CN106350397A - Anti-oxidization health-care wine and preparation method thereof - Google Patents
Anti-oxidization health-care wine and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
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Abstract
The invention disclsoes anti-oxidization health-care wine and a preparation method thereof, and belongs to the field of health-care foods. The anti-oxidization health-care wine is prepared from the following raw materials in parts by weight: 5 to 10 parts of radix cynanchi bungei, 1 to 2 parts of lepidium meyenii, 0.1 to 0.5 part of longan aril and a proper amount of Baijiu. The preparation method comprises: mixing the radix cynanchi bungei, the lepidium meyenii and the longan aril and extracting with water. The raw materials are extracted through selecting a proper extracting manner according to properties of functional components, so that the stability of the functional components is guaranteed, and a relatively high extracting rate is obtained. The health-care wine prepared by the invention has the advantages of novel food materials including the radix cynanchi bungei and the lepidium meyenii, and a traditional Chinese medicinal material longan aril, and has an anti-oxidization effect and the like.
Description
Technical field
The invention belongs to field of health care food is and in particular to a kind of anti-oxidation health wine and preparation method thereof.
Background technology
Antioxidation refers to the abbreviation of resisting oxidation free radical., because continuing and extraneous contact, including breathing, (oxidation is anti-for human body
Should), outside contamination, lonizing radiation irradiate etc. factor be constantly produced from by base in human body body.Scientific investigations showed that, old and feeble, cancer
Disease or Other diseases are mostly relevant with the generation of excessive free radicals.Research antioxidation can effectively overcome the harm that it is brought,
So antioxidation is classified as main study hotspot by health food enterprise, be also simultaneously market most important feature demand it
One.
So far declare on market that the life enhancement wine product with anti-oxidation function is still very few, empty for filling up this
Lack, my company combines numerous colleges and universities experts, scholar is planted in this cause, from selection to extraction process etc., each step is all meticulous
Design, checking, take infinite pains, and finally successfully research and develop a safety, excellent texture, the clear and definite anti-oxidation function of collecting in one
The health promoting wine of body.
By patent documentation and non-patent literature retrieval, and market survey, not yet find have Radix Cynanchi Auriculati (i.e. strand ear
Leaf cynanchum auriculatum Royle ex Wight), Lepidinm meyenii Walp, obtain the reported in literature of health promoting wine after Arillus Longan mixing.
Content of the invention
Technical problem solved by the invention is to provide a kind of health promoting wine with anti-oxidation efficacy, health promoting wine profit of the present invention
With Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan advantage, based on Radix Cynanchi Auriculati, add Lepidinm meyenii Walp, Arillus Longan and make.Antioxidation of the present invention is protected
Strong wine, raw material by weight ratio: 5～10 parts of Radix Cynanchi Auriculati, 1～2 part of Lepidinm meyenii Walp, 0.1～0.5 part of Arillus Longan, Chinese liquor 87.5～93.9
Part.
Anti-oxidation health wine of the present invention, including the following raw material medicine and Chinese liquor:
Crude drug, counts: 5～10 parts of Radix Cynanchi Auriculati, 1～2 part of Lepidinm meyenii Walp, 0.1～0.5 part of Arillus Longan by weight ratio；
Appropriate Chinese liquor.
Further preferably, anti-oxidation health wine of the present invention, the crude drug including following weight proportion and Chinese liquor:
Crude drug, 5～10 parts of Radix Cynanchi Auriculati, 1～2 part of Lepidinm meyenii Walp, 0.1～0.5 part of Arillus Longan；
87.5～93.9 parts of Chinese liquor.
Wherein, the Chinese liquor of employing is aromatic Chinese spirit.The alcoholic strength of anti-oxidation health wine of the present invention is 38～42%vol.
The preparation method of anti-oxidation health wine of the present invention, step is as follows:
(1) weigh crude drug；Count by weight ratio: 5～10 parts of Radix Cynanchi Auriculati, 1～2 part of Lepidinm meyenii Walp, 0.1～0.5 part of Arillus Longan；
(2) pulverize Radix Cynanchi Auriculati, Lepidinm meyenii Walp, cross 10-50 mesh sieve；
(3) take Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan, plus 10～20 times amount water soak extraction, filter to obtain compound material extracting solution；
(4) step (3) gained compound material extracting solution adds Chinese liquor adjustment alcoholic strength to setting.
Wherein, the preparation method of health promoting wine of the present invention at least meets following any one:
The described soak extraction of step (3) extracts for normal pressure；
The described Chinese liquor alcoholic strength of step (3) is 40～60%vol；
The soak extraction temperature of the described soak extraction of step (3) is 60～80 DEG C；
During step (3) described soak extraction, feed liquid mass ratio 1:20～1:10；
The soak extraction number of times of the described soak extraction of step (3) is 2-4 time (preferably 2 times)；
Each extraction time 2-4h of the described soak extraction of step (3)；
Step (4) described adjustment alcoholic strength is to 38～42%vol.
Specifically, the crude drug of health promoting wine of the present invention is weighed by following weight proportions: 5～10 parts of Radix Cynanchi Auriculati, Lepidinm meyenii Walp 1～2
Part, 0.1～0.5 part of Arillus Longan, preparation method comprises the steps:
1. Radix Cynanchi Auriculati, Lepidinm meyenii Walp are pulverized, cross 10-50 mesh sieve；
2. take Radix Cynanchi Auriculati powder, pueraria root powder and Arillus Longan, mix homogeneously, add the purified water of 10～20 times amount, 60～80
DEG C when normal pressure extraction, extraction can reasonable extensions, such as extraction 2-4 time, preferably 2 times, extract 2～4h every time, filter after extraction, conjunction
And filtrate, it is concentrated to give Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan extract；
In order to coordinate product difference alcoholic strength demand, add Chinese liquor adjustment alcoholic strength.As by Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan
Extracting solution is added in Chinese liquor, and adjustment alcoholic strength is 38～42%vol, and is settled to 1000l, filters, fill, obtain 38～
The anti-oxidation health wine of 42%vol.
The present invention adopts Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan as follows the reason being crude drug:
Radix Cynanchi Auriculati picks up from unique " township of the Radix Polygoni Multiflori " the Jiangsu Province Binhai County of China, the maturation of trailing plants section platymiscium cynanchum auriculatum Royle
Dry tuber；Selection is genuine, pure.Not only contain the general nutrient components such as crude protein, crude fat, free sugar and starch, be still rich in
Multivitamin, aminoacid, phospholipid, c21 steroidal aglycon, inorganic salt and trace element needed by human.It is rich in Radix Cynanchi Auriculati
The antioxidant contents such as c21 steroidal aglycon, vitamin e, c, b, trace selenium, Radix Cynanchi Auriculati diketone a, have removing free radical, suppressed
The formation of lipid oxide, reduces the content of lipid peroxide in the tissue such as serum, brain, liver, heart, protects body from free radical
Infringement, prevents the formation of the athero- speckle of tremulous pulse, protection neural cell resistance peroxide infringement, reduces metabolite malonaldehyde
Reduce the impact to liver for the lipid peroxidation, make myocardial cell from or damaged by free radical less, myocardium complete of protection
Just it has been described as, since whole structure and normal physiological function, extremely Gu, the good merchantable brand of health care, life lengthening of preserving youthful looks, enjoy everybody to like.
Lepidinm meyenii Walp contains rich in protein, aminoacid, reducing sugar, mineral, unsaturated fatty acid, wherein linolenic acid and Asia
Oleic acid is extremely advantageous to health.Reducing sugar-maca polysaccharide being rich in MAKA dry powder etc. is to removing free radical, suppression peroxide
Changing has clear and definite curative effect.In addition to conventional nutrients, metabolism also forms the distinctive work(with biological activity
Effect composition, such as alkaloid, macamide and maca ene series matter, isothiocyanate, glucosinolate, flavonol etc..High nutrition valency
Value, rational trophic structure and multiple secondary metabolite with biological activity make Lepidinm meyenii Walp possess plurality of health care functions.Pass
Can be used on system strengthening energy, improve fertility, improve sexual function, treat climacteric syndrome, rheumatism, depression, anemia,
In addition also have anticancer and effect of anti-leukemia.Modern medicine study shows, Lepidinm meyenii Walp has antioxidation, enhancing immunity, regulation
Multiple unique effects such as endocrine.
Arillus Longan is the aril of sapindaceous plant Arillus Longan, sweet in the mouth, warm in nature, containing glucose, protein, fat, dimension life
Plain b1, b2, p, c etc..Growth, health invigorating can be promoted, improve the hypoxic tolerance time；Integration of edible and medicinal herbs, takes for a long time and has no side effect,
Safe and reliable.
The beneficial effect of anti-oxidation health wine of the present invention:
1st, the present invention has played the advantage of food new raw material Radix Cynanchi Auriculati, Lepidinm meyenii Walp and Chinese crude drug Arillus Longan, has antioxidation etc.
Effect.
2nd, the present invention with natural product as raw material, pure in mouth feel, without food additive, no side effectses.
3rd, simple production process of the present invention, Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan mixing water extraction are fully extracted effect therein and are become
Point: crude polysaccharides.Needed using the extracting mode being suitable for it is ensured that its higher extraction ratio according to composition.
4th, product produce, storage etc. during functional component such as: c21 steroidal aglycon, Radix Cynanchi Auriculati diketone a, crude polysaccharides
Deng antioxidant, good stability, effect is notable, has larger market development potential.
Brief description
The impact that Fig. 1 raw material granularity extracts to total saponins, total alkaloidss.
The impact that Fig. 2 Chinese liquor number of degrees extract to total saponins, total alkaloidss.
The impact that Fig. 3 extraction time extracts to total saponins, total alkaloidss.
The impact that Fig. 4 extracting times extract to total saponins, total alkaloidss.
Specific embodiment
The following is the preparation method screening test of anti-oxidation health wine of the present invention.
First, Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan extract experiment of single factor
(1) impact that raw material granularity extracts to total saponins, total alkaloidss
Radix Cynanchi Auriculati, Lepidinm meyenii Walp are respectively crushed into following different-grain diameter, it is respectively 5 mesh, 10 mesh, 30 mesh, 50 mesh, 70 mesh.
Accurately weigh Radix Cynanchi Auriculati powder 30g, pueraria root powder 6g, the Arillus Longan 2g of different-grain diameter, with the Radix Cynanchi Auriculati powder of particle diameter, pueraria root powder and Arillus Longan
Meat mix homogeneously, is 1:10 by solid-liquid ratio, with the extraction of 60%vol Chinese liquor, collects lixiviating solution 300ml.Detection total saponins, always biology
The content of alkali, calculates extraction ratio, and result is shown in Fig. 1.
As shown in Figure 1, in certain limit class, reduce with raw material pulverizing granule, corresponding specific surface area increases, with solvent
Contact surface increase, beneficial to functional component dissolution substantially find total saponins, the extraction ratio of total alkaloidss gradually rises.Then raw material
Pulverized particles functional component extraction ratio after reducing increases inconspicuous, simultaneously with the reduction further of pulverized particles, to corresponding
Equipment requirements and energy consumption can improve further, now, in 10-50 mesh, functional component extraction rate reached is to higher for raw material granularity
Level.For this reason, raw material granularity is chosen as 10-50 mesh during extraction.
(2) impact that the Chinese liquor number of degrees extract to total saponins, total alkaloidss
Accurately weigh Radix Cynanchi Auriculati powder 30g, pueraria root powder 6g, the Arillus Longan 2g being crushed to 20 mesh, mix homogeneously, weigh 5 parts, point
20%vol, 30%vol, 40%vol, 50%vol, 60%vol Chinese liquor Yong not extract, be that 1:10 extracts by solid-liquid ratio, collect leaching
Extract 300ml.Detection total saponins, the content of total alkaloidss, calculate extraction ratio, and result is shown in Fig. 2.
As shown in Figure 2, with the rising of the Chinese liquor number of degrees, total saponins, total alkaloidss all assume first rising and then slightly lower
Process.Total saponins, total alkaloidss extraction ratio, when the Chinese liquor number of degrees are 38%vol, reach maximum, it is respectively 48.37%；
Extraction ratio is being 45.03% in the Chinese liquor number of degrees；Therefore select 30%vol, 40%vol, 50%vol as the extraction compared with orthogonal experiment
Number of times optimizes.
(3) impact that extraction time extracts to total saponins, total alkaloidss
Accurately weigh Radix Cynanchi Auriculati powder 30g, pueraria root powder 6g, the Arillus Longan 2g being crushed to 20 mesh, weigh 5 parts, when extracting every time
Between carry out the extraction of crude polysaccharides respectively under 1h, 2h, 3h, 4h, 5h time, be 1:10 by solid-liquid ratio, with the leaching of 60%vol Chinese liquor
Carry, collect lixiviating solution 300ml.Detection total saponins, the content of total alkaloidss, calculate extraction ratio, and result is shown in Fig. 3.
From the figure 3, it may be seen that increasing with extraction time, total saponins, total alkaloidss extraction ratio assume first rising and then tend to flat
Slow；Extraction ratio after 2 hours, selects 2h with the increase change of extraction time is inconspicuous it is considered to production economy timeliness, 3h, 4h make
It is the extraction time optimization compared with orthogonal experiment.
(4) impact that extracting times extract to total saponins, total alkaloidss
Accurately weigh Radix Cynanchi Auriculati powder 30g, pueraria root powder 6g, the Arillus Longan 2g being crushed to 20 mesh, mix homogeneously, weigh 5 parts,
Be 1:10 by solid-liquid ratio, with 60%vol Chinese liquor extraction, respectively collect lixiviating solution 300ml, 550ml, 870ml ml, 1150ml,
1450ml (extracting liquid volume is followed successively by 10,20,30,40,50 times of material).Detection total saponins, the content of total alkaloidss, calculate
Extraction ratio, result is shown in Fig. 4.
As shown in Figure 4, increase with extraction time, total saponins, total alkaloidss extraction ratio present first to raise and progressively reach afterwards
Stable.Excessive extraction time is unfavorable for industrialized production.Therefore selective extraction 1 time, 2 times, 3 times as carrying compared with orthogonal experiment
Take number of times optimization.
2nd, Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan extract orthogonal experiment
On the basis of single factor experiment, determine using the Chinese liquor number of degrees, extraction time, extracting times as orthogonal experiment optimization
Factor.3 factors respectively select three preferable levels, using l9 (34) orthogonal table, carry out orthogonal experiment.Three preferable levels are divided
Wei the Chinese liquor number of degrees: 30%vol, 40%vol, 50%vol；Extraction time: 2h, 3h, 4h, extracting times: 1 time, 2 times, 3 times,
The gauge outfit design of orthogonal experiment is shown in Table 1, and Orthogonal experiment results are as shown in table 2.
The gauge outfit design of table 1 orthogonal experiment
Table 2 total saponins, total alkaloidss percolation l9 (34) Orthogonal experiment results
The analysis that raw material extracts total saponins orthogonal test understands, this 3 factors affect the power of total saponins extraction ratio successively
For: extracting times (c) ＞ extraction time (b) the ＞ Chinese liquor number of degrees (a)；Optimal conditionss are a2b2c2Or a2b3c3, the carrying of its total saponins
Take rate difference 81.8%, 84%.It is proposed that a on the premise of considering the correlative factors such as big production operation, economic timeliness2b2c2
Scheme is i.e.: Chinese liquor number of degrees 40%vol, extraction time 2 hours, extracting times 2 times.
The analysis that raw material extracts total alkaloidss orthogonal test understands, this 3 factors affect the power of total alkaloidss extraction ratio
It is followed successively by: extracting times (c) the ＞ Chinese liquor number of degrees (a) ＞ extraction time (b)；Optimal conditionss are a2b2c2Or a2b3c3, it is always biological
The extraction ratio of alkali is 78.1%, 80.8% respectively；Consider big production operation and economic timeliness and the shadow that total saponins are extracted
Ring suggestion a2b2c2Scheme, i.e. Chinese liquor number of degrees 40%vol, extraction time 2 hours, extracting times 2 times, test optimum side for this
Case.
Further describe the present invention with reference to embodiment, the present invention is not limited only to described embodiment.
Embodiment one
1. Radix Cynanchi Auriculati, Lepidinm meyenii Walp are pulverized, cross 20 mesh sieves；
2. weigh Radix Cynanchi Auriculati powder 5kg, pueraria root powder 1kg and Arillus Longan 0.1kg, mix homogeneously, add the purified water of 10 times amount,
When 60 DEG C normal pressure extraction, extraction twice, every time extract 2h, after extraction filter, merging filtrate, be concentrated to give Radix Cynanchi Auriculati, pueraria root powder,
Arillus Longan extract；
3. Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan extract are added in Chinese liquor, adjustment alcoholic strength is 38%vol, and is settled to
1000l, filters, fill, obtains the anti-oxidation health wine of 38%vol.
Embodiment two
1. Radix Cynanchi Auriculati, Lepidinm meyenii Walp are pulverized, cross 10 mesh sieves；
2. weigh Radix Cynanchi Auriculati powder 8kg, pueraria root powder 1.5kg and Arillus Longan 0.2kg, mix homogeneously, add the purification of 15 times amount
Water, the normal pressure extraction when 70 DEG C, extraction twice, extracts 3h every time, filters, merging filtrate, be concentrated to give Radix Cynanchi Auriculati, Lepidinm meyenii Walp after extraction
Powder, Arillus Longan extract；
3. Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan extract are added in Chinese liquor, adjustment alcoholic strength is 40%vol, and is settled to
1000l, filters, fill, obtains the anti-oxidation health wine of 40%vol.
Embodiment three
1. Radix Cynanchi Auriculati, Lepidinm meyenii Walp are pulverized, cross 30 mesh sieves；
2. weigh Radix Cynanchi Auriculati powder 10kg, pueraria root powder 2kg and Arillus Longan 0.4kg, mix homogeneously, add the purification of 15 times amount
Water, the normal pressure extraction when 70 DEG C, extraction twice, extracts 4h every time, filters, merging filtrate, be concentrated to give Radix Cynanchi Auriculati, Lepidinm meyenii Walp after extraction
Powder, Arillus Longan extract；
3. Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan extract are added in Chinese liquor, adjustment alcoholic strength is 42%vol, and is settled to
1000l, filters, fill, obtains the anti-oxidation health wine of 42%vol.
The present invention is health promoting wine for oral administration, and the amount of drinking is 100ml daily, and long-term drink is i.e. up to good result.
To sum up, by Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan mixing water extraction, its raw material is according to functional component for preparation method of the present invention
Matter, selects the extracting mode being suitable for, while ensure that functional component is stablized, obtains higher extraction ratio again.The present invention
Prepared health promoting wine has played the advantage of food new raw material Radix Cynanchi Auriculati, Lepidinm meyenii Walp and Chinese crude drug Arillus Longan, the effects such as have antioxidation.
Above example is part specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, and appoints
What those skilled in the art the invention discloses technical scope in, the change or replacement that can readily occur in, it all should belong to
In the middle of the claims of the present invention.
Claims (8)
1. anti-oxidation health wine it is characterised in that: include the following raw material medicine and Chinese liquor:
Crude drug, counts: 5～10 parts of Radix Cynanchi Auriculati, 1～2 part of Lepidinm meyenii Walp, 0.1～0.5 part of Arillus Longan by weight ratio；
Appropriate Chinese liquor.
2. anti-oxidation health wine according to claim 1 it is characterised in that: include the crude drug of following weight proportion and white
Wine:
Crude drug, 5～10 parts of Radix Cynanchi Auriculati, 1～2 part of Lepidinm meyenii Walp, 0.1～0.5 part of Arillus Longan；
87.5～93.9 parts of Chinese liquor.
3. anti-oxidation health wine according to claim 1 and 2 it is characterised in that: described Chinese liquor be aromatic Chinese spirit.
4. the anti-oxidation health wine according to any one of claim 1-3 it is characterised in that: alcoholic strength be 38～42%vol.
5. the anti-oxidation health wine described in claim 1 preparation method it is characterised in that: step is as follows:
(1) weigh crude drug；Count by weight ratio: 5～10 parts of Radix Cynanchi Auriculati, 1～2 part of Lepidinm meyenii Walp, 0.1～0.5 part of Arillus Longan；
(2) pulverize Radix Cynanchi Auriculati, Lepidinm meyenii Walp, cross 10-50 mesh sieve；
(3) take Radix Cynanchi Auriculati, Lepidinm meyenii Walp, Arillus Longan, plus 10～20 times amount water soak extraction, filter to obtain compound material extracting solution；
(4) step (3) gained compound material extracting solution adds Chinese liquor adjustment alcoholic strength to setting.
6. anti-oxidation health wine according to claim 5 preparation method it is characterised in that: at least meet following any one
:
The described soak extraction of step (3) extracts for normal pressure；
The soak extraction temperature of the described soak extraction of step (3) is 60～80 DEG C；
The soak extraction number of times of the described soak extraction of step (3) is 2-4 time；
Each extraction time 2-4h of the described soak extraction of step (3).
7. anti-oxidation health wine according to claim 5 preparation method it is characterised in that: the described immersion of step (3) carries
The soak extraction number of times taking is 2 times.
8. anti-oxidation health wine according to claim 5 preparation method it is characterised in that: the described adjustment wine of step (4)
Precision is to 38～42%vol.
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| CN102787062A (en) * | 2012-09-08 | 2012-11-21 | 通化万嘉生物科技有限公司 | Okra and maca wine and preparation method of okra and maca wine |
| CN103571725A (en) * | 2013-11-25 | 2014-02-12 | 楚雄三平裕康商贸有限公司 | Maca health-care wine and manufacturing method thereof |
| CN104673597A (en) * | 2013-11-27 | 2015-06-03 | 尹江涛 | Multifunctional health preserving liquor and production method thereof |
| CN104293620A (en) * | 2014-10-10 | 2015-01-21 | 钱莉秋 | Maca health wine and preparation method thereof |
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Application publication date: 20170125 |