CN106381695A - Oil for improvement of automobile interior decorative part flashing point - Google Patents
Oil for improvement of automobile interior decorative part flashing point Download PDFInfo
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- CN106381695A CN106381695A CN201610764228.7A CN201610764228A CN106381695A CN 106381695 A CN106381695 A CN 106381695A CN 201610764228 A CN201610764228 A CN 201610764228A CN 106381695 A CN106381695 A CN 106381695A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2243—Mono-, di-, or triglycerides
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/328—Amines the amino group being bound to an acyclic or cycloaliphatic carbon atom
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/11—Starch or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/227—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of hydrocarbons, or reaction products thereof, e.g. afterhalogenated or sulfochlorinated
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses oil for improvement of an automobile interior decorative part flashing point. The oil comprises, by weight, 66-74 parts of a smooth agent, 10-14 parts of an emulsifier, 4-8 parts of an antistatic agent, 6-10 parts of a clustering agent and 3-5 parts of an additive. The oil has a stable spinning oil friction coefficient, high oil film strength and a high oil flashing point, ensures fiber drawing force stability, produces small spinning tension force fluctuation and does not easily produce winding and end breaking.
Description
Technical field
The invention belongs to technical field of automotive upholstery is and in particular to a kind of automotive upholstery fabric flash-point strengthening is oily
Agent.
Background technology
More than in automobile 40, individual loseing needs to use fabric, from cabin air filter, molding seat, roof, compartment lining
Bottom is required for carpet, how to improve the properties of fabric, thus improving comfortableness and the reliability of vehicle, becoming one and asking greatly
Topic.
Content of the invention
Goal of the invention：The problem and shortage existing for above-mentioned prior art, it is an object of the invention to provide a kind of automobile
Inside gadget fabric flash-point strengthening oil preparation.
Technical scheme：The invention discloses a kind of automotive upholstery fabric flash-point strengthening oil preparation, including smooth agent, emulsifying
Agent, antistatic additive, collecting agent and additive, its weight part ratio is：Smooth agent 66-74, emulsifying agent 10-14, antistatic additive 4-8,
Collecting agent 6-10, additive 3-5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or many
Plant the miscella 50-70, trimethylolpropane fatty acid ester 20-30, polyacrylate 10-20 with hydroxy silicon oil；
Described smooth agent adopts following steps：Take the hydroxy silicon oil that viscosity is 210-225 ten thousand CPS and viscosity 72-78CPS
In vegetable oil, animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxyl
The addition of base silicone oil is vegetable oil, animal oil, in mineral oil the addition of any one or more 10-25%；Take three hydroxyls
Methylpropane fatty acid ester, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, are formed primary smooth
Agent, in this primary smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, with acid
Adjust pH value to 4-5, obtain smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 30-60, dimethylamino second
Base acrylate 20-50, APES formaldehyde condensation product 10-30；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 5-20CPS, dimethylamino second
Base acrylate, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150
DEG C, stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：
Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorus in the presence of polyphosphoric acids
Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Again polyphosphoric acids are put in the product after etherificate after being first passed through nitrogen in phosphorylation reaction therein, temperature control
Below 40 DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, 2-4 is little for insulation
When；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% containing amylose content
Etherificate high amylose starchess 50-70, vegetable oil 20-30, Polyethylene Glycol Laurel acid diester 10-20；
The constituent of described additive and its mass fraction are：Fatty alcohol 20-30 part, acrylic acid 20-30 part, azo two
Isobutyl dimethyl phthalate 2-4 part, Polymeric sodium metaphosphate. 3-4 part, Pulvis Talci 20-30 part；
Described additive adopts following steps：By fatty alcohol 20-30 part, acrylic acid 20-30 part, azo two isopropylformic acid. diformazan
Ester 2-4 part, Pulvis Talci 20-30 part, stir at 50-60 DEG C, add Polymeric sodium metaphosphate. 3-4 part, obtain within ultrasonic 20 minutes.
As the optimization further of the present invention, the present invention includes smooth agent, emulsifying agent, antistatic additive, collecting agent and interpolation
Agent, its weight part ratio is：Smooth agent 71, emulsifying agent 14, antistatic additive 4, collecting agent 6, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or many
Plant the miscella 50 with hydroxy silicon oil, trimethylolpropane fatty acid ester 30, polyacrylate 20；
Described smooth agent adopts following steps：Take the hydroxy silicon oil that viscosity is 2,100,000 CPS and viscosity 78CPS vegetable oil,
In animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxy silicon oil
Addition be vegetable oil, animal oil, in mineral oil the addition of any one or more 25%；Take trimethylolpropane fat
Fat acid esters, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, in this primary
In smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, with acid for adjusting pH value extremely
4-5, obtains smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 30, dimethylaminoethyl
Acrylate 50, APES formaldehyde condensation product 20；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 15CPS, dimethylaminoethyl
Acrylate, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150 DEG C,
Stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：
Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorus in the presence of polyphosphoric acids
Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Again polyphosphoric acids are put in the product after etherificate after being first passed through nitrogen in phosphorylation reaction therein, temperature control
Below 40 DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, 2-4 is little for insulation
When；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% containing amylose content
Etherificate high amylose starchess 50, vegetable oil 30, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：20 parts of fatty alcohol, 30 parts of acrylic acid, azo two isopropylformic acid.
2 parts of dimethyl ester, 3 parts of Polymeric sodium metaphosphate., 20 parts of Pulvis Talci；
Described additive adopts following steps：By 20 parts of fatty alcohol, 30 parts of acrylic acid, 2 parts of azo-bis-iso-dimethyl,
20 parts of Pulvis Talci, stirs at 50-60 DEG C, adds 3 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
As the optimization further of the present invention, the present invention includes smooth agent, emulsifying agent, antistatic additive, collecting agent and interpolation
Agent, its weight part ratio is：Smooth agent 67, emulsifying agent 10, antistatic additive 8, collecting agent 10, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or many
Plant the miscella 70 with hydroxy silicon oil, trimethylolpropane fatty acid ester 20, polyacrylate 10；
Described smooth agent adopts following steps：Take the hydroxy silicon oil that viscosity is 2,250,000 CPS and viscosity 78CPS vegetable oil,
In animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxy silicon oil
Addition be vegetable oil, animal oil, in mineral oil the addition of any one or more 10-25%；Take trihydroxy methyl third
Alkane fatty acid ester, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, at this
In primary smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, uses acid for adjusting pH
It is worth to 4-5, obtain smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 50, dimethylaminoethyl
Acrylate 20, APES formaldehyde condensation product 30；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 5-20CPS, dimethylamino second
Base acrylate, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150
DEG C, stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：
Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorus in the presence of polyphosphoric acids
Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Again polyphosphoric acids are put in the product after etherificate after being first passed through nitrogen in phosphorylation reaction therein, temperature control
Below 40 DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, 2-4 is little for insulation
When；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% containing amylose content
Etherificate high amylose starchess 60, vegetable oil 20, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：28 parts of fatty alcohol, 28 parts of acrylic acid, azo two isopropylformic acid.
3 parts of dimethyl ester, 3 parts of Polymeric sodium metaphosphate., 20 parts of Pulvis Talci；
Described additive adopts following steps：By 28 parts of fatty alcohol, 28 parts of acrylic acid, 3 parts of azo-bis-iso-dimethyl,
20 parts of Pulvis Talci, stirs at 50-60 DEG C, adds 3 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
As the optimization further of the present invention, the present invention includes smooth agent, emulsifying agent, antistatic additive, collecting agent and interpolation
Agent, its weight part ratio is：Smooth agent 71, emulsifying agent 10, antistatic additive 4, collecting agent 10, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or many
Plant the miscella 58 with hydroxy silicon oil, trimethylolpropane fatty acid ester 22, polyacrylate 20；
Described smooth agent adopts following steps：Take the hydroxy silicon oil that viscosity is 210-225 ten thousand CPS and viscosity 72-78CPS
In vegetable oil, animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxyl
The addition of base silicone oil is vegetable oil, animal oil, in mineral oil the addition of any one or more 10-25%；Take three hydroxyls
Methylpropane fatty acid ester, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, are formed primary smooth
Agent, in this primary smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, with acid
Adjust pH value to 4-5, obtain smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 58, dimethylaminoethyl
Acrylate 32, APES formaldehyde condensation product 10；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 5-20CPS, dimethylamino second
Base acrylate, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150
DEG C, stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：
Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorus in the presence of polyphosphoric acids
Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Again polyphosphoric acids are put in the product after etherificate after being first passed through nitrogen in phosphorylation reaction therein, temperature control
Below 40 DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, 2-4 is little for insulation
When；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% containing amylose content
Etherificate high amylose starchess 56, vegetable oil 24, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：26 parts of fatty alcohol, 26 parts of acrylic acid, azo two isopropylformic acid.
4 parts of dimethyl ester, 4 parts of Polymeric sodium metaphosphate., 26 parts of Pulvis Talci；
Described additive adopts following steps：By 26 parts of fatty alcohol, 26 parts of acrylic acid, 4 parts of azo-bis-iso-dimethyl,
26 parts of Pulvis Talci, stirs at 50-60 DEG C, adds 4 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
Beneficial effect：The present invention compared with prior art, has advantages below：Spinning oil preparation coefficient of friction using the present invention
Stable, film strength is high, oil preparation flash-point is high it is ensured that traction force suffered by fiber is stable, and spinning tension fluctuation is less, is not susceptible to twine
Around, breakage phenomena.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is described in detail, but protection scope of the present invention is described simultaneously simultaneously
It is not limited to the concrete scope of the present embodiment, based on the embodiment in the present invention, those of ordinary skill in the art are not making
The every other embodiment being obtained under the premise of creative work, broadly falls into the scope of protection of the invention.
Embodiment 1
A kind of automotive upholstery fabric flash-point strengthening oil preparation of the present embodiment, including smooth agent, emulsifying agent, antistatic
Agent, collecting agent and additive, its weight part ratio is：Smooth agent 71, emulsifying agent 14, antistatic additive 4, collecting agent 6, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or many
Plant the miscella 50 with hydroxy silicon oil, trimethylolpropane fatty acid ester 30, polyacrylate 20；
Described smooth agent adopts following steps：Take the hydroxy silicon oil that viscosity is 2,100,000 CPS and viscosity 78CPS vegetable oil,
In animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxy silicon oil
Addition be vegetable oil, animal oil, in mineral oil the addition of any one or more 25%；Take trimethylolpropane fat
Fat acid esters, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, in this primary
In smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, with acid for adjusting pH value extremely
5, obtain smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 30, dimethylaminoethyl
Acrylate 50, APES formaldehyde condensation product 20；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 15CPS, dimethylaminoethyl
Acrylate, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 150 DEG C,
Stirring reaction be cooled to room temperature under 250 revs/min of mixing speeds；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：
Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorus in the presence of polyphosphoric acids
Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Again polyphosphoric acids are put in the product after etherificate after being first passed through nitrogen in phosphorylation reaction therein, temperature control
Below 40 DEG C, to stir under 250 revs/min of mixing speeds after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, is incubated 2 hours；
Wherein, described alkali is potassium hydroxide；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% containing amylose content
Etherificate high amylose starchess 50, vegetable oil 30, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：20 parts of fatty alcohol, 30 parts of acrylic acid, azo two isopropylformic acid.
2 parts of dimethyl ester, 3 parts of Polymeric sodium metaphosphate., 20 parts of Pulvis Talci；
Described additive adopts following steps：By 20 parts of fatty alcohol, 30 parts of acrylic acid, 2 parts of azo-bis-iso-dimethyl,
20 parts of Pulvis Talci, stirs at 60 DEG C, adds 3 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
The coefficient of friction of the present embodiment is maintained at 1.372 about, and film strength can arrive 758N, and flash-point is up to more than 205 DEG C.
Embodiment 2
A kind of automotive upholstery fabric flash-point strengthening oil preparation of the present embodiment, including smooth agent, emulsifying agent, antistatic
Agent, collecting agent and additive, its weight part ratio is：Smooth agent 67, emulsifying agent 10, antistatic additive 8, collecting agent 10, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or many
Plant the miscella 70 with hydroxy silicon oil, trimethylolpropane fatty acid ester 20, polyacrylate 10；
Described smooth agent adopts following steps：Take the hydroxy silicon oil that viscosity is 2,250,000 CPS and viscosity 78CPS vegetable oil,
In animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxy silicon oil
Addition be vegetable oil, animal oil, in mineral oil the addition of any one or more 25%；Take trimethylolpropane fat
Fat acid esters, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, in this primary
In smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, with acid for adjusting pH value extremely
5, obtain smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 50, dimethylaminoethyl
Acrylate 20, APES formaldehyde condensation product 30；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 18CPS, dimethylaminoethyl
Acrylate, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 150 DEG C,
Stirring reaction be cooled to room temperature under 350 revs/min of mixing speeds；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：
Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorus in the presence of polyphosphoric acids
Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Again polyphosphoric acids are put in the product after etherificate after being first passed through nitrogen in phosphorylation reaction therein, temperature control
Below 40 DEG C, to stir under 250 revs/min of mixing speeds after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, is incubated 4 hours；
Wherein, described alkali is diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% containing amylose content
Etherificate high amylose starchess 60, vegetable oil 20, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：28 parts of fatty alcohol, 28 parts of acrylic acid, azo two isopropylformic acid.
3 parts of dimethyl ester, 3 parts of Polymeric sodium metaphosphate., 20 parts of Pulvis Talci；
Described additive adopts following steps：By 28 parts of fatty alcohol, 28 parts of acrylic acid, 3 parts of azo-bis-iso-dimethyl,
20 parts of Pulvis Talci, stirs at 60 DEG C, adds 3 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
The coefficient of friction of the present embodiment is maintained at 1.364 about, and film strength can arrive 750N, and flash-point is up to more than 205 DEG C.
Embodiment 3
A kind of automotive upholstery fabric flash-point strengthening oil preparation of the present embodiment, including smooth agent, emulsifying agent, antistatic
Agent, collecting agent and additive, its weight part ratio is：Smooth agent 71, emulsifying agent 10, antistatic additive 4, collecting agent 10, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or many
Plant the miscella 58 with hydroxy silicon oil, trimethylolpropane fatty acid ester 22, polyacrylate 20；
Described smooth agent adopts following steps：Take the plant of the hydroxy silicon oil that viscosity is 2,200,000 CPS and viscosity 078CPS
In oil, animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxyl silicon
The addition of oil is vegetable oil, animal oil, in mineral oil the addition of any one or more 20%；Take trimethylolpropane
Fatty acid ester, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, first at this
In level smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, uses acid for adjusting pH value
To 4, obtain smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 58, dimethylaminoethyl
Acrylate 32, APES formaldehyde condensation product 10；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 18CPS, dimethylaminoethyl
Acrylate, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 150 DEG C,
Stirring reaction be cooled to room temperature under 250 revs/min of mixing speeds；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：
Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorus in the presence of polyphosphoric acids
Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Again polyphosphoric acids are put in the product after etherificate after being first passed through nitrogen in phosphorylation reaction therein, temperature control
Below 40 DEG C, to stir under 250 revs/min of mixing speeds after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, is incubated 4 hours；
Wherein, described alkali is ammonia；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% containing amylose content
Etherificate high amylose starchess 56, vegetable oil 24, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：26 parts of fatty alcohol, 26 parts of acrylic acid, azo two isopropylformic acid.
4 parts of dimethyl ester, 4 parts of Polymeric sodium metaphosphate., 26 parts of Pulvis Talci；
Described additive adopts following steps：By 26 parts of fatty alcohol, 26 parts of acrylic acid, 4 parts of azo-bis-iso-dimethyl,
26 parts of Pulvis Talci, stirs at 50 DEG C, adds 4 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
The coefficient of friction of the present embodiment is maintained at 1.370 about, and film strength can arrive 755N, and flash-point is up to more than 205 DEG C.
Embodiments of the invention in order to example and description for the sake of and be given, and be not exhaustively or by this
Bright it is limited to disclosed form.Many modifications and variations are obvious for the ordinary skill in the art.Choosing
Selecting and describe embodiment is in order to the principle of the present invention and practical application are more preferably described, and makes those of ordinary skill in the art
It will be appreciated that the present invention is thus design is suitable to the various embodiments with various modifications of special-purpose.
Claims (4)
1. a kind of automotive upholstery fabric flash-point strengthening oil preparation it is characterised in that：Including smooth agent, emulsifying agent, antistatic additive,
Collecting agent and additive, its weight part ratio is：Smooth agent 66-74, emulsifying agent 10-14, antistatic additive 4-8, collecting agent 6-10, add
Plus agent 3-5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or more with
The miscella 50-70 of hydroxy silicon oil, trimethylolpropane fatty acid ester 20-30, polyacrylate 10-20；
Described smooth agent adopts following steps：Take the plant of the hydroxy silicon oil that viscosity is 210-225 ten thousand CPS and viscosity 72-78CPS
In oil, animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxyl silicon
The addition of oil is vegetable oil, animal oil, in mineral oil the addition of any one or more 10-25%；Take trihydroxy methyl
Propane fatty acid ester, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent,
In this primary smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, is adjusted with acid
PH value, to 4-5, obtains smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 30-60, dimethylaminoethyl third
Olefin(e) acid ester 20-50, APES formaldehyde condensation product 10-30；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 5-20CPS, dimethylaminoethyl third
Olefin(e) acid ester, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150 DEG C,
Stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：New penta
Alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorylation in the presence of polyphosphoric acids
Reaction, is added water and is neutralized by alkali after being hydrolyzed；
First it is passed through in phosphorylation reaction therein and again polyphosphoric acids is put in the product after etherificate after nitrogen, temperature control is 40
Below DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, is incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% etherificate containing amylose content
High amylose starchess 50-70, vegetable oil 20-30, Polyethylene Glycol Laurel acid diester 10-20；
The constituent of described additive and its mass fraction are：Fatty alcohol 20-30 part, acrylic acid 20-30 part, azo two isobutyl
Dimethyl phthalate 2-4 part, Polymeric sodium metaphosphate. 3-4 part, Pulvis Talci 20-30 part；
Described additive adopts following steps：By fatty alcohol 20-30 part, acrylic acid 20-30 part, azo-bis-iso-dimethyl 2-
4 parts, Pulvis Talci 20-30 part, stir at 50-60 DEG C, add Polymeric sodium metaphosphate. 3-4 part, obtain within ultrasonic 20 minutes.
2. a kind of automotive upholstery fabric flash-point strengthening oil preparation according to claim 1 it is characterised in that：Including smooth
Agent, emulsifying agent, antistatic additive, collecting agent and additive, its weight part ratio is：Smooth agent 71, emulsifying agent 14, antistatic additive 4, collection
Bundle agent 6, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or more with
The miscella 50 of hydroxy silicon oil, trimethylolpropane fatty acid ester 30, polyacrylate 20；
Described smooth agent adopts following steps：Take vegetable oil, the animal of the hydroxy silicon oil that viscosity is 2,100,000 CPS and viscosity 78CPS
Oil, in mineral oil any one or more, put into high speed dispersor and disperseed, form miscella, wherein hydroxy silicon oil plus
Enter amount be vegetable oil, animal oil, in mineral oil the addition of any one or more 25%；Take trimethylolpropane fatty acid
Ester, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, smooth in this primary
In agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, with acid for adjusting pH value to 4-5,
Obtain smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 30, dimethylaminoethyl propylene
Acid esters 50, APES formaldehyde condensation product 20；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 15CPS, dimethylaminoethyl propylene
Acid esters, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150 DEG C,
Stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：New penta
Alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorylation in the presence of polyphosphoric acids
Reaction, is added water and is neutralized by alkali after being hydrolyzed；
First it is passed through in phosphorylation reaction therein and again polyphosphoric acids is put in the product after etherificate after nitrogen, temperature control is 40
Below DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, is incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% etherificate containing amylose content
High amylose starchess 50, vegetable oil 30, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：20 parts of fatty alcohol, 30 parts of acrylic acid, azo two isopropylformic acid. diformazan
2 parts of ester, 3 parts of Polymeric sodium metaphosphate., 20 parts of Pulvis Talci；
Described additive adopts following steps：By 20 parts of fatty alcohol, 30 parts of acrylic acid, 2 parts of azo-bis-iso-dimethyl, Talcum
20 parts of powder, stirs at 50-60 DEG C, adds 3 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
3. a kind of automotive upholstery fabric flash-point strengthening oil preparation according to claim 1 it is characterised in that：Including smooth
Agent, emulsifying agent, antistatic additive, collecting agent and additive, its weight part ratio is：Smooth agent 67, emulsifying agent 10, antistatic additive 8, collection
Bundle agent 10, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or more with
The miscella 70 of hydroxy silicon oil, trimethylolpropane fatty acid ester 20, polyacrylate 10；
Described smooth agent adopts following steps：Take vegetable oil, the animal of the hydroxy silicon oil that viscosity is 2,250,000 CPS and viscosity 78CPS
Oil, in mineral oil any one or more, put into high speed dispersor and disperseed, form miscella, wherein hydroxy silicon oil plus
Enter amount be vegetable oil, animal oil, in mineral oil the addition of any one or more 10-25%；Take trimethylolpropane fat
Fat acid esters, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, in this primary
In smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, with acid for adjusting pH value extremely
4-5, obtains smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 50, dimethylaminoethyl propylene
Acid esters 20, APES formaldehyde condensation product 30；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 5-20CPS, dimethylaminoethyl third
Olefin(e) acid ester, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150 DEG C,
Stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：New penta
Alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorylation in the presence of polyphosphoric acids
Reaction, is added water and is neutralized by alkali after being hydrolyzed；
First it is passed through in phosphorylation reaction therein and again polyphosphoric acids is put in the product after etherificate after nitrogen, temperature control is 40
Below DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, is incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% etherificate containing amylose content
High amylose starchess 60, vegetable oil 20, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：28 parts of fatty alcohol, 28 parts of acrylic acid, azo two isopropylformic acid. diformazan
3 parts of ester, 3 parts of Polymeric sodium metaphosphate., 20 parts of Pulvis Talci；
Described additive adopts following steps：By 28 parts of fatty alcohol, 28 parts of acrylic acid, 3 parts of azo-bis-iso-dimethyl, Talcum
20 parts of powder, stirs at 50-60 DEG C, adds 3 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
4. a kind of automotive upholstery fabric flash-point strengthening oil preparation according to claim 1 it is characterised in that：Including smooth
Agent, emulsifying agent, antistatic additive, collecting agent and additive, its weight part ratio is：Smooth agent 71, emulsifying agent 10, antistatic additive 4, collection
Bundle agent 10, additive 5；
The constituent of described smooth agent and its weight part ratio are：In vegetable oil, animal oil, mineral oil any one or more with
The miscella 58 of hydroxy silicon oil, trimethylolpropane fatty acid ester 22, polyacrylate 20；
Described smooth agent adopts following steps：Take the plant of the hydroxy silicon oil that viscosity is 210-225 ten thousand CPS and viscosity 72-78CPS
In oil, animal oil, mineral oil, any one or more, put into high speed dispersor and disperseed, and forms miscella, wherein hydroxyl silicon
The addition of oil is vegetable oil, animal oil, in mineral oil the addition of any one or more 10-25%；Take trihydroxy methyl
Propane fatty acid ester, polyacrylate and miscella are placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent,
In this primary smooth agent, addition addition is the nano oxidized polythene wax emulsion of the 2% of primary smooth agent weight, is adjusted with acid
PH value, to 4-5, obtains smooth agent；
The constituent of described emulsifying agent and its weight part ratio are：Alkyl ether type surfactant 58, dimethylaminoethyl propylene
Acid esters 32, APES formaldehyde condensation product 10；
Described emulsifying agent adopts following steps：Using the alkyl ether type surfactant of viscosity 5-20CPS, dimethylaminoethyl third
Olefin(e) acid ester, APES formaldehyde condensation product are sequentially placed in reactor, heating fusing, are warming up to 120-150 DEG C,
Stirring reaction be cooled to room temperature under 250-350 rev/min of mixing speed；
The main component of antistatic additive is neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, makes by the following method：New penta
Alcohol is etherified with glycerol, and gains are that glycol oligomer is etherified and carries out phosphorylation in the presence of polyphosphoric acids
Reaction, is added water and is neutralized by alkali after being hydrolyzed；
First it is passed through in phosphorylation reaction therein and again polyphosphoric acids is put in the product after etherificate after nitrogen, temperature control is 40
Below DEG C, to stir under 250-350 rev/min of mixing speed after the completion of feeding intake, after finishing, it is warming up to 80 DEG C, is incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and its mass parts ratio are：At least it is more than or equal to 50% etherificate containing amylose content
High amylose starchess 56, vegetable oil 24, Polyethylene Glycol Laurel acid diester 20；
The constituent of described additive and its mass fraction are：26 parts of fatty alcohol, 26 parts of acrylic acid, azo two isopropylformic acid. diformazan
4 parts of ester, 4 parts of Polymeric sodium metaphosphate., 26 parts of Pulvis Talci；
Described additive adopts following steps：By 26 parts of fatty alcohol, 26 parts of acrylic acid, 4 parts of azo-bis-iso-dimethyl, Talcum
26 parts of powder, stirs at 50-60 DEG C, adds 4 parts of Polymeric sodium metaphosphate., obtains within ultrasonic 20 minutes.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610764228.7A CN106381695A (en) | 2016-08-30 | 2016-08-30 | Oil for improvement of automobile interior decorative part flashing point |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610764228.7A CN106381695A (en) | 2016-08-30 | 2016-08-30 | Oil for improvement of automobile interior decorative part flashing point |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108930159A (en) * | 2018-08-06 | 2018-12-04 | 江苏悦孚油品有限公司 | A kind of DTY texturing oil and preparation method thereof |
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