CN106316370A - Novel jade ceramic material and preparation method and application of novel jade ceramic - Google Patents
Novel jade ceramic material and preparation method and application of novel jade ceramic Download PDFInfo
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- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3284—Zinc oxides, zincates, cadmium oxides, cadmiates, mercury oxides, mercurates or oxide forming salts thereof
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- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9646—Optical properties
Abstract
The invention discloses a novel jade ceramic material and a preparation method and application of novel jade ceramic, and belongs to the field of daily decorative materials. The novel jade ceramic material comprises the following chemical components in percentage by weight: 75-80% of Al203, 5-10% of SiO2, 5-10% of H2O, 1-3% of zinc oxide and 2-3% of epoxy resin. The jade ceramic provided by the invention is strong in jade sense, high in stability, good in practical effect and free of pollution and has a crystal clear effect of natural jade, so that the grade of the jade ceramic is greatly improved.
Description
Technical field
The present invention relates to a kind of daily ornament materials, particularly to a kind of Novel jade ceramics, Novel jade matter pottery
Preparation method and application.
Background technology
Along with people's living standard and the raising of cultural taste, there is natural jade, grace, succinct, high-grade effect
Beautiful matter pottery becomes the consumption main flow of people, and beautiful matter pottery becomes the first-selection of people, people because of its penetrating exquisiteness, color Smooth and moist
Utilizing various process means and new raw material to copy beautiful matter pottery, but because of its technical difficulty too long ream prestige the most always
Step.Owing to there is a lot of micro-gas in conventional ceramic, thus hole pottery is the most opaque.And Novel jade matter is ceramic, relative to
Conventional ceramic modification is big, and processing technology is more complicated.
The open translucent ceramic material of Chinese invention patent document CN 101898887 A, jade matter ceramic thin plate and system thereof
Preparation Method, the product clear-cut texture of the prior art, pattern is the most true to nature, and pattern stereoscopic impression is strong, glittering and translucent, decorative effect
Good, but it all can not meet at beautiful texture, stability, practical function and is actually needed.
Therefore, texture is strong, stability is high, good practical effect, free of contamination Novel jade matter pottery to need a kind of jade at present badly.
Summary of the invention
Demand according to above-mentioned field and deficiency, the present invention provide one to have beautiful texture is strong, stability is high, practical function
Beautiful matter pottery good, free of contamination and preparation method thereof.
Technical scheme is as follows:
A kind of Novel jade ceramics, the percentage by weight of the chemical composition of described material is: Al20375-80%,
SiO25-10%, H2O 5-10%, zinc oxide 1-3%, epoxy resin 2-3%.
The percentage by weight of the chemical composition of described material is: Al20375%, SiO210%H2O 10%, zinc oxide
3%, epoxy resin 2%.
The coefficient of expansion of described material is 5.8-7.7 × 10-6K, and/or the whiteness of described material is more than 85 degree.
Described material is made up of the raw material of following percentage by weight: described material is by the raw material system of following percentage by weight
Become: low temperature stone powder 10-20 part, albite 10-30 part, high potassium sand 1-8 part, potassium sodium stone powder 10-30 part, Pulvis Talci 1-5 part, ball
Soil 10-20 part, zinc oxide 0.5-5 binding agent and wollastonite 3-6 part.
Containing zinc oxide and/or epoxy resin in described binding agent.
A kind of Novel jade matter pottery, uses and includes above-mentioned Novel jade ceramics.
The preparation method of Novel jade matter pottery comprises the steps:
(1) dispensing is stacked old in proportion, mix homogeneously, and ball mill pulverizing adds water and is mixed to get embryo mud；
(2) by embryo slurry iron-removing, pulp storage tank injection forming are injected；
(3), after the idiosome drying after molding being processed, calcine 8 hours in the high temperature furnace of 1800 DEG C, then at, 750
Oxidizing flame biscuiting is used at DEG C；
(4) being that 1400 DEG C of roastings also height is fiery in temperature after glazing is incubated 30 minutes, and picks, packaging is put in storage；
The described stacking old time is 16-20 days
Described grinding time is 5-10 hour, tails over rate≤0.2% reaching sky
Using before glazing in step (4) uses the form of over-glaze decoration to decorate after decorating then glazing, or glazing under glaze.
The application of described Novel jade matter pottery.
The product that present invention process prepares has the natural beautiful sparkling and crystal-clear penetrating effect of matter, has filled up the another of beautiful matter Production of Ceramics
One blank.
After inventor makes the Novel jade matter pottery of the present invention burn by selected raw material and its proportioning, whiteness is more than
85 degree.
The beautiful ceramics of present invention exploitation, utilizes staged high temperature repeatedly to fire, makes every effort to the gas in white for pottery tire
Hole thoroughly solves, and reach truly is white as a jade.The product that the present invention program produces, true in conjunction with traditional ceramics technology
Reaching in positive meaning pottery always, greatly improve the class of product.
The present invention has the following technical effect that
1, the Novel jade matter pottery that the present invention provides have that beautiful texture is strong, stability is high, good practical effect, free of contamination spy
Point；
2, the Novel jade matter pottery that the present invention provides contains zinc oxide, has antibacterial action, and Folium Camelliae sinensis inside will not spoil and turn sour.
The intensity of the Novel jade matter pottery that 3, the present invention provides is more than 4 times of mill run
4, the Novel jade matter pottery that the present invention provides is applicable to oven, microwave oven and dish-washing machine.
5, the Novel jade matter ceramic product outward appearance that the present invention provides is milky white as pottery, sparkling and crystal-clear as beautiful, homogeneous, very
Aobvious top grade, beautiful in colour, pattern stereoscopic impression is strong, has the effect that natural beautiful matter stone material is sparkling and crystal-clear.
6, the Novel jade matter pottery opaque effect that the present invention provides is outstanding, and fluoride consumption is few, pollutes little, non-oxidation magnesium,
The cost of material is low.
7, the coefficient of expansion of the Novel jade ceramics that the present invention provides is 5.8-7.7 × 10-6K, and/or described material
Whiteness more than 85 degree.
Detailed description of the invention
Thering is provided following embodiment is to preferably be further appreciated by the present invention, it is not limited to described optimal embodiment party
Formula, is not construed as limiting present disclosure and protection domain, anyone under the enlightenment of the present invention or by the present invention and its
Product as any and present invention that the feature of his prior art is combined and draws is same or like, all falls within the present invention's
Within protection domain.
Unreceipted specific experiment step or condition person in embodiment, according to the normal experiment described by the document in this area
The operation of step or condition can be carried out.Agents useful for same or instrument unreceipted production firm person, be can by city available from
Conventional reagent product.
Embodiment 1. prepares beautiful matter pottery 1
(1) preparation process
The percentage by weight of raw material: low temperature stone powder 10-20 part, albite 10-30 part, high potassium sand 1-8 part, potassium sodium stone powder
10-30 part, Pulvis Talci 1-5 part, ball clay 10-20 part, binding agent 0.5-5 part and wollastonite 3-6 part.
The white raw material of selected height of proportional quantity is stacked old 16-20 days and mix homogeneously, then ball mill pulverizing 5-10 hour,
Tail over rate≤0.2% reaching sky, add water and be mixed to get embryo mud；Slurrying according to a conventional method, according to a conventional method except ferrum, and injects
Pulp storage tank, then injection forming, after the idiosome drying after molding processes, calcining 8 hours in the high temperature furnace of 1800 DEG C, so
After at 750 DEG C, use oxidizing flame biscuiting, pick, use before glazing and use overglaze color after decorating then glazing, or glazing under glaze
The form decoration painted is that 1400 DEG C of roastings also height is fiery in temperature after glazing is incubated 30 minutes, and picks finally pack warehouse-in.
Rapid multi-element analysis instrument (DHF82 type, hook Xiang Tan Xiang Yi Instrument Ltd.) is used to measure above-mentioned raw materials system
The chemical composition of standby Novel jade ceramics is following (by weight percentage):
Al20375%, SiO210%H2O 10%, zinc oxide 3%, epoxy resin 2%.
Embodiment 2. prepares beautiful matter pottery 2
(1) preparation process
The percentage by weight of raw material: low temperature stone powder 10-20 part, albite 10-30 part, high potassium sand 1-8 part, potassium sodium stone powder
10-30 part, Pulvis Talci 1-5 part, ball clay 10-20 part, binding agent 0.5-4 part and wollastonite 3-6 part.
The white raw material of selected height of proportional quantity is stacked old 16-20 days and mix homogeneously, then ball mill pulverizing 5-10 hour,
Tail over rate≤0.2% reaching sky, add water and be mixed to get embryo mud；Slurrying according to a conventional method, according to a conventional method except ferrum, and injects
Pulp storage tank, then injection forming, after the idiosome drying after molding processes, calcining 8 hours in the high temperature furnace of 1800 DEG C, so
After use at 750 DEG C use before oxidizing flame biscuiting pick glazing decorate then glazing, or glazing under glaze after use on glaze
The form decoration of colored drawing is that 1400 DEG C of roastings also height is fiery in temperature after glazing is incubated 30 minutes, and picks finally pack warehouse-in.
Rapid multi-element analysis instrument (DHF82 type, hook Xiang Tan Xiang Yi Instrument Ltd.) is used to measure above-mentioned raw materials system
The chemical composition of standby Novel jade ceramics is following (by weight percentage):
Al20380%, SiO25%H2O 7%, zinc oxide 1%, epoxy resin 3%.
Embodiment 3. prepares beautiful matter pottery 3
(1) preparation process
The percentage by weight of raw material: low temperature stone powder 10-20 part, albite 10-30 part, high potassium sand 1-8 part, potassium sodium stone powder
10-30 part, Pulvis Talci 1-5 part, ball clay 10-20 part, zinc oxide 0.5-5 part and wollastonite 3-6 part.
The white raw material of selected height of proportional quantity is stacked old 16-20 days and mix homogeneously, then ball mill pulverizing 5-10 hour,
Tail over rate≤0.2% reaching sky, add water and be mixed to get embryo mud；Slurrying according to a conventional method, according to a conventional method except ferrum, and injects
Pulp storage tank, then injection forming, after the idiosome drying after molding processes, calcining 8 hours in the high temperature furnace of 1800 DEG C, so
After use at 750 DEG C use before oxidizing flame biscuiting pick glazing decorate then glazing, or glazing under glaze after use on glaze
The form decoration of colored drawing is that 1400 DEG C of roastings also height is fiery in temperature after glazing is incubated 30 minutes, and picks finally pack warehouse-in.
Rapid multi-element analysis instrument (DHF82 type, hook Xiang Tan Xiang Yi Instrument Ltd.) is used to measure above-mentioned raw materials system
The chemical composition of standby Novel jade ceramics is following (by weight percentage):
Al20377%, SiO28%H2O5%, zinc oxide 2%, epoxy resin 2.5%.
The compliance test result of the Novel jade matter pottery prepared by embodiment 1-3:
Conventionally detecting the physical property of embodiment of the present invention 1-3 product, experimental data shows, product of the present invention
Opening's edge thickness when being 4 millimeters, impact resistance intensity is higher than 0.25lbf.ft, and when conventional ceramic tableware opening's edge thickness is 4 millimeters,
The intensity of the impact resistance intensity generally below 0.06lbf.ft. present invention is more than 4 times of mill run.
220 DEG C/20 DEG C thermal shocks of product of the present invention 3 times, the heat stability of test product, all by test；And it is common
Crockery can only partly pass through 180 DEG C/20 DEG C thermal shocks, and the thermal shock resistance properties of the present invention is more preferable；The water suction of product of the present invention
Rate is less than 0.1%, and mill run is typically between 0.5～0.1%, and product of the present invention is finer and close.It is applicable to oven, microwave oven
And dish-washing machine.
Product appearance of the present invention is milky white as pottery, sparkling and crystal-clear as beautiful, homogeneous, and the most aobvious top grade is beautiful in colour, figure
Case third dimension is strong, has the effect that natural beautiful matter stone material is sparkling and crystal-clear.
Jade matter pottery opaque effect of the present invention is outstanding, and fluoride consumption is few, pollutes little, and non-oxidation magnesium, the cost of material is low.
The coefficient of expansion of described material is 5.8-7.7 × 10-6K, and/or the whiteness of described material is more than 85 degree.
Comparative example 1
Translucent ceramic material open with Chinese invention patent CN201010122751, jade matter ceramic thin plate and preparation thereof
Disclosed in embodiment of the method 1, product (X1) compares
According to detecting the physical property of this comparative example product with the identical conventional method of embodiment 1-3, experimental data is as follows:
When the opening's edge thickness of product is 4 millimeters, impact resistance intensity is less than 0.06lbf.ft.；
Product can only partly pass through 180 DEG C/20 DEG C thermal shocks；
The water absorption rate of product；0.7%.
Product color is gorgeous, and pattern stereoscopic impression is strong.
The coefficient of expansion of material is 8.5 × 10-6K or 9.6 × 10-6K, whiteness 62 degree.
Obviously, above-described embodiment is only for clearly demonstrating example, and not restriction to embodiment.Right
For those of ordinary skill in the field, can also make on the basis of the above description other different component proportioning and
The change of process conditions or variation.Here without also cannot all of embodiment be given exhaustive.And thus extended out
Obviously change or change among still in the protection domain of the invention.
Claims (10)
1. a Novel jade ceramics, it is characterised in that the percentage by weight of the chemical composition of described material is: Al203
75-80%, SiO25-10%, H2O 5-10%, zinc oxide 1 3%, epoxy resin 2-3%.
Novel jade ceramics the most according to claim 1, it is characterised in that the weight of the chemical composition of described material
Percentage ratio is: Al20375%, SiO210%H2O 10%, zinc oxide 3%, epoxy resin 2%.
Novel jade ceramics the most according to claim 2, it is characterised in that the coefficient of expansion of described material is 5.8-
7.7×10-6K, and/or the whiteness of described material is more than 85 degree.
Novel jade ceramics the most according to claim 3, it is characterised in that described material is by following weight percent
The raw material of ratio is made: described material is made up of the raw material of following percentage by weight: low temperature stone powder 10-20 part, albite 10-30
Part, high potassium sand 1-8 part, potassium sodium stone powder 10-30 part, Pulvis Talci 1-5 part, ball clay 10-20 part, binding agent 0.5-5 part and wollastonite
3-6 part.
5. a Novel jade matter pottery, it is characterised in that use the arbitrary described Novel jade ceramics of claim 1-4.
6. the preparation method of the Novel jade matter pottery described in claim 5, it is characterised in that comprise the steps:
(1) dispensing is stacked old in proportion, mix homogeneously, and ball mill pulverizing adds water and is mixed to get embryo mud；
(2) by embryo slurry iron-removing, pulp storage tank injection forming are injected；
(3), after the idiosome drying after molding being processed, calcine 8 hours in the high temperature furnace of 1800 DEG C, then at, at 750 DEG C
Use oxidizing flame biscuiting；
(4) being that 1400 DEG C of roastings also height is fiery in temperature after glazing is incubated 30 minutes, and picks, packaging is put in storage.
Method the most according to claim 6, it is characterised in that the described stacking old time is 16-20 days.
Preparation method the most according to claim 7, it is characterised in that described grinding time is 5-10 hour, to reach empty
Tail over rate≤0.2%.
Preparation method the most according to claim 8, it is characterised in that use before glazing under glaze in step (4) and decorate then
The form using over-glaze decoration after glazing, or glazing is decorated.
10. the application of the arbitrary described Novel jade matter pottery of claim 1-4.
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| CN201610686700.XA CN106316370A (en) | 2016-08-18 | 2016-08-18 | Novel jade ceramic material and preparation method and application of novel jade ceramic |
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| CN201610686700.XA CN106316370A (en) | 2016-08-18 | 2016-08-18 | Novel jade ceramic material and preparation method and application of novel jade ceramic |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62123059A (en) * | 1985-11-25 | 1987-06-04 | 株式会社住友金属セラミックス | Ceramic composition with surface smoothness |
| CN101164658A (en) * | 2007-08-24 | 2008-04-23 | 晋城市富基新材料有限公司 | Aluminium oxide foam ceramic filter |
| CN102267808A (en) * | 2010-06-01 | 2011-12-07 | 由伟 | Preparation method of artificial jade |
| CN104310970A (en) * | 2014-09-27 | 2015-01-28 | 景德镇陶瓷学院 | A method of enhancing thermal shock resistance of a fully-dense high-aluminum ceramic material and a product prepared by the method |
| CN104803665A (en) * | 2015-03-31 | 2015-07-29 | 苏州维泰生物技术有限公司 | Anti-aging aluminum oxide ceramic and preparation method thereof |
| CN104816373A (en) * | 2015-05-15 | 2015-08-05 | 由伟 | Three-dimensional printing manufacturing method of artificial jade |
-
2016
- 2016-08-18 CN CN201610686700.XA patent/CN106316370A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62123059A (en) * | 1985-11-25 | 1987-06-04 | 株式会社住友金属セラミックス | Ceramic composition with surface smoothness |
| CN101164658A (en) * | 2007-08-24 | 2008-04-23 | 晋城市富基新材料有限公司 | Aluminium oxide foam ceramic filter |
| CN102267808A (en) * | 2010-06-01 | 2011-12-07 | 由伟 | Preparation method of artificial jade |
| CN104310970A (en) * | 2014-09-27 | 2015-01-28 | 景德镇陶瓷学院 | A method of enhancing thermal shock resistance of a fully-dense high-aluminum ceramic material and a product prepared by the method |
| CN104803665A (en) * | 2015-03-31 | 2015-07-29 | 苏州维泰生物技术有限公司 | Anti-aging aluminum oxide ceramic and preparation method thereof |
| CN104816373A (en) * | 2015-05-15 | 2015-08-05 | 由伟 | Three-dimensional printing manufacturing method of artificial jade |
Non-Patent Citations (1)
| Title |
|---|
| 王永康等: "《纳米材料科学与技术》", 31 March 2002 * |
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| CI02 | Correction of invention patent application | ||
| CI02 | Correction of invention patent application |
Correction item: Applicant Correct: Jingdezhen porcelain and jade Research Institute False: Jingdezhen porcelain and jade Research Institute Number: 02 Page: The title page Volume: 33 Correction item: Applicant Correct: Jingdezhen porcelain and jade Research Institute False: Jingdezhen porcelain and jade Research Institute Number: 02 Volume: 33 |
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Application publication date: 20170111 |