CN106319931A - Reinforced oil for automotive interior fabric - Google Patents

Reinforced oil for automotive interior fabric Download PDF

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Publication number
CN106319931A
CN106319931A CN201610768064.5A CN201610768064A CN106319931A CN 106319931 A CN106319931 A CN 106319931A CN 201610768064 A CN201610768064 A CN 201610768064A CN 106319931 A CN106319931 A CN 106319931A
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parts
agent
additive
silicon oil
smooth agent
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CN201610768064.5A
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周玉平
冯兵
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SUZHOU WANLONG AUTO PARTS CO Ltd
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SUZHOU WANLONG AUTO PARTS CO Ltd
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Priority to CN201610768064.5A priority Critical patent/CN106319931A/en
Publication of CN106319931A publication Critical patent/CN106319931A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
    • D06M11/72—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with metaphosphoric acids or their salts; with polyphosphoric acids or their salts; with perphosphoric acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • D06M13/2243—Mono-, di-, or triglycerides
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D06M15/11—Starch or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/227—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of hydrocarbons, or reaction products thereof, e.g. afterhalogenated or sulfochlorinated
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

Abstract

The invention discloses reinforced oil for automotive interior fabric. The reinforced oil is prepared from, in parts by weight, 66-74 parts of a smoothing agent, 10-14 parts of an emulsifier, 4-8 parts of an antistatic agent, 6-10 parts of a tow collecting agent and 3-5 parts of an additive. The spinning oil has stable friction coefficient, high oil film strength and high oil flash point, the drawing force of fibers is stable, the spinning tension fluctuation is smaller, and winding and end breakage cannot occur easily.

Description

A kind of automotive upholstery fabric strengthening oil preparation
Technical field
The invention belongs to technical field of automotive upholstery, be specifically related to a kind of automotive upholstery fabric strengthening oil preparation.
Background technology
More than in automobile 40, individual loseing needs to use fabric, from cabin air filter, molds seat, roof, compartment lining The end, is required for carpet, how to improve the properties of fabric, thus improves comfortableness and the reliability of vehicle, becomes one and ask greatly Topic.
Summary of the invention
Goal of the invention: the problem and shortage existed for above-mentioned prior art, it is an object of the invention to provide a kind of automobile Inside gadget fabric strengthening oil preparation.
Technical scheme: the invention discloses a kind of automotive upholstery fabric and strengthen oil preparation, including smooth agent, emulsifying agent, Antistatic additive, collecting agent and additive, its weight part ratio is: smooth agent 66-74, emulsifying agent 10-14, antistatic additive 4-8, boundling Agent 6-10, additive 3-5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 50-70 of amido silicon oil and hydroxy silicon oil, poly- Dimethyl siloxane 20-30,2-naphthol 10-20；
Described smooth agent uses following steps: take hydroxy silicon oil and viscosity 72-78CPS that viscosity is 210-225 ten thousand CPS Amido silicon oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is adding of amido silicon oil Enter the 10-25% of amount；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, shape Become primary smooth agent, this primary smooth agent adds the nano oxidized polyethylene of addition is primary smooth agent weight 2% Wax emulsion, with acid for adjusting pH value to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 30-60, dimethylamino second Base acrylate 20-50, alkylphenol polyoxyethylene formaldehyde condensation products 10-30；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 5-20CPS, dimethylamino second Base acrylate, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorus in the presence of polyphosphoric acids Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls again Below 40 DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, insulation 2-4 little Time；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains amylose content more than or equal to 50% Etherificate high amylose starches 50-70, vegetable oil 20-30, Polyethylene Glycol lauric acid dibasic acid esters 10-20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 20-30 part, acrylic acid 20-30 part, azo two Isopropylformic acid. dimethyl ester 2-4 part, Polymeric sodium metaphosphate. 3-4 part, Pulvis Talci 20-30 part；
Described additive uses following steps: by fatty alcohol 20-30 part, acrylic acid 20-30 part, azo two isopropylformic acid. diformazan Ester 2-4 part, Pulvis Talci 20-30 part, stir at 50-60 DEG C, adds Polymeric sodium metaphosphate. 3-4 part, within ultrasonic 20 minutes, obtains.
As the further optimization of the present invention, the present invention includes smooth agent, emulsifying agent, antistatic additive, collecting agent and interpolation Agent, its weight part ratio is: smooth agent 71, emulsifying agent 14, antistatic additive 4, collecting agent 6, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 50 of amido silicon oil and hydroxy silicon oil, poly-two Methylsiloxane 30,2-naphthol 20；
Described smooth agent uses following steps: take hydroxy silicon oil and the amino silicone of viscosity 78CPS that viscosity is 2,100,000 CPS Oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is the addition of amido silicon oil 25%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth Agent, adds the nano oxidized polythene wax emulsion of addition is primary smooth agent weight 2%, with acid in this primary smooth agent Regulation pH value is to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 30, dimethylaminoethyl Acrylate 50, alkylphenol polyoxyethylene formaldehyde condensation products 20；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 15CPS, dimethylaminoethyl Acrylate, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, Under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorus in the presence of polyphosphoric acids Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls again Below 40 DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, insulation 2-4 little Time；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains amylose content more than or equal to 50% Etherificate high amylose starches 50, vegetable oil 30, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 20 parts, 30 parts of acrylic acid, azo two isopropylformic acid. Dimethyl ester 2 parts, Polymeric sodium metaphosphate. 3 parts, Pulvis Talci 20 parts；
Described additive use following steps: by fatty alcohol 20 parts, 30 parts of acrylic acid, azo-bis-iso-dimethyl 2 parts, Pulvis Talci 20 parts, stirs at 50-60 DEG C, adds Polymeric sodium metaphosphate. 3 parts, within ultrasonic 20 minutes, obtains.
As the further optimization of the present invention, the present invention includes smooth agent, emulsifying agent, antistatic additive, collecting agent and interpolation Agent, its weight part ratio is: smooth agent 67, emulsifying agent 10, antistatic additive 8, collecting agent 10, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 70 of amido silicon oil and hydroxy silicon oil, poly-two Methylsiloxane 20,2-naphthol 10；
Described smooth agent uses following steps: take hydroxy silicon oil and the amino silicone of viscosity 78CPS that viscosity is 2,250,000 CPS Oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is the addition of amido silicon oil 10-25%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, form primary Smooth agent, adds the nano oxidized polythene wax emulsion of addition is primary smooth agent weight 2% in this primary smooth agent, With acid for adjusting pH value to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 50, dimethylaminoethyl Acrylate 20, alkylphenol polyoxyethylene formaldehyde condensation products 30；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 5-20CPS, dimethylamino second Base acrylate, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorus in the presence of polyphosphoric acids Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls again Below 40 DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, insulation 2-4 little Time；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains amylose content more than or equal to 50% Etherificate high amylose starches 60, vegetable oil 20, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 28 parts, 28 parts of acrylic acid, azo two isopropylformic acid. Dimethyl ester 3 parts, Polymeric sodium metaphosphate. 3 parts, Pulvis Talci 20 parts；
Described additive use following steps: by fatty alcohol 28 parts, 28 parts of acrylic acid, azo-bis-iso-dimethyl 3 parts, Pulvis Talci 20 parts, stirs at 50-60 DEG C, adds Polymeric sodium metaphosphate. 3 parts, within ultrasonic 20 minutes, obtains.
As the further optimization of the present invention, the present invention includes smooth agent, emulsifying agent, antistatic additive, collecting agent and interpolation Agent, its weight part ratio is: smooth agent 71, emulsifying agent 10, antistatic additive 4, collecting agent 10, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 58 of amido silicon oil and hydroxy silicon oil, poly-two Methylsiloxane 22,2-naphthol 20；
Described smooth agent uses following steps: take hydroxy silicon oil and viscosity 72-78CPS that viscosity is 210-225 ten thousand CPS Amido silicon oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is adding of amido silicon oil Enter the 10-25% of amount；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, shape Become primary smooth agent, this primary smooth agent adds the nano oxidized polyethylene of addition is primary smooth agent weight 2% Wax emulsion, with acid for adjusting pH value to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 58, dimethylaminoethyl Acrylate 32, alkylphenol polyoxyethylene formaldehyde condensation products 10；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 5-20CPS, dimethylamino second Base acrylate, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorus in the presence of polyphosphoric acids Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls again Below 40 DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, insulation 2-4 little Time；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains amylose content more than or equal to 50% Etherificate high amylose starches 56, vegetable oil 24, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 26 parts, 26 parts of acrylic acid, azo two isopropylformic acid. Dimethyl ester 4 parts, Polymeric sodium metaphosphate. 4 parts, Pulvis Talci 26 parts；
Described additive use following steps: by fatty alcohol 26 parts, 26 parts of acrylic acid, azo-bis-iso-dimethyl 4 parts, Pulvis Talci 26 parts, stirs at 50-60 DEG C, adds Polymeric sodium metaphosphate. 4 parts, within ultrasonic 20 minutes, obtains.
Beneficial effect: the present invention compared with prior art, has the advantage that and uses the present invention's to spin oil preparation coefficient of friction Stable, film strength is high, oil preparation flash-point is high, it is ensured that traction force suffered by fiber is stable, and spinning tension fluctuation is less, is not susceptible to twine Around, breakage phenomena.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail, but protection scope of the present invention is described also simultaneously Being not limited to the concrete scope of the present embodiment, based on the embodiment in the present invention, those of ordinary skill in the art are not making The every other embodiment obtained under creative work premise, broadly falls into the scope of protection of the invention.
Embodiment 1
A kind of automotive upholstery fabric strengthening oil preparation of the present embodiment, including smooth agent, emulsifying agent, antistatic additive, collection Bundle agent and additive, its weight part ratio is: smooth agent 71, emulsifying agent 14, antistatic additive 4, collecting agent 6, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 50 of amido silicon oil and hydroxy silicon oil, poly-two Methylsiloxane 30,2-naphthol 20；
Described smooth agent uses following steps: take hydroxy silicon oil and the amino silicone of viscosity 78CPS that viscosity is 2,100,000 CPS Oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is the addition of amido silicon oil 25%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth Agent, adds the nano oxidized polythene wax emulsion of addition is primary smooth agent weight 2%, with acid in this primary smooth agent Regulation pH value is to 5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 30, dimethylaminoethyl Acrylate 50, alkylphenol polyoxyethylene formaldehyde condensation products 20；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 15CPS, dimethylaminoethyl Acrylate, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 150 DEG C, Under 250 revs/min of mixing speeds, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorus in the presence of polyphosphoric acids Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls again Below 40 DEG C, after having fed intake with under 250 revs/min of mixing speeds stir, after be warming up to 80 DEG C, be incubated 2 hours；
Wherein, described alkali is potassium hydroxide；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains amylose content more than or equal to 50% Etherificate high amylose starches 50, vegetable oil 30, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 20 parts, 30 parts of acrylic acid, azo two isopropylformic acid. Dimethyl ester 2 parts, Polymeric sodium metaphosphate. 3 parts, Pulvis Talci 20 parts；
Described additive use following steps: by fatty alcohol 20 parts, 30 parts of acrylic acid, azo-bis-iso-dimethyl 2 parts, Pulvis Talci 20 parts, stirs at 60 DEG C, adds Polymeric sodium metaphosphate. 3 parts, within ultrasonic 20 minutes, obtains.
The coefficient of friction of the present embodiment is maintained at about 1.372, and film strength can arrive 758N, and flash-point is up to more than 205 DEG C.
Embodiment 2
A kind of automotive upholstery fabric strengthening oil preparation of the present embodiment, including smooth agent, emulsifying agent, antistatic additive, collection Bundle agent and additive, its weight part ratio is: smooth agent 67, emulsifying agent 10, antistatic additive 8, collecting agent 10, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 70 of amido silicon oil and hydroxy silicon oil, poly-two Methylsiloxane 20,2-naphthol 10；
Described smooth agent uses following steps: take hydroxy silicon oil and the amino silicone of viscosity 78CPS that viscosity is 2,250,000 CPS Oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is the addition of amido silicon oil 25%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth Agent, adds the nano oxidized polythene wax emulsion of addition is primary smooth agent weight 2%, with acid in this primary smooth agent Regulation pH value is to 5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 50, dimethylaminoethyl Acrylate 20, alkylphenol polyoxyethylene formaldehyde condensation products 30；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 18CPS, dimethylaminoethyl Acrylate, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 150 DEG C, Under 350 revs/min of mixing speeds, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorus in the presence of polyphosphoric acids Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls again Below 40 DEG C, after having fed intake with under 250 revs/min of mixing speeds stir, after be warming up to 80 DEG C, be incubated 4 hours；
Wherein, described alkali is diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains amylose content more than or equal to 50% Etherificate high amylose starches 60, vegetable oil 20, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 28 parts, 28 parts of acrylic acid, azo two isopropylformic acid. Dimethyl ester 3 parts, Polymeric sodium metaphosphate. 3 parts, Pulvis Talci 20 parts；
Described additive use following steps: by fatty alcohol 28 parts, 28 parts of acrylic acid, azo-bis-iso-dimethyl 3 parts, Pulvis Talci 20 parts, stirs at 60 DEG C, adds Polymeric sodium metaphosphate. 3 parts, within ultrasonic 20 minutes, obtains.
The coefficient of friction of the present embodiment is maintained at about 1.364, and film strength can arrive 750N, and flash-point is up to more than 205 DEG C.
Embodiment 3
A kind of automotive upholstery fabric strengthening oil preparation of the present embodiment, including smooth agent, emulsifying agent, antistatic additive, collection Bundle agent and additive, its weight part ratio is: smooth agent 71, emulsifying agent 10, antistatic additive 4, collecting agent 10, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 58 of amido silicon oil and hydroxy silicon oil, poly-two Methylsiloxane 22,2-naphthol 20；
Described smooth agent uses following steps: take hydroxy silicon oil and the amino silicone of viscosity 078CPS that viscosity is 2,200,000 CPS Oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is the addition of amido silicon oil 20%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth Agent, adds the nano oxidized polythene wax emulsion of addition is primary smooth agent weight 2%, with acid in this primary smooth agent Regulation pH value is to 4, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 58, dimethylaminoethyl Acrylate 32, alkylphenol polyoxyethylene formaldehyde condensation products 10；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 18CPS, dimethylaminoethyl Acrylate, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 150 DEG C, Under 250 revs/min of mixing speeds, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: Neopentyl alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorus in the presence of polyphosphoric acids Acidification reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls again Below 40 DEG C, after having fed intake with under 250 revs/min of mixing speeds stir, after be warming up to 80 DEG C, be incubated 4 hours；
Wherein, described alkali is ammonia；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains amylose content more than or equal to 50% Etherificate high amylose starches 56, vegetable oil 24, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 26 parts, 26 parts of acrylic acid, azo two isopropylformic acid. Dimethyl ester 4 parts, Polymeric sodium metaphosphate. 4 parts, Pulvis Talci 26 parts；
Described additive use following steps: by fatty alcohol 26 parts, 26 parts of acrylic acid, azo-bis-iso-dimethyl 4 parts, Pulvis Talci 26 parts, stirs at 50 DEG C, adds Polymeric sodium metaphosphate. 4 parts, within ultrasonic 20 minutes, obtains.
The coefficient of friction of the present embodiment is maintained at about 1.370, and film strength can arrive 755N, and flash-point is up to more than 205 DEG C.
Embodiments of the invention are given for example with for the sake of describing, and are not exhaustively or by this Bright it is limited to disclosed form.Many modifications and variations are apparent from for the ordinary skill in the art.Choosing Selecting and describe embodiment is in order to the principle of the present invention and actual application are more preferably described, and makes those of ordinary skill in the art It will be appreciated that the present invention thus design is suitable to the various embodiments with various amendments of special-purpose.

Claims (4)

1. an automotive upholstery fabric strengthening oil preparation, it is characterised in that: include smooth agent, emulsifying agent, antistatic additive, boundling Agent and additive, its weight part ratio is: smooth agent 66-74, emulsifying agent 10-14, antistatic additive 4-8, collecting agent 6-10, additive 3-5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 50-70 of amido silicon oil and hydroxy silicon oil, poly-diformazan Radical siloxane 20-30,2-naphthol 10-20；
Described smooth agent uses following steps: take hydroxy silicon oil and the amino of viscosity 72-78CPS that viscosity is 210-225 ten thousand CPS Silicone oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is the addition of amido silicon oil 10-25%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, at the beginning of formation Level smooth agent, adds the nano oxidized Tissuemat E breast of addition is primary smooth agent weight 2% in this primary smooth agent Liquid, with acid for adjusting pH value to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 30-60, dimethylaminoethyl third Olefin(e) acid ester 20-50, alkylphenol polyoxyethylene formaldehyde condensation products 10-30；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 5-20CPS, dimethylaminoethyl third Olefin(e) acid ester, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, Under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: new penta Alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorylation in the presence of polyphosphoric acids Reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls 40 again Below DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, be incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains the amylose content etherificate more than or equal to 50% High amylose starches 50-70, vegetable oil 20-30, Polyethylene Glycol lauric acid dibasic acid esters 10-20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 20-30 part, acrylic acid 20-30 part, azo two isobutyl Dimethyl phthalate 2-4 part, Polymeric sodium metaphosphate. 3-4 part, Pulvis Talci 20-30 part；
Described additive uses following steps: by fatty alcohol 20-30 part, acrylic acid 20-30 part, azo-bis-iso-dimethyl 2- 4 parts, Pulvis Talci 20-30 part, stir at 50-60 DEG C, adds Polymeric sodium metaphosphate. 3-4 part, within ultrasonic 20 minutes, obtains.
A kind of automotive upholstery fabric the most according to claim 1 strengthens oil preparation, it is characterised in that: include smooth agent, Emulsifying agent, antistatic additive, collecting agent and additive, its weight part ratio is: smooth agent 71, emulsifying agent 14, antistatic additive 4, boundling Agent 6, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 50 of amido silicon oil and hydroxy silicon oil, poly dimethyl Siloxanes 30,2-naphthol 20；
Described smooth agent uses following steps: takes hydroxy silicon oil and the amido silicon oil of viscosity 78CPS that viscosity is 2,100,000 CPS, puts Enter high speed dispersor to disperse, formed miscella, wherein the addition of hydroxy silicon oil be amido silicon oil addition 25%； Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth agent, This primary smooth agent adds the nano oxidized polythene wax emulsion of addition is primary smooth agent weight 2%, regulates with acid PH value is to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 30, dimethylaminoethyl propylene Acid esters 50, alkylphenol polyoxyethylene formaldehyde condensation products 20；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 15CPS, dimethylaminoethyl propylene Acid esters, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, Under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: new penta Alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorylation in the presence of polyphosphoric acids Reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls 40 again Below DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, be incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains the amylose content etherificate more than or equal to 50% High amylose starches 50, vegetable oil 30, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 20 parts, 30 parts of acrylic acid, azo two isopropylformic acid. diformazan Ester 2 parts, Polymeric sodium metaphosphate. 3 parts, Pulvis Talci 20 parts；
Described additive uses following steps: by fatty alcohol 20 parts, 30 parts of acrylic acid, azo-bis-iso-dimethyl 2 parts, Talcum 20 parts of powder, stirs at 50-60 DEG C, adds Polymeric sodium metaphosphate. 3 parts, within ultrasonic 20 minutes, obtains.
A kind of automotive upholstery fabric the most according to claim 1 strengthens oil preparation, it is characterised in that: include smooth agent, Emulsifying agent, antistatic additive, collecting agent and additive, its weight part ratio is: smooth agent 67, emulsifying agent 10, antistatic additive 8, boundling Agent 10, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 70 of amido silicon oil and hydroxy silicon oil, poly dimethyl Siloxanes 20,2-naphthol 10；
Described smooth agent uses following steps: takes hydroxy silicon oil and the amido silicon oil of viscosity 78CPS that viscosity is 2,250,000 CPS, puts Entering high speed dispersor to disperse, form miscella, wherein the addition of hydroxy silicon oil is the 10-of addition of amido silicon oil 25%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, form primary smooth Agent, adds the nano oxidized polythene wax emulsion of addition is primary smooth agent weight 2%, with acid in this primary smooth agent Regulation pH value is to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 50, dimethylaminoethyl propylene Acid esters 20, alkylphenol polyoxyethylene formaldehyde condensation products 30；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 5-20CPS, dimethylaminoethyl third Olefin(e) acid ester, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, Under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: new penta Alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorylation in the presence of polyphosphoric acids Reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls 40 again Below DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, be incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains the amylose content etherificate more than or equal to 50% High amylose starches 60, vegetable oil 20, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 28 parts, 28 parts of acrylic acid, azo two isopropylformic acid. diformazan Ester 3 parts, Polymeric sodium metaphosphate. 3 parts, Pulvis Talci 20 parts；
Described additive uses following steps: by fatty alcohol 28 parts, 28 parts of acrylic acid, azo-bis-iso-dimethyl 3 parts, Talcum 20 parts of powder, stirs at 50-60 DEG C, adds Polymeric sodium metaphosphate. 3 parts, within ultrasonic 20 minutes, obtains.
A kind of automotive upholstery fabric the most according to claim 1 strengthens oil preparation, it is characterised in that: include smooth agent, Emulsifying agent, antistatic additive, collecting agent and additive, its weight part ratio is: smooth agent 71, emulsifying agent 10, antistatic additive 4, boundling Agent 10, additive 5；
The constituent of described smooth agent and weight part ratio thereof be: the miscella 58 of amido silicon oil and hydroxy silicon oil, poly dimethyl Siloxanes 22,2-naphthol 20；
Described smooth agent uses following steps: take hydroxy silicon oil and the amino of viscosity 72-78CPS that viscosity is 210-225 ten thousand CPS Silicone oil, puts into high speed dispersor and disperses, and forms miscella, and wherein the addition of hydroxy silicon oil is the addition of amido silicon oil 10-25%；Take polydimethylsiloxane, 2-naphthol and miscella to be placed in emulsifying agent and carry out no less than 15 minutes, at the beginning of formation Level smooth agent, adds the nano oxidized Tissuemat E breast of addition is primary smooth agent weight 2% in this primary smooth agent Liquid, with acid for adjusting pH value to 4-5, it is thus achieved that smooth agent；
The constituent of described emulsifying agent and weight part ratio thereof be: dioctyl sodium sulfosuccinate 58, dimethylaminoethyl propylene Acid esters 32, alkylphenol polyoxyethylene formaldehyde condensation products 10；
Described emulsifying agent uses following steps: use the dioctyl sodium sulfosuccinate of viscosity 5-20CPS, dimethylaminoethyl third Olefin(e) acid ester, alkylphenol polyoxyethylene formaldehyde condensation products are sequentially placed in reactor, add heat fusing, are warming up to 120-150 DEG C, Under 250-350 rev/min of mixing speed, stirring is reacted and is cooled to room temperature；
Antistatic additive be mainly composed of neopentyl alcohol glycerin polyoxyethylene ether monoalkyl phosphate, make by the following method: new penta Alcohol is etherified with glycerol, and gains are that glycol oligomer carries out being etherified and carrying out phosphorylation in the presence of polyphosphoric acids Reaction, is added water and is neutralized by alkali after being hydrolyzed；
Being put into by polyphosphoric acids after being first passed through nitrogen in phosphorylation reaction therein in product after etherificate, temperature controls 40 again Below DEG C, after having fed intake with under 250-350 rev/min of mixing speed stir, after be warming up to 80 DEG C, be incubated 2-4 hour；
Wherein, described alkali is potassium hydroxide, ammonia or diethanolamine；
The constituent of described collecting agent and mass parts ratio thereof be: at least contains the amylose content etherificate more than or equal to 50% High amylose starches 56, vegetable oil 24, Polyethylene Glycol lauric acid dibasic acid esters 20；
The constituent of described additive and mass fraction thereof be: fatty alcohol 26 parts, 26 parts of acrylic acid, azo two isopropylformic acid. diformazan Ester 4 parts, Polymeric sodium metaphosphate. 4 parts, Pulvis Talci 26 parts；
Described additive uses following steps: by fatty alcohol 26 parts, 26 parts of acrylic acid, azo-bis-iso-dimethyl 4 parts, Talcum 26 parts of powder, stirs at 50-60 DEG C, adds Polymeric sodium metaphosphate. 4 parts, within ultrasonic 20 minutes, obtains.
CN201610768064.5A 2016-08-30 2016-08-30 Reinforced oil for automotive interior fabric Pending CN106319931A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1675427A (en) * 2002-09-30 2005-09-28 上海宏联电子材料有限公司 Sizing agent for glass fiber yarn and glass fiber yarn using the same
CN101644001A (en) * 2008-08-04 2010-02-10 河南瑞贝卡发制品股份有限公司 Preparation method and application of fiber pre-finishing auxiliary agent
CN102115978A (en) * 2011-01-06 2011-07-06 吴江市良燕纺织助剂厂 PET (polyester) high-speed spinning finish oil
CN103215806A (en) * 2013-04-27 2013-07-24 杭州传化精细化工有限公司 Antistatic agent for fabrics

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1675427A (en) * 2002-09-30 2005-09-28 上海宏联电子材料有限公司 Sizing agent for glass fiber yarn and glass fiber yarn using the same
CN101644001A (en) * 2008-08-04 2010-02-10 河南瑞贝卡发制品股份有限公司 Preparation method and application of fiber pre-finishing auxiliary agent
CN102115978A (en) * 2011-01-06 2011-07-06 吴江市良燕纺织助剂厂 PET (polyester) high-speed spinning finish oil
CN103215806A (en) * 2013-04-27 2013-07-24 杭州传化精细化工有限公司 Antistatic agent for fabrics

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Application publication date: 20170111