CN106367235A - Application of rutaceous plant extract serving as decontaminant - Google Patents
Application of rutaceous plant extract serving as decontaminant Download PDFInfo
- Publication number
- CN106367235A CN106367235A CN201610735573.8A CN201610735573A CN106367235A CN 106367235 A CN106367235 A CN 106367235A CN 201610735573 A CN201610735573 A CN 201610735573A CN 106367235 A CN106367235 A CN 106367235A
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- China
- Prior art keywords
- rutaceae
- extract
- distillation
- water
- application
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/24—Cleaning or pickling metallic material with solutions or molten salts with neutral solutions
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
Abstract
The invention relates to the technical field of fine chemical engineering and particularly discloses application of a rutaceous plant extract serving as a decontaminant. A preparation method the rutaceous plant extract comprises the steps that S1, flowers, fruits, leaves or/and peels of rutaceous plants are subjected to steam distillation by using a steam distillation method to obtain a liquid mixture of water and essential oil; S2, the liquid mixture of water and essential oil is separated, and a water phase is taken to obtain the rutaceous plant extract. The rutaceous plant extract includes but is not limited to lemons, shaddocks, tangerines, oranges, bergamots or peppers. The decontaminant has strong decontamination capability. Due to the fact that the decontaminant is separated from the plant essential oil extracting process, contained components are pure natural substances, and a PH value is basically neutral. Therefore, the human skin is not hurt in the using process, and secondary environmental pollution is also not caused in use.
Description
Technical field
The present invention relates to technical field of fine and in particular to a kind of rutaceae extract as detergent should
With.
Background technology
Existing cleaning agent is all by active alkali such as potassium carbonate, the solvent such as chemistry such as ammonia, isopropanol and surfactant
Product compound and form, and wherein contain strong volatile solvent, Harmful chemicals, permeability is extremely strong, have obvious stimulation to human eye,
There is corrosiveness to skin, need after cleaning to be carried out remaining with a large amount of water, waste water enters nature, brings secondary pollution.
Therefore, develop a kind of detergent natural, that clean effect is good health and environmental conservation are had great importance.
Rutaceae (scientific name: rutaceae) is a section of Angiospermae, Dicotyledoneae, Sapindales.Folium Symplocoris Caudatae
Section is evergreen or deciduous tree, shrub or climb up by holding on to liana or draft, all contain volatile oil, leaf has transparent oil droplet point, logical in plant body
Often there is oil storage cell or have secretory cavity.At present rutaceae maximum application is worth and is as industrial crops or flavoring agent, still
No correlation technique reports that it has clean effect, and specific decontamination effective site.
Content of the invention
The technical problem to be solved is, in order to overcome the shortcomings of natural detergent species in prior art, to carry
For a kind of rutaceae extract as detergent application.
Above-mentioned technical problem to be solved by this invention, is achieved by the following technical programs:
, as the application of detergent, described rutaceae extract is by comprising to walk as follows for a kind of rutaceae extract
Rapid method prepares:
S1. by the flower of rutaceae, really, leaf or/and peel carry out vapor distillation with steam distillation, obtain water and essence
The liquid mixture of oil；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract.
Preferably, described rutaceae include but is not limited to Fructus Citri Limoniae, Fructus Citri grandiss, orange, Citrus chachiensis Hort., Fructus Citri tangerinae (Fructus Citri tangerinae), Fructus Citri Sarcodactyliss or
Pericarpium Zanthoxyli.
Preferably, in step s1, the actual conditions of steam distillation is: by the flower of rutaceae, really, leaf or/and fruit
Skin is placed in distillation 1 ~ 3h in vapor distillation device, and vapo(u)rizing temperature is 90 ~ 110 DEG C.
Most preferably, in step s1, the actual conditions of steam distillation is: by the flower of rutaceae, really, leaf or/and
Peel is placed in distillation 2 ~ 3h in vapor distillation device, and vapo(u)rizing temperature is 100 ~ 106 DEG C.
Preferably, described detergent includes but is not limited to glass, pottery, metal or plastics detergent.
Most preferably, described glass includes but is not limited to vehicle glass, door glass, television screen or computer screen
Curtain；Described pottery includes but is not limited to crockery, ceramic sanitary ware, porcelain plate.
A kind of cleaning method of glass surface, the method includes: is extracted using above-mentioned rutaceae in cleaning process
Thing.
A kind of cleaning method of ceramic surface, the method includes: is extracted using above-mentioned rutaceae in cleaning process
Thing.
A kind of cleaning method of metal surface, the method includes: is extracted using above-mentioned rutaceae in cleaning process
Thing.
A kind of cleaning method of frosting, the method includes: is extracted using above-mentioned rutaceae in cleaning process
Thing.
Beneficial effect: (1) is the invention provides a kind of brand-new natural detergent；(2) the detergent dirt-removing power described in
By force, because this detergent is to separate from plants essential oil extraction process, therefore in use without compromising on human body skin
Skin, also will not cause secondary pollution to environment when using；(3) this detergent is by discarded water in the production process of quintessence oil
Rationally use, decrease the difficulty processing waste water in quintessence oil production process, realize turning waste into wealth.
Specific embodiment
The present invention is explained further below in conjunction with specific embodiment, but embodiment does not do any type of limit to the present invention
Fixed.
Unreceipted actual conditions person in embodiment, the condition according to normal condition or manufacturer's suggestion is carried out.Wherein, used
Reagent or the unreceipted production firm person of instrument, be can by city available from conventional products.
A kind of preparation of rutaceae extract of embodiment 1
The method that described rutaceae extract passes through to comprise the steps of prepares:
S1. rutaceae Fructus Citri Limoniae peel is carried out vapor distillation with steam distillation, obtain the liquid mixing of water and quintessence oil
Thing；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract；
In step s1, the actual conditions of steam distillation is: rutaceae Fructus Citri Limoniae peel is placed in distillation 2h in boiler,
Vapo(u)rizing temperature is 105 DEG C.
A kind of preparation of rutaceae extract of embodiment 2
The method that described rutaceae extract passes through to comprise the steps of prepares:
S1. carry out vapor distillation by size-reduced for rutaceae Fructus Citri grandiss young fruit with steam distillation, obtain the liquid of water and quintessence oil
Body mixture；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract；
In step s1, the actual conditions of steam distillation is: rutaceae Fructus Citri grandiss young fruit is placed in distillation 2h in boiler,
Vapo(u)rizing temperature is 105 DEG C.
A kind of preparation of rutaceae extract of embodiment 3
The method that described rutaceae extract passes through to comprise the steps of prepares:
S1. rutaceae Pericarpium Citri junoriss are carried out vapor distillation with steam distillation, obtain the liquid mixture of water and quintessence oil；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract；
In step s1, the actual conditions of steam distillation is: rutaceae Pericarpium Citri junoriss are placed in distillation 2h in boiler, distillation
Temperature is 105 DEG C.
A kind of preparation of rutaceae extract of embodiment 4
The method that described rutaceae extract passes through to comprise the steps of prepares:
S1. rutaceae Fructus Citri tangerinae leaf is carried out vapor distillation with steam distillation, obtain the liquid mixing of water and quintessence oil
Thing；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract；
In step s1, the actual conditions of steam distillation is: rutaceae Fructus Citri tangerinae leaf is placed in distillation 2h in boiler, steams
Evaporate temperature and be 103 DEG C.
A kind of preparation of rutaceae extract of embodiment 5
The method that described rutaceae extract passes through to comprise the steps of prepares:
S1. rutaceae Fructus Citri Sarcodactyliss fruit is carried out vapor distillation with steam distillation, the liquid obtaining water with quintessence oil mixes
Compound；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract；
In step s1, the actual conditions of steam distillation is: rutaceae Fructus Citri Sarcodactyliss fruit is placed in distillation in boiler
2h, vapo(u)rizing temperature is 105 DEG C.
A kind of preparation of rutaceae extract of embodiment 6
The method that described rutaceae extract passes through to comprise the steps of prepares:
S1. the peel of rutaceae Pericarpium Zanthoxyli is carried out vapor distillation with steam distillation, the liquid obtaining water with quintessence oil mixes
Compound；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract；
In step s1, the actual conditions of steam distillation is: the peel of rutaceae Pericarpium Zanthoxyli is placed in distillation in boiler
2h, vapo(u)rizing temperature is 103 DEG C.
A kind of preparation of rutaceae extract of embodiment 7
The method that described rutaceae extract passes through to comprise the steps of prepares:
S1. the flower of rutaceae orange is carried out vapor distillation with steam distillation, obtain the liquid mixing of water and quintessence oil
Thing；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract；
In step s1, the actual conditions of steam distillation is: the flower of rutaceae orange is placed in distillation 2h in boiler, steams
Evaporate temperature and be 101 DEG C.
Embodiment 8 is as bathroom detergent detergency test method
(1) configuration of artificial dirt
Formula: diammonium phosphate 10.0g, milk powder 20.0g, sodium phosphate 6.0g, calcium stearate 7.0 g, standard loess 6.0 g,
Carbamide 8.0, sulphur urine 5.0 g, hard water 70.0 g, egg 22.0 g.The collocation method of described hard water is: cacl216.7 g
And mgso4·7h20 24.7g, prepares 10l.The percentage composition of described standard loess is: silicon dioxide 65%, iron sesquioxide
15%th, aluminium sesquioxide 12%, calcium oxide 8%.
Collocation method: 80 DEG C of thawings will be heated in calcium stearate, the beaker of hard water, then other compositions are added mixed
With stir, obtain final product artificial dirt.
(2) soil removal efficiency measures
With reference to the method described in gb9985-2000 annex b1, dirt is coated on sheet glass, refer again to test side therein
Method evaluates the soil removal efficiency of the rutaceae extract described in embodiment 1 ~ 7.Concrete data is referring to table 1.
Can be seen that the decontamination of the rutaceae extract that the embodiment of the present invention 1 ~ 7 prepares by table 1 test data
Rate is all higher than 98%, illustrates that rutaceae extract of the present invention has very excellent decontamination
Effect, can use as bathroom detergent.
Embodiment 9 is as kitchen weight dirt cleaning agent detergency test method
(1) preparation of artificial dirt
The preparation of dirt: take Ballast convention (in every hectogram: Oleic acid 60g, linoleic acid 40g), with edible Adeps Sus domestica, solid stone
Wax, is mixed in the ratio of 4:4:2, and adds the monoglyceride of gross weight 4%, is heated to 180 degree, keeps 15 minutes, stirring
Under be cooled to room temperature.Take the above-mentioned grease preparing, after being heated to 80 degree, immerse test sample in grease at room temperature and keep
After 30 seconds, be slowly withdrawn, after grease falling speed slack-off to half curdled appearance, put into 40 degree of incubators more than 72 hours.
(2) soil removal efficiency measures
With reference to the method described in gb9985-2000 annex b1, dirt is coated on sheet glass, refer again to test side therein
Method evaluates the soil removal efficiency of the rutaceae extract described in embodiment 1 ~ 7.Concrete data is referring to table 2.
Can be seen that the decontamination of the rutaceae extract that the embodiment of the present invention 1 ~ 7 prepares by table 2 test data
Rate is all higher than 97%, illustrates that rutaceae extract of the present invention has very excellent decontamination
Effect, can use as kitchen weight dirt detergent.
Embodiment 10 is as glass cleaner soil removal efficiency method of testing
(1) configuration of artificial dirt
Formula: milk powder 20.0g, calcium stearate 7.0 g, standard loess 6.0 g, hard water 70.0 g.The configuration side of described hard water
Method is: cacl216.7 g and mgso4·7h20 24.7g, prepares 10l.The percentage composition of described standard loess is: titanium dioxide
Silicon 65%, iron sesquioxide 15%, aluminium sesquioxide 12%, calcium oxide 8%.
Collocation method: 80 DEG C of thawings will be heated in calcium stearate, the beaker of hard water, then other compositions are added mixed
With stir, obtain final product artificial dirt.
(2) soil removal efficiency measures
With reference to the method described in gb9985-2000 annex b1, dirt is coated on sheet glass, refer again to test side therein
Method evaluates the soil removal efficiency of the rutaceae extract described in embodiment 1 ~ 7.Concrete data is referring to table 1.
Can be seen that the decontamination of the rutaceae extract that the embodiment of the present invention 1 ~ 7 prepares by table 3 test data
Rate is all higher than 99%, illustrates that rutaceae extract of the present invention has very excellent decontamination
Effect, can use as glass decontaminating agent.
A kind of cleaning method of glass surface of embodiment 11
The method includes: the rutaceae extract being prepared using embodiment 1 in cleaning process.
A kind of cleaning method of ceramic surface of embodiment 12
The method includes: the rutaceae extract being prepared using embodiment 2 in cleaning process.
A kind of cleaning method of metal surface of embodiment 13
Method includes: the rutaceae extract being prepared using embodiment 3 in cleaning process.
A kind of cleaning method of frosting of embodiment 14
The method includes: the rutaceae extract being prepared using embodiment 4 in cleaning process.
Claims (10)
1. a kind of rutaceae extract as the application of detergent it is characterised in that described rutaceae extract
Prepared by the method comprising the steps of:
S1. by the flower of rutaceae, really, leaf or/and peel carry out vapor distillation with steam distillation, obtain water and essence
The liquid mixture of oil；
S2. separation water and the liquid mixture of quintessence oil, fetch water and mutually obtain final product described rutaceae extract.
2. application according to claim 1 it is characterised in that described rutaceae include but is not limited to Fructus Citri Limoniae, Fructus Citri grandiss,
Orange, Citrus chachiensis Hort., Fructus Citri tangerinae, Fructus Citri Sarcodactyliss or Pericarpium Zanthoxyli.
3. according to claim 1 application it is characterised in that in step s1 the actual conditions of steam distillation be: will
The flower of rutaceae, really, leaf or/and peel be placed in distillation 1 ~ 3h in vapor distillation device, vapo(u)rizing temperature is 90 ~ 110 DEG C.
4. according to claim 3 application it is characterised in that in step s1 the actual conditions of steam distillation be: will
The flower of rutaceae, really, leaf or/and peel be placed in distillation 2 ~ 3h in vapor distillation device, vapo(u)rizing temperature is 100 ~ 106
℃.
5. application according to claim 1 is it is characterised in that described detergent includes but is not limited to glass, pottery, gold
Belong to or plastics detergent.
6. application according to claim 1 is it is characterised in that described glass includes but is not limited to vehicle glass, door and window
Glass, television screen or computer screen；Described pottery includes but is not limited to crockery, ceramic sanitary ware, porcelain plate.
7. a kind of cleaning method of glass surface is it is characterised in that the method includes: in cleaning process usage right require 1 ~
Rutaceae extract described in 4 any one.
8. a kind of cleaning method of ceramic surface is it is characterised in that the method includes: in cleaning process usage right require 1 ~
Rutaceae extract described in 4 any one.
9. a kind of cleaning method of metal surface is it is characterised in that the method includes: in cleaning process usage right require 1 ~
Rutaceae extract described in 4 any one.
10. a kind of cleaning method of frosting is it is characterised in that the method includes: in cleaning process, usage right requires 1
Rutaceae extract described in ~ 4 any one.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610735573.8A CN106367235A (en) | 2016-08-26 | 2016-08-26 | Application of rutaceous plant extract serving as decontaminant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610735573.8A CN106367235A (en) | 2016-08-26 | 2016-08-26 | Application of rutaceous plant extract serving as decontaminant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106367235A true CN106367235A (en) | 2017-02-01 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610735573.8A Pending CN106367235A (en) | 2016-08-26 | 2016-08-26 | Application of rutaceous plant extract serving as decontaminant |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107118880A (en) * | 2017-06-15 | 2017-09-01 | 安徽师范大学 | A kind of Mobile phone cleaning liquid and preparation method thereof |
| CN110272784A (en) * | 2019-07-08 | 2019-09-24 | 江西理工大学 | A kind of bathroom detergent and preparation method thereof containing citrus reticulata"Chachi" blueness mandarin orange juice |
| CN110777010A (en) * | 2019-11-29 | 2020-02-11 | 陕西速源节能科技有限公司 | Bathroom cleaning agent and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1789398A (en) * | 2005-12-13 | 2006-06-21 | 张刚 | Natural plant type detergent |
| CN101962601A (en) * | 2010-10-31 | 2011-02-02 | 无锡龙腾画材有限公司 | Environment-friendly orange peel extract limonene degumming and decontaminating agent and preparation method thereof |
| CN103242978A (en) * | 2013-05-08 | 2013-08-14 | 任航 | Natural plant cleaning agent for cleaning heavy oil in kitchen and preparation method of natural plant cleaning agent |
| CN104031773A (en) * | 2014-06-04 | 2014-09-10 | 韩城市司马迁旅游文化发展有限公司 | Method for preparing pepper volatile oil fragrant skin care soap |
-
2016
- 2016-08-26 CN CN201610735573.8A patent/CN106367235A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1789398A (en) * | 2005-12-13 | 2006-06-21 | 张刚 | Natural plant type detergent |
| CN101962601A (en) * | 2010-10-31 | 2011-02-02 | 无锡龙腾画材有限公司 | Environment-friendly orange peel extract limonene degumming and decontaminating agent and preparation method thereof |
| CN103242978A (en) * | 2013-05-08 | 2013-08-14 | 任航 | Natural plant cleaning agent for cleaning heavy oil in kitchen and preparation method of natural plant cleaning agent |
| CN104031773A (en) * | 2014-06-04 | 2014-09-10 | 韩城市司马迁旅游文化发展有限公司 | Method for preparing pepper volatile oil fragrant skin care soap |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107118880A (en) * | 2017-06-15 | 2017-09-01 | 安徽师范大学 | A kind of Mobile phone cleaning liquid and preparation method thereof |
| CN110272784A (en) * | 2019-07-08 | 2019-09-24 | 江西理工大学 | A kind of bathroom detergent and preparation method thereof containing citrus reticulata"Chachi" blueness mandarin orange juice |
| CN110777010A (en) * | 2019-11-29 | 2020-02-11 | 陕西速源节能科技有限公司 | Bathroom cleaning agent and preparation method thereof |
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