CN106349724A - Method for producing low-viscosity rubber asphalt from cottonseed oil, product produced thereby and paving of thin-layer pavement - Google Patents

Method for producing low-viscosity rubber asphalt from cottonseed oil, product produced thereby and paving of thin-layer pavement Download PDF

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Publication number
CN106349724A
CN106349724A CN201610772621.0A CN201610772621A CN106349724A CN 106349724 A CN106349724 A CN 106349724A CN 201610772621 A CN201610772621 A CN 201610772621A CN 106349724 A CN106349724 A CN 106349724A
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China
Prior art keywords
low
asphalt
oleum gossypii
gossypii semen
product
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CN201610772621.0A
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Inventor
李廷刚
李峰
杜滨
赵晓涛
毛彪
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Beijing Zhongtian Industry Technology Co Ltd
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Beijing Zhongtian Industry Technology Co Ltd
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Priority to CN201610772621.0A priority Critical patent/CN106349724A/en
Publication of CN106349724A publication Critical patent/CN106349724A/en
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L95/00Compositions of bituminous materials, e.g. asphalt, tar, pitch
    • EFIXED CONSTRUCTIONS
    • E01CONSTRUCTION OF ROADS, RAILWAYS, OR BRIDGES
    • E01CCONSTRUCTION OF, OR SURFACES FOR, ROADS, SPORTS GROUNDS, OR THE LIKE; MACHINES OR AUXILIARY TOOLS FOR CONSTRUCTION OR REPAIR
    • E01C7/00Coherent pavings made in situ
    • E01C7/08Coherent pavings made in situ made of road-metal and binders
    • E01C7/35Toppings or surface dressings; Methods of mixing, impregnating, or spreading them
    • E01C7/358Toppings or surface dressings; Methods of mixing, impregnating, or spreading them with a combination of two or more binders according to groups E01C7/351 - E01C7/356
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Architecture (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Road Paving Structures (AREA)

Abstract

The invention discloses a method for producing low-viscosity rubber asphalt from cottonseed oil, a product produced thereby and paving of a thin-layer pavement. The product produced by the method comprises the following components in percent by weight: 50-60% of petroleum asphalt, 10-20% of waste tire rubber powder and 20-30% of the cottonseed oil. The method provided by the method is simple in process and easy to implement; through adoption of the cottonseed oil with very low pollution and relatively low price and through formula optimization, by a scientific production process, a cottonseed oil-containing low-viscosity rubber asphalt product with good constructability and workability and low pollution can be produced; the cottonseed oil-containing low-viscosity rubber asphalt product can be used as an ultrathin wearing layer during preventive maintenance of an asphalt pavement, and has the advantages of low cost, good constructability and workability, no soot pollution, no odor and the like; the constructed pavement is high in low-temperature anti-cracking capability, good in durability and good in overall performance, so that petroleum resources are saved, the environment is protected and the cost is reduced; therefore, wide popularization and application is beneficial.

Description

Produce low-viscosity rubber asphalt method and its product, making thin layer using Oleum Gossypii semen Road surface
Technical field
The invention belongs to Colophonium Lamina technical field is and in particular to a kind of produce low viscosity rubber drip using Oleum Gossypii semen Blue or green method and its product, making Lamina.
Background technology
Oleum Gossypii semen is the oil with cotton seed as raw material production, is divided into squeezing Oleum Gossypii semen, leaches Oleum Gossypii semen, transgenic cotton seed Oil, Semen Gossypii crude oil, finished product Oleum Gossypii semen are several.The more other oil of color is dark red, after refine can human consumption, containing needed by human in a large number Fatty acid, the most preferably with Animal fat mixed edible.But eating rough Oleum Gossypii semen can cause spermatogenic cell to damage, and lead to azoospermia not Educate, therefore the market price of Oleum Gossypii semen is always below other edible vegetable oils, suitable with the price of asphalt.Oleum Gossypii semen has Good greasy property, therefore can partly be added in lubricating oil and use.
Rubber asphalt is a kind of Load materials obtaining wide popularization and application in recent years at home, and it is to grind junked tire A kind of modified asphalt material that thin rubber powder and common petroleum Colophonium stir under the high temperature conditions, has high temperature performance The good, advantage of good endurance.But rubber asphalt is both needed to carry out under the high temperature conditions during production and construction usage, construction is difficult Degree is big, and volatility flue dust is gentle highly seasoned.Carry out both at home and abroad a lot of rubber asphalts that reduce and implement temperature and smoke pollution Research, achieves certain achievement, but is on the one hand that the temperature reducing is limited, typically can only reduce 20-30 DEG C, on the other hand some Although effective by adding thinner, thinner causes extra escaping gas pollution.
Content of the invention
For above-mentioned deficiency, one of the object of the invention is, provides a kind of technique simple it is easy to construct, contaminative pole Low and relative low price, the strong utilization Oleum Gossypii semen of low temperature performance well, anti-cracking ability produces low-viscosity rubber asphalt method;
The two of the object of the invention are, provide a kind of above-mentioned utilization Oleum Gossypii semen of enforcement to produce low-viscosity rubber asphalt method system The product obtaining.
The two of the object of the invention are, provide a kind of above-mentioned utilization Oleum Gossypii semen to produce low-viscosity rubber asphalt method system The product obtaining carrys out making Lamina.
For achieving the above object, technical scheme provided by the present invention is:
One kind produces low-viscosity rubber asphalt method using Oleum Gossypii semen, and it comprises the following steps:
(1) preparing material: each component of raw material and percentage by weight are as follows:
Asphalt 50~60%,
Waste-tyre rubber-powder 10~20%,
Oleum Gossypii semen 20~30%;
(2) room temperature mixing: first waste-tyre rubber-powder is mixed at normal temperatures with Oleum Gossypii semen, obtain mixture;
(3) heating mixing: when asphalt is heated to 170~190 DEG C, be subsequently adding mixture, after growth to be mixed Cool to 100~120 DEG C, make to obtain Oleum Gossypii semen low-viscosity rubber asphalt product.
As a modification of the present invention, described step (3) specifically includes following steps:
(3.1) asphalt is heated to 170~190 DEG C, stirs when adding mixture, the speed setting of agitator is extremely Few 900 revs/min, continue heated and stirred,;
(3.2) continue 170~190 DEG C of keeping temperature, to be mixed develop 20~60 minutes after, subsequent natural cooling, work as temperature Degree is reduced to 100~120 DEG C, makes to obtain Oleum Gossypii semen low-viscosity rubber asphalt product.
A kind of implement above-mentioned utilization Oleum Gossypii semen and produce the product that low-viscosity rubber asphalt method is obtained, its each component and weight Amount percentage ratio is as follows:
Asphalt 50~60%,
Waste-tyre rubber-powder 10~20%,
Oleum Gossypii semen 20~30%.
A kind of above-mentioned utilization Oleum Gossypii semen produces the prepared product of low-viscosity rubber asphalt method come making Lamina, Oleum Gossypii semen low-viscosity rubber asphalt product is mixed with having the mineral aggregate phase that a deciding grade and level joins, obtains asphalt, wherein Colophonium Compound mix drop temperature is 95~105 DEG C, forms Lamina after bituminous mixture laying is rolled.
As a modification of the present invention, the thickness of described Lamina is 1~2.5cm.
The invention has the benefit that the technique of the method for present invention offer is simple, it is easy to accomplish, extremely low using contaminative And the Oleum Gossypii semen of relative low price, by optimization of C/C composites and adopt science preparation technology, can prepare have good application property, Workability and oligosaprobic Oleum Gossypii semen low-viscosity rubber asphalt product, simultaneously take account of its low temperature performance well, anti-cracking ability by force, But the weaker feature of high-temperature behavior, uses it for making Lamina in bituminous pavement preventive maintenance, the thickness after decking and rolling Degree controls between 1~2.5cm, can use as ultra-thin wearing layer during bituminous pavement preventive maintenance, has low cost, apply Work workability is good, and the advantages of smoke dust pollution, free from extraneous odour, the road surface low temperature anti-cracking ability of making is strong, and good endurance is comprehensive Can be good, thus saving petroleum resources, environmental protection, reduces cost, beneficial to wide popularization and application simultaneously.
With reference to embodiment, the invention will be further described.
Specific embodiment
Embodiment 1: one kind that the present embodiment provides utilizes Oleum Gossypii semen to produce low-viscosity rubber asphalt method, and it includes following Step:
(1) preparing material: each component of raw material and percentage by weight are as follows: asphalt 60%, waste-tyre rubber-powder 20%, Oleum Gossypii semen 20%;
(2) room temperature mixing: first waste-tyre rubber-powder is mixed at normal temperatures with Oleum Gossypii semen, obtain mixture;
(3) heating mixing: when asphalt is heated to 170~190 DEG C, be subsequently adding mixture, after growth to be mixed Cool to 100~120 DEG C, make to obtain Oleum Gossypii semen low-viscosity rubber asphalt product.Specifically, described step (3) specifically include with Lower step: asphalt is heated to 170~190 DEG C by (3.1), stirs when adding mixture, the speed setting of agitator is extremely Few 900 revs/min, continue heated and stirred,;(3.2) 170~190 DEG C of keeping temperature, growth to be mixed 20~60 minutes are continued Afterwards, subsequent natural cooling, when temperature is reduced to 100~120 DEG C, makes to obtain Oleum Gossypii semen low-viscosity rubber asphalt product.
A kind of implement above-mentioned utilization Oleum Gossypii semen and produce the product that low-viscosity rubber asphalt method is obtained, its each component and weight Amount percentage ratio is as follows: asphalt 60%, waste-tyre rubber-powder 20%, Oleum Gossypii semen 20%.
A kind of above-mentioned utilization Oleum Gossypii semen produces the prepared product of low-viscosity rubber asphalt method come making Lamina, Oleum Gossypii semen low-viscosity rubber asphalt product is mixed with having the mineral aggregate phase that a deciding grade and level joins, obtains asphalt.Concrete level is joined See table.
Ac-8 mineral aggregate formate gradation composition
Wherein asphalt mixture mixing drop temperature is 95~105 DEG C, forms thin layer after bituminous mixture laying is rolled Road surface.Preferably, the thickness of described Lamina is 1~2.5cm.
Produce the Oleum Gossypii semen low-viscosity rubber asphalt product that low-viscosity rubber asphalt method is obtained through above-mentioned utilization Oleum Gossypii semen Index is:
Embodiment 2, one kind that the present embodiment provides utilizes Oleum Gossypii semen to produce low-viscosity rubber asphalt method and its product, paving Build Lamina, it is substantially the same manner as Example 1, its difference is, each component of raw material and its percentage by weight are as follows: Asphalt 50%, waste-tyre rubber-powder 20%, Oleum Gossypii semen 30%.Produce low-viscosity rubber asphalt side through above-mentioned utilization Oleum Gossypii semen The Oleum Gossypii semen low-viscosity rubber asphalt product index that method is obtained is:
Embodiment 3, one kind that the present embodiment provides utilizes Oleum Gossypii semen to produce low-viscosity rubber asphalt method and its product, paving Build Lamina, it is substantially the same manner as Example 1, its difference is, each component of raw material and its percentage by weight are as follows: Asphalt 54%, waste-tyre rubber-powder 16%, Oleum Gossypii semen 30%.Produce low-viscosity rubber asphalt side through above-mentioned utilization Oleum Gossypii semen The Oleum Gossypii semen low-viscosity rubber asphalt product index that method is obtained is:
Embodiment 4, one kind that the present embodiment provides utilizes Oleum Gossypii semen to produce low-viscosity rubber asphalt method and its product, paving Build Lamina, it is substantially the same manner as Example 1, its difference is, each component of raw material and its percentage by weight are as follows: Asphalt 60%, waste-tyre rubber-powder 10%, Oleum Gossypii semen 30%.
Embodiment 5, one kind that the present embodiment provides utilizes Oleum Gossypii semen to produce low-viscosity rubber asphalt method and its product, paving Build Lamina, it is substantially the same manner as Example 1, its difference is, each component of raw material and its percentage by weight are as follows: Asphalt 56%, waste-tyre rubber-powder 18%, Oleum Gossypii semen 26%.
Embodiment 5, one kind that the present embodiment provides utilizes Oleum Gossypii semen to produce low-viscosity rubber asphalt method and its product, paving Build Lamina, it is substantially the same manner as Example 1, its difference is, each component of raw material and its percentage by weight are as follows: Asphalt 56%, waste-tyre rubber-powder 18%, Oleum Gossypii semen 26%.
Embodiment 6, one kind that the present embodiment provides utilizes Oleum Gossypii semen to produce low-viscosity rubber asphalt method and its product, paving Build Lamina, it is substantially the same manner as Example 1, its difference is, each component of raw material and its percentage by weight are as follows: Asphalt 58%, waste-tyre rubber-powder 17%, Oleum Gossypii semen 25%.
The softening point of the Oleum Gossypii semen low-viscosity rubber asphalt product that the present invention is obtained is lower slightly, but ductility is greatly improved, viscosity It is greatly reduced.Show that it has more preferable cryogenic property and construction workability, and high-temperature behavior slightly reduces.Specifically, this The performance parameter of bright Oleum Gossypii semen low-viscosity rubber asphalt product is as follows:
The present invention adopts that contaminative is extremely low and the Oleum Gossypii semen of relative low price, by optimization of C/C composites with using science preparation Technique, can prepare and have good application property, workability and oligosaprobic Oleum Gossypii semen low-viscosity rubber asphalt product, by Oleum Gossypii semen Low-viscosity rubber asphalt product mixes with having the mineral aggregate phase that a deciding grade and level joins, and obtains asphalt, and mineral aggregate temperature control is 100 ~110 DEG C, 100 ± 5 DEG C of asphalt mixture mixing drop temperature.This asphalt is paved using conventional laying equipment, paves THICKNESS CONTROL after rolling, between 1~2.5cm, can use as ultra-thin wearing layer during bituminous pavement preventive maintenance, tool Have low cost, construction workability is good, smoke dust pollution, free from extraneous odour the advantages of.The road surface low temperature anti-cracking ability of making is strong, durable Property is good.In addition, in other embodiment when carrying out each component ratio selection, can within the above range according to actual needs Select, to obtain the product of different specific performance features.
Above-described embodiment is only the preferable embodiment of the present invention, and the present invention can not enumerate out whole embodiment party Formula, the technical scheme of one of all employing above-described embodiments, or the equivalent variations done according to above-described embodiment, all protect in the present invention In the range of shield.
The announcement of book and teaching according to the above description, those skilled in the art in the invention can also be to above-mentioned embodiment party Formula is changed and is changed.Therefore, the invention is not limited in specific embodiment disclosed and described above, to the present invention's In the scope of the claims that some modifications and changes should also be as fall into the present invention.Although additionally, using in this specification Some specific terms, but these terms are merely for convenience of description, constitute any restriction to the present invention, using and its Other methods and product etc. obtained from same or similar method and component, all in the scope of the present invention.

Claims (5)

1. one kind produces low-viscosity rubber asphalt method it is characterised in that it comprises the following steps using Oleum Gossypii semen:
(1) preparing material: each component of raw material and percentage by weight are as follows:
Asphalt 50~60%,
Waste-tyre rubber-powder 10~20%,
Oleum Gossypii semen 20~30%;
(2) room temperature mixing: first waste-tyre rubber-powder is mixed at normal temperatures with Oleum Gossypii semen, obtain mixture;
(3) heating mixing: when asphalt is heated to 170~190 DEG C, be subsequently adding mixture, lower the temperature after growth to be mixed To 100~120 DEG C, make to obtain Oleum Gossypii semen low-viscosity rubber asphalt product.
2. utilization Oleum Gossypii semen according to claim 1 produces low-viscosity rubber asphalt method it is characterised in that described step (3) following steps are specifically included:
(3.1) asphalt is heated to 170~190 DEG C, stirs when adding mixture, the speed setting of agitator is at least 900 revs/min, continue heated and stirred,;
(3.2) continue 170~190 DEG C of keeping temperature, to be mixed develop 20~60 minutes after, subsequent natural cooling, when temperature fall Low to 100~120 DEG C, make to obtain Oleum Gossypii semen low-viscosity rubber asphalt product.
3. a kind of product implementing to be obtained using Oleum Gossypii semen production low-viscosity rubber asphalt method described in claim 1 or 2, it is special Levy and be, its each component and percentage by weight are as follows:
Asphalt 50~60%,
Waste-tyre rubber-powder 10~20%,
Oleum Gossypii semen 20~30%.
4. a kind of product being obtained with the utilization Oleum Gossypii semen production low-viscosity rubber asphalt method described in claim 3 is thin come making Layer road surface, it is characterised in that mix Oleum Gossypii semen low-viscosity rubber asphalt product with having the mineral aggregate phase that a deciding grade and level joins, obtains and drips Blue or green compound, wherein asphalt mixture mixing drop temperature are 95~105 DEG C, form thin layer after bituminous mixture laying is rolled Road surface.
5. the product being obtained using Oleum Gossypii semen production low-viscosity rubber asphalt method according to claim 4 is come making thin layer Road surface is it is characterised in that the thickness of described Lamina is 1~2.5cm.
CN201610772621.0A 2016-08-30 2016-08-30 Method for producing low-viscosity rubber asphalt from cottonseed oil, product produced thereby and paving of thin-layer pavement Pending CN106349724A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107880573A (en) * 2017-11-23 2018-04-06 新疆天之泽化工有限公司 A kind of pitch ready-mixed oil and its accord method
CN109161212A (en) * 2018-08-28 2019-01-08 重庆坤星源新材料科技有限公司 The method for preparing soft pitch modifying agent and modified soft pitch

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4085078A (en) * 1976-12-27 1978-04-18 Mcdonald Charles H Low viscosity asphalt-rubber paving material
CN1733843A (en) * 2004-08-12 2006-02-15 徐延庆 Rubber powder modified asphalt manufacturing technique and attle layer-sealing technique
CN101735628A (en) * 2010-01-19 2010-06-16 陕西长大华础工程材料科技股份有限公司 Waste tire rubber powder modified asphalt and preparation method thereof
CN103497521A (en) * 2013-09-18 2014-01-08 交通运输部公路科学研究所 Vegetable oil modified asphalt composite and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4085078A (en) * 1976-12-27 1978-04-18 Mcdonald Charles H Low viscosity asphalt-rubber paving material
CN1733843A (en) * 2004-08-12 2006-02-15 徐延庆 Rubber powder modified asphalt manufacturing technique and attle layer-sealing technique
CN101735628A (en) * 2010-01-19 2010-06-16 陕西长大华础工程材料科技股份有限公司 Waste tire rubber powder modified asphalt and preparation method thereof
CN103497521A (en) * 2013-09-18 2014-01-08 交通运输部公路科学研究所 Vegetable oil modified asphalt composite and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
陈开勋等: "《精细化工产品化学及应用(第1版)》", 30 September 1995, 西北大学出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107880573A (en) * 2017-11-23 2018-04-06 新疆天之泽化工有限公司 A kind of pitch ready-mixed oil and its accord method
CN109161212A (en) * 2018-08-28 2019-01-08 重庆坤星源新材料科技有限公司 The method for preparing soft pitch modifying agent and modified soft pitch

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