CN106366895A - Wood-used environment-friendly fragrant sumac and preparation method thereof - Google Patents
Wood-used environment-friendly fragrant sumac and preparation method thereof Download PDFInfo
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- CN106366895A CN106366895A CN201610741350.2A CN201610741350A CN106366895A CN 106366895 A CN106366895 A CN 106366895A CN 201610741350 A CN201610741350 A CN 201610741350A CN 106366895 A CN106366895 A CN 106366895A
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- sumac
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/08—Polyurethanes from polyethers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/06—Polyurethanes from polyesters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a wood-used environment-friendly fragrant sumac. The wood-used environment-friendly fragrant sumac consists of the following raw materials in parts by weight: 50-60 parts of a modified aqueous polyurethane emulsion, 15-20 parts of a styrene-acrylic emulsion, 5-10 parts of a cyclodextrin inclusion compound, 3-6 parts of glass dust, 2-4 parts of N-methyl pyrrolidone, 2-4 parts of acetic ether, 5-8 parts of 2,2,4-trimethyl-1,3-pentanediol monoisobutyrate, 1-2 parts of carboxymethyl cellulose, 0.5-1 part of polyethylene wax, 10-15 parts of deionized water, 0.3-0.8 part of a wetting agent, 0.3-0.8 part of a flattening agent and 1-3 parts of a light stabilizer. The invention further discloses a preparation method of the wood-used environment-friendly fragrant sumac. An obtained paint has good film forming property, strong adherence to a substrate, excellent such comprehensive properties as water resistance, aging resistance and scratch resistance and high fullness, and the paint film can reach the hardness of 2H and can stably give out natural plant aromatic odor in a lasting manner to purify air and benefit human health. The wood-used environment-friendly fragrant sumac has an extensive market prospect and an important application value.
Description
Technical field
The present invention relates to technical field of coatings uses environment-friendly type fragrant sumac and preparation method thereof and in particular to one kind is wooden.
Background technology
With the development of modern economy society, the raising of people's living standard, fragrant sumac paints with respect to tradition, with certain
The fragrance of feature, will greatly improve added value and the using effect of paint vehicle, meet the continuous demand to material life for the people.Mesh
Before, wood paint on the market has many kinds, but mostly contains the composition that human body and environment are harmful to, and causes serious environmental pollution
And destruction, delicate fragrance environmental-protecting performance is generally poor.With people life taste lifting and to healthy highest attention, for paint vehicle
Safety and environmental protection index also require that more and more higher, and the wood paint developing a kind of delicate fragrance environmental protection is the trend institute of current environmental protection
?.
Content of the invention
For the deficiencies in the prior art, the invention provides a kind of wood ring easy to make, that pure and fresh fragrance can be given out
Guarantor's type fragrant sumac and preparation method thereof.
For realizing object above, the present invention is achieved by the following technical programs:
Environment-friendly type fragrant sumac used by a kind of wood, is made up of the raw material of following weight portion: modified aqueous polyurethane emulsion 50-60
Part, styrene-acrylic emulsion 15-20 part, cyclodextrin clathrate 5-10 part, glass dust 3-6 part, n- methyl pyrrolidone 2-4 part, acetic acid second
Ester 2-4 part, Lauryl Alcohol ester 5-8 part, carboxymethyl cellulose 1-2 part, Tissuemat E 0.5-1 part, deionized water 10-15 part, profit
Humectant 0.3-0.8 part, levelling agent 0.3-0.8 part, light stabilizer 1-3 part.
Preferably, it is made up of the raw material of following weight portion: 55 parts of modified aqueous polyurethane emulsion, 17 parts of styrene-acrylic emulsion, ring
7 parts of cyclodextrin inclusion compound, 5 parts of glass dust, 2.5 parts of n- methyl pyrrolidone, 3 parts of ethyl acetate, 7 parts of Lauryl Alcohol ester, carboxymethyl
1.2 parts of cellulose, 0.6 part of Tissuemat E, 14 parts of deionized water, 0.4 part of wetting agent, 0.4 part of levelling agent, 1.8 parts of light stabilizer.
Preferably, described aqueous polyurethane emulsion is the polyether-modified aqueous polyurethane emulsion of aliphatic polyester, and solid content is
35-40%.
Preferably, described light stabilizer is 2- (the tertiary phenyl of 2'- hydroxyl -3', 5'- bis-) -5- chlorination benzotriazole and 4- benzene
Formyloxy -2, the compositionss of 2,6,6- tetramethyl piperidines.
Preferably, the preparation method of described cyclodextrin clathrate is as follows: make saturated solution by soluble in water for beta-schardinger dextrin-,
Then aromatic oil is dissolved in ethanol in proper amount dilution, is added dropwise in beta-schardinger dextrin-saturated aqueous solution, adjusting ph value is 6,25
Stir 3-4h, cooling, sucking filtration at DEG C, clean 2-3 time, vacuum drying, obtain cyclodextrin clathrate.
Preferably, described aromatic oil is natural plant aromatic oil.
The wood preparation method of environment-friendly type fragrant sumac, step is as follows:
1) modified aqueous polyurethane emulsion, styrene-acrylic emulsion and suitable quantity of water are added in high speed dispersor, stir 5-
10min；
2) to step 1) add n- methyl pyrrolidone, ethyl acetate in system, stir 3-5min, continuously add cyclodextrin
Clathrate, glass dust, stir 5-10min；
3) to step 2) add Lauryl Alcohol ester, carboxymethyl cellulose, Tissuemat E, stirring in system, continuously add profit
Humectant, levelling agent, light stabilizer and balance deionized water, stir 30-40min, obtain final product.
The invention has the advantages that: it is main component that the present invention adopts styrene-acrylic emulsion and modified aqueous polyurethane emulsion, obtain
Paint vehicle good film-forming property, the excellent combination property such as water-fast, ageing-resistant, scratch resistance strong with base material adhesive force, richness is high, paint film
Hardness is up to 2h, long service life.Product does not contain the harmful substance such as formaldehyde, benzene, environmental protection, and the cyclodextrin clathrate adding
Can stablize lasting give out natural plants aromatic odor, purify air, beneficial health, the present invention has extensive market
Prospect and important using value.
Specific embodiment
Purpose, technical scheme and advantage for making the embodiment of the present invention are clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the present invention is clearly and completely described it is clear that described embodiment is the present invention one
Divide embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making
The every other embodiment being obtained under the premise of creative work, broadly falls into the scope of protection of the invention.
Embodiment 1:
Environment-friendly type fragrant sumac used by a kind of wood, is made up of the raw material of following weight portion: the polyether-modified aqueouss of aliphatic polyester are gathered
55 parts of urethane emulsion (solid content is 38%), 17 parts of styrene-acrylic emulsion, 7 parts of cyclodextrin clathrate, 5 parts of glass dust, n- methylpyrrole
2.5 parts of alkanone, 3 parts of ethyl acetate, 7 parts of Lauryl Alcohol ester, 1.2 parts of carboxymethyl cellulose, 0.6 part of Tissuemat E, deionized water
14 parts, 0.4 part of wetting agent, 0.4 part of levelling agent, 1.8 parts of light stabilizer.Wherein, light stabilizer is 2- (2'- hydroxyl -3', 5'- bis-
Tertiary phenyl) -5- chlorination benzotriazole and 4- benzoyloxy -2, the compositionss of 2,6,6- tetramethyl piperidines.
The preparation method of cyclodextrin clathrate is as follows: make saturated solution by soluble in water for beta-schardinger dextrin-, then will be natural
Essential oil is dissolved in ethanol in proper amount dilution, is added dropwise in beta-schardinger dextrin-saturated aqueous solution, and adjusting ph value is 6, at 25 DEG C
Lower stirring 3.5h, cooling, sucking filtration, cleans 2 times, vacuum drying, obtains cyclodextrin clathrate.
The wood preparation method of environment-friendly type fragrant sumac, step is as follows:
1) modified aqueous polyurethane emulsion, styrene-acrylic emulsion and suitable quantity of water are added in high speed dispersor, stir 8min；
2) to step 1) add n- methyl pyrrolidone, ethyl acetate in system, stir 4min, continuously add cyclodextrin bag
Compound, glass dust, stir 8min；
3) to step 2) add Lauryl Alcohol ester, carboxymethyl cellulose, Tissuemat E, stirring in system, continuously add profit
Humectant, levelling agent, light stabilizer and balance deionized water, stir 30min, obtain final product.
Embodiment 2:
Environment-friendly type fragrant sumac used by a kind of wood, is made up of the raw material of following weight portion: the polyether-modified aqueouss of aliphatic polyester are gathered
52 parts of urethane emulsion (solid content is 35%), 18 parts of styrene-acrylic emulsion, 6 parts of cyclodextrin clathrate, 4 parts of glass dust, n- methylpyrrole
3 parts of alkanone, 2.5 parts of ethyl acetate, 6 parts of Lauryl Alcohol ester, 1 part of carboxymethyl cellulose, 0.5 part of Tissuemat E, deionized water 13
Part, 0.4 part of wetting agent, 0.4 part of levelling agent, 1.5 parts of light stabilizer.Wherein, light stabilizer is 2- (2'- hydroxyl -3', 5'- bis- uncle
Phenyl) -5- chlorination benzotriazole and 4- benzoyloxy -2, the compositionss of 2,6,6- tetramethyl piperidines.
The preparation method of cyclodextrin clathrate is as follows: make saturated solution by soluble in water for beta-schardinger dextrin-, then will be natural
Essential oil is dissolved in ethanol in proper amount dilution, is added dropwise in beta-schardinger dextrin-saturated aqueous solution, and adjusting ph value is 6, at 25 DEG C
Lower stirring 3h, cooling, sucking filtration, cleans 2 times, vacuum drying, obtains cyclodextrin clathrate.
The wood preparation method of environment-friendly type fragrant sumac, step is as follows:
1) modified aqueous polyurethane emulsion, styrene-acrylic emulsion and suitable quantity of water are added in high speed dispersor, stir 5min；
2) to step 1) add n- methyl pyrrolidone, ethyl acetate in system, stir 3min, continuously add cyclodextrin bag
Compound, glass dust, stir 5min；
3) to step 2) add Lauryl Alcohol ester, carboxymethyl cellulose, Tissuemat E, stirring in system, continuously add profit
Humectant, levelling agent, light stabilizer and balance deionized water, stir 35min, obtain final product.
Embodiment 3:
Environment-friendly type fragrant sumac used by a kind of wood, is made up of the raw material of following weight portion: the polyether-modified aqueouss of aliphatic polyester are gathered
58 parts of urethane emulsion (solid content is 35%), 16 parts of styrene-acrylic emulsion, 8 parts of cyclodextrin clathrate, 4.5 parts of glass dust, n- methyl pyrrole
3 parts of pyrrolidone, 23 parts of ethyl acetate, 7 parts of Lauryl Alcohol ester, 1.2 parts of carboxymethyl cellulose, 0.7 part of Tissuemat E, deionized water
15 parts, 0.5 part of wetting agent, 0.5 part of levelling agent, 2 parts of light stabilizer.Wherein, light stabilizer is 2- (2'- hydroxyl -3', 5'- bis- uncle
Phenyl) -5- chlorination benzotriazole and 4- benzoyloxy -2, the compositionss of 2,6,6- tetramethyl piperidines.
The preparation method of cyclodextrin clathrate is as follows: make saturated solution by soluble in water for beta-schardinger dextrin-, then will be natural
Essential oil is dissolved in ethanol in proper amount dilution, is added dropwise in beta-schardinger dextrin-saturated aqueous solution, and adjusting ph value is 6, at 25 DEG C
Lower stirring 4h, cooling, sucking filtration, cleans 3 times, vacuum drying, obtains cyclodextrin clathrate.
The wood preparation method of environment-friendly type fragrant sumac, step is as follows:
1) modified aqueous polyurethane emulsion, styrene-acrylic emulsion and suitable quantity of water are added in high speed dispersor, stir 5min；
2) to step 1) add n- methyl pyrrolidone, ethyl acetate in system, stir 3min, continuously add cyclodextrin bag
Compound, glass dust, stir 10min；
3) to step 2) add Lauryl Alcohol ester, carboxymethyl cellulose, Tissuemat E, stirring in system, continuously add profit
Humectant, levelling agent, light stabilizer and balance deionized water, stir 40min, obtain final product.
Embodiment 4:
Environment-friendly type fragrant sumac used by a kind of wood, is made up of the raw material of following weight portion: the polyether-modified aqueouss of aliphatic polyester are gathered
60 parts of urethane emulsion (solid content is 37%), 15 parts of styrene-acrylic emulsion, 10 parts of Benexate Hydrochloride, 3 parts of glass dust, n- methyl pyrrole
4 parts of pyrrolidone, 2 parts of ethyl acetate, 8 parts of Lauryl Alcohol ester, 1 part of carboxymethyl cellulose, 1 part of Tissuemat E, 10 parts of deionized water,
0.8 part of wetting agent, 0.3 part of levelling agent, 3 parts of light stabilizer.Wherein, light stabilizer is 2- (the tertiary benzene of 2'- hydroxyl -3', 5'- bis-
Base) -5- chlorination benzotriazole and 4- benzoyloxy -2, the compositionss of 2,6,6- tetramethyl piperidines.
The preparation method of cyclodextrin clathrate is as follows: make saturated solution by soluble in water for beta-schardinger dextrin-, then will be natural
Essential oil is dissolved in ethanol in proper amount dilution, is added dropwise in beta-schardinger dextrin-saturated aqueous solution, and adjusting ph value is 6, at 25 DEG C
Lower stirring 3h, cooling, sucking filtration, cleans 3 times, vacuum drying, obtains cyclodextrin clathrate.
The wood preparation method of environment-friendly type fragrant sumac, step is as follows:
1) modified aqueous polyurethane emulsion, styrene-acrylic emulsion and suitable quantity of water are added in high speed dispersor, stir 7min；
2) to step 1) add n- methyl pyrrolidone, ethyl acetate in system, stir 4min, continuously add cyclodextrin bag
Compound, glass dust, stir 7min；
3) to step 2) add Lauryl Alcohol ester, carboxymethyl cellulose, Tissuemat E, stirring in system, continuously add profit
Humectant, levelling agent, light stabilizer and balance deionized water, stir 30min, obtain final product.
Embodiment 5:
Environment-friendly type fragrant sumac used by a kind of wood, is made up of the raw material of following weight portion: the polyether-modified aqueouss of aliphatic polyester are gathered
50 parts of urethane emulsion (solid content is 40%), 20 parts of styrene-acrylic emulsion, 5 parts of cyclodextrin clathrate, 6 parts of glass dust, n- methylpyrrole
2 parts of alkanone, 4 parts of ethyl acetate, 5 parts of Lauryl Alcohol ester, 2 parts of carboxymethyl cellulose, 0.5 part of Tissuemat E, 15 parts of deionized water,
0.3 part of wetting agent, 0.8 part of levelling agent, 1 part of light stabilizer.Wherein, light stabilizer is 2- (the tertiary benzene of 2'- hydroxyl -3', 5'- bis-
Base) -5- chlorination benzotriazole and 4- benzoyloxy -2, the compositionss of 2,6,6- tetramethyl piperidines.
The preparation method of cyclodextrin clathrate is as follows: make saturated solution by soluble in water for beta-schardinger dextrin-, then will be natural
Essential oil is dissolved in ethanol in proper amount dilution, is added dropwise in beta-schardinger dextrin-saturated aqueous solution, and adjusting ph value is 6, at 25 DEG C
Lower stirring 4h, cooling, sucking filtration, cleans 2 times, vacuum drying, obtains cyclodextrin clathrate.
The wood preparation method of environment-friendly type fragrant sumac, step is as follows:
1) modified aqueous polyurethane emulsion, styrene-acrylic emulsion and suitable quantity of water are added in high speed dispersor, stir 10min；
2) to step 1) add n- methyl pyrrolidone, ethyl acetate in system, stir 5min, continuously add cyclodextrin bag
Compound, glass dust, stir 10min；
3) to step 2) add Lauryl Alcohol ester, carboxymethyl cellulose, Tissuemat E, stirring in system, continuously add profit
Humectant, levelling agent, light stabilizer and balance deionized water, stir 40min, obtain final product.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation are made a distinction with another entity or operation, and not necessarily require or imply these entities or deposit between operating
In any this actual relation or order.And, term " inclusion ", "comprising" or its any other variant are intended to
Comprising of nonexcludability, wants so that including a series of process of key elements, method, article or equipment and not only including those
Element, but also include other key elements being not expressly set out, or also include for this process, method, article or equipment
Intrinsic key element.In the absence of more restrictions, the key element that limited by sentence "including a ..." it is not excluded that
Also there is other identical element including in the process of described key element, method, article or equipment.
Above example only in order to technical scheme to be described, is not intended to limit；Although with reference to the foregoing embodiments
The present invention has been described in detail, it will be understood by those within the art that: it still can be to aforementioned each enforcement
Technical scheme described in example is modified, or carries out equivalent to wherein some technical characteristics；And these modification or
Replace, do not make the essence of appropriate technical solution depart from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (7)
1. a kind of wood environment-friendly type fragrant sumac is it is characterised in that be made up of the raw material of following weight portion: modified aqueous polyurethane breast
Liquid 50-60 part, styrene-acrylic emulsion 15-20 part, cyclodextrin clathrate 5-10 part, glass dust 3-6 part, n- methyl pyrrolidone 2-4 part,
Ethyl acetate 2-4 part, Lauryl Alcohol ester 5-8 part, carboxymethyl cellulose 1-2 part, Tissuemat E 0.5-1 part, deionized water 10-15
Part, wetting agent 0.3-0.8 part, levelling agent 0.3-0.8 part, light stabilizer 1-3 part.
2. wood environment-friendly type fragrant sumac as claimed in claim 1 is it is characterised in that be made up of the raw material of following weight portion: changes
55 parts of aqueous polyurethane emulsion of property, 17 parts of styrene-acrylic emulsion, 7 parts of cyclodextrin clathrate, 5 parts of glass dust, n- methyl pyrrolidone 2.5
Part, 3 parts of ethyl acetate, 7 parts of Lauryl Alcohol ester, 1.2 parts of carboxymethyl cellulose, 0.6 part of Tissuemat E, 14 parts of deionized water, profit
0.4 part of humectant, 0.4 part of levelling agent, 1.8 parts of light stabilizer.
3. wood environment-friendly type fragrant sumac as claimed in claim 2 is it is characterised in that described aqueous polyurethane emulsion is aliphatic
The polyether-modified aqueous polyurethane emulsion of polyester, solid content is 35-40%.
4. wood environment-friendly type fragrant sumac as claimed in claim 2 it is characterised in that described light stabilizer be 2- (2'- hydroxyl-
The tertiary phenyl of 3', 5'- bis-) -5- chlorination benzotriazole and 4- benzoyloxy -2, the compositionss of 2,6,6- tetramethyl piperidines.
5. wood environment-friendly type fragrant sumac as claimed in claim 2 is it is characterised in that the preparation method of described cyclodextrin clathrate
As follows: make saturated solution by soluble in water for beta-schardinger dextrin-, then by aromatic oil be dissolved in ethanol in proper amount dilution, be added dropwise to β-
In cyclodextrin saturated aqueous solution, adjusting ph value is 6, stirs 3-4h, cooling, sucking filtration, clean 2-3 time at 25 DEG C, vacuum drying,
Obtain cyclodextrin clathrate.
6. wood environment-friendly type fragrant sumac as claimed in claim 5 is it is characterised in that described aromatic oil is natural plants fragrance
Oil.
7. described wood as arbitrary in the claim 1-6 preparation method of environment-friendly type fragrant sumac is it is characterised in that step is as follows:
1) modified aqueous polyurethane emulsion, styrene-acrylic emulsion and suitable quantity of water are added in high speed dispersor, stir 5-10min；
2) to step 1) add n- methyl pyrrolidone, ethyl acetate in system, stir 3-5min, continuously add cyclodextrin inclusion compound
Thing, glass dust, stir 5-10min；
3) to step 2) add Lauryl Alcohol ester, carboxymethyl cellulose, Tissuemat E, stirring in system, continuously add wetting agent,
Levelling agent, light stabilizer and balance deionized water, stir 30-40min, obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610741350.2A CN106366895A (en) | 2016-08-27 | 2016-08-27 | Wood-used environment-friendly fragrant sumac and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610741350.2A CN106366895A (en) | 2016-08-27 | 2016-08-27 | Wood-used environment-friendly fragrant sumac and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN106366895A true CN106366895A (en) | 2017-02-01 |
Family
ID=57904184
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201610741350.2A Pending CN106366895A (en) | 2016-08-27 | 2016-08-27 | Wood-used environment-friendly fragrant sumac and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114702889A (en) * | 2022-05-12 | 2022-07-05 | 广东家实多集团有限公司 | Waterborne polyurethane coating |
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