CN106393350A - Preparation method for insect preventing powder for rattan-weaved artware - Google Patents

Preparation method for insect preventing powder for rattan-weaved artware Download PDF

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Publication number
CN106393350A
CN106393350A CN201610783458.8A CN201610783458A CN106393350A CN 106393350 A CN106393350 A CN 106393350A CN 201610783458 A CN201610783458 A CN 201610783458A CN 106393350 A CN106393350 A CN 106393350A
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China
Prior art keywords
powder
radix
water
mixed solution
mixture
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CN201610783458.8A
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Chinese (zh)
Inventor
张晓玲
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Sky Funan County Hundred Million Arts & Crafts Co Ltd
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Sky Funan County Hundred Million Arts & Crafts Co Ltd
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Priority to CN201610783458.8A priority Critical patent/CN106393350A/en
Publication of CN106393350A publication Critical patent/CN106393350A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/002Cane, bamboo
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/20Removing fungi, molds or insects

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention relates to a preparation method for insect preventing powder for rattan-weaved artware. The preparation method mainly comprises the following steps of: firstly preparing powder of root of kudzu vine, putting the powder in a bottle, igniting the powder, putting residual burned black particles in a bowl, adding 3 parts of edible oil and stirring the mixture for later use; adding epoxy resin and floral water in a stirrer, stirring the mixture to obtain a mixed solution, then heating and stirring the mixture, and taking out 70% of the mixed solution for later use; adding diethylenetriamine, tricresyl phosphate and butadiene-acrylonitrile rubber into the stirrer and continuously stirring the mixture with 30% of the mixed solution for 10 minutes to obtain a mixed solution II, adding essence into the mixed solution II, stirring and mixing the mixture, screening the mixture by a 200-mesh sieve, taking out a solid residue, adding the particles mixed with the edible oil, and burning the mixture obtained to obtain an insect preventing particle semi-product; and grinding the insect preventing particle semi-product, mixing the ground insect preventing particle semi-product with the 70% of the mixed solution, performing distillation till water is evaporated, taking out the residue, and performing granulation and crushing to obtain the insect preventing powder. The preparation method provided by the invention is colorless, tasteless and non-toxic, plays an insect-preventing role and does not corrode the artware.

Description

A kind of rattan plaited artware insect protected powder, preparation method thereof
Technical field:
The present invention relates to artware cleaning maintenance field is and in particular to a kind of rattan plaited artware insect protected powder, preparation method thereof.
Background technology:
Existing artware is attractive in appearance and unique, and typically mostly wooden, bamboo weaving, rattan are prepared from, this artware Outward appearance has stronger aesthetics, but is easily damaged by worms, and now needs a kind of colorless and odorless insect protected powder to be applied on artware, you can Ensure not damaged by worms, degree of not affecting the appearance again.
Content of the invention:
The technical problem to be solved is to overcome the defect of prior art, provides a kind of rattan plaited artware insect protected Powder, preparation method thereof.
The technical problem to be solved employs the following technical solutions to realize.
A kind of rattan plaited artware insect protected powder, preparation method thereof it is characterised in that:Mainly include the following steps that:
Take 50 parts of Radix Puerariaes, dry in the sun, the moisture to Radix Puerariae is less than 10%;
By 1:3 ratio adds confection, is soaked, and winter, with 100 DEG C of boiled water, soaks five or six hours, etc. Substantially blotted to soaking water by Radix Puerariae, with clear water wash away mud in Radix Puerariae fry, impurity, then proceed in cold water, the water surface exceeds bean 10-15 centimetre of face, carries out second immersion, and winter wants 18 hours;
Confection mainly includes Radix Salviae Miltiorrhizae 5-10 part, Cortex Eucommiae 5-10 part, Semen Ginkgo core 10-20 part, Semen Cucumidis sativi 10-20 part, black Bean 2-5 part, Semen Glyciness 2-5 part, remaining is water;First medical material is smashed to pieces, mix with water;
By soaked Radix Puerariae, first pulverized with pulverizer, then use the levigate mill of steel, during upper mill, elder generation Radix Puerariae in 1: 2 ratio Convert medicament, medicament includes:Radix Codonopsis 1-2 part, Radix Ophiopogonis 1-2 part, Bulbus Fritillariae Uninbracteatae 1-2 part, Radix Astragali 5-8 part, Fructus Aurantii 1-2 part, Radix Platycodoniss 1-2 Part, Radix Glycyrrhizae Preparata 1-2 part, Fructus Schisandrae Chinensis 1-2 part, Radix Stemonae 1-2 part, Fructus Perillae 1-2 part, Radix Peucedani 1-2 part, Rhizoma Pinelliae 1-2 part, Fructus Citri tangerinae core 1-2 part, Rhizoma Polygonati Odorati 8-10 part, remaining is water, grinds in filling, adds 1-3 part edible oil, in order to froth breaking, pump used by the slurry of milled during mill bean Stamp the vibrosieve coarse filtration of 50-80 mesh;
Using the Calyx seu fructus physaliss sedimentation method, with pump, the serosity of milled is squeezed in vat, add 30% Calyx seu fructus physaliss, be sufficiently stirred for, extremely PH value is 5.2 about, the time of static 30 minutes, waits after fully precipitating, then the clear water in powder is outwelled, and will form sediment in vat Bisque levers up and stirs evenly, and then, these underflows is pumped on the dusting cover of 150-180 mesh and carries out second filtration, method with thick Filter is identical, and the pulp-water filtering through second is pumped in cylinder, adds the clear water of equivalent, is sufficiently stirred for, then stands, make starch Fully precipitate;
After starch water stands, the supernatant is skimmed standby in little slurry cylinder, pure white solid starch will be left in cylinder Settled layer levers up, and is sling with long cloth, filters off residual moisture, shines powder, extremely to when not dripping, taking out powder ball and transferring on solarization powder platform In powder, water content is less than 20%;
By powder as in bottle, light, be left burned black granule, by granule as in bowl, add 3-5 part edible oil, stir, Stand-by;
Take 10-13 part epoxy resin, 23-24 part floral water to add in agitator, stir 10 minutes, obtain mixed solution, Then in heated and stirred, temperature control at 60-70 DEG C, 10-20 minute, take out 70% mixed solution stand-by;
3-4 part diethylenetriamine, 3-4 part tricresyl phosphate, 30-40 part nitrile rubber is taken to add in agitator, with 30% mixed solution continues stirring 10 minutes, obtains mixed solution two, takes 1-3 part essence to add in mixed solution two, stirring is mixed After conjunction, 200 mesh sieve, and take solid residue, add in the mixed granule of edible oil, are burnt again, obtain insect protected Grain semi-finished product;
Insect protected pellet product is pulverized, mixes with 70% mixed solution, distillation, it is evaporated to moisture content, takes residue, make Grain, pulverizes, obtains insect protected powder.
The present invention has the beneficial effects that:The insect protected powder colorless and odorless of this method preparation is nontoxic, environmental and durable, for artware system After the completion of standby, it is applied to handicraft surface, on the one hand play insect protected effect, there is stronger adsorption function, be difficult to drop, once , up to 30-35 days, on the other hand the insect protected dried bean noodles of this method preparation is dry for vermins-proof effect, will not etching process product, and have certain Burr bating effect, make handicraft surface brighter and cleaner, feel aesthetics is more preferable.
Specific embodiment:
In order that technological means, creation characteristic, reached purpose and effect that the present invention realizes are easy to understand, tie below Conjunction is embodied as, and specifically includes following steps:
Specific embodiment 1:A kind of rattan plaited artware insect protected powder, preparation method thereof, mainly includes the following steps that:
Take 50 parts of Radix Puerariaes, dry in the sun, the moisture to Radix Puerariae is less than 10%;
By 1:3 ratio adds confection, is soaked, and winter, with 100 DEG C of boiled water, soaks five or six hours, etc. Substantially blotted to soaking water by Radix Puerariae, with clear water wash away mud in Radix Puerariae fry, impurity, then proceed in cold water, the water surface exceeds bean 10-15 centimetre of face, carries out second immersion, and winter wants 18 hours;
Confection mainly includes 5 parts of Radix Salviae Miltiorrhizae, 5 parts of the Cortex Eucommiae, 10 parts of Semen Ginkgo core, 10 parts of Semen Cucumidis sativi, 2 parts of Semen sojae atricolor, Semen Glyciness 2 Part, remaining is water;First medical material is smashed to pieces, mix with water;
By soaked Radix Puerariae, first pulverized with pulverizer, then use the levigate mill of steel, during upper mill, elder generation Radix Puerariae in 1: 2 ratio Convert medicament, medicament includes:1 part of Radix Codonopsis, 1 part of Radix Ophiopogonis, 1 part of Bulbus Fritillariae Uninbracteatae, 5 parts of the Radix Astragali, 1 part of Fructus Aurantii, 1 part of Radix Platycodoniss, 1 part of Radix Glycyrrhizae Preparata, 1 part of Fructus Schisandrae Chinensis, 1 part of the Radix Stemonae, 1 part of Fructus Perillae, 1 part of Radix Peucedani, 1 part of the Rhizoma Pinelliae, 1 part of Fructus Citri tangerinae core, 8 parts of Rhizoma Polygonati Odorati, remaining is water, grinds in filling, Add 1 part of edible oil during mill bean, in order to froth breaking, the vibrosieve coarse filtration of 50-80 mesh stamped by the slurry of milled with pump;
Using the Calyx seu fructus physaliss sedimentation method, with pump, the serosity of milled is squeezed in vat, add 30% Calyx seu fructus physaliss, be sufficiently stirred for, extremely PH value is 5.2 about, the time of static 30 minutes, waits after fully precipitating, then the clear water in powder is outwelled, and will form sediment in vat Bisque levers up and stirs evenly, and then, these underflows is pumped on the dusting cover of 150-180 mesh and carries out second filtration, method with thick Filter is identical, and the pulp-water filtering through second is pumped in cylinder, adds the clear water of equivalent, is sufficiently stirred for, then stands, make starch Fully precipitate;
After starch water stands, the supernatant is skimmed standby in little slurry cylinder, pure white solid starch will be left in cylinder Settled layer levers up, and is sling with long cloth, filters off residual moisture, shines powder, extremely to when not dripping, taking out powder ball and transferring on solarization powder platform In powder, water content is less than 20%;
By powder as in bottle, light, be left burned black granule, by granule as in bowl, adding 3 parts of edible oil, stirring, treat With;
Take 10 parts of epoxy resin, 23 parts of floral water to add in agitator, stir 10 minutes, obtain mixed solution, Ran Hou Heated and stirred, temperature control at 60-70 DEG C, 10-20 minute, take out 70% mixed solution stand-by;
Take 3 parts of diethylenetriamines, 3 parts of tricresyl phosphates, 30 parts of nitrile rubbers to add in agitator, mix with 30% molten Liquid continues stirring 10 minutes, obtains mixed solution two, takes 1 part of essence to add in mixed solution two, after stirring mixing, 200 mesh mistakes Sieve, takes solid residue, adds in the mixed granule of edible oil, is burnt again, obtain insect protected pellet product;
Insect protected pellet product is pulverized, mixes with 70% mixed solution, distillation, it is evaporated to moisture content, takes residue, make Grain, pulverizes, obtains insect protected powder.
Specific embodiment 2:A kind of rattan plaited artware insect protected powder, preparation method thereof, mainly includes the following steps that:
Take 50 parts of Radix Puerariaes, dry in the sun, the moisture to Radix Puerariae is less than 10%;
By 1:3 ratio adds confection, is soaked, and winter, with 100 DEG C of boiled water, soaks five or six hours, etc. Substantially blotted to soaking water by Radix Puerariae, with clear water wash away mud in Radix Puerariae fry, impurity, then proceed in cold water, the water surface exceeds bean 10-15 centimetre of face, carries out second immersion, and winter wants 18 hours;
Confection mainly includes 10 parts of Radix Salviae Miltiorrhizae, 10 parts of the Cortex Eucommiae, 20 parts of Semen Ginkgo core, 20 parts of Semen Cucumidis sativi, 5 parts of Semen sojae atricolor, Semen Glyciness 5 Part, remaining is water;First medical material is smashed to pieces, mix with water;
By soaked Radix Puerariae, first pulverized with pulverizer, then use the levigate mill of steel, during upper mill, elder generation Radix Puerariae in 1: 2 ratio Convert medicament, medicament includes:2 parts of Radix Codonopsis, 2 parts of Radix Ophiopogonis, 2 parts of Bulbus Fritillariae Uninbracteatae, 8 parts of the Radix Astragali, 2 parts of Fructus Aurantii, 2 parts of Radix Platycodoniss, 2 parts of Radix Glycyrrhizae Preparata, 2 parts of Fructus Schisandrae Chinensis, 2 parts of the Radix Stemonae, 2 parts of Fructus Perillae, 2 parts of Radix Peucedani, 2 parts of the Rhizoma Pinelliae, 2 parts of Fructus Citri tangerinae core, 10 parts of Rhizoma Polygonati Odorati, remaining is water, grinds in filling, Add 3 parts of edible oil during mill bean, in order to froth breaking, the vibrosieve coarse filtration of 50-80 mesh stamped by the slurry of milled with pump;
Using the Calyx seu fructus physaliss sedimentation method, with pump, the serosity of milled is squeezed in vat, add 30% Calyx seu fructus physaliss, be sufficiently stirred for, extremely PH value is 5.2 about, the time of static 30 minutes, waits after fully precipitating, then the clear water in powder is outwelled, and will form sediment in vat Bisque levers up and stirs evenly, and then, these underflows is pumped on the dusting cover of 150-180 mesh and carries out second filtration, method with thick Filter is identical, and the pulp-water filtering through second is pumped in cylinder, adds the clear water of equivalent, is sufficiently stirred for, then stands, make starch Fully precipitate;
After starch water stands, the supernatant is skimmed standby in little slurry cylinder, pure white solid starch will be left in cylinder Settled layer levers up, and is sling with long cloth, filters off residual moisture, shines powder, extremely to when not dripping, taking out powder ball and transferring on solarization powder platform In powder, water content is less than 20%;
By powder as in bottle, light, be left burned black granule, by granule as in bowl, adding 5 parts of edible oil, stirring, treat With;
Take 13 parts of epoxy resin, 24 parts of floral water to add in agitator, stir 10 minutes, obtain mixed solution, Ran Hou Heated and stirred, temperature control at 60-70 DEG C, 10-20 minute, take out 70% mixed solution stand-by;
Take 4 parts of diethylenetriamines, 4 parts of tricresyl phosphates, 40 parts of nitrile rubbers to add in agitator, mix with 30% molten Liquid continues stirring 10 minutes, obtains mixed solution two, takes 1-3 part essence to add in mixed solution two, after stirring mixing, 200 mesh Sieve, take solid residue, add in the mixed granule of edible oil, burnt again, obtain insect protected pellet product;
Insect protected pellet product is pulverized, mixes with 70% mixed solution, distillation, it is evaporated to moisture content, takes residue, make Grain, pulverizes, obtains insect protected powder.
Ultimate principle, principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of the industry , it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and description is originally for personnel The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and its Equivalent thereof.

Claims (1)

1. a kind of rattan plaited artware insect protected powder, preparation method thereof it is characterised in that:Mainly include the following steps that:
Take 50 parts of Radix Puerariaes, dry in the sun, the moisture to Radix Puerariae is less than 10%;
By 1:3 ratio adds confection, is soaked, and winter, with 100 DEG C of boiled water, soaks five or six hours, when leaching Soaked substantially blotted by Radix Puerariae, with clear water wash away mud in Radix Puerariae fry, impurity, then proceed in cold water, the water surface exceeds bean flour 10- 15 centimetres, carry out second immersion, winter wants 18 hours;
Confection mainly includes Radix Salviae Miltiorrhizae 5-10 part, Cortex Eucommiae 5-10 part, Semen Ginkgo core 10-20 part, Semen Cucumidis sativi 10-20 part, Semen sojae atricolor 2-5 Part, Semen Glyciness 2-5 part, remaining is water;First medical material is smashed to pieces, mix with water;
By soaked Radix Puerariae, first pulverized with pulverizer, then with the levigate mill of steel, during upper mill, first Radix Puerariae is converted in 1: 2 ratio Medicament, medicament includes:Radix Codonopsis 1-2 part, Radix Ophiopogonis 1-2 part, Bulbus Fritillariae Uninbracteatae 1-2 part, Radix Astragali 5-8 part, Fructus Aurantii 1-2 part, Radix Platycodoniss 1-2 part, process Radix Glycyrrhizae 1-2 part, Fructus Schisandrae Chinensis 1-2 part, Radix Stemonae 1-2 part, Fructus Perillae 1-2 part, Radix Peucedani 1-2 part, Rhizoma Pinelliae 1-2 part, Fructus Citri tangerinae core 1-2 part, Rhizoma Polygonati Odorati 8-10 part, remaining is water, grinds in filling, adds 1-3 part edible oil, in order to froth breaking, the slurry of milled is stamped with pump during mill bean The vibrosieve coarse filtration of 50-80 mesh;
Using the Calyx seu fructus physaliss sedimentation method, with pump, the serosity of milled is squeezed in vat, add 30% Calyx seu fructus physaliss, be sufficiently stirred for, to pH value For 5.2 about, the time of static 30 minutes, wait after fully precipitating, then the clear water in powder is outwelled, by stratum granulosum in vat Lever up and stir evenly, then, these underflows are pumped on the dusting cover of 150-180 mesh and carry out second filtration, method and coarse filtration phase Same, the pulp-water filtering through second is pumped in cylinder, adds the clear water of equivalent, be sufficiently stirred for, then stand, make starch abundant Precipitation;
After starch water stands, the supernatant is skimmed standby in little slurry cylinder, settle leaving pure white solid starch in cylinder Layer levers up, and is sling with long cloth, filters off residual moisture, shines powder, to when not dripping, taking out powder ball and transferring to powder on solarization powder platform Water content is less than 20%;
By powder as in bottle, light, be left burned black granule, by granule as in bowl, adding 3-5 part edible oil, stirring, treat With;
Take 10-13 part epoxy resin, 23-24 part floral water to add in agitator, stir 10 minutes, obtain mixed solution, then In heated and stirred, temperature control at 60-70 DEG C, 10-20 minute, take out 70% mixed solution stand-by;
3-4 part diethylenetriamine, 3-4 part tricresyl phosphate, 30-40 part nitrile rubber is taken to add in agitator, mixed with 30% Close solution and continue stirring 10 minutes, obtain mixed solution two, take 1-3 part essence to add in mixed solution two, after stirring mixing, 200 mesh sieve, and take solid residue, add in the mixed granule of edible oil, are burnt again, obtain insect protected granule half and become Product;
Insect protected pellet product is pulverized, mixes with 70% mixed solution, distillation, it is evaporated to moisture content, take residue, pelletize, Pulverize, obtain insect protected powder.
CN201610783458.8A 2016-08-30 2016-08-30 Preparation method for insect preventing powder for rattan-weaved artware Pending CN106393350A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111015865A (en) * 2019-12-10 2020-04-17 阜南县利民工艺品有限公司 Processing technology of mildew-proof insect-proof rattan plaited handicraft

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103931841A (en) * 2014-04-09 2014-07-23 郎溪县黄香茶叶有限公司 Formula of tea drink beneficial to invigorating spleen and supplementing qi and preparation method of tea drink
CN103960597A (en) * 2014-03-11 2014-08-06 郎溪县天子粉丝厂 Preparation method of broad bean vermicelli
CN104441143A (en) * 2014-09-25 2015-03-25 阜南县星光工艺品有限公司 Cracking-prevention and insect-prevention treatment agent of bamboo skin
CN105010935A (en) * 2015-06-17 2015-11-04 蚌埠市天星树脂有限责任公司 Resin for extracting crude drug of cough relieving medicine and preparation method of the resin for extracting crude drug of cough relieving medicine
CN105695124A (en) * 2016-02-29 2016-06-22 安徽海德石油化工有限公司 Faint scent plant mixed cleaning agent and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103960597A (en) * 2014-03-11 2014-08-06 郎溪县天子粉丝厂 Preparation method of broad bean vermicelli
CN103931841A (en) * 2014-04-09 2014-07-23 郎溪县黄香茶叶有限公司 Formula of tea drink beneficial to invigorating spleen and supplementing qi and preparation method of tea drink
CN104441143A (en) * 2014-09-25 2015-03-25 阜南县星光工艺品有限公司 Cracking-prevention and insect-prevention treatment agent of bamboo skin
CN105010935A (en) * 2015-06-17 2015-11-04 蚌埠市天星树脂有限责任公司 Resin for extracting crude drug of cough relieving medicine and preparation method of the resin for extracting crude drug of cough relieving medicine
CN105695124A (en) * 2016-02-29 2016-06-22 安徽海德石油化工有限公司 Faint scent plant mixed cleaning agent and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111015865A (en) * 2019-12-10 2020-04-17 阜南县利民工艺品有限公司 Processing technology of mildew-proof insect-proof rattan plaited handicraft

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