-strength rubber

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6548570B1 (en) * 1999-11-16 2003-04-15 Arntz Beteiligungs Gmbh & Co. Kg Method for manufacturing a radiation shielding material
CN103421326A (en) * 2013-08-30 2013-12-04 安徽金科橡塑制品有限公司 Cold-resistant rubber and preparation method thereof
CN103756329A (en) * 2013-12-25 2014-04-30 广东阿尔派新材料股份有限公司 Non-conducting rubber applied to power cable accessories and preparation method of non-conducting rubber
CN104592655A (en) * 2015-01-21 2015-05-06 柳州市颖航汽配有限公司 Preparation method of insulated rubber

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6548570B1 (en) * 1999-11-16 2003-04-15 Arntz Beteiligungs Gmbh & Co. Kg Method for manufacturing a radiation shielding material
CN103421326A (en) * 2013-08-30 2013-12-04 安徽金科橡塑制品有限公司 Cold-resistant rubber and preparation method thereof
CN103756329A (en) * 2013-12-25 2014-04-30 广东阿尔派新材料股份有限公司 Non-conducting rubber applied to power cable accessories and preparation method of non-conducting rubber
CN104592655A (en) * 2015-01-21 2015-05-06 柳州市颖航汽配有限公司 Preparation method of insulated rubber

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107400300A (en) * 2017-08-25 2017-11-28 江苏菲勒电气有限公司 A kind of high-strength rubber

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Application publication date: 20170215

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